University of Wollongong Research Online University of Wollongong Thesis Collection University of Wollongong Thesis Collections 1992 Soil stabilisation using some pozzolanic industrial and agricultural products Chassan Chmeisse University of Wollongong Recommended Citation Chmeisse, Chassan, Soil stabilisation using some pozzolanic industrial and agricultural products, Doctor of Philosophy thesis, Department of Civil and Mining Engineering, University of Wollongong, 1992. http://ro.uow.edu.au/theses/1268 Research Online is the open access institutional repository for the University of Wollongong. For further information contact Manager Repository Services: morgan@uow.edu.au. SOIL STABILISATION USING SOME POZZOLANIC INDUSTRIAL AND AGRICULTURAL BY PRODUCT A thesis submitted in fulfilment of the requirements for the award of the degree of Doctor of Philosophy from THE UNIVERSITY OF WOLLONGONG by CHASSAN CHMEISSE, B.E.(Civil), M.Eng.Sc DEPARTMENT OF CIVIL AND MINING ENGINEERING January 1992 DECLARATION This is to certify that the work presented in this thesis was carried out by the author in the Department of Civil and Mining Engineering, The University of Wollongong and has not been submitted for a degree to any other University or such Institution. Ghassan Chmeisse ACKNOWLEDGEMENT The Author wishes to express his gratitude to his Supervisors, Associate Professors, R.N. Chowdhury and D.G. Montgomery from the Department of Civil and Mining Engineering, University of Wollongong, NSW, for their guidance, encouragement and support throughout this research and to all others who helped in the preparation of this Thesis. He also wishes to thank his Parents, Wife and children for their support, patience and understanding during the years of study. i CONTENTS: Page Abstract: xi List of Notations: xiv List of Figures: xv List of Tables: xx List of Appendicies: xxvii Chapter I - Introduction, Aims and Scope 1.1 Basic concepts of Soil Stabilisation 1 1.2 Historical Background 2 1.3 Soil Stabilisation in Australia 5 1.4 Applications of Soil Stabilisation 6 1.5 Types of Soil Stabilisation 7 1.6 Pozzolans 9 1.7 Mechanism of Pozzolanic Activity 9 1.8 Types of Pozzolans and Pozzolanic by-products 10 1.9 Products Investigated as Stabilising Agents 12 during research work reported in this Thesis Rice Husk Ash and Granulated Blast Furnace Slag 1.10 Aims and Scope of this Thesis 13 ii Page Chapter II - Review Of Relevant Previous Work Concerning Rice Husk Ash and Granulated Blast Furnace Slag 2.1 Rice Husk - Description and Production 17 2.2 Disposal of Rice Husks 17 2.3 Properties of Rice Husk Ash 18 2.4 Engineering Applications of Rice Husk Ash 19 2.5 Applications of Rice Husk Ash to Soil 20 Stabilisation 2.5.1 Rice Husk Ash : Soil Stabilisation 20 2.5.2 Lime - Rice Husk Ash : Soil 21 Stabilisation 2.5.3 Cement - Lime-Rice Husk Ash : Soil 22 Stabilisation 2.6 Scope for further research 23 2.7 Blast Furnace Slag - Description and 25 Production 2.8 Types of Blast Furnace Slag 27 2.8.1 Air Cooled Slag 27 2.8.2 Foamed Expanded Slag 27 2.8.3 Granulated Blast Furnace Slag 28 2.9 Properties and Engineering Applications of 28 Granulated Blast Furnace Slag (GBFS) 2.9.1 Use of Granulated Blast Furnace Slag 29 in the manufacture of cement 2.9.2 Use of Granulated Blast Furnace Slag 30 in road construction 2.9.2a Use of Granulated Blast Furnace 30 Slag in road works Overseas 2.9.2b Use of Granulated Blast Furnace 33 Slag in road works in Australia 2.10 Scope for further research 35 iii Page Chapter III 3.1 - Experimental Techniques and Methodology Scope of chapter 38 3.2 Existing tests used in soil stabilisation 38 3.3 The validity of existing tests 39 3.4 Tests used in this investigation 40 3.4.1 Grading and compaction tests 41 3.4.2 Plasticity and volume changes 42 3.4.3 Compressive strength - Unconfined 44 compressive strength (UCS) and undrained triaxial strength (UTS) 3.4.4 California Bearing Ratio test (CBR test) 45 3.4.5 Repeated dynamic load test 47 3.4.5a General 47 3.4.5b The loading system 48 3.4.5c Measurement of the permanent 49 deformation 3.4.6 Powder X-ray diffraction 50 3.4.7 Scanning Electron Microscopy 51 Chapter IV 4.1 - Experimental Investigation using Rice Husk Ash Scope of chapter 4.2 Objectives of investigation 62 4.3 Materials used 63 4.3.1 Rice Husk Ash 63 4.3.2 Cement 64 4.3.3 Lime 64 4.3.4 Soils 64 62 iv Page 4.4 Testing regime 65 4.5 Initial tests - optimum ratios of lime to 66 RHA and Cement to RHA 4.5.1 Preparation, curing and testing of 67 specimens 4.6 Treatment of soils with various additives 68 4.7 Testing of stabilised soils 68 4.7.1 Compaction characteristics 68 4.7.2 Unconfined compressive strength 69 4.7.3 Linear Shrinkage 69 4.7.4 Atterberg limits 70 4.7.5 Effect of delay in compaction on the 71 strength of stabilised soils 4.7.6 Effect of various additives on the 72 shear strength parameters of soils 4.7.7 Effect of various additives on the CBR 74 value of soils 4.7.8 Repeated dynamic load test 75 4.7.9 Scanning Electron Microscopy 78 4.7.10 Powder X-ray Diffraction Analysis 79 Chapter V - Discussion and Analysis of Results concerning Rice Husk Ash 5.1 RHA as a single additive 137 5.1.1 Effect of RHA additive on compaction 137 characteristics of soils 5.1.2 Effect of RHA additive on the strength 139 properties of soils 5.1.2a Effect on UCS 139 5.1.2b Effect on CBR 140 V Page 5.1.3 Effect of RHA on the Atterberg limits 140 and linear shrinkage of soils 5.1.4 Effect of RHA on the behaviour of soils 142 under the action of repeated dynamic load Lime-RHA additives 143 5.2.1 Effect of lime-RHA additives on 143 compaction characteristics of soils 5.2.2 Effect of lime-RHA additives on the 144 strength properties of soils 5.2.2a Effect on UCS 144 5.2.2b Effect on CBR 146 5.2.3 Effect of delay in compaction on the 147 strength of lime-RHA treated soils 5.2.4 Effect of lime-RHA additives on the 148 shear strength parameters of soils 5.2.5 Discussion of the results of the XRD 150 analysis of lime-RHA stabilised soils 5.2.6 Discussion of the results of the SEM 152 examination of lime-RHA stabilised soils 5.2.7 Effect of lime-RHA additives on the 153 Atterberg limits and linear shrinkage of soils 5.2.8 Implications of lime savings 155 5.2.9 Effect of lime-RHA additives on the 156 behaviour of soils under the action of repeated dynamic load Cement-RHA additives 159 5.3.1 Effect of various cement-RHA additives 159 on compaction characteristics of soils 5.3.2 Effect of cement-RHA additives on the 161 strength properties of soils 5.3.2a Effect on UCS 161 5.3.2b Effect on CBR 163 vi Page 5.3.3 Effect of delay in compaction on the 163 strength of cement-RHA treated soils 5.3.4 Effect of cement-RHA additives on the 164 shear strength parameters of soils 5.3.5 Effect of cement-RHA additives on the 166 Atterberg limits and linear shrinkage of soils Implications of cement saving 167 5.3.6 5.3.7 Chapter VT - Effect of cement - RHA additives on the 169 behaviour of soils under the action of repeated dynamic load Experimental Investigations using Granulated Blast Furnace Slag (GBFS) 6.1 Scope of chapter 179 6.2 Objectives of research 179 6.3 Materials 180 6.3.1 Blast furnace slag (GBFS) 180 6.3.2 Cement 181 6.3.3 Lime 181 6.3.4 Soils 181 6.4 Testing regime 181 6.5 Optimum ratios of lime or cement to GBFS 183 6.6 Treatment of soils with various additives 184 6.7 Testing of stabilised soils 184 6.7.1 Compaction characteristics 184 6.7.2 Unconfined compressive strength 185 6.7.3 Linear shrinkage 185 6.7.4 Atterberg limits 186 vii 6.7.5 Effect of delay in compaction on the strength of stabilised soils 6.7.6 Effect of various additives on the 187 shear strength parameters of soils 6.7.7 Effect of various additives on the CBR 189 value of soils 6.7.8 Repeated dynamic load test 190 6.7.9 Scanning Electron Microscopy 191 6.7.10 Powder X-ray Diffraction Analysis 192 Chapter VTI - Discussion and Analysis of Results concerning GBFS 7.1 GBFS as a single additive to soils 239 7.1.1 Effect of GBFS additive on compaction 239 characteristics of soils 7.1.2 Effect of GBFS additive on the strength 240 properties of soils 7.1.2a Effect on UCS 240 7.1.2b Effect on CBR 241 7.1.3 Effect of GBFS additive on the Atterberg 241 limits and linear shrinkage of soils 7.1.4 Effect of GBFS additive on the behaviour 243 of soils under the action of repeated dynamic load 7.2 Lime-GBFS additives 244 7.2.1 Effect of lime-GBFS additives on 244 compaction characteristics of soils 7.2.2 Effect of lime-GBFS additives on the 246 strength properties of soils 7.2.2a Effect on UCS 246 7.2.2b Effect on CBR 248 viii Page 7.2.3 Effect of delay in compaction on the 249 strength of lime-GBFS treated soils 7.2.4 Effect of lime-GBFS additives on the 250 shear strength parameters of soils 7.2.5 Discussion of the results of the XRD 251 analysis of lime-GBFS stabilised soils 7.2.6 Discussion of the results of the SEM 252 examination of lime-GBFS stabilised soils 7.2.7 Effect of lime-GBFS additives on the 253 Atterberg limits and linear shrinkage of soils 7.2.8 Implications of lime savings 255 7.2.9 Effect of lime-GBFS additive on the 256 behaviour of soils under the action of repeated dynamic load 7.3 Cement-GBFS Additives 259 7.3.1 Effect of various cement-GBFS additives 259 on compaction characteristics 7.3.2 Effect of cement-GBFS additives on the 260 strength properties of soils 7.3.2a Effect on UCS 260 7.3.2b Effect on CBR 262 7.3.3 Effect of delay in compaction on the 263 strength of cement-GBFS treated soils 7.3.4 Effect of cement-GBFS additives on the 264 shear strength parameters of soils 7.3.5 Effect of cement-GBFS additives on the 265 Atterberg limits and linear shrinkage of soils 7.3.6 Implications of cement saving 266 7.3.7 Effect of cement-GBFS additives on the 268 behaviour of soils under the action of repeated dynamic load ix Page Chapter VIII - 8.1 Discussion of Economic Feasibility of the applications of RHA and GBFS to soil stabilisation Introduction 278 8.2 Availability of RHA 279 8.3 Economic feasibility of RHA as a single 281 additive to soils 8.4 Economic feasibility of lime-RHA additives 281 to soils 8.5 Economic feasibility of cement-RHA additives 282 to soils Summary 283 8. .6 .7 8. Availability of GBFS 283 8. .8 Economic feasibility of GBFS as a single 284 additives to soils 8. .9 Economic feasibility of lime-GBFS additives 286 to soils 8. ,10 Economic feasibility of cement-GBFS 287 additives to soils Chapter IX - Recommended Design Procedure 9.1 Introduction 289 9.2 Mix design procedures of lime-RHA soil 290 stabilisation 9.3 Mix design procedures of lime-GBFS, 293 cement-GBFS and cement-RHA soil stabilisation Chapter X References - Conclusions, Recommendations and Suggestions for Future Work 310 X Appendices Appendix A - Methods of operation of the fatigue control panel used in the repeated dynamic load test Appendix B - Equivalent specific gravity and calculated porosity of various mixes xi ABSTRACT Rice husk ash (RHA) and granulated blast furnace slag (GBFS have been investigated as pozzolanic materials for soil stabilisation. They contain siliceous and aluminous materials, and react with lime or cement, having the economic potential to replace some of the lime or cement presently used as an additive in the stabilisation of soil. Four (4) types of soils were treated with varying quantitie of lime, cement, rice husk ash, granulated blast furnace slag, combinations of rice husk ash with lime or cement and combinations of granulated blast furnace slag with lime or cement under laboratory conditions. To determine the effectiveness of RHA and GBFS as stabilisers, general geotechnical soil properties, including unconfined compressive strength, undrained shear strength, CBR, plasticity index and linear shrinkage, were measured. X-ray diffraction analysis, scanning electron microscopy an a repeated dynamic load test were also carried out in this investigation. It is revealed that rice husk ash alone is not suitable for modifying soil properties, however, beneficial results are obtained when it is used in combinations with lime or cement. It is shown that lime-rice husk ash and cement xii rice-husk ash additives increase the unconfined compressive strength, the CBR and the undrained shear strength of soils. They also improve the behaviour of soils under the action of repeated dynamic loads and improve the workability and volume stability of soils. It is revealed that granulated blast furnace slag alone is suitable for modifying the volume stability of heavy clays and the workability of gravel-sand soils. It increases the unconfined compressive strength and the CBR of soils and improves their behaviour under the action of repeated dynamic loads. The effects of lime-granulated blast furnace slag and cement-granulated blast furnace slag additives on soils are shown to be similar to those of lime-rice husk ash and cement-rice husk ash additives. The effectiveness of rice husk ash and granulated blast furnace slag can be expressed in terms of ratios of rice husk ash and granulated blast furnace slag required to lime or cement saved. Information relevant to these ratios and the current and projected future availability of granulated blast furnace slag and rice husk ash in Australia is presented. xiii A suggested mix design procedures for lime-rice husk ash, cement-rice husk ash, lime-granulated blast furnace slag and cement-granulated blast furnace slag soil stabilisation is also presented. xiv LIST OF NOTATIONS c Cohesion Cc Compression index CBR California bearing ratio e Voids ratio GBFS Granulated blast furnace slag IP Plasticity index L.L Liquid limit L.S Linear shrinkage MDD Maximum dry density OMC Optimum moisture content P.L Plastic limit RHA Rice husk ash SEM Scanning Electron Microscopy UCS Unconfined compressive strength UTS Unconsolidated triaxial shear strength Wt Weight XRD X-ray Diffraction 0 Angle of internal friction CV Effective vertical stress <r n Effective normal stress on the plane of failure T Shear stress XV LIST OF FIGURES Figures Description 3.1 Repeated dynamic load test - View of 56 test structure and pavement 3.2 Repeated dynamic load test - Principle 57 of longitudinal movement due to rotation 3.3 Repeated dynamic load test - Initial 58 setup arrangement 3.4 Repeated dynamic load test - The 59 fatigue control panel during operation 3.5 Diagram showing grid of locations at 60 which deflection measurements were taken in relation to the wheel and the pavement boundaries 3.6 Repeated dynamic load test 61 - Illustrations of deflection beam in use 4,1 UCS of lime-RHA pastes 113 4.2 UCS of cement-RHA pastes 114 4.3 UCS of lime, RHA and lime-RHA 115 stabilised soils 4.4 UCS of cement, RHA and cement-RHA 116 stabilised soils 4.5 Linear shrinkage of lime, RHA and 117 lime-RHA stabilised soils 4.6 Linear shrinkage of cement, RHA and 118 cement-RHA stabilised soils 4.7 Plasticity index of lime, RHA and 119 lime-RHA stabilised soils 4.8 Plasticity index of cement, RHA of 120 cement-RHA stabilised soils Page xv i Figures Description 4.9 Effect of delay in compaction on the 121 UCS of cement and cement-RHA stabilised Soil A 4.10 Effect of delay in compaction on the 122 UCS of lime and lime-RHA stabilised Soil A 4.11 CBR of cement, cement-RHA, lime, 123 lime-RHA and RHA stabilised Soil A 4.12 Effect of lime, cement, RHA and 124 lime-RHA additives on the CBR of Soil B 4.13 Effect of lime, lime-RHA and RHA 125 additives on the CBR of Soil C 4.14 Permanent deformation of the 126 untreated pavement at row H (row of max deformation) of the grid after various number of load cycles 4.15 Permanent deformation of the 2% 126 lime stabilised pavement at row H (row of max deformation) of the grid after various number of load cycles 4.16 Permanent deformation of the 3% 1:1 126 lime-RHA stabilised pavement at row H (row of max deformation) of the grid after various number of load cycles 4.17 Permanent deformation of the 1.5% 127 cement stabilised pavement at row H (row of max deformation) of the grid after various number of load cycles 4.18 Permanent deformation of the 3% 1:1 127 cement-RHA stabilised pavement at row G (row of max deformation) of the grid after various number of load cycles 4.19 Permanent deformation of the 8% RHA 127 stabilised pavement at row G (row of max deformation) of the grid after various number of load cycles Page xvii Figures Description Page 4.20 Repeated dynamic load test - Removal 128 of trolley from beneath materials containment bin 4.21 Scanning electron micrograph of the 129 fracture surface of the untreated Soil A 4.22 Scanning electron micrograph of the 130 fracture surface of the untreated Soil C 4.23 Scanning electron micrograph of the 131 fracture surface of Soil A stabilised with 8% content of 1:1 lime-RHA additive after 7 days accelerated curing 4.24 Scanning electron micrograph of the 132 fracture surface of Soil C stabilised with 8% content of 1:1 lime-RHA additive after 7 days accelerated curing 4.25 X-ray diffraction pattern of 133 untreated Soil A 4.26 X-ray diffraction pattern of 134 untreated Soil C 4.27 X-ray diffraction pattern of Soil A 135 stabilised with 8% content of 1:1 lime-RHA additive after 7 days accelerated curing 4.28 X-ray diffraction pattern of Soil C 136 stabilised with 8% content of 1:1 lime-RHA additive after 7 days accelerated curing 6.1 UCS of lime-GBFS specimens 221 6.2 UCS of cement-GBFS specimens 222 6.3 UCS of lime, GBFS and lime-GBFS 223 stabilised soils 6.4 UCS of cement, GBFS and cement-GBFS 224 stabilised soils 6.5 Linear shrinkage of lime, GBFS and lime-GBFS stabilised soils 225 xviii Figures Description 6.6 Linear shrinkage of cement, GBFS and 226 cement-GBFS stabilised soils 6.7 Plasticity index of lime, GBFS and 227 lime-GBFS stabilised soils 6.8 Plasticity index of cement, GBFS and 228 cement-GBFS stabilised soils 6.9 Effect of delay in compaction of the 229 UCS of cement and cement-GBFS stabilised Soil A 6.10 Effect of delay in compaction on the 230 UCS of lime and lime-GBFS stabilised Soil C 6.11 Effect of lime, cement, GBFS, 231 lime-GBFS and cement-GBFS additives on the CBR of Soil A 6.12 Effect of lime, cement, GBFS, 232 lime-GBFS and cement-GBFS additives on the CBR of Soil B 6.13 Effect of lime, cement, GBFS, 233 lime-GBFS and cement-GBFS additives on the CBR of Soil C 6.14 Permanent deformation of the 8% GBFS 234 stabilised pavement at row H (row of max deformation) on the grid after various number of load cycles 6.15 Permanent deformation of the 3% 1:1 234 lime-GBFS stabilised pavement at row H (row of max deformation) on the grid after various number of load cycles 6.16 Permanent deformation of the 3% 1:1 234 cement-GBFS stabilised pavement at row H (row of max deformation) on the grid after various number of load cycles 6.17 Scanning electron micrograph of the 235 fracture surface of Soil A stabilised with 8% content of 1:1 lime-GBFS additive after 7 days accelerated curing Page xix Figures Description 6.18 Scanning electron micrograph of the 236 fracture surface of Soil C stabilised with 8% content of 1:1 lime-GBFS additive after 7 days accelerated curing 6.19 X-ray diffraction pattern of Soil A 237 stabilised with 8% content of 1:1 lime-GBFS additive after 7 days accelerated curing 6.20 X-ray diffraction pattern of Soil C 238 stabilised with 8% content of 1:1 lime-GBFS additive after 7 days accelerated curing 9.1 Determination of the composition of the 294 preferred mix in a lime-RHA soil stabilisation Page XX LIST OF TABLES Table Description 2.1 Typical oxide composition of blast 37 furnace slag compared to Portland cement, after Spence and Cook (2) 3.1 Tests used for evaluating stabilised 53 soils, after Shackel (44) 3.2 Suggested utilities for various 54 simulation tests, after Shackel (44) 3.3 Laboratory tests used in this study 55 4.1 Properties of soils used 81 4.2a Compaction characteristics of lime, 82 RHA and lime-RHA stabilised Soil A 4.2b Compaction characteristics of lime, 83 RHA and lime-RHA stabilised Soil B 4.2c Compaction characteristics of lime, 84 RHA and lime-RHA stabilised Soil C 4.3a Compaction characteristics of cement, 85 RHA and cement-RHA stabilised Soil A 4.3b Compaction characteristics of cement, 86 RHA and cement-RHA stabilised Soil B 4.3c Compaction characteristics of cement, 87 RHA and cement-RHA stabilised Soil C 4.4a UCS of lime, RHA and lime-RHA 88 stabilised Soil A 4.4b UCS of lime, RHA and lime-RHA 89 stabilised Soil B 4.4c UCS of lime, RHA and lime-RHA 90 stabilised Soil C 4.5a UCS of cement, RHA and cement-RHA 91 stabilised Soil A Page xxi Table Description 4.5b UCS of cement, RHA and cement-RHA 92 stabilised Soil B 4.5c UCS of cement, RHA and cement-RHA 93 stabilised Soil C 4.6a Effect of lime, RHA and lime-RHA 94 additives on the Atterberg limits and linear shrinkage of Soil A 4.6b Effect of lime, RHA and lime-RHA 95 additives on the Atterberg limits and linear shrinkage of Soil B 4.6c Effect of lime, RHA and lime-RHA 96 additives on the Atterberg limits and linear shrinkage of Soil C 4.7a Effect of cement, RHA and cement-RHA 97 additives on the Atterberg limits and linear shrinkage of Soil A 4.7b Effect of cement, RHA and cement-RHA 98 additives on