See discussions, stats, and author profiles for this publication at: https://www.researchgate.net/publication/338708478 Influence of sample conditions on shear wave velocity measurements in a sedimentary stiff clay Article in Marine Georesources and Geotechnology · January 2020 DOI: 10.1080/1064119X.2020.1711833 CITATION READS 1 354 4 authors: Paulina Janusz Kenny Kataoka Sorensen ETH Zurich Aarhus University 11 PUBLICATIONS 13 CITATIONS 41 PUBLICATIONS 905 CITATIONS SEE PROFILE SEE PROFILE O. R. Clausen Katrine Juul Andresen Aarhus University Aarhus University 120 PUBLICATIONS 2,462 CITATIONS 66 PUBLICATIONS 649 CITATIONS SEE PROFILE Some of the authors of this publication are also working on these related projects: Tight Reservoir Development - Lower Cretaceous View project NorthGreen2017 View project All content following this page was uploaded by Kenny Kataoka Sorensen on 05 February 2020. The user has requested enhancement of the downloaded file. SEE PROFILE Marine Georesources & Geotechnology ISSN: 1064-119X (Print) 1521-0618 (Online) Journal homepage: https://www.tandfonline.com/loi/umgt20 Influence of sample conditions on shear wave velocity measurements in a sedimentary stiff clay Paulina A. Janusz, Kenny K. Sørensen, Ole R. Clausen & Katrine J. Andresen To cite this article: Paulina A. Janusz, Kenny K. Sørensen, Ole R. Clausen & Katrine J. Andresen (2020): Influence of sample conditions on shear wave velocity measurements in a sedimentary stiff clay, Marine Georesources & Geotechnology, DOI: 10.1080/1064119X.2020.1711833 To link to this article: https://doi.org/10.1080/1064119X.2020.1711833 Published online: 20 Jan 2020. Submit your article to this journal View related articles View Crossmark data Full Terms & Conditions of access and use can be found at https://www.tandfonline.com/action/journalInformation?journalCode=umgt20 MARINE GEORESOURCES & GEOTECHNOLOGY https://doi.org/10.1080/1064119X.2020.1711833 Influence of sample conditions on shear wave velocity measurements in a sedimentary stiff clay Paulina A. Janusza, Kenny K. Sørensena , Ole R. Clausenb and Katrine J. Andresenb a Department of Engineering, Aarhus University, Aarhus, Denmark; bDepartment of Geoscience, Aarhus University, Aarhus, Denmark ABSTRACT ARTICLE HISTORY The study presented in this paper aims to investigate the prospects of using bender elements in the offshore industry for determining shear wave velocity of fragmented, fragile and brittle clay samples and cuttings. The result from the study shows that the laboratory-measured S-wave velocities of intact samples of Søvind Marl, a sedimentary stiff Palaeogene clay, in general, are lower than those determined from in-situ seismic cone penetration testing. The reason may be unavoidable volume-constant distortion and changes to effective stress conditions experienced by the natural clay upon sampling and subsequent sample preparation. Correlation between the size of the samples and velocity is not noticed. In contrast, the S-wave velocities for natural samples that were remoulded and then reconstructed are observed to be comparable with the in-situ seismic measurements, however, the results are found to be dependent on sample density. The influence of cross-talk, near-field, and boundary effects on the results is assessed. Received 13 June 2019 Accepted 30 December 2019 Introduction Prediction of shear wave (S-wave) velocity in offshore sediments in the overburden and reservoir rocks is crucial in the oil industry for instance in seismic modelling, AVO (Amplitude Versus Offset) analysis (Lee 2006) and in the oil well drilling process. It also plays an important role in marine geotechnical engineering because of the direct relation between shear wave velocity and the dynamic shear modulus. The dynamic shear modulus of shallow depth offshore sediments is a controlling factor in e.g. the response of offshore wind turbines towers or oil platforms to wave loading. However, information about S-wave velocity is usually not sufficient. In-situ determination of S-wave velocity in offshore conditions is usually very expensive and technically complex (e.g. petrophysical well-logging, seismic surveys, seismic Cone Penetration Tests S-CPT), in addition, indirect measurements are difficult to interpret. For some deep seismic applications, shear wave velocity is still often estimated using only empirical relations with compression wave (Pwave) velocity (Castagna et al. 1985). In shallow depth geotechnical engineering, even more uncertain correlations based on soil index parameters such as soil type, density and porosity are used (Yi and Yi 2016; L’Heureux and Long 2016). Laboratory measurements can provide more precise information; however, the availability of soil and rock cores is limited mainly because of the cost of offshore core drilling. In the hydrocarbon industry cores are usually retrieved only from reservoir units. For shallower units, often only drill cuttings or disturbed or fragmented soil and rock samples are accessible. This is a problem since well-preserved CONTACT Kenny K. Sørensen kks@eng.au.dk Bender elements; clay sediments; offshore constructions; shear wave velocity intact samples are essential to obtain reliable results from the on-sample