the Atterberg limits and linear shrinkage of Soil B 4.7c Effect of cement, RHA and cement-RHA 99 additives on the Atterberg limits and linear shrinkage of Soil C 4.8 Effect of delay in compaction on the 100 UCS of lime and lime-RHA stabilised Soil C 4.9 Effect of delay in compaction on the 101 UCS of cement and cement-RHA stabilised Soil A 4.10 Effect of lime and lime-RHA additives 102 on the shear strength parameters of Soil C 4.11 Effect of cement and cement-RHA 103 additives on the shear strength parameters of Soil B 4.12 Effect of various additives and curing 104 time the CBR of stabilised Soil A 4.13 Effect of various additives and curing 105 time the CBR of stabilised Soil B Page xxii Table Description 4.14 Effect of various additives and curing 106 time the CBR of stabilised Soil C 4.15 Permanent deformations of untreated 107 pavement 4.16 Permanent deformations of 2% lime 108 treated pavement 4.17 Permanent deformations of 3% 1:1 109 lime:RHA treated pavement 4.18 Permanent deformations of 1.5% cement 110 treated pavement 4.19 Permanent deformations of 3% 1:1 111 cement:RHA treated pavement 4.20 Permanent deformations of 8% RHA 112 treated pavement 5.1 Effect of RHA additive on the grading 172 of soils 5.2a Deflection per load as number of load 173 applications increases at point eH of 3% 1:1 lime-RHA treated pavement 5.2b Deflection per load as number of load 173 applications increases at point eH of 2% lime treated pavement 5.2c Deflection per load as number of load 174 applications increases at point eH of untreated pavement 5.2d Deflection per load as number of load 174 applications increases at point eH on the grid of 8% RHA treated pavement 5.3 Ratio of RHA required to lime saved or 175 identical economic cost ratio of lime to RHA 5.4 Ratios of strength at 7 days to strength 176 at 90 days of soils treated with 8% content of various additives 5.5 Ratios of strength at 28 days to strength 176 at 90 days of soils treated with 8% content of various additives Page xxiii Table Description 5.6 Ratios of RHA required to cement saved 177 or identical economic cost ratios of cement to RHA 5.7a Deflection per load as number of load 178 applications increases at point eH on the grid of untreated pavement 5.7b Deflection per load as number of load 178 applications increases at point eH on the grid of 1.5% cement treated pavement 5.7c Deflection per load as number of load 178 applications increases at point dG on the grid of the 3% content of 1:1 cement-RHA treated pavement 6.1a Compaction characteristics of lime, 193 GBFS and lime-GBFS stabilised Soil A 6.1b Compaction characteristics of lime, 194 GBFS and lime-GBFS stabilised Soil B 6.1c Compaction characteristics of lime, 195 GBFS and lime-GBFS stabilised Soil C 6.2a Compaction characteristics of cement, 196 GBFS and cement-GBFS stabilised Soil A 6.2b Compaction characteristics of cement, 197 GBFS and cement-GBFS stabilised Soil B 6.2c Compaction characteristics of cement, 198 GBFS and cement-GBFS stabilised Soil C 6.3a UCS of lime, GBFS and lime-GBFS 199 stabilised Soil A 6.3b UCS of lime, GBFS and lime-GBFS 200 stabilised Soil B 6.3c UCS of lime, GBFS and lime-GBFS 201 stabilised Soil C 6.4a UCS of cement, GBFS and cement-GBFS 202 stabilised Soil A 6.4b UCS of cement, GBFS and cement-GBFS 203 stabilised Soil B Page xx iv Table Description 6.4c UCS of cement, GBFS and cement-GBFS 204 stabilised Soil C 6.5a Effect of lime, GBFS and lime-GBFS 205 additives on the Atterberg limits and linear shrinkage of Soil A 6.5b Effect of lime, GBFS and lime-GBFS 206 additives on the Atterberg limits and linear shrinkage of Soil B 6.5c Effect of lime, GBFS and lime-GBFS 207 additives on the Atterberg limits and linear shrinkage of Soil C 6.6a Effect of cement, GBFS and cement-GBFS 208 additives on the Atterberg limits and linear shrinkage Soil A 6.6b Effect of cement, GBFS and cement-GBFS 209 additives on the Atterberg limits and linear shrinkage Soil B 6.6c Effect of cement, GBFS and cement-GBFS 210 additives on the Atterberg limits and linear shrinkage Soil C 6.7 Effect of delay in compaction on the 211 UCS of cement and cement-GBFS stabilised Soil A 6.8 Effect of delay in compaction on the 212 UCS of lime and lime-GBFS stabilised Soil C 6.9a Effect of lime and lime-GBFS additives 213 on the shear strength parameters of Soil B 6.9b Effect of lime and lime-GBFS additives 213 on the shear strength parameters of Soil C 6.10 Effect of cement and cement-GBFS 214 additives on the shear strength parameters of Soil B 6.11 Effect of various additives and curing 215 time on the CBR of stabilised Soil A Page XXV Table 6.12 Description Effect of various additives and curing time on the CBR of stabilised Soil B 6.13 Effect of various additives and curing 217 time on the CBR of stabilised Soil C 6.14 Permanent deformations of 3% content of 1:1 cement:GBFS treated pavement 6.15 Permanent deformations of 3% content of 219 1:1 lime:GBFS treated pavement 6.16 Permanent deformations of 8% GBFS 220 treated pavement 7.1 Effect of GBFS additive on the grading 271 of Soils A,B and C 7.2 Deflection per load as number of load 272 increases at point of maximum deflection on the grid (ie, point eH) of the 8% GBFS treated pavement 7.3 Ratio of GBFS required to lime saved or 27 3 identical economic cost ratio of lime to GBFS 7.4a Deflection per load as number of load 274 applications increases at point eH on 3% 1:1 lime-GBFS treated pavement 7.4b Deflection per load as number of load 274 applications increases at point eH on 2% lime treated pavement 7.4c Deflection per load as number of load 274 applications increases at point eH on untreated pavement 7.5 Ratio of UCS at 28 days to UCS at 90 275 days for soils treated with 8% content of cement and cement-GBFS additives 7.6 Ratio of GBFS required to cement saved 276 or identical economic cost ratio of cement to GBFS 7.7a Deflection per load as number of load 277 applications increases at point eH on the grid of the untreated pavement 218 xxv i Table 7.7b Description Deflection per load as number of load applications increases at point eH on the grid of the 1.5% cement treated pavement 7.7c Deflection per load as number of load 277 applications increases at point dH on the grid of the 3% 1:1 cement-GBFS treated pavements 277 xxvii LIST OF APPENDICES Appendix Description Methods of operation of the fatigue control panel used in the repeated dynamic load test B Equivalent specific gravity and calculated porosity of various mixes 1 Chapter I INTRODUCTION. AIMS AND SCOPE 1.1 Basic Concepts of Soil Stabilisation Soils are formed by the decomposition of rocks and through the subsequent removal, transportation and weathering of the products of decomposition. The concept of soil may also include the accumulations of inorganic sediments, organic peats, plant roots and various wastes and rubbles of an industrial society. defined as rocks" (1). in ordinary "any The soil in the general context can be loose surface material overlying solid It is usually the surface which is dealt with construction activities for buildings and transport systems. It is understandable that soil, which is one of the most ancient construction materials, is still among the most widely used materials because of its low cost of winning, wide spread availability and easy workability. Besides its use in dams and roads construction, soil has been used for building in a great variety of ways. In different traditions, it is used for walling, flooring and roofing and in some instances, for all three (2). 2 Many soils, in their untreated state, lack strength and/or dimensional stability which render them unsuitable, wholly or partially, to the requirements of construction. The Engineer the then will have the choice of "accepting limitations imposed by the insitu soil properties, replacing the available soil by another one which complies with the specified requirements or improving the properties of the existing soil by stabilisation so as to fulfil the design criteria" (3). 1.2 Historical Background In the area of building practice, soil stabilisation has a history which reaches at least 5000 years into the past (4). Compacted masses of clay and lime were used construction of the pyramids of Shensi in Mexico. in the Ancient buildings in India and China, in which lime-clay mixture were used, are still standing (5). Even in ages and places where engineering skill has been minimal, soil stabilisation has often been used: for example, in the lime stabilised floors of Saxon England, or the straw and blood stabilised mud houses of West Africa (4). In pre Roman times, there were many trafficable roads throughout much of England (The Pilgrim's Way), Europe (Denmark to Tuscany) and Asia (Afghanistan to Egypt, China 3 to Persia) (6). Periodically, however these roads were transformed into masses of mud by rains, whereas in dry seasons the carts created clouds of dust. It is obvious for these reasons that the history of stabilised roads began (7). Despite significant work by the ancient Egyptians, Persians and Greeks, the Romans were the great road builders of the ancient world. They built 80,000km of excellent roads with a base of heavy, hand fitted stones. Above this was a course of smaller stones, topped by a layer of broken tiles, brick or chalk, held together with pozzolan mortar. For many hundreds of years after the fall of the Roman Empire in the fifth century, few new roads were built in Europe and few Roman roads were regularly maintained. The wheeled vehicle began to gain popularity again in the seventeenth century and subsequently craftsmen developed the stagecoach. While these vehicles created some demand for better roads, it was the Industrial Revolution, with its great need for trade and transportation, which gave encouragement to the development and improvement of the transport system in the western world. John Loudon Macadam (1756 - 1836) developed the thick, one size stone pavement, made up of 25mm broken 4 stones. In Europe the Macadam roads received no competition for almost a whole century. The first highways of the United States, too, were constructed using Macadam methods (7). The roads thus constructed did not meet the requirements of the continuously were ruined increasing and accelerating faster than they could be traffic and repaired. New economic methods had to be developed, therefore, to enable construction of durable roads. In the field of urban roads and highways, this development has led to the introduction of concrete and block paving, and in the case of secondary roads, to the regular use of stabilised soil. The first experiments in the USA were conducted with sandclay mixtures in 1906 (7). The favourable results motivated subsequent construction projects using various mixtures. Cement, bitumen and certain chemicals were employed for soil stabilisation purposes and a number of different stabilisation techniques were established. In Europe, it was not until the 1930's, when the vast increase in the motor vehicle traffic had begun and soil mechanics approaches entered the field of road construction, that the idea of stabilisation was accepted (7). During the second world war 1939 - 1945, more than 140 military air fields are known to have been constructed with cement 5 stabilised bases by the Germans and their allies, in places as far north as Finland and as far south as Sicily, in addition to an unknown number in Russia (26). After the war many European countries continued soil stabilisation for secondary road construction and as highway base courses. 1.3 Soil Stabilisation in Australia In Australia, it was not until the 1940's that the idea of stabilisation was accepted. This acceptance has grown dramatically since then. A survey conducted by Ingles (8) has shown that 56.5 million square yards (47.2 million square metres) of pavement were stabilised in Australia between 1963 and 1968. The Cruickshank Survey (9) into the use of stabilisation by local governments and road authorities has revealed that:- a) The area of stabilised pavement constructed by 12 of the 14 Main Roads Department districts covering Queensland, between 1970 and 1975, was about two million square metres. b) Fifty percent of local government authorities in NSW and Victoria had constructed four million square metres during the same period. 6 The use of stabilisation is still increasing in Australia. It is carried out virtually in every road construction, rehabilitation and heavy patching maintenance throughout the countryside areas. The Author has had extensive experience of soil stabilisation (more than 90,000 square metres of pavement) while working with the Roads and Traffic Authority at Glen Innes Works Office in NSW between 1986 - 1989 and has known of tens of thousands of square metres of pavement stabilised by South Grafton, Tenterfield, Moree and Armidale Works Offices during the same period. Ingles (8) has predicted that, in the next one hundred years, there will be a rapidly improving technology for stabilisation techniques, a marked increase in applied research for stabilisation and an increased usage of soil stabilisation in a wider range of applications. 1.4 Applications of Soil Stabilisation Soil stabilisation is the treatment of soil in order to rectify its deficiencies in engineering properties and especially as a road construction material. Among the important aims of soil stabilisation are the following:- 7 Increase in strength and stiffness of soils Increase in durability Enhancement of workability Reduction of compressibility Reduction of permeability Reduction of volume instability Control of dust and protection from erosion 1.5 Types of Soil Stabilisation Soil stabilisation is often classified into two main types, namely "shallow stabilisation" and "deep stabilisation" (10). The best known techniques of deep stabilisation are:preloading, surcharging, freezing, prewetting, grouting, thermal treatment (heating), dynamic consolidation, vibro compaction, blasting and the use of fabrics and meshes. In conventional shallow soil stabilisation several methods have been used, such as granular or mechanical soil stabilisation, compaction and additive-use soil stabilisation. Regarding the additives, the materials used may be divided into a relatively few types, being, bitumen, Portland cement, lime, lime-pozzolan, chlorides of salts and chemical materials. In this classification, chemical 8 materials are not considered to involve cement and lime although these are chemically effective agents. Methods using additives form the basis for soil stabilisation. proportion, Cruickshank by type of (9) has stabilisation, shown for that the the work undertaken by the local governments in Victoria and NSW between 1970 and 1975 were:- Mechanical stabilisation 34.75% Lime stabilisation 38.00% Cement stabilisation 22.00% Bitumen stabilisation 3.75% Other 1.50% The survey has also shown that cement stabilisation accounted for 45% of the total stabilisation conducted by the Main Roads Department in Queensland between 1970 and 1975. As the general knowledge on the conventional additive-use method is common to soil engineers, attention is given in this thesis to the practicality of utilizing pozzolanic byproducts in soil stabilisation because a large number of these materials have not been used in practice although they may have a stabilisation. significant role in the future of soil The Author wishes to discuss the properties 9 of some of these materials and their potential contribution to the soil stabilisation. 1.6 Pozzolans Lea (11) has defined pozzolans as "materials which, though not cementitous in themselves, contain constituents which will combine with lime at ordinary temperature in the presence of water to form insoluble compounds possessing cementitous properties". 1.7 Mechanism of Pozzolanic Activity Suwanvitaya (27) stated that in 1980 Takemoto and Uchikawa have proposed the following mechanism for the paste hydration of a lime-pozzolan reaction. When mixed with water and lime the SiOH^- group on the surface of the pozzolan dissociates to SiOH 4- and H + leaving the grain negatively charged. This is followed by the dissolution of alkalis leaving Si and Al~ rich layer which dissolves and combines with Ca 2 + . The reaction products form a layer around the pozzolan grain. Further dissolution and reaction is achieved by breaks in the layer due to osmotic pressure developed from the difference of concentration of ions such as alkalis and SiO 4- and AlO 2between the outside and inside of the layer. 10 The concentration of Ca 2 + which enables Ca-Al hydrate to precipitate is higher than that of CSH. The precipitation of Ca-Al hydrate therefore occurs at locations apart from the grain. 1.8 Types of Pozzolans and Pozzolanic By-Products Traditionally pozzolans have been divided into two groups, natural and artificial. In Europe the natural materials which have been most exploited are the Italian pozzolans and the German trass (2) whereas inorganic volcanic ash soils are often utilised in Japan for soil-cement and soil-lime stabilisation (12). Pozzolanic by-products or artificially burnt inorganic materials obtained as industrial or agricultural by-products are similar to such volcanic soils from the view point of good cementation products are construction, with hydrative increasingly hence additives. playing minimising the a Those part problem in of byroad resource depletion, environmental degradation and energy consumption. Of the artificial pozzolans probably fly ash, which is the residue from the combustion of pulverised coal in power stations, is the most commonly used globally. In 1976 it was estimated that some 30,000,000 tonnes were used annually and that the annual increase was about 10% (2). 11 With the discovery by Havelin and Khan (13) that lime and fly ash impart particular properties to fine aggregates and soils, attention was drawn to the use of fly ash in soil stabilisation. Much valuable work has since been carried out in this field by Minnick and Miller (14) and Davidson and his associates (15) at the engineering experimental station of Iowa State College. In Great Britain the Central Electricity Generating Board was active in the field of possible uses for fly ash (16). In Australia valuable work was done by Davidson and Mulling (5), Croft (18), Herzoc and Brock (19) and others. This research has led to the utilisation of fly ash in soil stabilisation in USA and Europe. In Australia the use of this new technique was further encouraged by the Department of Main Roads, NSW, issue of Circular M&R 115 (20). The bottom ash, which is a residue collected from the bottom of the furnace, is generally not as reactive as the fly ash (2). However, reports from USA (21) have shown that bottom ash has been used, either singly, in combination with fly ash, or with other materials, in a variety of highway applications in West Virginia and the surrounding states. Apart from fly ash and bottom ash, there are a number of other industrial wastes which have pozzolanic properties. Mehta (22), (23) discussed them in detail. They include 12 blast furnace slag which is more reactive with cement than with lime (2) and the kiln dust, collected during the manufacture of cement. This material contains large amounts of alkalies and free lime. Dave (24) has reported that in India, cinder obtained from railway locomotives and certain thermal power stations has pozzolanic activity but generally less than that of fly ash. Shale, clay and bauxitic soil can be converted into pozzolans by heat treatment. (25) has shown that bauxitic waste Hammond is also suitable as pozzolan after calcination and up to 40% of Portland cement can be replaced with little effect on the characteristics of cement. Many plant ashes have a high silica content which, by suitable treatment, can be made to be pozzolanic. In recent years, attention has been drawn to the uses of rice husk ash as a pozzolan although other agricultural residues such as bagasse, bamboo leaves and some timber species are also of interest. 1.9 Products Investigated as Stabilising Agents during Research Work Reported in this Thesis - Rice Husk Ash and Granulated Blast Furnace Slag It is understandable that a fundamental investigation in which all the pozzolans mentioned above could be assessed as soil stabilisers, is beyond the reach of this research. 13 However, the emphasis in this thesis has been directed towards two of these materials, rice husk ash and granulated blast furnace slag because:- i) There is an increasing need for research to find solutions for the disposal problem of the accumulating surplus of these by-products worldwide. ii) Employing the pozzolanic properties of these wastes in soil stabilisation may reduce the cost of roadmaking and help minimise the problem of resource depletion and fuel consumption. iii) The state of knowledge concerning this employment has not been sufficient to permit an effective application of these materials to soil stabilisation. 1.10 Aims and Scope of this Thesis The main aims of the work reported in this thesis are as follows:- a) To investigate the pozzolanic reactivity of rice husk ash and granulated blast furnace slag, produced in NSW, with lime and cement. 14 b) To study the influence of rice husk ash and granulated blast furnace slag as lone additives on various properties of a range of soils. c) To examine the effects of lime-rice husk ash, cementrice husk ash, lime-granulated blast furnace slag and cement-granulated blast furnace slag combined additives on the properties of soils. d) To discuss the economical feasibility of the use of rice husk ash and granulated blast furnace slag in soil stabilisation. e) To develop a mix design procedure for soil stabilisation with rice husk ash and granulated blast furnace slag additives. The two stabilising agents, rice husk ash and granulated blast furnace slag are discussed in Chapter 2 with emphasis on their production, characteristics and applications. this chapter the existing knowledge and practice In are reviewed and attention is given to the application of these materials to soil stabilisation, some gaps in this knowledge are highlighted and areas investigations are identified. which require further 15 The experimental investigation reported in this thesis, has been based on the conventional laboratory tests currently used in the design of stabilised soil mixes. Chapter 3 summarises the tests used, discusses their suitability and gives a brief note on supplementary tests conducted in this research, particularly those relevant to the prediction of the in-service behaviour of stabilised pavements. Chapter 4 is devoted to providing details of the experimental investigation carried out to evaluate the pozzolanic reaction of RHA with lime and cement and to study the influence of RHA mixes with lime and cement on the geotechnical properties and behaviour of soils. used, tests conducted and results Materials are all presented in detail in this chapter whereas analysis and discussion of these results are given in Chapter 5. Details of the work carried out to determine the pozzolanic reactivity of GBFS with lime and cement and to examine the effect of GBFS various mixes with lime and cement on the properties and behaviour of soils are given in Chapter 6. Details of materials, soils and tests used are all presented in this chapter together with the results derived. Analysis and discussion of these results are reported in Chapter 7. 16 The economic feasibility of the application of RHA and GBFS to soil stabilisation is discussed in Chapter 8 whereas Chapter 9 contains a recommended design procedure for the lime-RHA, cement-RHA, lime-GBFS and cement-GBFS soil mixes. General conclusions and recommendations are reported in Chapter 10. 17 Chapter II REVIEW OF RELEVANT PREVIOUS WORK CONCERNING RICE HUSK ASH AND GRANULATED BLAST FURNACE SLAG 2.1 Rice Husk - Description and Production A constituent of the crop popularly known as paddy, rice husks are the harsh woody outer covering of the rice grain, consisting of two interlocking halves. The husk content of paddy varies, depending on the differences in season, temperature, geographic location and cultivation practices. Most variations however, are confined to a narrow range, (variation of 4-5%) and a husk content of 20% of dried paddy is generally expected. With the world's annual production of rice at about 400 million tonnes (17), the husk produced each year amounts to approximately 80 million tonnes on the basis of these 1983 figures. 2.2 Disposal of Rice Husks Due to seasonal variability, high transport cost, bulkiness, high abrasiveness, slow biodegradation and poor nutritive value, only a small percentage of the husks can be disposed 18 of in certain low value applications, such as animal feed, fertilizer and fuel. The remainder serves no useful purpose and simply poses disposal problems. The simple disposal methods used are openfield burning and combustion in an incinerator with a defined controlled temperature. 2.3 Properties of Rice Husk Ash Incineration of rice husks produces ash with properties which vary considerably incineration. dependent on the manner of The parameters affecting these properties are temperature, the time of incineration and the environment in which the burning takes place. The weight percentage of ash, for example, can vary from about 17% for complete combustion to approximately 35% for cases where only the volatiles are driven off the raw husk and the full content of carbon is retained. Rapid burning at low temperature produces ash carbon burning at with high high temperature content, while results in prolonged predominantly crystalline silica in the ash. Rice husk ash (RHA) has generally been accepted as being pozzolanic. is based materials. Its use as a component in cementitous materials on its reaction with lime to form cementing The lime may be present as a primary constituent of the mix or as a result of the hydration of Portland cement. The development of mechanical strength is 19 influenced by the nature of silica, the carbon content and the fineness of the ash. 2.4 Engineering Applications of Rice Husk Ash Hough and Bar (28) reported the use of rice husk ash (RHA) in the manufacture of building blocks as early as 1923. A large house had been constructed from these blocks and was reported to be in excellent condition thirty years later. They also reported a study on concrete using rice husk and RHA with cement and concluded that although the mixture of the three components gave a better insulator than normal concrete, the low strength made it unsuitable for structural use. A potential application of the ash which has received increasing interest in recent years has been in the cement industry. Mehta and Pitt (23) described a furnace for producing a predominantly amorphous silica ash. The concept was adopted in a pilot plant near Sacramento, California and a 7.5 tonne/hour plant began operation. Data on the ash produced indicated that cement containing the ash was highly resistant to dilute organic extremely useful in Increasing attention the and mineral acids making it food and chemical has since been directed based cements, particularly in South East Asia. industries. toward RHA At least 20 three workshops have been organised since 1979, resulting in the adaptation of the Indian standard (50) for masonary cement based on RHA. 2.5 Applications of Rice Husk Ash to Soil Stabilisation 2.5.1 Rice Husk Ash : Soil Stabilisation The use of rice husk ash as a single additive for the purpose of soil stabilisation has received attention in the relevant literature. very little However, Rahman (29) has made an attempt in this direction to find the effects of rice husk ash on various geotechnical properties of lateritic A-7-6 group soil obtained from the University of Ife Campus, Ile-Ife, Nigeria. The researcher concluded that well burnt rice husk ash has appreciable effects on the geotechnical properties of the lateritic soil tested and that "the liquid limit and plastic limit increase with the increase of decreases. in ash rice ash but, the plasticity index The maximum dry density decreases with increase content, increases. husk while the The unconfined optimum compressive increases with increase in ash content. moisture content strength and CBR The undrained shear strength parameters, cohesion as well as angle of internal friction, also increase with increase in ash content". such work has been conducted or reported in Australia. No 21 2.5.2 Lime-Rice Husk Ash : Soil Stabilisation Lazaro and Moh (30) probably were the first who tried to stabilise deltaic black clay soil by a mixture of lime and rice husk ash. Subrahmanyam et al (31) followed the steps of Lazaro and Moh and conducted their experimental programme in the Department of Civil Engineering, University of Malaya, Kuala Lumpur to study the effect of lime-rice husk ash mixtures on the properties of an inorganic black clay soil taken from an open pit near a house construction site at Klangtown. They concluded that:- i) Rice husk ash in combination with lime can be used for the stabilisation of clays. ii) The plasticity index of clay is significantly reduced by the addition of lime and RHA admixture. iii) The maximum dry density is decreased and the optimum moisture content is increased when the clay is treated with the admixture of lime and RHA. 22 iv) The unconfined compressive strength of the clay is increased when the clay is treated with admixture of lime and RHA. The unconfined compressive strength is maximum when the quantity of admixture added to the soil is 10% of the total weight. v) As the curing time is increased, the strength of the treated clay is increased. No such study has been conducted or reported in Australia. 2.5.3 Cement-Lime-Rice Husk Ash : Soil Stabilisation Raj an et al (32) in the Karnataka Engineering Research Station, Krishnarajasagara, India have studied the effect of cement-lime-RHA admixtures on the consolidation and strength properties of black cotton soil of Yelandur in Mysore district, India. The study considered the undrained triaxial shear strength and the compression index Cc (the usual method of presenting compressibility data is to plot the void ratio, e, against the log of the vertical effective stress, v""V. Compression index is the slope of compressibility curves which plot as straight lines on the e-log v"V presentation where Cc=e0-e log ZTTp) and has revealed that:- i) In the soaked condition, the soil stabilised with RHA will have little strength. 23 ii) Rice husk ash, to a certain extent, contributes to the development of strength when used as an additive in conjunction with lime and cement which indicates that RHA may be acting in a pozzolanic role for the improvement of strength behaviour of black cotton soil. iii) In the presence of lime, rice husk ash considerably decreases the compression index. iv) For a given percentage the compression index value decreases as the quantity of lime in each proportion increases. v) The compression index values of lime-rice husk ash stabilised soil closely follow that of lime stabilised soil. No such study has been conducted or reported in Australia. 2.6 Scope for further research It can be easily seen that there are still certain gaps in the fundamental understanding of the applicability of RHA to soil stabilisation. The following are identified:- a) The results of Rajan et al (32) concerning the effect of RHA as a lone additive on the properties of soils 24 are not consistent with those results of Rahman (29). Further studies, therefore, are required to clarify this ambiguity. b) Rajan et al (32) have studied the influence of cementlime-RHA additives on the properties of clay. However, cement-RHA additives have not been contemplated and it is not known whether RHA in combination with cement alone can be used for the stabilisation of soils. c) Lazaro and Moh (30), Subrahmanyam et al (31) and Raj an et al (32) have examined the effect of lime-RHA and cement-lime-RHA Although the properties on the effect of non of properties these cohesive soils of clays additives may be only. on of the more importance, this application has not been attempted. The effect of these additives on the properties of organic clays has also not been tested. d) The effect of lime-RHA additives on some properties of soils relevant to roads and road performance are still to be defined. parameters, Such properties are the shear strength the California Bearing Ratio (CBR), shrinkage, swelling and in-service behaviour. e) The proportions of lime to RHA in the lime-RHA and cement-lime-RHA additives tested literature were all arbitrary. in the surveyed No comprehensive study 25 was made to find the optimum proportions to be used. Design procedures need to be developed to specify both proportions and best application rates for these additives to soils. f) The resultant properties due to the use of lime-RHA and cement-lime-RHA additives have not been compared with those that may result from adding lime or cement to the same soils. The economical feasibility of using RHA singly or in combination with lime or cement to stabilise soils is still to be determined. A major aim of one part of this research work is to bridge some of these gaps in the knowledge of the use of rice husk ash in soil stabilisation. 2.7 Blast Furnace Slag - Description and Production Blast furnace slag consists essentially of silicates and alumino-silicates of lime and of other bases produced simultaneously with iron in a blast furnace. An iron blast furnace is a facility for converting iron ore into iron, to the stage called 'pig iron'. The blast furnace derives its name from the fact that the air to support combustion must be forced into it under pressure because of the resistance offered by the column of raw materials to the passage of the combustion gases. 26 Iron ore is a mixture of oxides of iron, silica and alumina and the chemical reactions within the blast furnace reduce the iron oxides to iron; the silica and alumina compounds combine with the calcium of the fluxing stone (limestone and dolomite) to form the slag. The chemical reactions occur at temperatures between 1300 and 1600°C produced by the burning of coke which is fed into the furnace along with the ore, limestone and dolomite. When preheated air is blown into the furnace the oxygen combines with the carbon of the coke to produce heat and carbon monoxide. The iron ore is reduced to iron, mainly through the reaction of the carbon monoxide with the iron oxide to yield carbon dioxide and metallic iron. The fluxing stone is calcined by the heat and dissociates into calcium and magnesium oxides and carbon dioxide. These oxides of calcium and magnesium combine with the silica and alumina of the iron ore to form slag. Thus, compounds of lime-silica-alumina and magnesia are formed which collect in molten strata at temperatures between 1300 and 1600°C and which form a liquid layer that floats on top of the liquid iron. The liquid iron is tapped and run along freshly made sand channels either to the casting bed or, in the case of the most modern fully integrated works, into large torpedo cars for conveyance direct to the steel conversion works. 27 The slag is usually run into ladles having a capacity of between five and twenty tonnes or more for conveyance to the cooling pit. In some cases it is allowed to solidify in the ladle. 2.8 Types of Blast Furnace Slag 2.8.1 Air Cooled Slag When slag is allow to solidify either in the ladle or the pit, it develops a crystalline structure similar to that of a natural igneous rock. Crystals range from microscopic sizes to as large as three metres. This slag is used as road stone, concrete aggregate, filter media in sewage purification plants and as a railway ballast. 2.8.2 Foamed or Expanded Slag If water is introduced under controlled conditions into the molten slag as it is tipped into a special pit or container, the sudden generation of the occluded gases and steam produces an expanded product. This is a strong lightweight aggregate suitable for making lightweight concrete, either as building blocks or as insitu structural element for buildings, roof screed and for the decks of bridges. 28 2.8.3 Granulated Blast Furnace Slag When the molten slag is cooled rapidly by means of high pressure waterjets and excess of water is maintained, crystals do not have time to form and it solidifies as a glassy type material. This material is known as granulated slag because it takes the form of small granules. 2.9 Properties and Engineering Applications of Granulated Blast Furnace Slag (GBFS) The essential components of granulated blast furnace slag are the same oxides produced in the manufacture of Portland cement but as can be seen from Table 2.1, they are present in different proportions. Granulated blast furnace slag has marked hydraulic-setting properties when ground to a powder and mixed with an alkaline activating agent such as lime, portland cement or gypsum. Besides its use as sand, in the manufacture of concrete and certain types of glass, granulated blast furnace slag has been used in two other applications concerned with the manufacture of cement and the construction and strengthening for roads. 29 2.9.1 Use Of Granulated Blast Furnace Slag In The Manufacture Of Cement It has been said that the year 1862 marked the industrial start to the production of well integrated mixture of slag cement and clinker when Hangen in Germany confirmed what Vicat foresaw of the hydraulic properties of slag (33). Since then Germany, France, USA, Japan, South Africa and many other countries have used slag in cement manufacture. Although granulated slag itself can be used as raw material in the production of cement (34), it is more common for the slag to be utilisating slag. cement with other raw materials thereby the hydraulic-setting properties of granulated Three produced. cement blended types of blended slag cements have been The first is low heat portland blast furnace which is clinker manufactured with the by intergrinding granulated slag. portland Various specifications permit the cement to contain as much as 80% granulated slag. The second, super sulphated cement, is made from granulated blast furnace slag activated by calcium sulphate (anhydrite). It is commonly made by intergrinding a mixture of 80 to 85% granulated slag, 10 to 15% anhydrite and about 5% of portland cement or lime. slag cement, lime-slag cement about 30 to 40% hydrated slag. The third type of is manufactured by mixing lime with 60 to 70% of granulated 30 2.9.2 Use Of Granulated Blast Furnace Slag In Road Construction 2.9.2a Use Of Granulated Blast Furnace Slag In Roadworks Overseas France was the first country to utilise granulated slag in The Ponts et Chaussees Departement took road construction. a special interest in this field and carried out research and development in three of its laboratories, situated at Autum in Burgundy, Versailles. Vitri-le-Francois near Nancy and The soil stabilisation group at the Laboratoire Central in Paris undertook the more fundamental aspects of research and laboratories. work of co-ordinated work of the other This interest had arisen from the pioneer Monsieur Department, who the Prandi, showed formerly that a an engineer slow setting of the concrete is produced when 15 to 25% of granulated slag is mixed with a coarse aggregate such as limestone, or crushed air-cooled slag (35). The setting properties of this mix have made it possible to manufacture slabs giving a compressive strength of 50MPa (33). The development of this technique led the French roadmakers into further research to try to master this hardening effect with addition of lime while at the time improving the (gravel-sand mix). size distribution of "sable-grave" 31 The outcome of this research has permitted the adoption of the "grave laitier" (gravel-slag) or "sable laitier" (sandslag) which became commercially available in 1960. Similarly, in Rhodesia (now Zimbabwe) tests were carried out on various gravels, plastic quartz and granitic sand using 10 and 20% of ground and unground GBFS (41). One percent lime was added in all samples to act as a catalyst. Results have shown that:- a) In all cases there was an increase in compressive strength. b) Ground GBFS is a better material than unground GBFS even when as little as 10% is used. In Great Britain GBFS is not produced in sufficient quantities to cater for a substantial use of this kind of stabilisation (34). Any relevant research therefore, is unlikely to be found. In Japan little research concerning the application of steel slag to concrete aggregate and soil stabilisation has been established (36, 37). With an eye to the hydraulicity stimulating effects of steel slag, Haga and his associates conducted various experiments in co-operation with Hirohata 32 slab processing Co Ltd, on a mixture of crushed steel slag and GBFS, called SBS and used as fills on poor road beds and soft clay subgrades. This study (38) revealed the technical feasibility of SBS as a shielding bed fill. (Fill usually required entering to prevent poor road beds from the subgrade and to provide a working platform for plant and equipment). Although an efficient proposition regarding a useful application of GBFS to soil stabilisation in Japan is unlikely to be found (39) Hasaba and his associates (40) used X-ray diffraction analysis and scanning electron microscopy to examine the reaction products and strength characteristics of lime-gypsum-GBFS stabilised soil. Their observations indicate that:- a) The high compressive strength was mainly attributed to the formation of ettringite (3CaO-AL203-3CaS04-31H20). b) The reaction between lime and clay minerals is restricted with high gypsum content. c) A "reticulated network" type C-S-H gel and plate shaped calcium aluminate hydrate co-exist with needle like ettringite crystals in the stabilised soil containing high granulated slag content. 