measurements. Especially the interval between 50–100 m below the seafloor is critical since indirect measurements like petrophysical well-logging are not commonly performed, and intact samples from coring or from shallow depth geotechnical boreholes are sparse. Often, only very disturbed drill cuttings are accessible. One of the simple methods of measuring the shear wave velocity in the laboratory is bender element testing which has been used in geotechnical research for many decades to determine the soil properties such as small strain dynamic shear modulus (G0) (Black et al. 2009; Lee and Santamarina 2005). The bender element method is a simple, non-destructive, inexpensive and quick procedure that is generally used to determine shear wave velocity for relatively big, intact samples. In this study, the possibilities of estimating S-wave velocity in a situation of material shortage are investigated. This situation is common in the offshore industry, where often only disturbed drill cuttings, fragile heavily fractured rocks or completely remoulded or broken-down soil and rock samples are available. In this study, the shear wave velocity was measured for both intact small clay samples and reconstructed samples and then compared to the results of in-situ Seismic Cone Penetration Testing (S-CPT) for verification. Materials and methods Bender element principle Bender elements are piezoelectric bimorph transducers which are characterized by a capability of conversion of Department of Engineering, Aarhus University, Aarhus, Denmark ß 2020 Informa UK Limited, trading as Taylor & Francis Group KEYWORDS 2 P. A. JANUSZ ET AL. Figure 1. a) Bender element’s schematic cross-section. b) Series element. c) Parallel element. After Lee and Santamarina (2005). electrical energy into mechanical deflection and vice versa. The typical experimental setup consists of two thin bender elements: one, used as a transmitter which when excited with a small voltage generates a bending motion that propagates as a wave through the medium. The second bender element detects vibrations and transforms it into a voltage output (Black et al. 2009; Chee-Ming 2010). The generation of motion is possible due to the bender element’s layered internal structure (Figure 1). In the centre, there is a conductive metal shim, surrounded by two piezoceramic sheets and two conductive outer electrodes. While one piezoelectric layer contracts, another one expands. Two connection configurations are possible (Figure 1): series, where the polarities of the piezoelectrical layers are opposite to each other, and the element is connected only at the outer electrodes and parallel, where two piezoelectrical layers have the same poling direction, and the element is connected both at the outer electrodes and metal shim. It is generally recommended to use a parallel bender element as the transmitter and a series element as the receiver to attain optimal signal quality (Lee and Santamarina 2005). Shear wave velocity Vs can be calculated by dividing the tip-to-tip distance Ltt between bender elements by travel time t of the S-wave determined from the bender element test (Black et al. 2009). One of the main reasons for the popularity of the bender element tests is the simplicity of the procedure which is fast, inexpensive and non-destructive. However, the output signal can be strongly affected among others by electromagnetic coupling, near-field (Lee and Santamarina 2005) or boundary effects (Ingale et al. 2017). Electromagnetic coupling between source and receiver (cross-talk) is a common issue related to bender element testing, especially in wet and conductive materials. It is manifested by the apparently almost instantaneous arrival of the transmitted wave. The amplitude of that early component is relatively high, and it can significantly affect the determination of travel time (Lee and Santamarina 2005; Rio 2006). Different methods to remove or reduce the crosstalk effect are discussed among others in Lee and Santamarina (2005), Zhu et al. (2011) and Rio (2006). Figure 2 shows how grounding of the receiving element effectively removes cross-talk in a test on an intact subsample. Figure 2a shows the signal before the receiving element was grounded. A closer look at the received signal from the grounded receiver is shown in Figure 2b (notice that the y-axis scale has been adjusted). Although grounding effectively removes most of the cross-talk, some are still seen to remain, but the interpretation is now possible. Many authors report the significant influence of nearfield effects on the determination of shear wave velocity (Black et al. 2009; Arroyo et al. 2003). The phenomenon of near-field effect is caused by very complex processes near the source of wavefield (Arroyo et al. 2003), usually, it is understood as a distortion of the transmitted signal due to unknown early wave components (Ingale et al. 2017). With reducing sample size, the influence of boundary effects increases on the received wave. Distortion of the signal due to the interference of shear wave with side reflections, refractions, and converted waves may make identification of S-wave travel time impossible. Experimental setup Both intact and reconstructed samples were tested under unconfined