33 2.9.2b Use of Granulated Blast Furnace Slag in Roadworks in Australia In Australia, slag has been used in pavements since the late sixties (53) in areas from Wollongong to Newcastle. In recent years, with changes in the iron making process, the chemical composition of GBFS has altered and the crushing strength has dropped (42). Under these conditions there was concern that the slag could break down under traffic leading to rutting conditions and/or were significant implications. surfacing needed to environmental, To generate loss. resolve Realistic testing the doubt industrial and political short term the data in the which had Department of Main Roads, NSW, in co-operation with the Australian Road Research Board, arranged for an Accelerated Loading Facility (ALF) testing at the Prospect test site, 30 kilometres west of Sydney and approximately one kilometre west of the start of the Western Freeway (F4). Five base materials consisting of a control of basalt crushed rock and four other materials consisting either of slag or slag mixtures were used in the trials. Over two million load cycles were applied to 18 test sections before the trials were concluded on 23 May 1988. of these trials were:- The main findings 34 a) Unbound crushed slag had equivalent performance to high quality crushed rock as a road base under heavy traffic conditions. b) The performance of crushed rock, stabilised with 20% GBFS and 1% lime exceeded the design expectations. These findings have resulted in the use of crushed slag stabilised with cement-flyash additive as a base course at Port Kembla Access Road and Appin Road in the Wollongong regional area. Crushed slag was also used as base course at several locations on the F3 Freeway, the Pacific Highway (SH10) and Lake Macquarie district in the Newcastle regional area. Laboratory tests are currently being undertaken in the Roads and Traffic Authority Divisional Office at Wollongong to examine the performance of crushed rocks stabilised with 20% GBFS and 1% lime. A base course constituted of crushed rocks stabilised with 20% GBFS and 1% lime was also used in the trial section at Tomago on the Pacific Highway near Hexham in the Newcastle regional area in September 1989. However, the pavement developed some shrinkage approximately six months after construction. cracks This raised the concern that some measures should be taken to waterproof or slow the propagation of these cracks. 35 Although France has used GBFS to stabilise crushed rocks for almost 30 years the transverse cracking as a result of shrinkage of the hydraulic GBFS treated materials has not been successfully controlled there to date (43). A range of techniques have been used to waterproof these cracks or to slow down their propagation. These include the placement of 200mm of bituminous mix over the stabilised layers. techniques include interlayers or a bitumen 25mm impregnated thick surfacing of Other geotextile gap graded aggregate bound with polymer modified bitumen. 2.10 Scope for Further Research The application of GBFS to soil stabilisation in France and almost the entire relevant research in Australia and overseas has been restricted to the addition of 15-25% of GBFS with 1% lime to selectively graded crushed rocks or slags. In this context GBFS is mainly acting as a mechanical stabiliser with relatively little emphasis given to its hydraulic cementing effect. In contrast an important aim of the research reported here was to try and extend the use of GBFS to the stabilisation sand-silt soils and clays. of natural gravels, A totally different approach was planned, namely the use of lime-GBFS and cement-GBFS in different proportions and at low additive rate of not more than eight percent of the total dry weight of treated soils 36 to avoid the occurrence of shrinkage cracking in pavements with high percentages of GBFS. The possible partial replacement of lime or cement with GBFS and the lime-GBFS economical and feasibility cement-GBFS examined in this Thesis. for of soil the application stabilisation of are 37 Table 2.1 OXIDE Typical oxide composition of blast furnace slag compared to Portland cement, after Spence and Cook (2) BLAST FURNACE SLAG PORTLAND CEMENT CaO 35 63 Si02 35 22 A1 2 0 3 15 6 Fe 2 0 3 1.5 2.5 8 2.5 Na20 1.5 <1.0 K20 1.5 <1.0 so 3 <1.0 2.0 MgO 38 Chapter III EXPERIMENTAL TECHNIQUES AND METHODOLOGY 3.1 Scope of Chapter This chapter is concerned with a broad examination of the research programme and other an tests evaluation which were of used the various laboratory and during the research. It contains a summary of all the conventional laboratory tests used in this investigation together with a brief note on other unconventional tests used. 3.2 Existing Tests Used in Soil Stabilisation A summary of the most common tests used, in Australia and overseas, for soil stabilisation is given in Table 3.1. This table shows that the physical, chemical and engineering tests vary in number and type between different methods of stabilisation. The widest range of tests comprise those associated with bituminous stabilisation whereas only few tests are specified for evaluating stabilisation by lime or chemical additives. The assessment made by Shackel (44) of the functions fulfilled by each of the tests is included in Table 3.1. It may be seen that the majority of tests serve either in the 39 selection of a soil for stabilisation or in the design of the stabilised mix while few provide any indication of the likely in-service performance of stabilised material. 3.3 The Validity of Existing Tests Tests used to evaluate the suitability of soils for stabilisation are generally based on physical or chemical attributes and have been shown, by experience, to be satisfactory (44). By comparison, tests used in the design of stabilised mix are less satisfactory for providing a reliable indication of pavement performance in relation to mix design. The majority of engineering tests shown in Table 3.1 are based measurement of solely on static some direct strength. or Moreover, indirect even such physical criteria as those based on grading are established to promote maximum strength. However, strength improvement is not the only reason for soil stabilisation and attention should be paid to whether the treated soil is adequate in playing its role in the field application. established that In this simulation regard, tests Shackel are (45) has capable of contributing towards the evaluation of service performance and the design of stabilised mixes. simulation testing Shackel (46). The various methods of have been described and evaluated by Table 3.2 shows the suggested utilities for 40 each type of simulation test and for the major categories of stabilisation as presented by Shackel (44). These utilities were intended to reflect the amount and usefulness of the engineering information which the tests yield and do not take into account either the cost or complexity of each technique. 3.4 Tests Used in this Investigation Lime-pozzolan and cement-pozzolan stabilised materials have many of the behavioural characteristics of lime and cement stabilised materials. It is not uncommon therefore, that methods used for the evaluation of lime-pozzolan and cement-pozzolan products are similar to those required for cement and lime stabilisation (47). Therefore, in the present investigation, all of the tests associated with lime and cement stabilisation, listed in Table 3.1, were used. These tests are those concerned with grading, compaction, liquid limit, plasticity index, compressive strength and CBR. However, additional tests such as linear shrinkage, scanning electron microscopy and X-ray diffraction analysis were carried out to determine more comprehensively the physical and chemical attributes of the components of the stabilised products. In addition, a repeated dynamic load test, being the best 41 suggested technique behaviour of the (refer Table stabilised 3.2) materials to under traffic, was also used in this research work. performed in the laboratory. evaluate the simulated This was also Most of the laboratory tests used in this study were carried out in accordance with test methods specified by the Department of Main Roads, NSW. (Subsequently, Roads and Traffic Authority, NSW) (56). The titles of the methods used are listed in Table 3.3. Brief comments on these tests, together with brief notes on other tests used, are provided in the following subsections. 3.4.1 Grading and Compaction Tests Grading and compaction tests are still some of the most valuable guides to the engineering behaviour of soils in the context of road engineering. Ingles and Noble (1975) have shown that, for base course materials, these tests have high utility ( utility refers to the combined precision, cost benefit and predictive values of tests). Coarse particle and fine particle size distributions were determined, in this study, in accordance with test methods T106 and T107 (56), respectively, whereas test method T110 (56) (ie., Standard Compaction Test) was used to determine the OMC (optimum moisture content) and the maximum density to which various mixes can be compacted at this moisture content. 42 Although these tests form a part of the procedures of other tests used, they were performed primarily to determine whether or not there was an increase in density upon the addition of various additives to the soil. Improvement of grading and/or compaction of soil to higher density results in reduction in settlement, reduction in permeability and an increase in shear strength. 3.4.2 Plasticity and Volume Changes Plasticity refers to the ability of a material to deform without cracking or crumbling and then to maintain that deformed shape after the deforming force has been released. This non-reversible, or plastic, deformation is probably the sum of a large number of small slippages at grain-to-grain contact points and minute throughout the soil mass. local structure collapses Frequently, deformation occurs in soil masses without any application or removal of external loads. This may be the result of what is known as swell or shrinkage by the action of moisture change within the soil mass. Plastic deformation and volume change can become large and are important factors in highway and foundation engineering work. In most highway engineering applications, soils with high plasticity and volume change are avoided as far as possible. Where their use cannot be avoided, stabilisation 43 measures often are taken to improve soil properties (reduction of volume change and deformation). tests are available to help Laboratory identify and determine the volume change and plasticity of soils. These tests do not give a precise measurement of a definite soil property, but are merely arbitrary tests relying on a strictly standardised procedure for their wide application and reproducibility. It field of was in this general context that it was decided to use Atterberg limits and Linear Shrinkage tests as quick, convenient and standard methods, familiar differences to all engineers, for determining the in magnitude and nature of the effects of various additives on soils. Plasticity is assessed by the plasticity index which is the numerical difference between the liquid limit and plastic limit of a soil. Liquid limit can be defined as the water content corresponding to a shear strength of about 2.5 KPa (10). Liquid limit is determined by test method T108 (56). Plastic limit is the lower boundary of the range of water contents within which soil exhibits plastic behaviour. is determined by test method T109 (56). This 44 Linear shrinkage is a valuable test due to the lack of other good tests for the determination of volume It is expressed as the decrease in stability of soils. length relative to the initial length when a sample is oven dried from the liquid limit. This is determined by test method T113 (56). 3.4.3 Compressive Strength - Unconfined Compressive Strength (UCS) and Undrained Triaxial Strength (UTS) The effect of the various additives on the strength of stabilised soil has little direct application to pavement design. Compressive strength test has been used to determine the relative response of materials to cement and lime stabilisation (47) and to give an overall picture of the quality of stabilised materials. It is generally assumed that the higher the compressive strength the better the quality of stabilised mixes (48). However, it is interesting to note that the Department of Transportation , California USA, has recently reached the conclusion that: "unconfined compressive strength is more appropriate for evaluating the effects of adding lime to soils than is the result which derives from CBR and the so called "R-Value" test" (49). 45 In this study the unconfined compressive strength tests were performed in determine the accordance effect with of test adding method various T116 (56) to additives, of different proportions and at various rates of application, to different soils. Moreover, the undrained triaxial compression test was also carried out on selected stabilised mixes to determine whether or not the increase in UCS of the stabilised mixes was influenced by an increase in cohesion, angle of internal friction or both. out in accordance with Australian This test was carried Standards test method AS1289.F4.1. 3.4.4 California Bearing Ratio Test (CBR Test) The CBR test is a penetration test which gives a measure of the load spreading ability of the pavement. This is only justified in the case of flexible pavements and modified pavements (5) but not in the case of bound materials (47). There are no established criteria for demarcation between "modified" and "bound" although an arbitrary limit of 0.8MPa UCS after seven days moist curing (modified < 0.8MPa, bound > 0.8MPa). has been suggested However, there are limitations to the use of CBR tests in modified materials. Some studies suggest that it is applicable within the range of UCS between 0.5MPa and 1.5MPa, depending on the nature of 46 the physical properties of the soil,the chemical reaction with the stabiliser and on curing and preparation techniques (49). Elsewhere, it was established that it is the most suitable method to use where the stabilised strength is less than three times that of the unstabilised soil (47). Larger strength increases cementation of will usually particles, modified behaviour. result negating the extensive assumption of This large increase in strength may lead to large increase in measured CBR. 1.76MPa would from give CBR values For example, UCS of ranging from 100 to 600 depending upon soil type (3). As the original CBR procedure related all materials to a satisfactory, well graded, noncohesive crushed rock which was given the ratio 100, the significance of any value in excess of this is in question. For these reasons the application of the CBR test in this study was limited to some selected mixes. Its main role was to determine the general trend of the effect of various additives on the CBR property of soils and to confirm results derived from the UCS test. The procedures specified in test method T117 (56) were adhered to with instead of the the exception standard mould, of to extraction for the purpose of curing. using a split-mould, facilitate specimen 47 3.4.5 Repeated Dynamic Load Test 3.4.5a General The procedure for such a test was developed some years previously to utilise testing equipment already commissioned at the University of Wollongong for testing pavements. The test structure is illustrated in Figure 3.1. Due to the dimensions and restrictions of the test structure the pavement section for testing was determined as 2. Om square in area and 0.8m in depth. The pavement was loaded in the central portion by the 1000mm diameter pneumatic tyred wheel. Some longitudinal travel of the loading was obtained by allowing the pavement to oscillate up and down at one end of the pavement and having the other end on a rotating support. The principle of the operation is shown in Figure 3.2. Springs of sufficient stiffness at one end and a rotating joint at the other end were placed to allow the movement illustrated in Figure 3.2. The bin which enclosed the pavement structure was set up outside the testing frame area to facilitate filling with the pavement materials. A trolley was then used to move the 48 bin into the testing frame after the pavement structure had been compacted. The trolley and initial arrangements are illustrated in Figure 3.3. 3.4.5b The Loading System Loads are applied by a pneumatic tyred wheel, 1000mm in diameter and 200mm in width, with an inflation pressure of 0.7 MPa (approximately lOOpsi) . The maximum load which can be applied by means of a double acting servo controlled hydraulic jack is 100KN. The jack, which is connected to the tyre, is controlled by a fatigue control panel, some 20 metres away. Figure 3.4 shows the fatigue control panel in some detail. The fatigue control panel has a display meter for indication of loads and displacement. The meter may be used for the indication of mean, upper or lower peak load and deflection values. The panel has controls for selecting and applying static or dynamic loads or deflections to the pavement and an oscillator provides dynamic loads, with sine, triangular or square wave cyclic wave forms and ramp functions. counter records the number of completed cycles. A Appendix A contains a list of the panel controls and the method used in operating the panel for the test. 49 3.4.5c Measurement of the Permanent Deformation A "deflection beam" was built to measure the permanent deformation of points in a grid which covered the loaded section of the pavement. The beam was made of an aluminium channel section to which seven dial gauges were attached. The dial gauges had a 20mm travel and were graduated to 0.01mm. The reference points at which deflections were measured are illustrated in Figure 3.5. The grid was located with reference to the wheel so that the centreline of the wheel (longitudinally) and the wheel axle (transversely) coincided with the centrelines of the grid. The spacing between grid lines was chosen to be 150mm. Each grid line was labelled by either an upper or lower case letter depending on whether the longitudinal or transerve direction. grid could be referenced. grid line was in the Hence any point in the For example, the centre point of the grid, directly below the wheel, was designated as point Gd. The use of the deflection beam is illustrated in Figure 3.6. Deflection readings were taken for the whole grid, following the application of a certain number of loads, by positioning the beam on the marked points on the two bin walls. 50 3.4.6 Powder X-Ray Diffraction Powder X-ray diffraction is a method widely used in the analysis of solid solution, crystallinity and, particularly, with small angle scattering, the size and, to some extent, the shape of small particles. The diffraction technique in this study was used to identify the hydration products of lime-RHA and lime-GBFS stabilised materials. Theory of X-Ray Diffraction When a beam of monochromatic X-rays is directed onto a crystalline surface, diffraction occurs, the diffracted beam being built up of rays scattered by the atoms in the crystal lying in its path. The reinforcement of scattered rays occurs when Bragg's law is satisfied. n X = 2d sin 6 where X = d = wave length of the X-ray crystal spacing characteristic of each mineral component 0 = angle of incidence of the X-ray n = integral number By using X-rays of known wave length, and measuring the set of 6 which produced diffracted beams, d spacings of the 51 various planes in a crystal can be calculated. In the powder diffraction method, the sample is reduced to a very fine powder and placed in the beam of X-rays. Each particle is therefore a crystal oriented randomly with respect to the beam. However, some particles must be oriented so that a particular set of lattice planes makes the correct Bragg angle for the beam diffraction. The presence of a large number of particles having all possible orientations ensures that the diffracted beams represent every set of lattice planes in the crystal. The diffracted beams are detected and their intensities and associated angles determined and recorded by a movable counter. The d spacings and their associated intensities form the pattern which is characteristic of the substance. Identification of a particular substance is made with the aid of standard tables of crystal reflections and their intensities. 3.4.7 Scanning Electron Microscopy The SEM in this study was used to investigate the morphology of the reaction products of the lime-RHA and lime-GBFS soil stabilisation. The basic operation of the microscope comprises the following. Electrons emitted from the filament are 52 accelerated down the electron optical column. The electron beam is focused by three magnetic lenses onto the specimen surface as a fine probe. The probe is directed by scan coils to scan the specimen surface in the form of square rasters. The cathode ray tube screen is simultaneously scanned in synchronisation with that of the probe. Its brightness is modulated by secondary electrons leaving the specimen which are collected and amplified. There is thus a point-to-point correspondence between the CRT screen and the rasters on the specimen. progressively formed. The image of the specimen is thus The three magnetic lenses mentioned are not image forming lenses as in optical microscopes. They act as condenser lenses for the probe incident on the specimen surface. The magnification of the image is a function of geometrical effect, ie., the ratio of the size of the scanned raster on the CRT screen to that on the specimen. The range of magnification that can be achieved is from about 20 times to 10,000 times. The brightness of the image is a function of the intensity of electron emission from the irradiated surface characteristics of while the the sample contrast depends surface, eg., on the topographic features, back scatter coefficient, composition and crystal orientation. Thus high points on the sample surface would appear bright and low points dark. On smooth surfaces other characteristics determine the contrast. 53 Tests used for evaluating stabilised soils, after Shackel (44). Plasticity index X X X X O Grading X X Compaction X X X X X 0 X X X 0 Sulphate content X 0 Organic matter X O X X O Swell X o Water absorption X 0 X Permeability ^ X X Compressive strength Hveem stability Hveem cohesion Hubbard-Field stability Triaxial tests Freeze-thaw or wet or dry X 0 0 0 X 0 x X X X X X X X X x x x o o o o o o o = Test commonly used = Function fulfilled by test X X X | X Florida bearing Cone penetration O X Seepage intensity CBR 0 0 pH Linear shrinkage Performance 0 Silicification X Resin Stabilisation X Thermal Stabilisation X Bitumen Stabilisation X Lime Stabilisation Liquid limit TEST Cement Stabilisation Selection of Material Test Function Chloride Stabilisation Mechanical Stabilisation Stabilisation Technique Mix Design Table 3.1 [ 54 Table 3.2 Suggested utilities for various simulation tests, after Shackel (44). i Soil-Cement Soil-Bitumen Repeated compression C B A C B B B B Repeated tension D B B D D B B D Repeated flexure D B B D D B B D Repeated plate load D C C C B B B B Rolling load or test track D C C C A A A A B C D useful useful useful little Soil-Lime Soil-Cement TEST Soil-Bitumen Mechanical Stabilisation Mechanical Stabilisation Mix Design as primary test as secondary test supplement to conventional tests or no useful application Soil-Lime Performance Evaluation A 55 c id 1 5 2 2 •H «««««««« QQQ QQQQQQQQ 4-1 •H co •H V H u id id 1-1 "0 4-> m 3 c id 4J < to I W 0) 9 r> t- to C r» ro> <n rt H P •n *H •A •H •W n 0 &; CD 8 M M Q 0 •* r» 1-1 1-1 Ol 0) 0J <H A ja 0 O >i •P +J <-t 3 oo o O s *"3 o CO •a* r> r- 00 (T> r» r- rH a\ as rH i-H «* U rCO CT* H P- ro CO 00 0\ rH >i Ol fl)CT>00 Vl H rH 01 0) i2 t-i cr> id fl) u u A A g 0) O 0 0) o c 4O-> -P0 <D 3 h) o o Q ri 3 J 5-1 O .H >i ja .P r> ro > rH >i 3 id 0) o *3 S fa O >1 •p •H SH 0 -P 3 <: o •H . -a -^ to idc M 0) to c >i 0 -rl 4-i id 4J g • «—1. c 5; 0) -H •r| X ) id CO Cl) r-{ ^- IQ .* en to c rH •A u w 4-> 0 to •H cd i <u -u £4-> SH Q) g 4-> ^-* co O 4-1 T3 (D » •r| c CO i-H 0) •H U 4J w 4J I 0 •p •P •p id to M 0 g c id 73 id 4J 4-> id SH •W 4-1 g 10 CO 0 id ~ >H TJ r-{ id ft >1 <rl •P 0 0 u -a •H •-1 fl) CO N g id g id u -o ai U 4J 1H •H TJ -H •rl 0) 01 rH rH 0) TJ N a A CO +J id • ft CO S rH O id O -rl id >1 •rl 4-> id id (0 to TJ CO (fl 0) • X ai T) C 1 O •H •P c O 3 -H XI -P •W 3 H JQ •-H •P O •H to ai to CO 0) CO id C Oi MH c tH <u rH 0) id O 4-1 •O ,* O 0) 0 O •rl 1 rH 4J •rl c •rl 4J O c c e >i-r< !H 1H 0 •rl 0 U -H c 0 •r| •H e id -u •H rH •o si ••H 4J 4-1 Ol 1H 4J rH to id <d i d U g n> 1-1 1H 0) Qi 4-1 •a •H id id CO •rl 4J SH 0) id 3 CO id c 0 O1 id SH 1H O -H ai •-H rA 04 U fa •a (J Ol ft 0) a a> a. c 3 g il id •rl Q) X c Id -rl X rH 73 0) •o 0) co TJ c 4-> CO Tl 0) id -a MH id 4-1 4-1 3 0 C O 0) .C s: g 4-> 4-1 •H •rl • Ol u u) 3 0I) _ c d 1 73 0) ft C SH O SH CO 0 3 •rl to J3 J3 4J 4J 4J (0 4-4 CO CO a i 0 o> g 0) C0O) 0SH) ci • a > -C ft SH CO 73 •rl 4-> u ft 4J e U CO cn g SH CO 0) id in c 0 0) g Tl 0) 0) 0 4i-d1 0) •rl c SH SH id ft 4-1 H > •rl u 0) 4J g CO id s to ft CO O fl) (0 to *~. 0 0) X SH 0) > id 0 !H Tl 4-1 MH •rl •rl ft OI 01 C 0 to U Tl fl) CO 4J 4-4 g 0 •-t 4-1 0 c SH0) 0 3 0 c •H o 4J O 0 ft 0) Tl g 0 4J g rl c 0) 0) id O •c fl) SH 0) 0 i d s •c rl rl SH •c u fl) MH 4H 3 s 1 73 SH O 4-1 u C 3 c 0 to 0) H 3 CO id 0 (X •r| 4-> •rl CQ O 0) O B fl) Dc u s Q CO •rl e r-< c 0 •H • u 4-> id • -—. 0) C Q) Cn s •p 4-1 id •H •rl •-H id C id 4-1 id 3 O g 0) •r| id 0 « fl) •P CO id c o c 3 o 2 CO 73 id 0 « c •rl id X >w 0 4J C 0) g •p V4 id ft 0) Q S • a H •8 En X) in in vo r^ o o o o H H rH rH H M H H fa ooionior^Ofli O O H H H r K S O ) iHrHrHrHrHrHrHCN H H U H h f H H H CO fl! Q 56 ELEVATION PLAN FIG.3.1 - Repeated dynamic load test - View of test structure and pavement 57 WHEEL BIN FIXED X* RELATIVE MOVEMENT OF BIN TO WHEEL FIG.3.2 - Repeated dynamic load test - Principle of longitudinal movement due to rotation 53 N TEST • FRAME f WHEEL STOCKPILE OF MATERIALS • -w • J^.- — J — REMOVABLE BEAM BIN PUSHED IN TROLLEY SPRINGS " L_S TONNE'SKATE' U OFF) ELEVATION FIG.3.3 - Repeated dynamic load test - Initial setup arrangement 59 FIG.3.4 - Repeated dynamic load test - The fatigue control panel during operation 60 FIG.3.5 - DIAGRAM SHOWING GRID OF LOCATIONS AT WHICH DEFLECTION MEASUREMENTS WERE TAKEN IN RELATION TO THE WHEEL AND THE PAVEMENT BOUNDARIES TRANSVERSE DIRECTION o o o H S o o E En U W F G H Q XT AXLE H <: M Q I EH h H o o r- O o rH rH f g W w IS BOUNDARY OF PAVEMENT h 550 900mm 550 NOTES: 1. Dimensions of pavement 2. Scale is 1:20 2000 x 2000mm 61 FIG.3.6 - Repeated dynamic load test - Illustration of deflection beam in use 62 Chapter IV EXPERIMENTAL INVESTIGATION USING RICE HUSK ASH 4.1 Scope of Chapter This chapter is concerned with the experimental investigation used to determine the behaviour of rice husk ash in relation to its use in soil stabilisation. It sets the objectives of this part of the investigation, describes the materials used and details the programme and procedures for testing. The results of all the various tests used are presented. 4.2 Objectives of Investigation The main aims of the investigation reported in this chapter are as follows: a) To study the influence of rice husk ash as a single additive on various properties of a range of soils. b) To examine the effects of lime-rice husk ash and cement-rice husk ash additives on the properties of soils. 63 4.3 Materials Used 4.3.1 Rice Husk Ash The rice husk ash used was a light-weight, fine black ash produced in Griffith, NSW, and brought in 200 litre drums to the Department of Civil and Mining Engineering, University of Wollongong. The specific gravity of the sample was 1.79 and the grading was: % passing 2.36mm 100 % passing 425 pirn 60 % passing 75 pm 17 % passing 13.5 /jm 12.5 The chemical analysis of the sample was: Si02 58.2% A1203 0.10% Fe203 1.09% CaO 0.37% MgO 0.21% Na20 0.21% K20 1.37% Loss on ignition 34.2% 64 4.3.2 Cement 'Kandos' commercial grade, ordinary portland cement was used, conforming to Australian standards (AS1315) as given below: Loss on ignition Max 3.1% Insoluble residue Max 2.1% Sulphuric anhydride (SO3) Max 3.1% Magnesia Max 4.2% Time for initial set •£ 1 hour Time for final set $> 12 hours 4.3.3 Lime 'Blue Circle' commercial grade, hydrated lime was used, conforming to Australian standards (AS1672) as given below: Ca(OH)2 > 70% MgO < 4.5% C02 < 5% Particles Fineness, passing 250/jm <$ 98% 4.3.4 Soils Four soils were selected to be stablised and tested in this investigation. 65 Soil A was a crushed rock conglomerate from a deposit known as Yeoman's Pit in the Shire of Guyra, NSW. Soil B was taken from a sandy silt pit at Stone Henge in the Shire of Severn, NSW. Soil C was an organic clay taken from a construction site in the town of Glen Innes, NSW. were taken in Samples of these three soils plastic bags and kept in the laboratory of the Divisional Office of Road and Traffic Authority at Glen Innes to be used as and when required. Soil D was a marginal roadbase material consisting of igneous dolerite crushed rock. This material was quarried at Prospect in the western suburbs of Sydney, NSW. cubic metres of this material was obtained from Four local suppliers by the Department of Civil and Mining Engineering, University of Wollongong and used in the repeated dynamic load tests. The properties of the four soils (A,B,C and D) are shown in Table 4.1. 4.4 Testing Regime RHA varies according to the environment in which the combustion of the rice husks takes place. The variations 66 are reflected in the chemical composition of the RHA with particular emphasis on carbon content. The pozzolanic reaction between lime, either added directly or from the hydration reaction of cement and RHA is governed largely by the carbon content of the ash. It was considered that initial testing be carried out to determine RHA reactivity and the optimum ratio of lime or cement to RHA. The second step in the programme was then to treat the three soils A, B and C with lime-RHA and cement-RHA additives at their optimum and practical ratios. Soils A, B and C were also teated with cement, lime and RHA single additives. The treated soils were then subjected to the various laboratory tests described in Chapter 3. The final stage in the programme was to treat soil D with various additives in the light of best results, derived from the second step in the programme and subject this treated soil to the repeated dynamic load test described in Chapter 3. 4.5 Initial tests - optimum ratios of lime to RHA and cement to RHA The use of an unconfined compressive strength test on lime-RHA and cement-RHA paste specimens was selected as a suitable indicator of the RHA reactivity. 67 4.5.1 Preparation, curing and testing of specimens Dry mixtures of lime-RHA and cement-RHA were prepared, mixed and proportioned by weight. The ratio of lime to RHA and cement to RHA was in the range of 1:1 to 1:10. of compacted specimens were then prepared Two series at optimum moisture content using standard Proctor equipment. All specimens were wrapped in paper, aluminium foil and contained in plastic bags at constant (22°C) during the curing periods. room temperature At the conclusion of the various curing periods (28 days and 90 days) the specimens were air dried for approximately 30 minutes and subjected to the unconfined compressive strength test. The results of the UCS tests on the lime-RHA paste specimens are presented in Figure 4.1, whereas those of cement-RHA paste specimens are presented in Figure 4.2. The results presented in Figure 4.1 for both curing periods (28 days and 90 days) indicate that the optimum ratio of lime to RHA is the ratio 1:2. Figure 4.2 shows that there is no optimum ratio of cement to RHA. This is indicative that the strength of cement-RHA pastes is dominated by the hydration reactions of cement rather than by the pozzolanic reaction between the released lime and the RHA. 68 4.6 Treatment of soils with various additives Various additives, namely RHA, lime, lime-RHA, cement, cement-RHA, were used individually to stabilise the soils (A,B & C). The various quantities of additives were 2%, 4%, 6% and 8% of the total weight of the dry soil and additive. The ratio of lime to RHA for each quantity of additive was varied as 1:1, 1:2, 1:3 and 1:4. Although the ratio 1:2 was found to be the optimum ratio of lime to RHA (section 4.5), the values 1:1, 1:3 and 1:4 were considered to be within the practical range. The initial testing indicated that no optimum ratio of cement to RHA occurs (section 4.5). In the test series the values 1:1, 1:2, 1:3 and 1:4 were considered to be within the practical range and were used for comparison. 4.7 Testing of stabilised soils 4.7.1 Compaction characteristics The optimum moisture contents (OMC) and the maximum dry densities (MDD) of soils stabilised with various additives and various quantities (section 4.6) were determined by carrying out the standard compaction test T110 (56). test results are presented in Tables 4.2 and 4.3. The 69 4.7.2 Unconfined compressive strength Three series of specimens of soils stabilised with the various additives and various quantities were prepared and compacted to their maximum dry densities at their OMC using the standard compaction test equipment. All specimens were wrapped in paper, aluminium foil and contained in plastic bags at constant room temperature (22°C) during the curing periods. At the conclusion of the various curing periods (7 days, 28 days, 90 days) the specimens were air dried for 30 minutes and then subjected to unconfined compression. are shown in Tables 4.4 and 4.5. The results The 90 days test results for the treated soil A, B and C are also shown in Figures 4.3 and 4.4. 4.7.3 Linear shrinkage The linear shrinkage of all mixes was determined using materials collected from unconfined compressive strength crushed specimens which had been previously cured for 7 and 28 days. The materials were ground using a porcelain mortar and rubber pestle to produce samples passing a 2.36mm sieve. The prepared samples were air dried and sufficient water was then added to the samples to bring them to a consistancy 70 similar to the liquid limit. Shrinkage samples were prepared using linear shrinkage moulds of 250mm length. After air drying and subsequent oven drying, values of linear shrinkage were determined. The results are presented in Tables 4.6 and 4.7, results of the 28 days curing period are shown in Figures 4.5 and 4.6. 4.7.4 Atterberg limits Plastic limit, liquid limit and plasticity index of all mixes were determined using materials collected from unconfined compressive strength crushed specimens which had been previously cured for 7 and 28 days. of each specimen were collected and Individual pieces ground to powder fraction using a porcelain mortar and rubber pestle. All prepared fractions were then air dried and subjected to testing. The Atterberg limits of the various treatments after the curing periods of 7 days and 28 days are given in Tables 4.6 and 4.7. The results of the plasticity index of the 28 days curing period also are given in Figures 4.7 and 4.8. 71 4.7.5 Effect of delay in compaction on the strength of stabilised soils. It was decided that limited testing of some of the soil mixes would be sufficient for determining the general trend of the effect of delay in compaction on the strength of the stabilised soils. Samples of dry soil A were mixed with cement and cement-RHA additives. The ratio of cement to RHA was varied as 1:1 and 1:4, whereas the quantity of additives used in each case was 8% of the total dry weight of the treated soil. Samples of dry soil C also were mixed with lime and lime-RHA additives. The ratio of lime to RHA was varied as 1:1 and 1:3, whereas the quantity of additives used in each case was 8% of the total dry weight of the treated soil. Water was added and every mix was put in a covered metal container periods. and maintained at its OMC during the delay At the conclusion of the various delay periods (2 hours, 4 hours, 6 hours and 24 hours) the various mixtures were immediately compacted using the standard compaction test equipment. The compacted specimens were then wrapped in paper, aluminium foil and contained in plastic bags at constant 72 room temperature (22°C) for 90 days. the 90 days curing period the unconfined compression. At the conclusion of specimens were subjected to The strength of these specimens is given in Tables 4.8 and 4.9. The losses in strength due to delays in compaction, expressed as percentage of strength of undelayed compaction specimens, also are given in Tables 4.8 and 4.9 and shown in Figures 4.9 and 4.10. 4.7.6 Effect of various additives on the shear strength parameters of soils As discussed in section 3.4.3, the undrained triaxial compression test was carried out on selected stabilised mixes to determine whether or not the increase in UCS of stabilised mixes was influenced by an increase in cohesion, angle of internal friction or both. Samples of dry soil B were mixed with cement and cement-RHA additives. 1:4. The ratio of cement to RHA was varied as 1:2 and The quantities of additives in each case were 4% and 8% of total dry weight of the treated soil. Samples of dry soil C also were mixed with lime and lime-RHA additives. 1:3. The ratio of lime to RHA was varied as 1:1 and The quantities in each case were 4% and 8% of the total dry weight of the treated soil. 73 Water was added and every mix was compacted at its OMC using standard compaction test equipment. A thin walled steel pipe was driven into the compacted mixes to collect two cylindrical specimens, 50mm in diameter, from each compacted mix. The specimens were extruded from the pipe by pushing them with a manual jack extruder. The specimens were then trimmed to size (50mm dia x 100mm) by cutting with a sharp edge spatula. All prepared specimens were wrapped in paper, aluminium foil and put in pastic bags at constant room temperature (22°C) during the curing periods. At the conclusion of the various curing periods (7 and 28 days) the specimens were subjected to the unconsolidated, undrained test in accordance with Australian Standards test method AS1289.F4.1. Data obtained from the tests were used to plot a Mohr's stress circle using the cell pressure cr3 and the corresponding major principal stress a\ at specimen failure. By plotting two Mohr's circles using test data based on different initial cell pressure a3 for each test and on two identical specimens of every mix, an approximate tangent to the circles was established. The slope of this tangent was taken as angle of internal friction 0, of the mix, and the intercept of the tangent on the Y axis was taken as the cohesion C in Coulomb's equation ( T = C + crn tan 0) . The values of 0 and C for the various mixes are given in Tables 4.10 and 4.11. 74 4.7.7 Effect of various additives on the CBR value of soils As discussed in section 3.4.4, there are limitations to the use of CBR tests in the context of stabilised materials. However, application of the CBR test in this study was limited to some selected mixes. determine the general trend Its main role was to of additives on the CBR property the of effect soils of various and to confirm results derived from the UCS test. Dry samples of soil A, B and C were mixed with RHA, lime-RHA and cement-RHA additives. cement to RHA was The ratio of lime to RHA and varied as 1:1, 1:2 and 1:3. The quantities of additives in each case were 4% and 8% of the total dry weight of treated soil. Cement and lime, at the rates of 2% and 4% of total dry weight of treated soil, also were used for comparison. Water was added and all mixes were compacted at their OMC in accordance with the standard procedures of the CBR test with the exception of using a special split CBR mould to facilitate specimen extraction for the purpose of curing. The split mould was opened and the specimens were taken out, wrapped in paper, aluminium foil and put in plastic bags at constant room temperature (22°C) during the curing periods. 75 At the conclusion of the various curing periods (28 days and 90 days) the specimens were put again in the split mould, the surcharge weights were added and the specimens were subjected to the standard piston penetration at a uniform rate of 1.27mm per minute. The CBR values of the various mixes for the various curing times are presented in Tables 4.12 to 4.14, and the results of the 90 days curing period are shown in Figures 4.11 to 4.13. 