conditions to ensure that testing could be performed using a fast and simple procedure. Bender element testing was performed by placing the sample between a stainless-steel pedestal and a top cap with embedded bender elements protruding into the sample at either end, as shown from the photos in Figure 3. Bender elements Bender elements were manufactured in-house. Only series elements were used in this study for simplicity. Standard 0.51 mm thick brass-reinforced extension actuators T200-H4-503X (Piezo Systems) were used. A coaxial cable (RG174/U) was soldered to each element. To ensure waterproofing and protection of the electrical circuit, the soldering points were encapsulated in a thin epoxy coating (LOCTITE EA 3430) before a thin polyurethane coat was added to the element. The bender elements were cast into stainless-steel rings using a 2-part epoxy (Figure 3). Only the bottom end of the element was fixated in the ring to allow for greater free length and deflection of the element. The protrusion of the element above the ring, which equals the embedment depth of the element into the sample, was chosen to be around 4 mm to minimize sample disturbance. The measured sizes of used bender elements and their protrusion above the ring are given in the Table 1. To improve the quality and strength of the transmitted signal, bigger (X0) series elements were used as the transmitter as compared to the receiver (X2 or X5). Shear wave velocity measurement A Function Generator (Aim-TTi TG1010A 10 MHz DDS Function Generator) (Figure 4) was used to excite the MARINE GEORESOURCES & GEOTECHNOLOGY 3 Figure 2. Examples of the output signals disturbed by cross-talk, near-field, and boundary effects. a) Intact subsample si1_2 before the receiver was grounded. b) Intact subsample si1_2 after the receiver was grounded (different scale). transmitter with multiple sine pulses with a peak-to-peak amplitude of 10 or 20 V. The transmitted signal was amplified by a factor of 10 by a power amplifier (High Voltage Linear Amplifier P200, FLC Electronics x10). Both transmitted and received electrical signals were digitalised and recorded on an oscilloscope (Pico Technology, PicoScope 4224, 16 bit), and were preliminarily examined using PicoScope 6 software. Then, the results were exported and analysed using self-prepared Matlab scripts. the signal was not good enough to perform cross-correlation. Therefore, it was decided to use a time-domain to determine travel time. Figure 5 shows three signals with a different number of pulses recorded for the transmitted frequency of 5.5 kHz. For each signal, the last transmitted peak and the last major received peak before the signal starts to show damping (marked using dots) are matched together and used to calculate shear wave velocity. Output signals for a different number of pulses were plotted together to find a consistent solution independent of the number of pulses. Signal interpretation The travel time determination is usually the source of the greatest uncertainties in the bender element method. Techniques of finding shear wave travel time in the frequency domain (e.g. cross-correlation) are claimed to be more reliable while time-domain methods (e.g. visual picking) are more subjective and but certainly more straightforward. Even though different methods have their advantages and disadvantages, final outcomes are usually comparable (Chee-Ming 2010). Because some of the received signals were greatly affected by cross-talk, near-field and boundary effects, the quality of Material Søvind Marl samples were retrieved from a test field near the town Randers (Figure 6). The geological profile at the site consists of about 4 m of postglacial clay till underlaid by Søvind Marl clay formation extending at least to 15 m below the ground (Simonsen and Sørensen 2018). Søvind Marl is a highly plastic, stiff and very low permeable, light grey to almost white marl or calcareous clay, deposited in middle and late Eocene within a deep shelf marine environment. It is fine-grained (less than 0.01 mm) 4 P. A. JANUSZ ET AL. Table 1. Measured sizes of bender elements used in the study. Name Type Free length [mm] Width [mm] Thickness [mm] Protrusion [mm] Figure 3. a) Reconstructed sample placed between stainless-steel pedestal and stainless-steel top cap. b) Bender element in the stainless-steel ring in the top cap. with a clay fraction of 65–70% that mainly consists of smectite (60%) and to a lesser extent also illite and chlorine. Samples appear fissured with the presence of slickensides. Even though it is in general highly calcareous, the CaC03 content is found to vary from 0 to 70%. Both thick layers of white marl with high CaC03 content and thinner, dark green, almost CaC03 free clay can be found, a few glauconite-rich horizons also appear in the profile (Simonsen and Sørensen 2018; Simonsen 2018). After deposition, the Søvind Marl formation was covered by a thick sequence of younger strata which in certain areas have been eroded or dislocated during Quaternary (Figure 6). Due to the removal of the load from eroded layers and the weight of numerous glaciers, the formation is heavily overconsolidated. The overconsolidation ratio is estimated to be in the order of 10 to 20 based on the geological loading history, but significant swelling of the clay after unloading is likely to have disturbed the intact structure to such a degree that it can be considered lightly overconsolidated rather than heavily overconsolidated (Simonsen and Sørensen 2018; Simonsen 2018). The properties and composition of Søvind Marl are changing quite significantly across the profile even on the centimetre scale, especially when it comes to carbonate content, which is also reflected in the water content, plasticity index, stiffness and shear strength (Simonsen 2018). In Table 2 representative geotechnical properties determined from samples from the test field are listed. More general information about Søvind Marl, its geology, and geotechnical properties can be found in Grønbech et al. (2015) and Heilmann-Clausen et al. (1985). Sample preparation Intact samples Three different intact samples (si1, si2, and si3) of Søvind Marl from two different depths intervals were studied (Table 3). The X0 X2 X5 Y3 Y4 Series 10.8 8.0 1.7 3.4 Series 7.7 6.3 1.6 3.9 Series 7.4 6.4 1.4 3.8 Parallel 7.4 6.3 1.7 3.6 Parallel 7.4 5.6 1.3 3.8 Figure 4. Bender element experimental setup. variability of the tested samples was clearly visible; samples si1 and si2 were dark green clay, quite easy to break, while si3 was more brownish and plastic. Moreover, si2 appeared much more fissured than si1, even though both samples were from the same depth interval. To investigate the applicability of the bender element method in a situation of low material availability, the size of the quasi-cylindrical samples was reduced after every measurement, both in height and in diameter. Reconstructed samples To estimate the shear wave velocity for very disturbed material, a quite innovative technique of reconstructing samples from a destroyed material was used. A similar method has been used before by Mehrabi Mazidi et al. (2012) to estimate the uniaxial compressive strength of cuttings. Based on a preliminary laboratory study the optimal procedure of producing reconstructed specimens was found. The material from previously tested intact samples (Table 2) was oven-dried at 110 C, then crushed until achieving grain sizes less than 0.5 mm. This was found to ensure visual homogeneity of the subsample and at the same time, the preparation did not take too much time. The crushed material was then compressed in 3–5 layers in a thick-walled stainless-steel compression cell to the desired density by applying a static load using a stiff load frame. The load was applied in small incremental steps to ensure homogenous compaction of the specimens. Subsamples were compressed until they reached the measured natural dry density of the intact material (Table 2) or to higher density if they were initially too fragile to perform the bender element test. Available equipment made it possible to build small, cylindrical subsamples with a diameter of 31.5 mm and height up to 35 mm, which however gave height to diameter ratio below the recommended ratio of 2. To measure shear wave velocity using bender elements, piezoelectric transducers should have a good connection MARINE GEORESOURCES & GEOTECHNOLOGY 5 Figure 5. Example of determination of the S-wave travel time. with the sample interface to transmit vibrations effectively. To ensure a good connection for dry reconstructed specimens, especially with low density, it was decided to add a small amount of extra material which would fill in the small gap between the bender element and the sides of the groves made in the test specimens. Two materials were tested: ordinary gypsum and Polyfilla. In-situ seismic S-CPT testing The results of laboratory measurements were compared to shear wave velocities derived from in-situ Seismic Cone Penetration testing (S-CPT) performed by the Danish geotechnical engineering contractor Geo at the test site (Figure 6). The seismic signals were recorded using a seismic module consisting of two accelerometers located 0.5 m from each other behind the electric cone (A.P. van den Berg’s Icone Seismic Module). At each time step, the seismic module was pushed 1 m into the soil, and the seismic wave was generated by hitting a wooden beam placed at ground level using a hammer from respectively left and right side. The difference in the arrival time of the wave recorded on two accelerometers was used to calculate the value of shear wave velocity. For each depth, 6 measurements were carried out (respectively 3 from the left and 3 from the right side) and then stacked to enhance quality. Figure 7 shows an example of measured seismic signals for different depths. In the shallow part, the signal is seen to be noisier, but the interpretation is still possible with support from signals captured at larger depth. Results and discussion Tables 4 and 5 give an overview of the sample dimensions and the measurement results from the performed bender element tests on intact and reconstructed samples respectively. Subsample with irregular shape is marked with in Table 4 and subsamples with added gypsum (G) and Polyfilla (P) respectively are shown in Table 5. The shear wave velocities shown in Tables 4 and 5 are weighted averages of several measurements. The weights correspond to the uncertainties of the single