4.7.8 Repeated dynamic load test This test was conducted on six pavements. Soil D stabilised with various additives formed the base course of five pavements, whereas the untreated soil D formed the control base course of the sixth pavement. The various additives used to stabilise soil D were cement, lime, RHA, cement-RHA and lime-RHA mixtures. The ratio of cement to RHA and lime to RHA used was 1:1, whereas the quantity of additives used was 1.5%, 2%, 8%, 3% and 3% respectively and expressed as percentage of the total dry weight of the treated soil. The sub-base of all of the six pavements consisted of beach sand from the Illawarra region. of sand was as follows: Particle size distribution 76 % passing 1.18mm sieve 100 % passing 600 ym sieve 90 % passing 425 pm. sieve 74 % passing 300 pm sieve 49 % passing 150 pm sieve 5 % passing 75 pm sieve 0 The sand sub-base was placed, by shovel, in the bin in its natural state (moisture content 3%) in six, approximately 100mm thick layers and compacted. plate compactor was used to A walk-behind vibratory compact the layers. The compaction was carried out until the layer showed no further movement under the compacting equipment. The top of the surface was then levelled and screeded with an appropriate implement. A protective section of stiff rubber conveyor belting (900mm x 600mm x 20mm thick) was put in the centre of the sub-base surface. This material was selected because it is compressible, elastic and maintains its properties in all tests. Thus the results from the tests can be related to the various stabilised pavement bases. The various stabilised base materials were mixed and prepared at their OMCs and then placed, by shovel, in two layers of 100mm thickness. carried out compactor. by using Compaction of the two layers was a walk-behind vibratory plate 77 Once the material containment bin had been filled and the pavement constructed, the next step was to assemble and connect all the components to allow the test to proceed. Prior to the bin being pushed into place under the wheel, the springs were tied to the bin (see Figure 3.3). With the aid of a block and tackle and some manpower the bin was rolled into position by means of the 'skate' trolley. The trolley was then removed by raising the bin clear of the trolley. This was done as follows: Two hydraulic hand operated jacks were placed at position A and B beneath channels supporting the bin (see Figure 4.20). They were then jacked up simultaneously causing the eastern side of the bin to rise and to rotate about axis E of the trolley. Continued lifting of the bin resulted in the semi- circular bearer of the hinge joint (line C-D) resting on the test frame. Further raising caused rotation about line C-D. The raising continued until the tolley was completely free and could be removed. The pressure on the jacks was then released slowly allowing the springs on the eastern side to be positioned over the bearing plates on the testing frame. Once the springs were located, the jacks were completely released. After the pavement had been constructed and the test rig assembled, zero readings were taken at the grid points at 78 which the deflections were to be measured. The pavement was covered by a damp cloth and cured for 7 days. At the conclusion of the curing period the pavement was subjected to 50,000 42kN load applications during which deflection readings were taken at intervals. The basic criteria for the evaluation of the stabilised road bases was the relationship between the load and deformation. In total, 840 readings were taken of the deflections of various pavements at various intervals during the tests and at various positions on the pavements. The results of the deflections are given in a tabular form in Tables 4.15 to 4.20. Figures 4.14. to 4.19 show the deflections of pavements after the various intervals at the cross sections of the maximum deflections. 4.7.9 Scanning Electron Microscopy It was decided that limited testing of some of the soil mixes would be sufficient for determining the morphology of the RHA pozzolanic reaction products in soil stabilisation. Samples of untreated Soil A, untreated Soil C, lime-RHA treated Soil A and lime-RHA treated Soil C were compacted at their OMC using the standard compaction test equipment. The ratio of lime to RHA was 1:1 and the quantity of lime-RHA additive was 8% of the total dry weight of the treated soil. 79 Each sample of the treated soils was then wrapped in wet newspaper, sealed with aluminium foil, put in an oven bag and stored for 7 days in an oven at a maintained temperature of 65°c. At the conclusion of this accelerated curing, all samples were fractured and small specimens of the fractured materials were taken for testing. The specimens were of the order 8-12mm maximum dimensions and had a length to width ratio in the general range of 1:1 to 2:1. The thickness was in the range 4-6mm. All specimens were oven dried at 110°c for 24 hours and then glued to aluminium stubs with organic adhesive. The specimens were coated with a thin layer of gold alloy to provide an electrically conducting surface. The surface from the gold layer to the stub was also painted with silver to ensure a good electrical contact with the stub. All specimens were then examined in a Hitachi S450 Scanning Electron Microscope and micrographs were obtained. These micrographs are shown in Figures 4.21 to 4.24. 4.7.10 Powder X-ray Diffraction Analysis. X-ray diffraction patterns were determined for all soil mixes used in the preceding scanning electron microscopy examination. 80 Samples of the fractured material of the treated and untreated Soils A and C were pulverised with a mortar and pestle to produce a powdered material suitable for placing in aluminium mounts ready for powder X-ray diffractometry (Cukoc Source). Figures 4.25 to 4.28 show the X-ray diffraction patterns determined for the untreated Soil A, untreated Soil C, lime-RHA treated treated Soil C. Soil A and lime-RHA 81 Table 4.1 Properties of Soils Properties Soil A Soil B Soil C Soil D 1. Grading % passing 19mm 9 .5mm 4.75mm 2.36mm 425pm 75pm 13.5pm 100 73 36 22 15 8 4 100 100 100 85 43 24 17 100 100 100 100 85 71 53 100 88 69 43 16 4 2. Atterberg limits L.L P.L P.I 33 24 9 32 24 8 100 45 55 22 16 6 3. Volume stability Linear shrinkage % 3.5 2.75 17 - 4. Compaction characteristics OMC % Max dry density g/cm3 13 1.83 15 1.82 22 1.32 9.00 2.01 5. Unconfined compressive strength (MPa) .33 .26 .21 - 6. Unified soil classification GMu SMu OH GW Gravel/sand Sand Organic Well graded silt mix silt mix clay gravel/sand 7. Description mix 8. Colour White Reddish Black brown 9. Specific gravity 2.93 2.86 2.83 Blue 82 T A B L E 4.2a ADDITIVE Compaction characteristics of lime, R H A and Lime-RHA stabilised soil A OMC (%) (%) MDD gnn/cm3 LIME LIME:RHA 0% 2% 4% 6% 8% 1:1 13.00 14.50 16.00 16.50 17.00 1.83 1.82 1.77 1.74 1.73 0% 2% 4% 6% 8% 13.00 15.00 16.00 16.50 17.00 1.83 1.82 1.77 1.74 1.73 LIME:RHA 1:2 13.00 15.00 16.00 16.50 17.00 1.83 1.82 1.76 1.73 1.73 LIME.RHA 0% 2% 4% 6% 8% 1:3 13.00 15.00 16.00 16.50 17.50 1.83 1.81 1.76 1.73 1.72 LIME:RHA 0% 2% 4% 6% 8% 1:4 0% 2% 4% 6% 8% 13.00 15.00 16.00 17.00 18.50 1.83 1.81 1.75 1.72 1.69 0% 2% 4% 6% 8% 13.00 15.00 16.50 17.50 18.50 1.83 1.79 1.74 1.70 1.66 RHA 83 T A B L E 4.2b ADDITIVE Compaction characteristics of lime, R H A and lime-RHA stabilised soil B (%) OMC (%) MDD gm/cm 3 LIME LIME:RHA 0% 2% 4% 6% 8% 1:1 15.00 16.00 16.50 17.00 18.00 1.82 1.81 1.78 1.75 1.73 0% 2% 4% 6% 8% 15.00 16.00 16.00 17.00 18.50 1.82 1.80 1.77 1.73 1.70 LIME:RHA 1:2 15.00 16.00 16.00 17.00 19.00 1.82 1.79 1.76 1.72 1.66 LIME:RHA 0% 2% 4% 6% 8% 1:3 15.00 16.50 16.50 17.50 19.00 1.82 1.78 1.76 1.70 1.66 LIME:RHA 0% 2% 4% 6% 8% 1:4 0% 2% 4% 6% 8% 15.00 16.50 16.50 18.00 19.00 1.82 1.78 1.76 1.70 1.65 0% 2% 4% 6% 8% 15.00 16.00 16.00 17.00 19.00 1.82 1.78 1.76 1.70 1.65 RHA 84 Compaction characteristics of lime, R H A and lime-RHA stabilised soil C T A B L E 4.2c ADDITIVE (%) OMC (%) MDD gm/cm3 LIME 22.00 23.00 24.00 24.50 25.00 1.32 1.32 1.31 1.30 1.29 22.00 23.00 24.00 25.00 26.00 1.32 1.30 1.26 1.24 1.21 22.00 23.00 24.50 26.00 26.50 1.32 1.29 1.27 1.23 1.23 0% 2% 4% 6% 8% 22.00 24.00 25.00 26.00 27.00 1.32 1.26 1.25 1.23 1.22 0% 2% 4% 6% 8% 22.00 24.00 25.00 26.00 26.00 1.32 1.28 1.24 1.22 1.21 0% 2% 4% 6% 8% LIME:RHA 1:1 0% 2% 4% 6% 8% LIME:RHA 1:2 0% 2% 4% 6% 8% LIME:RHA 1:3 RHA 85 T A B L E 4.3a ADDITIVE Compaction characteristics of cement, R H A and cementR H A stabilised soil A OMC (%) (%) MDD gin/cm3 CEMENT 0% 2% 4% 6% 8% CEMENT:RHA 1:2 13.00 14.00 14.50 15.50 16.50 1.83 1.85 1.85 1.85 1.85 0% 2% 4% 6% 8% 13.00 14.00 14.50 15.50 16.50 1.83 1.83 1.81 1.75 1.76 0% 2% 4% 6% 8% CEMENT:RHA 1:4 13.00 14.00 14.50 16.00 17.00 1.83 1.83 1.80 1.78 1.73 0% 2% 4% 6% 8% 13.00 14.50 15.00 16.00 17.50 1.83 1.81 1.78 1.76 1.72 0% 2% 4% 6% 8% 13.00 15.00 16.50 17.50 18.50 1.83 1.79 1.74 1.70 1.66 CEMENT:RHA 1:3 RHA 86 T A B L E 4.3b ADDITIVE Compaction characteristics of cement, R H A and cementR H A stabilised soil B OMC (%) (%) MDD gm/cm3 CEMENT 0% 2% 4% 6% 8% CEMENT:RHA 1:2 15.00 15.50 16.50 17.00 17.50 1.82 1.82 1.84 1.84 1.84 0% 2% 4% 6% 8% 15.00 16.00 17.00 17.50 18.00 1.82 1.82 1.78 1.73 1.70 0% 2% 4% 6% 8% CEMENT:RHA 1:4 15.00 16.00 17.00 17.50 18.50 1.82 1.82 1.78 1.72 1.68 0% 2% 4% 6% 8% 15.00 16.00 17.00 17.50 18.50 1.82 1.82 1.76 1.71 1.67 0% 2% 4% 6% 8% 15.00 16.00 16.00 17.00 19.00 1.82 1.78 1.76 1.70 1.65 CEMENT:RHA 1:3 RHA 87 T A B L E 4.3c ADDITIVE Compaction characteristics of cement, R H A and cementR H A stabilised soil C. OMC (%) (%) MDD gm/cm 3 CEMENT 0% 2% 4% 6% 8% CEMENT:RHA 1:1 22.00 23.00 24.50 25.00 26.00 1.32 1.34 1.35 1.39 1.40 22.00 24.00 25.00 26.00 27.00 1.32 1.32 1.30 1.28 1.26 22.00 24.00 25.00 26.00 27.00 1.32 1.31 1.29 1.26 1.25 0% 2% 4% 6% 8% 22.00 24.00 25.00 26.00 27.00 1.32 1.30 1.28 1.26 1.24 0% 2% 4% 6% 8% 22.00 24.00 25.00 26.00 26.00 1.32 1.28 1.24 1.22 1.21 0% 2% 4% 6% 8% CEMENT:RHA 1:2 0% 2% 4% 6% 8% CEMENT:RHA 1:3 RHA 88 TABLE 4.4a ADDITIVE U C S (MPa) of lime, R H A and lime-RHA stabilised soil A (%) 7 C U R I N G (DAYS) 90 28 LIME 0% 2% 4% 6% 8% LIME:RHA 1:1 0.33 0.43 0.46 0.43 0.41 0.33 0.55 0.76 0.73 0.70 0.33 0.69 1.00 0.95 0.90 0% 2% 4% 6% 8% 0.33 0.36 0.63 0.61 0.58 0.33 0.50 0.68 0.73 0.71 0.33 0.55 0.92 1.00 0.97 0.33 0.36 0.60 0.58 0.55 0.33 0.45 0.68 0.70 0.68 0.33 0.58 0.85 0.92 0.89 0.33 0.35 0.64 0.58 0.52 0.33 0.45 0.68 0.70 0.65 0.33 0.50 0.75 0.82 0.81 0% 2% 4% 6% 8% 0.33 0.34 0.46 0.44 0.44 0.33 0.45 0.50 0.48 0.46 0.33 0.50 0.66 0.67 0.65 0% 2% 4% 6% 8% 0.33 0.33 0.34 0.34 0.34 0.33 0.34 0.34 0.34 0.34 0.33 0.34 0.34 0.34 0.34 LIME:RHA 1:2 0% 2% 4% 6% 8% LIME:RHA 1:3 0% 2% 4% 6% 8% LIME: R H A 1:4 RHA 89 TABLE 4.4b ADDITIVE U C S (MPa) of lime, RHA and lime-RHA stabilised soil B (%) 7 C U R I N G (DAYS) 90 28 LIME 0% 2% 4% 6% 8% LIME:RHA 1:1 0.26 0.32 0.34 0.28 0.27 0.26 0.40 0.42 0.38 0.36 0.26 0.50 0.57 0.50 0.45 0% 2% 4% 6% 8% 0.26 0.30 0.40 0.34 0.34 0.26 0.38 0.46 0.41 0.38 0.26 0.45 0.54 0.53 0.48 0.26 0.27 0.36 0.33 0.32 0.26 0.31 0.43 0.39 0.36 0.26 0.41 0.52 0.52 0.45 0% 2% 4% 6% 8% LIME:RHA 1:4 0.26 0.26 0.28 0.28 0.27 0.26 0.30 0.32 0.32 0.30 0.26 0.40 0.45 0.46 0.38 0% 2% 4% 6% 8% 0.26 0.26 0.26 0.26 0.26 0.26 0.31 0.32 0.32 0.29 0.26 0.36 0.42 0.43 0.35 0% 2% 4% 6% 8% 0.26 0.24 0.24 0.24 0.25 0.26 0.24 0.24 0.24 0.25 0.26 0.24 0.24 0.24 0.25 LIME:RHA 1:2 0% 2% 4% 6% 8% LIME:RHA 1:3 RHA 90 TABLE 4.4c ADDITIVE U C S (MPa) of lime, RHA and lime-RHA stabilised soil C (%) 7 C U R I N G (DAYS) 90 28 LIME 0% 2% 4% 6% 8% 0.21 0.25 0.34 0.43 0.41 0.21 0.30 0.41 0.51 0.50 0.21 0.33 0.44 0.56 0.55 0% 2% 4% 6% 8% 0.21 0.24 0.26 0.34 0.34 0.21 0.27 0.34 0.41 0.39 0.21 0.31 0.37 0.45 0.44 0.21 0.23 0.25 0.29 0.33 0.21 0.25 0.30 0.34 0.37 0.21 0.27 0.32 0.39 0.41 0% 2% 4% 6% 8% 0.21 0.24 0.24 0.26 0.29 0.21 0.24 0.26 0.30 0.32 0.21 0.25 0.29 0.33 0.35 0% 2% 4% 6% 8% 0.21 0.21 0.22 0.23 0.23 0.21 0.21 0.22 0.23 0.23 0.21 0.21 0.22 0.23 0.23 LIME: R H A 1:1 LIME:RHA 1:2 0% 2% 4% 6% 8% LIME:RHA 1:3 RHA 91 TABLE 4.5a ADDITIVE U C S (MPa) of cement, RHA and cement-RHA stabilised soil A (%) 7 CURING (DAYS) 90 28 CEMENT 0% 2% 4% 6% 8% 0.33 1.26 1.75 2.45 3.00 0.33 1.95 2.70 3.50 4.30 0.33 2.00 3.15 4.00 4.60 0.33 0.68 1.00 1.40 1.75 0.33 0.98 1.65 2.10 2.30 0.33 1.35 2.27 2.53 3.10 0.33 0.62 0.90 1.25 1.50 0.33 0.80 1.25 1.68 2.00 0.33 1.08 1.70 2.30 2.70 0% 2% 4% 6% 8% 0.33 0.52 0.70 0.57 1.00 0.33 0.55 0.85 1.10 1.40 0.33 0.70 1.10 1.42 1.80 0% 2% 4% 6% 8% 0.33 0.33 0.34 0.34 0.34 0.33 0.34 0.34 0.34 0.34 0.33 0.34 0.34 0.34 0.34 CEMENT:RHA 1:2 0% 2% 4% 6% 8% CEMENT:RHA 1:3 0% 2% 4% 6% 8% CEMENT:RHA 1:4 RHA 92 TABLE 4.5b ADDITIVE U C S (MPa) of cement, R H A and cement-RHA stabilised soil B (%) 7 C U R I N G (DAYS) 90 28 CEMENT 0% 2% 4% 6% 8% CEMENT:RHA 1:2 0.26 0.43 0.62 0.90 1.40 0.26 0.67 1.02 1.50 2.30 0.26 0.74 1.15 1.70 2.57 0.26 0.28 0.35 0.48 0.55 0.26 0.42 0.60 0.77 0.90 0.26 0.57 0.83 1.05 1.25 0.26 0.28 0.32 0.45 0.48 0.26 0.37 0.51 0.69 0.82 0.26 0.55 0.75 1.00 1.18 0% 2% 4% 6% 8% 0.26 0.26 0.31 0.42 0.45 0.26 0.32 0.42 0.50 0.61 0.26 0.40 0.52 0.62 0.77 0% 2% 4% 6% 8% 0.26 0.24 0.24 0.24 0.24 0.26 0.24 0.24 0.24 0.24 0.26 0.24 0.24 0.24 0.25 0% 2% 4% 6% 8% CEMENT:RHA 1:3 0% 2% 4% 6% 8% CEMENT:RHA 1:4 RHA 93 TABLE 4.5c ADDITIVE U C S (MPa) of cement, RHA and cement-RHA stabilised soil C (%) 7 C U R I N G (DAYS) 90 28 CEMENT 0% 2% 4% 6% 8% CEMENT:RHA 1:1 0.21 0.25 0.32 0.42 0.48 0.21 0.32 0.41 0.52 0.60 0.21 0.35 0.46 0.58 0.70 0.21 0.23 0.25 0.30 0.39 0.21 0.26 0.29 0.35 0.41 0.21 0.28 0.37 0.43 0.48 0.21 0.22 0.24 0.30 0.32 0.21 0.25 0.26 0.32 0.37 0.21 0.27 0.32 0.37 0.41 0% 2% 4% 6% 8% 0.21 0.21 0.23 0.28 0.26 0.21 0.23 0.26 0.30 0.32 0.21 0.26 0.30 0.34 0.37 0% 2% 4% 6% 8% 0.21 0.21 0.22 0.23 0.23 0.21 0.21 0.22 0.23 0.24 0.21 0.21 0.22 0.23 0.24 0% 2% 4% 6% 8% CEMENT:RHA 1:2 0% 2% 4% 6% 8% CEMENT:RHA 1:3 RHA 94 u JS o m o m tn o o o m o o o o o m u in r« in CN CN co rH o o o m in in r- m ro CN rH o o m in in o r- a ^ o o o o o o o o o o OS en m «-H o rH z M PO CN rH rH O o m in m in O o o o m in r- r- CN r- in o m m r("0 rH rH rH O ro ro CN rn o o o o o o o o in o o O O O O O O O O O O o o o o o o o in o o O O O O O O O O O O OS VO •<»• CN rH CM t~- VO rH ro at oo vo in ^* otcsMsm o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o •"** co O EU EU «* CN OS VO O O O O O O O O O O ** ai m oo CN CN CN ro co ** o o o o o o o o o o o o o o o o o in in m o m CN r» CM o ro ro CN CN CN o o o o o o o in in in as as t-» vo m Doe 1 00 CN •dP O 1" r-l CO 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O Ol iH ro Ol H h M O i n dP dP dP dP dp O CNtf*VO CO © . . . . r^ . . . . • © © in © rH 00 CO P- P- © H ttf oi r~ H Ol CO P~ P- © . . . . © vo C N oi in H Ol Ol CO CO dP dP dP dP dP O CNtf*VO CO dP dP dP dP dP © CNtf"VO CO dp dP dP dP dP © CNtf*VO CO dP dP dP dP dP O CN "tf VO CO H CN ro oi CN r~ vo ?—i ^^ dP a. aa H rH rH 03 £ *iOS £K •a Cd > H EH os EH EH Z •• Z Cd X Cd U •• H pj Q § Cd Z Cd X Cd U U § EH . . . . • * • EH Z H X Cd u P 2 100 T A B L E 4.8 Additive % Effect of delay in compaction on the U C S of lime and lime-RHA stabilised soil C. Time elapsed Since mixing 90 days U C S (MPa) loss in strength % 8 % LIME 0.00 hours 2.00 hours 4.00 hours 6.00 hours 24.00 hours 0.55 0.52 0.51 0.51 0.48 0.00 5.45 7.27 7.27 12.72 0.00 hours 2.00 hours 4.00 hours 6.00 hours 24.00 hours 0.44 0.42 0.41 0.40 0.39 0.00 4.50 6.80 9.09 12.04 0.00 hours 2.00 hours 4.00 hours 6.00 hours 24.00 hours 0.35 0.33 0.32 0.32 0.30 0.00 5.70 8.57 8.57 14.28 8 % LIME: R H A 1:1 8%LIME:RHA1:3 101 T A B L E 4.9 Effect of delay in compaction on the U C S of cement and cement-RHA stabilised soil A. Additive % Time elapsed Since mixing 90 days loss in U.C.S. (MPa) strength % 8% CEMENT 0.00 hours 2.00 hours 4.00 hours 6.00 hours 4.60 3.22 2.34 1.47 0.00 30.00 49.00 68.00 0.00 2.00 4.00 6.00 hours hours hours hours 3.10 2.82 2.60 2.44 0.00 9.00 16.00 21.00 0.00 2.00 4.00 6.00 hours hours hours hours 1.80 1.65 1.55 1.51 0.00 8.00 14.00 16.00 8% CEMENT:RHA 1:2 8% CEMENT: RHA 1:4 102 T A B L E 4.10 Effect of lime and lime-RHA additives on the shear strength parameters of Soil C. ADDITIVES 7 DAYS CURING Lime 0% 4% 6% Lime: RHA 1:1 0% 4% 8% Lime: RHA 0 (degrees) C (MPa) 28 D A Y S C U R I N G 0 (degrees) C (MPa) 7.0 30.0 28.0 0.08 0.16 0.23 7.0 35.5 33.0 0.08 0.17 0.22 7.0 20.0 34.5 0.08 0.12 0.15 7.0 21.0 38.0 0.08 0.13 0.17 7.0 13.0 21.0 0.08 0.11 0.11 7.0 15.5 25.0 0.08 0.12 0.14 1:3 0% 4% 8% 103 T A B L E 4.11 Effect of cement and cement-RHA additives on the shear strength parameters of Soil B. 7 DAYS CURING ADDITIVES 0 (degrees) Cement 0% 4% 8% Cement: RHA 1:2 Cement: RHA C(MPa) 28 DAYS CURING 0 (degrees) C(MPa) 19.0 36.5 44.0 0.08 0.11 0.16 19.0 40.0 46.0 0.08 0.19 0.29 0% 4% 8% 1:4 19.0 30.0 31.0 0.08 0.12 0.16 19.0 37.0 38.0 0.08 0.20 0.24 0% 4% 8% 19.0 21.5 30.0 0.08 0.09 0.16 19.0 22.0 32.0 0.08 0.15 0.17 104 T A B L E 4.12 Effect of various additives and curing time on the C B R of stabilised soil A. CBR 28 Days 90 Days 0% 4% 8% 55 75 72 55 81 76 0% 4% 8% 55 70 75 55 74 80 0% 4% 8% 55 60 65 55 60 68 0% 4% 8% 55 50 45 55 50 45 0% 2% 4% 55 100 120 55 105 116 55 60 102 55 61 112 55 56 100 55 60 110 ADDITIVES (%) LIME LIME:RHA1:1 LIME:RHA1:3 RHA CEMENT CEMENT:RHA1:2 0% 4% 8% CEMENT:RHA1:3 0% 4% 8% 105 T A B L E 4.13 Effect of various additives and curing time on the C B R of stabilised soil B. CBR 28 Days 90 Days 0% 4% 8% 30 40 37 30 43 41 0% 4% 8% 30 37 39 30 41 42 0% 4% 8% 30 32 35 30 35 37 0% 4% 8% 30 25 25 30 25 24 0% 2% 30 108 30 100 ADDITIVES (%) LIME LIME:RHA1:1 LIME:RHA 1:3 RHA CEMENT 106 T A B L E 4.14 Effect of various additives and curing time on the C B R of stabilised soil C. CBR 28 Days 90 Days 0% 4% 8% 19 31 55 19 32 60 0% 4% 8% 19 25 32 19 27 34 0% 4% 8% 19 22 24 19 23 27 0% 4% 8% 19 19 20 19 19 19 0% 4% 8% 19 32 51 19 35 56 ADDITIVES (%) LIME LIME:RHA1:1 LIME:RHA1:3 RHA CEMENT 107 TABLE 4.15 No. of Load Applications 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 Permanent deformations of untreated pavement (mm) Row/Column a b c d e f g E 1.15 0.96 1.95 -0.11 1.00 4.11 3.00 3.15 0.90 4.00 4.30 5.00 1.15 4.11 4.89 5.42 2.20 4.00 4.95 5.50 1.80 1.95 2.72 3.72 0.25 0.40 0.75 -0.25 F 0.30 0.60 0.80 -0.11 1.80 2.36 3.36 4.56 1.90 3.60 5.00 6.96 2.50 3.60 5.00 6.03 2.50 3.57 4.91 6.50 2.00 3.11 4.02 5.15 -0.04 0.05 0.61 0.86 0.41 0.61 2.30 2.40 2.00 2.50 4.20 5.72 2.85 3.75 5.80 7.88 3.00 4.11 6.74 7.95 3.12 3.95 6.70 8.02 1.60 3.08 4.50 5.34 -0.04 0.25 2.01 2.18 0.05 0.30 0.50 -0.80 2.11 2.33 4.30 6.80 3.00 3.80 5.65 7.90 3.15 4.12 6.90 8.00 3.12 4.25 6.97 8.95 1.51 1.71 2.91 3.80 0.62 0.95 1.01 1.35 0.05 0.80 0.71 -0.50 1.30 1.65 1.85 2.00 1.60 2.00 2.52 2.98 1.00 2.33 4.11 4.98 1.50 1.91 4.30 5.10 1.49 1.63 0.80 0.40 0.41 0.43 0.00 -0.60 G H I 108 TABLE 4.16 No. of Load Applications 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 Permanent deformation of 2 % lime treated pavement (mm) Row/Column a b E 0.30 0.60 1.30 1.70 F 0.20 0.40 0.95 1.55 d e f g 0.57 1.57 0.75 2.40 1.12 4.25 1.19 4.45 1.70 2.17 2.85 2.90 3.80 4.15 4.58 4.78 1.76 2.20 2.71 2.46 0.50 0.98 1.18 1.01 1.29 1.79 2.17 2.86 3.28 4.44 5.10 5.90 2.39 3.68 3.96 4.41 2.34 3.69 3.52 4.84 1.45 2.29 2.87 3.65 0.40 0.67 0.68 1.68 G 0.95 1.10 1.30 1.43 1.58 1.73 2.56 2.66 4.26 5.01 5.54 6.64 3.12 4.42 4.75 4.69 3.93 4.68 5.32 6.53 1.94 2.55 2.55 3.15 0.47 0.52 0.80 1.49 H 0.20 0.50 0.96 1.33 1.63 2.00 2.40 2.60 4.14 5.03 6.50 7.16 5.50 6.83 5.94 6.83 5.95 6.90 7.12 7.20 2.16 3.48 3.63 3.74 -0.15 0.18 0.10 0.28 I 0.35 0.25 0.25 0.00 0.35 0.30 0.67 0.90 0.58 1.29 1.88 1.85 1.31 3.32 4.15 3.06 2.40 3.35 3.75 4.85 0.45 0.61 1.30 1.48 0.23 0.26 0.30 0.40 c 109 TABLE 4.17 No. of Load Applications 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 Permanent deformations of 3 % 1:1 lime.RHA treated pavement (mm) Row/Column a b c d e f g E 0.40 0.50 0.90 1.30 1.36 0.76 1.00 1.15 1.85 2.90 4.30 4.90 1.60 1.97 2.00 2.10 2.00 2.80 3.44 4.00 1.60 1.80 1.90 1.90 0.32 0.79 0.99 0.00 0.30 0.40 0.80 1.00 1.40 1.60 1.80 2.46 2.30 3.30 3.92 4.40 2.20 3.20 3.79 4.40 2.20 3.00 3.70 4.50 1.70 2.08 2.67 3.24 0.50 0.70 1.00 1.15 0.90 1.00 1.31 1.40 1.60 1.80 2.40 2.60 3.95 4.99 5.80 6.00 3.00 4.00 4.40 4.50 3.15 3.75 4.60 5.50 2.10 2.56 2.90 2.95 0.55 0.90 1.11 1.32 0.30 0.70 0.90 1.10 1.50 2.15 2.30 2.40 4.05 4.86 5.60 6.00 4.50 5.16 5.50 6.10 5.85 6.75 6.45 7.00 2.16 3.20 3.42 3.70 0.49 0.60 0.72 0.80 0.30 0.35 0.40 0.20 0.30 0.40 0.60 0.65 1.00 4.00 1.90 2.00 1.30 2.11 2.89 3.00 1.90 2.96 3.48 4.50 0.90 1.25 1.50 1.50 0.30 0.32 0.15 0.22 F G H I 110 TABLE 4.18 No. of Load Applications 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 Permanent deformations of 1.5% cement treated pavement (mm) b c d e E -0.71 -1.15 0.12 1.11 -0.36 -1.05 0.28 -1.31 1.50 0.43 1.75 1.63 0.61 1.86 0.28 1.74 1.51 1.34 1.41 2.19 0.19 -1.12 -1.34 0.02 -0.36 0.11 0.97 1.42 F -1.70 -1.00 0.80 -1.90 -0.79 0.10 0.90 -0.16 -1.65 -0.37 1.87 2.39 3.04 3.40 4.11 4.04 2.43 3.18 3.97 4.13 4.29 2.80 1.77 3.07 1.43 1.84 1.41 1.85 -0.88 -2.15 -1.90 -2.15 -0.49 -0.82 -0.80 -0.65 -0.45 -0.35 1.05 1.25 1.26 1.05 1.34 2.62 1.27 0.35 1.56 2.32 0.91 0.09 0.18 0.90 -0.29 0.90 1.00 0.11 -0.68 -0.14 0.06 -0.91 0.31 0.25 0.02 0.25 1.29 1.79 2.43 2.68 1.56 1.96 1.56 2.00 1.30 2.23 2.53 2.96 -0.33 -0.24 1.22 -0.24 1.22 -0.21 1.52 -0.12 0.02 0.87 0.10 -0.23 0.00 0.35 0.60 -0.73 0.00 0.77 0.64 0.80 0.84 1.58 1.05 1.64 -0.69 2.06 1.47 0.77 1.11 1.55 1.92 1.35 Row/Column a G H I f g -0.29 0.78 -0.69 -0.07 Ill TABLE 4.19 No. of Load Applications 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 Permanent deformations of 3 % 1:1 cement.RHA treated pavement (mm) Row/Column a E F G H I f b c d e 0.10 2.20 2.34 1.64 0.33 0.08 0.57 -0.20 0.69 0.19 0.45 -0.13 0.75 1.57 2.43 1.39 0.25 0.80 1.14 1.41 -1.86 1.08 -0.40 0.00 0.37 0.15 -0.44 -0.23 1.44 1.00 0.27 -0.32 1.28 1.45 2.43 2.11 1.65 0.75 1.78 1.76 2.53 1.56 2.57 2.40 2.29 0.01 3.69 4.22 1.60 1.11 2.22 1.55 3.50 2.50 2.33 2.92 0.00 0.04 0.29 1.35 0.82 1.17 1.79 2.90 1.37 1.41 1.88 2.63 2.04 2.55 2.82 2.91 1.61 1.75 1.78 2.41 1.18 1.27 1.15 2.87 0.76 0.81 1.05 2.53 0.00 1.78 2.53 1.90 0.67 1.13 1.46 1.87 0.64 1.14 1.86 2.23 0.05 1.46 1.85 2.01 0.60 1.05 1.77 1.96 0.60 0.53 0.77 1.62 0.00 0.02 0.15 0.30 1.27 0.00 1.28 1.52 0.13 0.62 1.00 1.03 1.05 0.00 1.27 1.30 0.42 0.42 1.53 1.80 2.40 -0.82 -1.22 -0.55 1.18 1.18 0.68 0.94 0.19 -0.42 -0.06 0.47 g 112 TABLE 4.20 No. of Load Applications 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 Permanent deformations of 8 % R H A treated pavement (mm) Row/Column a f c d e E 1.10 1.20 1.15 3.20 -0.30 3.80 0.10 3.60 1.50 3.50 4.16 4.60 1.80 3.80 4.70 5.10 2.00 3.80 4.80 5.00 1.70 2.10 2.80 3.75 0.41 0.30 0.70 -0.40 F 1.30 1.46 0.44 0.00 1.65 2.23 3.41 4.50 1.92 3.13 4.79 6.00 2.40 3.43 4.89 6.25 2.25 3.75 4.85 6.50 1.95 3.00 4.30 4.75 0.05 0.20 0.55 0.91 1.50 1.75 1.90 2.00 2.00 2.50 4.00 5.80 3.00 3.68 5.50 8.13 3.20 4.00 6.55 8.00 3.36 4.23 6.75 8.16 1.70 3.10 4.20 6.03 0.26 0.41 1.98 2.28 H 1.50 1.60 1.20 1.20 2.20 2.51 4.00 6.30 3.20 3.61 5.91 8.00 3.32 4.00 7.02 8.00 3.40 4.25 7.00 8.20 1.60 2.21 3.00 3.60 0.70 0.95 1.21 1.41 1 0.25 0.30 0.40 0.00 1.60 1.91 2.15 2.70 2.00 2.44 3.06 4.90 2.00 2.50 4.17 5.20 2.40 2.50 4.36 5.30 1.40 1.69 1.90 2.00 0.70 0.99 0.00 -0.40 G b g M.