tests (including i.e. uncertainty of determination of the sample height, the protrusion length of the elements and their location, as well as the precision of finding the positions of the peaks). Presented shear wave velocities were determined for each subsample at the natural frequencies given in the tables. The natural frequency of the specimen is the frequency at which the amplitude is the highest and the signal is the clearest (Black et al. 2009). It is accepted that at the natural frequency, obtained results are the most reliable as the transmitted shear wave will not be subjected to transformation. The ratio between the tip-to-tip length Ltt (height reduced by the protrusion length of the bender elements) and wavelength k is also stated. According to the common recommendation, it should be higher than 2 to reduce the impact of near-field effects (Arroyo et al. 2003) Comparison of the in-situ and laboratory measurements Figure 8 compares the shear wave velocities of intact and reconstructed subsamples determined from the bender element test to the shear wave profile from Seismic Cone Penetration Testing. All plotted subsamples were prepared from one of three original samples (si1, si2, and si3). For visualisation reasons, points are plotted at different depths, however, each sample was retrieved from a specific but unknown depth within the respective intervals (grey shading) on the plot. The position of the subsample located 6 P. A. JANUSZ ET AL. furthest to the right (marked using a frame with dashed line) is incorrect, its S-wave velocity is much higher, however, for visualisation reasons, it was moved to the left. Figure 6. Map of Denmark (Jutland and Funen) with a marked test site near the town of Randers (red circle). Areas, where Eocene clays are just below Quaternary, are marked using grey bands. After Simonsen and Sørensen (2018). Table 2. Some geotechnical parameters measured for Søvind Marl samples from the test site. After Simonsen and Sørensen (2018). Property Clay fraction Smectite content Calcite content Natural water content Liquid limit Plasticity index Unit weight Undrained shear strength/effective cohesion cu/c0 Angle of shearing resistance /0 Coefficient of permeability k CPT cone tip resistance qnet Value 65–70% 60% 8–30% 44–62% 160–220% 110–177% 17–19 kN/m3 70/25 kPa 20 210–11 m/s 1–3 MPa The uncertainty of the results is shown as an error bar. The uncertainty includes both the variations of the results between different tests and uncertainties of individual measurements. The uncertainty in the shear wave velocities varies from 3 to 20 m/s with an average of 7 m/s. The shear wave velocity for the intact subsamples is generally much lower than the S-wave velocity from the in-situ seismic survey. The main reasons for the observed discrepancy are believed to be an unavoidable disturbance of the intact samples due to volume constant distortion during sample preparation and lack of in-situ confinement pressure. It is possible to perform bender element test for confined samples using a triaxial cell, however, this would be much more time consuming and furthermore require modifications to the standard setup to accommodate the smaller samples. If the only reason for the discrepancy is a change of pressure conditions, the results from the bender element test can be corrected accordingly and used as a proxy of in-situ shear wave velocity. However, many more measurements are needed to find such a relation. The intact subsamples from the shallower interval (si3) are characterized by a higher velocity (Figure 8) than from the deeper one (si1 and si2), although the seismic velocity is generally expected to increase with depth in homogeneous sediment due to increasing overburden and hence density. The reason may be that the impact of the confining pressure removal in connection to sampling has been more pronounced for the deeper samples. However, geological factors can explain part of the difference in velocity as well—as sample si1 and si2 had more fissures and were more fragile than si3. Søvind Marl is characterized by significant horizontal and vertical variability. In the shown 16 m interval (Figure 8), shear wave velocity is changing from about 110 to 190 m/s. Søvind Marl can vary even on the scale of centimeters. Because seismic measurement was performed for every 1 m, small-scale variations cannot be distinguished, that is why reliable laboratory tests are needed. But for the same reason, even if the obtained results can be corrected for the effect of pressure, their verification using the in-situ seismic profile may be difficult due to the difference of resolution and sampling error. Reconstructed subsamples The difference between shear wave velocity for dry and saturated rocks or soils is usually low (Mavko 2005), however, in this study, reconstructed, pseudo-dry specimens were almost always characterized by significantly higher velocity than wet intact subsamples (Figure 8). Only in one case, when the reconstructed subsample had a very low density (s2_2_r1), the result was found to be comparable to those obtained for intact samples. It is suspected that the Table 3. Properties and characteristics of Søvind Marl intact samples tested in this study. Name Depth interval [m] Water content [%] Wet density [g/cm3] Dry density [g/cm3] Characteristic si1 si2 si3 14–14.7 47 2.23 ± 0.37 1.52 ± 0.25 Dark green, fissured 14–14.7 50 1.75 ± 0.05 1.16 ± 0.04 Dark green, highly fissured 8–8.7 45 1.71 ± 0.13 1.19 ± 0.09 Brown-green, plastic MARINE GEORESOURCES & GEOTECHNOLOGY 7 Figure 7. Examples of measured seismic signals for different depths. explanation for the disparity may be a result of suctioninduced stress which has changed the properties of the dry, compressed subsamples. However, this has not been possible to confirm. The obtained shear wave velocities of the reconstructed specimens generally fit the in-situ seismic results well (Figure 8), which seems promising. Figure 9 shows results for all tested subsamples expressed as a normalized shear velocity which is the S-wave velocity from the bender element test divided by the velocity from the in-situ seismic profile for the corresponding interval. In Figure 9a normalized shear wave velocity was juxtaposed with density. Some of the reconstructed subsamples almost exactly reflect the seismic measurement (points close to 1 on vertical scale). However, the best fit is not necessarily for the subsamples compressed exactly to the dry density of the corresponding intact material. For example, the dry density of sample si2 is 1.16 g/cm3 (Table 2), however, the reconstructed subsample with a density of 1.3 g/cm3 is the closest to the seismic measurement. For practical reasons, it is positive that subsamples with higher density show results which are a closer match to the in-situ seismic measurements because specimens with a density below 1.3 g/cm3 are very fragile and break easily. It was expected to see a clear positive correlation between density and the S-wave velocity (Figure 9a), however, the relation is clear only for samples with added gypsum. Many other factors can be crucial here, among other variations in the properties of the compressed material, amount and type of filler used or moisture content of the specimen. Influence of the size and shape It has been suggested that to reduce the impact of the nearfield effect, the ratio between the tip-to-tip distance Ltt and wavelength k of a transmitted signal should at least be higher than 2 but lower than 4 (Arroyo et al. 2003). An aspect ratio (height/diameter) of the sample of at least 2 has been recommended by many authors to minimize the boundary effects (Ingale et al. 2017). In addition, because of complicated wave propagation in irregular samples, tested specimens should be ideally cylindrical. However, because of the scarcity of the undisturbed samples from drilling in the offshore industry, the intact specimens which fulfil all listed requirements may be unavailable. That is why quite small and slightly irregular intact samples which were sometimes below or on the verge of the recommended size (Table 4) were tested in this study. In addition, very often retrieved samples are prone to breakage, which makes it difficult to prepare ideally cylindrical specimens. Therefore, Søvind Marl with its fissured character was a good example of determining the likely challenges. Indeed, the prepared samples had very often rough, irregular boundaries and broke easily while their size was reduced (Figure 10). The reconstructed subsamples were even smaller than the intact ones, mainly due to technical limitations, however, it reflected the real conditions where availability of suitable material may be very low. In addition, the preparation of bigger specimens is relatively time-consuming while the intention in this study is to provide a simple and fast method of estimating shear wave velocity. Normalized shear wave velocities for intact subsamples are plotted against their size in Figure 9b. Because both diameter and height were changed, the size is expressed as a ratio of height to diameter. In theory, if the same travel path is maintained, the change of shape or diameter of the sample should not affect the arrival time. In addition, a change of height for almost homogenous samples should 8 P. A. JANUSZ ET AL. Table 4. Overview of all measured quasi-cylindrical intact subsamples including their sizes and the measurement results. No Name Height [mm] Diameter [mm] Natural frequency [kHz] Shear wave velocity [m/s] Ltt k 1 2 3 4 5 6 7 13 14 15 19 20 21 22 23 24 25 si1_1 si1_2 si1_3 si1_4 si1_5 si1_6 si1_7 si2_1 si2_2 si2_3 si3_1 si3_2 si3_3 si3_4 si3_5 si3_6 si3_7 60.2 50.6 39.1 39.1 39.1 39.1 39.1 44.6 44.6 44.6 59.2 50.4 43.6 31.8 31.8 31.8 31.8 70.0 70.0 70.0 65.4 59.3 51.2 42.5 70.0 49.4 41.0 70.0 70.0 70.0 70.0 57.3 47.8 37.3 5.5 5.5 5.5 5.5 5.5 5.5 5.5 5.7 6.0 4.8 5.3 5.3 5.5 5.3 5.8 6.8 5.7 89.30 80.44 70.55 77.92 114.04 83.60 69.28 64.72 87.38 88.05 103.06 98.20 105.74 111.91 112.76 73.33 75.64 3.26 2.96 2.48 2.25 1.54 2.10 2.53 3.28 2.56 2.03 2.67 2.33 1.89 1.16 1.27 2.28 1.85 Table 5. List of all measured quasi-cylindrical reconstructed subsamples including their sizes and the measurement results. P ¼ Polyfilla; G ¼ Gypsum. No Name Height [mm] Density [g/cm3] Filing material Natural frequency [kHz] Shear wave velocity [m/s] Ltt k 8 9 10 11 12 16 17 18 26 si1_7_r1 si1_7_r2 si1_7_r3 si1_6_r1 si1_7_r4 si2_2_r1 si2_2_r2 si2_2_r3 si3_5_r1 30.4 30.2 30.0 30.2 29.9 