-V 113 CO LU CO Q O 0) SI LU < (13 Z DC D O CO Li. $ O Q CO CM a CO o D CD LL o z DC D O \\d 114 CO CO < Q_ < D o O) < 1 I CC LU 2 I z rr I- O z LU LU o i Q co CM II ix. 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J-S H fa 137 Chapter V DISCUSSION AND ANALYSIS OF RESULTS CONCERNING RICE HUSK ASH 5.1 RHA as a single additive 5.1.1 Effect of RHA additive on compaction characteristics of soils It has been observed that when RHA was added to the soils A, B and C the maximum dry densities decrease and the optimum moisture contents increased (see Tables 4.2a to 4.2c). The increase in the OMC of all treated soils was related to the additive quantities. As a general rule, it can be said that the addition of a quantity of RHA to a soil may lead to an increase corresponding to about 50%-75% of that quantity, in the OMC of that soil. The increase in the OMC was mainly due to the additional water required for wetting the large surface area of the fine RHA particles. However, as the RHA is not finer than soil C it is believed that the increase in the OMC of this treated soil and other soils could be influenced by the morphology of the RHA particles' surface and their great affinity for absorbing water, a characteristic which was subjectively noticed during the testing programme. 138 The decrease in density of all treated soils was mainly due to the partial replacement of comparatively heavy soils with the light weight RHA (specific gravity 1.79). The decrease in density could also be influenced by the increase in porosity of all compacted soils due to addition of RHA. The porosity was calculated in accordance with the following simple equation: P = Po(l-E) where: P is the apparent density of a compacted specimen. P0 is the equivalent specific gravity of a mix taking into account the specific gravity of all constituents. E is the value of porosity. Knowing the specific gravity of soils and RHA, it was found that by adding 8% of RHA to the soils A, B and C, the corresponding porosities were increased by 10%, 11% and 5% respectively. The calculations of porosities are shown in the Appendix B. The treatment of a soil, therefore, by RHA single additive increases the OMC of the soil. This can be utilised in improving the workability of wet soils, particularly if the 139 increase in OMC of the soils due to addition of RHA was more than that which occurred by adding lime or cement to the soils (see Tables 4.2 and 4.3). However, this improvement in workability could be offset by the increase in porosity which may affect the strength properties of treated soils. 5.1.2 Effect of RHA additive on the strength properties of soils 5.1.2a Effect on UCS It can be observed, as shown in Tables 4.5 and Figure 4.3, that RHA as a single additive has no positive effect on the UCS of soils. This can be explained by: a) The partial replacement of soils with RHA does not significantly change the grading of the soils to satisfy the requirement of the maximum density curve as shown in Table 5.1. b) The minor change in grading was accompanied by an increase in porosity of the compacted specimens. c) The RHA used can be chemically termed silica as it contains 58% silica. with soil. Thus it does not chemically react 140 5.1.2b Effect on CBR It can be observed from Tables 4.12 and Figure 4.13 that the CBR values of treated soil A and B decreased with the increase in the quantity of RHA additive. This could be attributed to the increase in compressibility caused by the increase in porosity of these treated soils (see 5.1.1). A reduction in CBR value was not observed in the case of treated soil C. This is consistent with the fact that the increase in porosity in that case was minimal (ie 5%) as shown in section 5.1.1. The CBR values of all of the treated soils did not vary with the variation of curing time. This implies that no reactions have taken place between RHA and the soil during the various curing times. 5.1.3 Effect of RHA on the Atterberg limits and linear shrinkage of soils Liquid limit and plastic limit of RHA treated soils increased with the increase in additive quantity, with the notable exception of high liquid limit soil C, where the liquid limit decreased with the increase in additive quantity. In general, the plasticity of all soils is decreased by the addition of RHA. This is clearly shown by 141 the fact that plasticity index and linear shrinkage of all RHA treated soils decreased with increasing additive quantity. These effects are due to the partial replacement of plastic soil particles with RHA which is an abrasive non-plastic material. However, the effects on the plasticity and linear shrinkage of soils treated with RHA are less than those which occur by the addition of lime or cement to soils. For example, the addition of 8% RHA to soils A and B did not result in comparable linear shrinkage and plasticity index to that achieved by the addition of 2% lime or 2% cement. For soil C, which is very suitable for lime treatment, the addition of 8% RHA resulted in lower values than were achieved by 1% lime addition. From Figures 4.5 and 4.7, it can also be deduced that 5 - 6% of RHA is required to achieve the same results as 1% lime addition. The use of RHA, to modify the plasticity and linear shrinkage of soils, therefore is not efficient. From Table 4.6 it can be observed that liquid limit, plastic limit, plasticity index and linear shrinkage, after a curing period of 28 days, are similar to those after a curing period of 7 days. This implies that no reaction has taken place between RHA and the soils during this period. This is consistent with the finding for strength (section 5.1.2). 142 5.1.4 Effect of RHA on the behaviour of soils under the action of repeated dynamic load The various measurements of deflections for both pavements (the untreated soil D and the 8% RHA treated soil D) shown in Tables 4.15 and 4.20 reveal that: i) For any point on the grid, where measurements were taken, the deflection increased with the increase in number of load applications. ii) As the number of total load applications to the pavements increased, the actual deflection per single load applied decreased, indicating that pavement stiffness had increased (see Tables 5.2c and 5.2d). iii) The maximum values of deflection for the various number of load cycles occurred close to wheel contact area and particularly under the wheel edge. iv) Deflection profiles for both pavements (Figures 4.14 and 4.19) appear to be similar. The maximum values of deflection, for both pavements, after 50,000 load cycles were also similar (ie, 8.95mm for untreated soil and 8.20mm for 8% RHA treated soil). 143 All of these observations indicate that the behaviour of RHA treated pavement under the action of repeated loads does not vary from that of untreated pavement subjected to similar loading. This implies that RHA does not affect favourably the stiffness or compressibility of soils and this is consistent with the finding of strength (section 5.1.2). 5.2 Lime-RHA Additives 5.2.1 Effect of lime-RHA additives on compaction characteristics of soils It has been observed that when lime-RHA additives are added to the soils A, B and C the maximum dry densities decrease and the optimum moisture contents increase (see Tables 4.2a to 4.2c). These effects are more pronounced as the quantity of RHA in the additives is increased. The increase in OMC is due to the water required for the hydration of lime as well as to assist flocculation of the clay clods. Additional water also is required for wetting the large surface area of the fine RHA particles or is absorbed by the fine particles of the RHA as described in section 5.1.1. The decrease in density of all treated soils is mainly due to the partial replacement of comparatively heavy soils with 144 the light weight lime-RHA additives (specific gravity of lime = 2.35 : specific gravity of RHA = 1.79). As indicated above, the decrease in density is more pronounced as the quantity of the lighter constituent (ie RHA) in the additives is increased. The decrease in density could also be influenced by the increase in porosity due to the addition of lime-RHA additives. The porosity was calculated by the method described in section 5.1.1 and calculations are listed in Appendix B. the porosities of all compacted, It can be seen that treated soils were increased by the increase of the quantity of RHA in the additives. The increase in OMC of a soil due to treatment by lime-RHA additives can be utilised in improving the workability of wet soils. Any adverse effect on strength due to increase in porosity or reduction in density is unlikely to occur due to the expected substantial gain in strength of treated soils because of the cementing action of lime-RHA additives. 5.2.2 Effect of Lime-RHA additives on the strength properties of soils 5.2.2a Effect on UCS It can be seen from Table 4.4 that: 145 For a given quantity of additive, as lime in the additive increases, the strength at all ages, for all treated soils, increases. The highest strengths for all treated soils have been achieved by using 1:1 lime-RHA additive. This is not consistent with the case for lime-RHA pastes (section 4.5.3) and implies that lime reacts more readily with soils than with ash. A sufficient quantity of lime (ICL or initial consumption of lime) is required to increase the pH of soils to about 12.4 at which reaction takes place between lime and clay minerals and other pozzolans to produce cementitous hydrated calcium silicate and aluminate gels (51). As the curing time increases, strength increases due to the pozzolanic reaction which takes place over a long time. By inspecting the long term strength (ie, the 90 days curing strength) shown in Figure 4.3, it can be observed that: For all additives, the strength of treated soil increases with increasing quantity of additive, up to a peak value, then decreases with the continuous increase of the quantity of additive similar to that in the case of lime stabilisation. 146 iv) The quantity of additive, at which a peak value of strength occurs, tends to increase with increasing amount of RHA in the additive. This conforms to the previous finding that lime reacts more readily with soils than with RHA. v) For all soils tested, the lime-RHA additives were not able to achieve the highest strength achieved by lime additive. This is more pronounced in the case of soil C which, as a heavy clay, is very suitable to lime stabilisation. This indicates that lime-RHA additives are more efficient in modifying the strength of non-cohesive soils than they are in modifying the strength of cohesive soils. It can also be deduced from Figure 4.3 that the UCS of soils treated with 4% content of 1:1, 1:2 and 1:3 lime-RHA additives are equal or greater than those of 2%, 1.3% and 1% lime stabilisation. This indicates that RHA is acting as a pozzolan and has a role in strength development of lime-RHA soil stabilisation. The effectiveness of this role will be examined further in section 5.2.7. 5.2.2b Effect on CBR It can be seen from Tables 4.12 to 4.14 and Figures 4.11 to 4.13 that: 147 i) For a given quantity of additive, as lime in the additive increases, the CBR of all treated soils increases. ii) As the curing time increases, the CBR increases. This is due to the pozzolanic reaction which takes place over a long period of time. iii) For all additives, the CBR of treated soil increases with increasing quantity of additive and no peak value is observed. iv) For all soils tested, the lime-RHA additives were not able to achieve the highest CBR achieved by lime additive. This is more pronounced in the case of soil C which is very suitable to lime stabilisation. These observations conform to the findings of UCS in section 5.2.2a with the only exception of CBR not having a peak value at an optimum quantity of lime-RHA additive. 5.2.3 Effect of delay in compaction on the strength of lime-RHA treated soils The results presented in Table 4.8 have shown that delay in compaction of lime and lime-RHA treated soil decreases the 148 strength of these mixes. This is more pronounced as the time elapsed since mixing is increased. This can be explained by the fact that delay in compaction allows some cementitous bonds to occur and resist the applied compactive effort. The final density achieved will, therefore, be lower and a loss in strength will occur. The results presented in Table 4.8 have also revealed that, in lime and lime-RHA stabilisation, the losses in strength due to delay in compaction were not great and almost similar. This implies that the rate of reaction in lime-RHA stabilisation is relatively slow and somewhat similar to lime stabilisation. Accordingly, the time constraints in respect of compaction, including delays caused by plant breakdown, etc and the effects of rain are not so critical. 5.2.4 Effect of lime-RHA additives on the shear strength parameters of soils A perusal of Table 4.10 reveals the general increase in the shear strength parameters (cohesion and angle of internal friction) of the soil both with respect to the proportion and percentage of additives. With increase in lime content, the parameters increase for a given percentage; also for a given proportion, as the percentage of total additive increases, an increase in the parameters is observed in almost all cases. It can also be seen that the cohesion and 149 angle of internal friction of soil stabilised with 8% content of 1:1 lime-RHA additive were higher than those with 4% lime additive. This confirms the belief that RHA has a role in strength development of lime-RHA stabilisation. The results presented in Table 4.10 also show that shear strength parameters increase with increasing curing time. As the shear strength of a soil is determined by its parameters and effective normal stress (ie T= C + cfn tan 0), it can easily be seen that the abovementioned observations are applicable to the effect of lime-RHA additives on the shear strength of soils. These observations conform to the findings with respect to CBR and UCS (sections 5.2.2a and 5.2.2b) which are, more or less, measures of the combined effects of cohesion and internal friction of a soil. Accordingly, it can be stated that the increase in strength (UCS, CBR and shear strength) due to lime-RHA stabilisation is caused by the increase in both the angle of internal friction and cohesion of the stabilised soil. The increase in the angle of internal friction could be attributed to the formation of bigger size particles (ie, aggregation of clay particles) due to the cation exchange reactions, whereas cohesion is increased mainly by the formation of calcium silicate gel due to the reaction of lime with pozzolanic components of soil and RHA. This gel 150 gradually crystalises into well defined calcium silicate hydrate micro-crystals which can interlock mechanically and cause the development of interparticle bonds. 5.2.5 Discussion of the results of the XRD analysis of lime-RHA stabilised soils A computer analysis for the d spacings and intensities of the peaks on each X-ray diffraction chart was used in identifying the compounds that existed in the various samples examined. The XRD chart of the untreated Soil C, as shown in Figure 4.26, exhibits peaks at d spacings of 4.26, 3.343, 2.458, 2.282, 2.128 and 1.817 A° indicating the presence of Quartz (Si02). Peaks exhibited at d spacings of 7.18, 4.48, 3.58, 2.565 and 2.386 A° indicate the presence of Kaolinite (Aluminium Silicate Hydroxide). The analysis also shows low peaks at d spacings of 9.95 and 4.97 A° indicating the presence of Muscovite (Potassium Aluminium Silicate Hydroxide). Similarly the XRD chart of the untreated Soil A, as shown in Figure 4.25, exhibits peaks at d spacings of 4.26, 3.343, 2.282 and 2.128 A° indicating the presence of Quartz. The chart also shows peaks at d spacings of 7.18, 4.48, 3.58, 2.565 and 2.502 A° indicating the presence of Kaolinite. 151 The XRD chart of the lime-RHA treated Soil A, as shown in Figure 4.27, exhibits peaks similar to that of the control sample of the untreated Soil A indicating the presence of Quartz and Kaolinite. This chart has proved inconclusive in showing the nature of lime-RHA hydration product. Possible existence of Calcium Silicate Hydrate compounds could be hindered by the presence of Calcite (Calcium Carbonate) in the sample. This presence could be attributed to the effect of atmospheric carbon dioxide on the thin dispersion of fine material. The Calcite can be identified by the intensities and peaks shown at d spacings of 3.86, 3.035, 2.285, 2.095, 1.913 and 1.875 A°. Figure 4.28 shows the XRD chart of the lime-RHA treated Soil C. It can be clearly seen that the treated soil retained some of the details of the original structure. Quartz can be easily identified by the peaks at d spacings of 4.26, 3.343, 2.458, 2.282, 2.128 and 1.817 A°. Kaolinite and Muscovite disappeared and were replaced by Illite (another form of Potassium Aluminium Silicate Hydroxide). The Illite was identified by the peaks shown at d spacings of 10.30, 4.49 and 2.583 A° whereas Calcite was identified by the peaks at d spacings of 3.035 and 2.285 A°. Again, the XRD analysis has proved inconclusive in identifying the lime-RHA hydration products. No indication of the presence of calcium silicate hydrate and calcium aluminate hydrate appeared. 152 5.2.6 Discussion of the results of the SEM examination of lime-RHA stabilised Soils The scanning electron micrograph of the fracture surface of the untreated Soil A, as shown in Figure 4.21, has clearly indicated that upon fracturing of the specimen, several areas of the matrix exhibited extensive cracking. Cracks can be seen at the top and bottom of the centre of the micrograph. It can also be seen that the matrix exhibited poor bonding and considerable amount of microporosity. Such porosity can be seen in the centre and at the bottom right of the micrograph. Figure 4.22 shows the fracture surface topography of the untreated Soil C (Clay). It indicates a relatively smooth textured surface although areas with some associated microporosity appear in the centre and the right side of the micrograph. In comparison, the micrograph of the fracture surface of lime-RHA treated Soil A, as shown in Figure 4.23, indicates that the surface of the treated soil retained some details of the original texture. Areas with associated microporosity can clearly be seen at the top and the bottom of the micrograph. However, patches of amorphous components, which are presumably the non crystalline lime-RHA reaction products, can be seen in the micrograph. 153 Figure 4.24 indicates that such amorphous components are also shown to cover the fracture surface of lime-RHA treated Soil C, particularly in areas shown at the lower left corner of the micrograph. The rope-like fibres shown in the upper portion of the micrograph are presumably some plant growth contamination in the soil. It has to be noted that comparison of micromorphological results has an apparent limitation because of the small number of micrographs usually published and the correspondingly small area represented by these micrographs, which might not be representative of the structure. The description of the features given here are, somewhat, subjective. Consequently, speculations on the origin of strength and other properties, when based on these observations have limited validity. 5.2.7 Effect of lime-RHA additives on the Atterberg limits and linear shrinkage of soils It can be observed from Table 4.6 that liquid limit and plastic limit of lime-RHA treated soils increase with the increase of additive quantity with one notable exception where the very high liquid limit of soil C decreases with the increase of additive quantity. However, the plasticity 154 index and linear shrinkage of all treated soils decrease with the increase in additive quantity. These effects are more pronounced as the amount of lime in the lime-RHA additive is increased. These effects could be attributed to the combined action of the partial replacement of plastic soil particles with the abrasive non-plastic particles of RHA, and the ionic exchange between lime and the clay minerals of soils. It can also be observed from Table 4.6 that liquid limit, plastic limit, plasticity index and linear shrinkage of treated soil after a curing period of 28 days are almost equal to those after a curing period of 7 days. This can be explained by the fact that the reactions responsible for reducing plasticity and shrinkage (ie, cation exchange) occur during a short period of time and mostly in the first 7 days of the curing time and the RHA does not react with soils as was discussed in sections 5.1.2 and 5.1.3. A perusal of Figures 4.5 and 4.7 reveals that lime-RHA additives could not attain the results achieved by 4% lime additive. Hence, their use to modify the plasticity and shrinkage of soils could be restricted to a lower level of achievement. However, their limited role in this context (ie, to replace 2-3% lime additive in modifying plasticity and shrinkage of soils) could be justified by the amount of 155 lime saving they can achieve. This will be discussed in the following section. 