35.8 34.3 29.6 34.3 1.43 1.44 1.46 1.48 1.50 1.21 1.31 1.51 1.30 P P P P P G G G G 31 26 23 28 28 6 26 30 23 174.06 194.42 149.45 209.51 210.58 77.33 185.73 302.68 155.74 4.13 3.07 3.36 3.07 3.01 2.15 3.77 2.20 3.98 Figure 8. Shear wave velocity determined from the bender element test for intact and reconstructed subsamples compared to the results from the in-situ seismic survey. MARINE GEORESOURCES & GEOTECHNOLOGY 9 Figure 9. Results for all tested subsamples expressed as a normalized shear wave velocity a) plotted against density; b) plotted against height/diameter ratio. Figure 10. a) Søvind Marl intact subsample. When the size of the subsample was reduced, specimen b) broke easily, c) as well as during drying. d) Reconstructed subsamples. not influence the outcome significantly. In reality, any irregularity of the shape or size reduction magnifies the undesired effects in the near-field and generates unexpected reflections that affect the determination of travel time. Indeed, Figure 9b shows that the results for the same sample with a variation in the ratio of height to diameter not consistent. Any clear correlation between size and velocity cannot be seen, however, some subsamples show weak trends, for example, for specimens no. 1, 2 and 3 which have the same diameter but respectively lower height, velocity is seen to decrease almost linearly. However, many other factors can effectively mask the eventual influence of the size which is something that needs further attention. Other factors affecting the measurements Generally, both the natural frequency of the sample and the shear wave velocity are expected to increase with increasing stiffness of the sample. Table 5 shows a clear relationship between the shear wave velocity and the natural frequency for the reconstructed samples, while similar consistency is not found for the intact samples, as seen in Table 4. The natural frequency of the reconstructed samples is generally found to be 23 to 31 kHz (apart from sample si2_2_r1 which is seen to display a much lower natural frequency), while much lower natural frequencies are found for the intact samples. The lack of consistency for the more irregular shaped intact samples compared to the reconstructed samples is a likely result of boundary effects which will have an 10 P. A. JANUSZ ET AL. increased influence on the received signals due to the irregularities in dimensions. Some above-mentioned issues like variation of properties of the Søvind Marl, change of the size of the subsamples or signal disturbances are mainly responsible for the inconsistency of the results visible in Figure 9. However, another important factor may be the deterioration of the quality of the connection between the bender element and the sample’s interface. In addition, the drying of intact wet subsamples may change their strength and elastic properties (Tovar and Julio 2011). For reconstructed subsamples also amount and type of the filling material can be the issue. However, it was found that when filling material was gypsum the effect was minimal when measurements were performed after at least 3 hours after the bender elements were placed in the sample. On the other hand, tests for subsamples with added Polyfilla performed later than 3 hours were rejected because of high disturbance of the signal. Wrong identification of natural frequency may also affect the results, in the performed experiments a difference of up to 16% with a mean of 14 % was found, when a different frequency than the natural frequency was chosen. Moreover, the S-wave velocity for one sample was not found to be the same when a different number of pulses was used. In this study, the velocity was found to differ by up to 4% when a signal with a different number of pulses was chosen, but the mean uncertainty is only about 1%, hence this is of minor importance. The reason for this can be a dispersion or more complex boundary reflections that may interfere with the “true” signal. The above-mentioned factors have led to the accuracy of the results being less than optimal. However, in some applications where shear velocity is derived using uncertain empirical relations, a large number of simple and fast but low precision measurements would be useful to better estimate the S-wave velocity. Applicability for drill cuttings and other heavily disturbed samples The preliminary aim of the project was to investigate the possibility of applying the presented method of sample reconstruction to drill cuttings to estimate the shear wave velocity in the depth intervals where cores are not available. However, even though cuttings samples must be stored (Danish Energy Agency 2009), their amount and weight may not be sufficient to conduct a proper analysis. Moreover, because stored wet samples are contaminated by drilling mud, dry samples should be washed (Danish Energy Agency 2009). Nevertheless, it is suspected that the remains of drilling mud would change their properties. The possibility of using the presented method for drill cuttings has not been completely excluded. However, it seems more promising and applicable to perform the bender element test to estimate shear wave velocity for intact uncontaminated samples or for reconstructed samples if the specimen is highly disturbed but the procedure can be time-consuming, and the choice of proper density is decisive to find the correct velocity. Conclusion The study shows that the bender element method can provide a simple, fast and cheap procedure to estimate shear wave velocity even in the case of scarcity of good-quality samples. Generally, there is an agreement between S-wave velocity from the in-situ Seismic Cone Penetration Testing and laboratory measurements of the reconstructed samples using bender elements. Moreover, it is suspected that the laboratory results for the intact samples can be corrected for the change of pressure conditions and also used as a proxy of in-situ S-wave velocity. However, the signal interpretation for very small or fractured specimens which were mostly used in this study was impeded because of near-field and boundary effects. A correlation between the size of the samples and the velocity has not been found. The study shows the direction for further investigations and highlight problems that should be focused on. More research is necessary to understand better the obtained results and their significance. Acknowledgments Geo is acknowledged for carrying out and providing results from the in-situ Seismic Cone Penetration Testing at the test site, in addition to providing intact samples. Funding This work was supported by the Danish Hydrocarbon Research and Technology Centre (DHRTC) under Grant no. RIS-16 2918. ORCID Kenny K. Sørensen http://orcid.org/0000-0001-9400-7753 http://orcid.org/0000-0002-6825-9065 Ole R. Clausen http://orcid.org/0000-0001-8029-3234 Katrine J. Andresen References Arroyo, M., D. Muir Wood, and P. Greening. 2003. Source Near-Field Effects and Pulse Tests in Soil Samples. Geotechnique 53 (3): 337–345. doi:10.1680/geot.2003.53.3.337. Black, J., S. Stanier, and S. Clarke. 2009. Shear Wave Velocity Measurement of Kaolin during Undrained Unconsolidated Triaxial Compression. In Halifax, Proceedings of the 62nd Canadian Geotechnical Conference. Castagna, J. P., M. L. Batzle, and R. L. Eastwood. 1985. Relationships between Compressional-Wave and Shear-Wave Velocities in Clastic Silicate Rocks. Geophysics 50 (4): 571–581. doi:10.1190/1.1441933. Chee-Ming, C. 2010. Bender Element Test in Soil Specimens: Identifying the Shear Wave Arrival Time. Geotechnical and Geological Engineering 15: 1–8. Danish Energy Agency. 2009. Guidelines for Drilling. Denmark: Danish Energy Agency. Grønbech, G., B. N. Nielsen, L. B. Ibsen, and P. Stockmarr. 2015. Geotechnical Properties of Søvind Marl—a Plastic Eocene Clay. Canadian Geotechnical Journal 52 (4): 469–478. doi:10.1139/cgj-20140066. MARINE GEORESOURCES & GEOTECHNOLOGY Heilmann-Clausen, C., O. Nielsen, and F. Gersner. 1985. Lithostratigraphy and Depositional Environments in the Upper Paleocene and Eocene of Denmark. Bulletin of the Geological Society of Denmark 33: 287–323. Ingale, R., A. Patel, and A. Mandal. 2017. Performance Analysis of Piezoceramic Elements in Soil: A Review. Sensors and Actuators A: Physical 262: 46–63. doi:10.1016/j.sna.2017.05.025. L’Heureux, J.-S., and M. Long. 2016. Correlations between Shear Wave Velocity and Geotechnical Parameters in Norwegian Clays. In 17th Nordic Geotechnical Meeting (NGM 2016). Reykjavik, Iceland. Lee, J.-S., and J. Santamarina. 2005. Bender Elements: Performance and Signal Interpretation. Journal of Geotechnical and Geoenvironmental Engineering 131 (9): 1063–1070. doi:10.1061/ (ASCE)1090-0241(2005)131:9(1063). Lee, M. W. 2006. A Simple Method of Predicting S-Wave Velocity. Geophysics 71 (6): F161–F164. doi:10.1190/1.2357833. Mavko, G. 2005. Conceptual Overview of Rock and Fluid Factors That Impact Seismic Velocity and Impedance. Stanford, CA: Stanford Rock Physics Laboratory. Mehrabi Mazidi, S., M. Haftani, B. Bohloli, and A. Cheshomi. 2012. Measurement of Uniaxial Compressive Strength of Rocks Using Reconstructed Cores. Journal of Petroleum Science and Engineering 86–87: 39–43. doi:10.1016/j.petrol.2012.03.015. View publication stats 11 Rio, J. F. M. E. 2006. Advances in Laboratory Geophysics Using Bender Elements. Doctoral Thesis, London: University College London, Department of Civil & Environmental Engineering. Simonsen, T. R. 2018. Pore Water Pressure Response and Heave of Palaeogene Clays in Connection with Deep Excavation and Pile Driving. Doctoral Thesis, Aarhus: Department of Engineering, Aarhus University. Simonsen, T. R., and K. K. Sørensen. 2018. Performance of Vibrating Wire Piezometers in Very Low Permeable Clay. In 10th International Symposium on Field Measurements in Geomechanics (FMGM2018). Rio de Janeiro, Brazil. Tovar, R., and C. Julio. 2011. Effect of Drying and Wetting Cycles on the Shear Strength of Argillaceous Rocks. In Proceedings of the 5th International Conference on Unsaturated Soils, 1471–1476. London. Yi, F., and F. P. Yi. 2016. Estimation of Shear Wave Velocity Based on SPT Profile Data. In 5th International Conference on Geotechnical and Geophysical Site Characterisation. Jupiters Gold Coast, Queensland, Australia. Zhu, J., Y.-T. Tsai, and S.-H. Kee. 2011. Monitoring Early Age Property of Cement and Concrete Using Piezoceramic Bender Elements. Smart Materials and Structures 20 (11): 115014–115017. doi:10.1088/0964-1726/20/11/115014.