5.2.8 Implications of lime savings By examining Figure 4.30 it can be deduced that the UCS of 2% lime treated soil A can be achieved by 2.72% of 1:1 lime-RHA additive (ie 1.36% lime + 1.36% RHA). The lime saving is therefore equal to 2 - 1.36 = 0.64% and the ratio of RHA required to lime saved is 1.36/0.64 = 2.12. Therefore 1:1 lime-RHA additive is not economically feasible to replace the 2% lime stabilisation unless the cost of lime is equal to or greater than 2.12 times the cost of RHA. Table 5.3 has been derived in a similar manner utilising Figures 4.3, 4.5 and 4.7 and applying the same calculations for the various values of strength, shrinkage and plasticity for each case of soil treatment. From Table 5.3 it can be deduced that: i) At a low level of achievement, RHA has a significant role in the lime-RHA soil stabilisation. 156 ii) 1:1 lime-RHA additive tends to be the most economical mixture of all lime-RHA additives used. iii) Lime-RHA additives are more efficient for strength improvement of soils than for reduction of plasticity and shrinkage. iv) Lime-RHA additives are more efficient in stabilising low cohesion soils than in stabilising clays. v) 1:1 lime-RHA additive cannot be recommended for improvement of soil strength unless the cost of lime is at least three times the cost of RHA. However, for modifying the plasticity, the cost of lime must be at least 5-6 times the cost of RHA. 5.2.9 Effect of lime-RHA additives on the behaviour of soils under the action of repeated dynamic load Soils (A, B and C) treated with 3% content of 1:1 lime-RHA additives were found to have UCS equal to or greater than those of 2% lime treated soils, (see Figure 4.3). To find whether or not the behaviour of these treatments under the action of repeated dynamic loads are consistent with 157 strength findings, it was decided to compare the pavements having 2% lime treated soil D and 3% content of 1:1 lime-RHA treated soil D with the control pavement of untreated soil D. The various measurements of deflections of the three pavements, shown in Tables 4.15, 4.16 and 4.17, reveal that: i) For any point on the grid, where measurements were taken, the deflection of the three pavements increased with the increase in number of loads applied. ii) As the number of total load applications to the pavements increases, the actual deflection per single load applied decreases, indicating the pavement stiffness has increased (see Table 5.2). iii) The maximum deflections for the various number of load cycles occurred close to wheel contact area and particularly under the wheel edge (ie point eH on the grid) for all cases. iv) For any number of load cycles the deflections, at any point on the grid, of the lime and lime-RHA treated pavements were less than the deflection of the untreated pavement. This indicates that lime 158 and lime-RHA additives increase the stiffness and reduce the compressibility of soils. The deflection of the lime-RHA treated pavement after any number of load applications was less than the deflection of the lime treated pavement at most points on the grid and all points within the wheel contact area. The maximum deflection of the lime-RHA treated pavement after 50,000 load cycles was less than the maximum deflection of the lime treated pavement (7.2mm for 2% lime treated pavement and 7.0mm for 3% content of 1:1 lime-RHA treated pavement). This signifies the positive role of RHA as a pozzolan in lime-RHA additive, in improving the stiffness of a soil and reducing its compressibility. This is consistent with the findings of strength in sections 5.2.2 and 5.2.4 and may imply that the lengthy and costly repeated load test is less significant than the economical and simple UCS test as a tool for the selection and design of lime-RHA soil stabilisation. A perusal of Tables 4.15, 4.16 and 4.17 reveals that, for all pavements, there were downward movements of all points on the grid where 159 measurements were taken and the permanent deformations of the three pavements were caused by the densification of the pavements rather than by any shear failure of these pavements (see also Figures 4.14, 4.15 and 4.16). vii) A visual assessment of the surface of all pavements showed that no fatigue cracks or shrinkage cracks were developed and the pavements were intact and sound at the conclusion of the test. In general, the observations derived from the results of the repeated dynamic load test have demonstrated that 1:1 lime-RHA additive is effective and efficient in improving the behaviour of soils under the action of repeated loads. 5.3 Cement-RHA Additives 5.3.1 Effect of various cement-RHA additives on compaction characteristics of soils It has been observed that when cement-RHA additives are added to the soils A, B and C, the maximum dry densities decrease and the optimum moisture contents increase (see Tables 4.3a to 4.3c). These effects are more pronounced as the quantity of RHA in the additives is increased. The 160 increase in OMC is due to the water required for the hydration of cement as well as to assist flocculation of the clay clods. Additional water also is required for wetting the large surface area of the fine RHA particles or is absorbed by the fine particles of RHA as mentioned in sections 5.1.1 and 5.2.1. The decrease in densities of all treated soils was mainly due to the partial replacement of soil with lighter cement-RHA additives (specific gravities for 1:1, 1:2, 1:3 and 1:4 proportions are 2.465, 2.24, 2.127 and 2.06 respectively). As stated above, the decrease in density is more pronounced as the quantity of the lighter constituent (ie RHA) in the additives is increased. The decrease in density could also be influenced by the increase in porosity due to the addition of cement-RHA additives which in turn could be attributed either to the rapid development of bonds, between particles, which resist compaction effort or to the morphology of RHA particles itself (see section 5.1.1). The porosity of values were calculated by a method similar to that specified in sections 5.1.1 and 5.2.1 and are presented in Appendix B. The increase in OMC of a soil due to treatment by cement-RHA additives can be utilised in improving the workability of wet soils. Any adverse effect on strength due to increase in porosity or reduction in density is unlikely to occur due 161 to the expected substantial gain in strength of treated soil because of the cementing action of cement-RHA additives. 5.3.2 Effect of cement-RHA additives on the strength properties of soils 5.3.2a Effect on UCS It can be seen from Table 4.5 that: i) For a given quantity of additive as cement content in the additive increases the strength at all ages, for all treated soil, increases. This is consistent with the case of cement-RHA pastes (section 4.5.3) and implies that the strength development is dominated by the hydration reactions of cement rather than by the pozzolanic reaction between the released lime (from the hydration of cement) and the RHA and clay particles of the soils. ii) For all additives and all curing periods there is continuous increase in strength with increasing quantity of additive. No peak value of strength was observed. These are consistent with the findings above. 162 iii) As curing time increases the strength of treated soil increases. The rates of strength development of soils treated with cement-RHA additives are slower than those of cement treated soils. Rates of strength development, as ratios of 7 days strength to 90 days strength, and 28 days strength to 90 days strength for various treated soils are derived from Tables 4.5 and presented in Tables 5.4 and 5.5. From these Tables, it can be easily seen that RHA is acting somewhat as a retarder and hence may have some favourable effect on the workability of cement-RHA soil stabilisation. This effect will be further examined in the later discussion on the effect of delay in compaction on strength of treated soils (section 5.3.3). From Figure 4.4, it can be seen that the UCS of soils treated with 4% content of 1:1, 1:2 and 1:3 cement-RHA additives are greater than those of 2%, 1.3% and 1% cement treatment. This indicates that RHA is acting as a pozzolan and has a role in strength development of cement-RHA soil stabilisation. This is consistent with the findings of section 5.2.2a. The effectiveness of this role is investigated in section 5.3.7. 163 5.3.2b Effect on CBR It can be seen from Tables 4.12 and 4.14 that: i) CBR increases with increasing curing time or decrease in the amount of RHA in the additive. ii) There is a continuous increase in CBR due to increase in the additive quantity in almost all cases and no peak value for CBR is observed. Implication of cement saving cannot be derived from the CBR values as some of these values are greater than 100 and considered meaningless in accordance with the discussion of the appropriateness of the test in section 3.4.4. 5.3.3 Effect of delay in compaction on the strength of cement-RHA treated soils The results presented in Table 4.9 show that a loss in strength occurs if the compaction of cement or cement-RHA treated soil is delayed. The loss in strength is more pronounced as the time elapsed since mixing is increased. The delay in compaction of cement treated soil A was so critical that 30% to 70% of strength was lost due to 2 - 6 hours delay in compaction. However, this loss in strength was decreased by using cement-RHA additives. The decrease 164 in the loss of strength is more pronounced as the amount of RHA in the additive is increased. This could be attributed to the fact that the RHA acts as a retarder in slowing the rate of strength development of cement-RHA treated soils (see section 5.3.2a). The loss in strength due to delay in compaction of cement-RHA treated soil is significantly less than that of cement treated soil. Accordingly, the time constraints in respect of compaction, including delays caused by plant breakdown, etc, and the effects of rain are not so critical. 5.3.4 Effect of cement-RHA additives on the shear strength parameters of soils A perusal of Table 4.11 reveals that: i) For a given additive, shear strength parameters increase with increase in additive quantity. ii) For a given quantity of additive, the shear strength parameters increase with decrease in RHA content in the additive. iii) Shear strength parameters increase with increase in curing time in almost all cases. 165 As the shear strength of a soil is determined by its parameters and normal stress (ie V = C + Cntan 0) , it can easily be seen that the above mentioned observations are applicable to the effect of cement-RHA additives on the shear strength of soils. These observations conform to the findings for CBR and UCS (sections 5.3 2a and 5.3.2b) which are, more or less, measures of the combined effects of cohesion and internal friction of a soil. Accordingly, it can be stated that the increase in strength (UCS, shear strength and CBR) of cement-RHA stabilised soil is influenced by the increase in both its internal friction and cohesion. As discussed in section 5.2.4, the increase in the angle of internal friction could be attributed to the formation of bigger size particles (ie aggregation of clay particles) due to the cation exchange reactions of the clay minerals of the soil with the lime released from the hydration reactions of cement in the additive. The cohesion is increased mainly by the formation of cementitous material (calcium silicate and aluminate hydrates as in concrete) due to the hydration reactions of the cement with the water in the soil. These reactions release hydrated lime (about 30% by mass of added cement) which can cause secondary reactions with RHA and clay particles within the soil. The secondary reactions produce cementitous products similar to those of the hydration reactions of the cement. These cementitous 166 products gradually crystalise and interlock mechanically to increase the cohesion. 5.3.5 Effect of cement-RHA additives on the Atterberg limits and linear shrinkage of soils It can be seen from Table 4.7 that liquid limit and plastic limit of cement-RHA treated soils increase with the increase of additive quantity with one notable exception where the very high liquid limit of soil C decreases with the increase of additive quantity. However, the plasticity index and linear shrinkage of all treated soils decrease with the increase in additive quantity. These effects are more pronounced as the amount of RHA in the cement-RHA additive is decreased. These effects could be attributed to the combined action of the partial replacement of plastic soil particles with the abrasive non-plastic particles of RHA, and the cation exchange reactions of clay minerals in the soil with the released lime from the hydration reactions of cement. It can also be seen from Table 4.7 that liquid limit, plastic limit, plasticity index and linear shrinkage of treated soils after a curing period of 28 days are almost equal to those after a curing period of 7 days. This implies that the reactions responsible for reducing 167 plasticity and shrinkage (cation exchange) occur during a short period of time and mainly in the first 7 days and that RHA does not react with soil. All of these observations are consistent with those of lime-RHA additives as discussed in section 5.2.6. Figures 4.6 and 4.8 indicate that, for modifying the plasticity and the shrinkage of soils, the replacement of cement with cement-RHA additives should be restricted to an upper limit of cement additive of 4%. However, this limited role has to be justified by the amount of cement that can be saved. 5.3.6 Implications of cement saving By examining Figure 4.4a it can be deduced that the UCS of 2% cement treated soil A can be achieved by 3.3% content of 1:2 cement-RHA additive (ie 1.1% cement + 2.2% RHA). The cement saving is therefore equal to 2 - 1.1 = 0.9% and the ratio of RHA required to cement saved is 2.2/0.9 = 2.44. Therefore 1:2 cement-RHA additive is not economically feasible to replace the 2% of cement in stabilising soil A unless the cost of cement is equal to or greater than 2.44 times the cost of RHA. Table 5.6 has been derived in a similar manner, utilising Figures 4.4, 4.6 and 4.8 and applying the same calculations 168 for the various values of strength, plasticity and shrinkage for each case of soil treatment. From Table 5.6, it can be deduced that: i) At a low level of achievement, RHA has a significant role in cement-RHA soil stabilisation. ii) 1:1 cement-RHA additive tends to be the most economical used. mixture of all cement-RHA additives The additive tends to be less economical as the RHA content in the additive increases. iii) Cement-RHA additives are more efficient in improving the properties of low cohesion soils than in improving the properties of clays. iv) Cement-RHA additives are not efficient in achieving the plasticity and shrinkage of 4% cement soil stabilisation. v) 1:2 cement-RHA additives can be recommended for replacing 2% cement in modifying the strength of low cohesion soils provided that the cost of cement is equal to or greater than, 2.4 times the cost of RHA. For higher levels of achievement 169 (ie, strength of 4% cement stabilised soil) or to achieve the plasticity and shrinkage achieved with 2% cement stabilised soil, the cement-RHA additive is not economical unless the cost of cement is equal to or greater than 4 times the cost of RHA. vi) 1:3 and 1:4 cement-RHA additives are not efficient and cannot be recommended to be used in soil stabilisation. 5.3.7 Effect of cement-RHA additive on the behaviour of soils under the action of repeated dynamic load In section 5.3.2a, it was found that RHA acted as a pozzolan and has a role in strength development of cement-RHA stabilisation. To inspect the effectiveness of this role in improving the behaviour of soils under the action of repeated dynamic loads, it was decided to compare the pavements containing 1.5% cement treated soil D and 3% content of 1:1 cement-RHA treated soil D with the control pavement of untreated soil D. The various measurements of surface deflection for the three pavements, shown in Tables 4.15, 4.18 and 4.19 reveal that: i) For any point on the grid, where measurements were taken, the surface deflection in all three 170 pavements increased with the increase in number of load applications. ii) As the number of total load applications to the pavements increases, the actual deflection per single load applied decreases, indicating that the pavement stiffness had increased (see Table 5.7). iii) The maximum deflections for the various number of load cycles occurred close to wheel contact area (ie point Gd and eH on the grid). iv) For any number of load cycles, the deflections, at any point on the grid, of the cement and cement-RHA treated pavements were less than the deflection of the untreated pavement. This indicates that cement and cement-RHA additives increase the stiffness and reduce the compressibility of soils. v) The maximum deflection of the 3% content of 1:1 cement-RHA treated pavement after 50,000 load cycles was equal to 2.91mm, which was slightly less than the maximum deflection of the 1.5% cement treated pavement which was equal to 2.96mm. However, the role of RHA as a pozzolan in cement-RHA additive for improving the stiffness of 171 a soil and reducing its compressibility could be more significant had the curing period (7 days) and the age of the pavement at time of test (7 days) been greater. vi) For all pavements, most of the points where measurements were taken, exhibited a downward movement and the permanent deformations of the pavements were caused by the densification of the pavements rather than by any shear failure of these pavements. The upward movements of the points at the edges of the grid of the cement treated pavement, as shown in Figure 4.17, are probably caused by an incorrect initial measurement reading at zero load cycle at these points. vii) A visual assessment of the surface of all pavements showed that no fatigue cracks or shrinkage cracks were developed and the pavements were intact and sound at the conclusion of the test. In general, the observations derived from the results of the repeated dynamic load test have demonstrated that 1:1 cement-RHA additive is effective, but not very efficient, in improving the behaviour of soils under the action of repeated loads. 172 Table 5.1 Soil A B C Effect of RHA additive on the grading of soils. Grading of untreated soil % passing Grading of RHA % passing Grading of soil + 8% RHA % passing Grading of Max. density curve % passing 19mm 100 100 100 100 95mm 73 100 75 70 4.75mm 36 100 41 50 2.36mm 22 100 28 35 425pm 15 60 19 15 75pm 8 17 9 6 13.5pm 4 12.5 5 3 4.75mm 100 100 100 100 2.36mm 85 100 86.2 90 42 5pm 43 60 44 30 75pm 24 17 23 13 13.5pm 17 12.5 17 5 2.36mm 100 100 100 100 425pm 95 60 83 42 75pm 71 17 67 18 13.5pn 53 12.5 50 8 Sieve size 173 Table 5.2a Progressive total of loads applied 50 500 5,000 50,000 Deflection per load as number of load applications increases at point eH of 3% 1:1 lime-RHA treated pavement. No. of loads applied Deflection due to loads applied (mm) Average deflection due to one load application (mm) 50 450 4,500 45,000 5.85 6.75-5.85 6.45-6.75 7.00-6.75 0.117 0.0018 -6.6 x 10~ 5 * 5.55 x 10" 7 Error in reading Table 5.2b Progressive total of loads applied 50 500 5,000 50,000 Deflection per load as number of load applications increases at point eH of 2% lime treated pavement. No. of loads applied Deflection due to loads applied (mm) Average deflection due to one load application (mm) 50 450 4,500 45,000 5.95 6.90-5.95 7.12-6.90 7.20-7.12 0.119 0.002 4.88 x IO - 5 1.77 x IO" 6 174 Table 5.2c Progressive total of loads applied 50 500 5,000 50,000 Table 5.2d Progressive total of loads applied 50 500 5,000 50,000 Deflection per load as number of load applications increases at point eH of untreated pavement. No. of loads applied Deflection due to loads applied (mm) Average deflection due to one load application (mm) 50 450 4,500 45,000 3.12 4.25-3.12 6.97-4.25 8.95-6.97 0.062 0.0025 0.0006 0.0004 Deflection per load as number of load applications increases at point eH on the grid of 8% RHA treated pavement. No. of loads applied Deflection due to loads applied (mm) Average deflection due to one load application (mm) 50 450 4,500 45,000 3.40 4.25-3.40 7.00-4.25 8.20-7.00 0.068 1.88 x IO - 3 6.11 x 10~ 4 2.66 x 1 0 - 5 175 Table 5.3 Ratio of RHA required to lime saved or identical economic cost ratio of lime to RHA. Level of Achievements UCS of 2% lime treated soil UCS of 4% lime treated soil Plasticity index of 2% lime treated soil Plasticity index of 4% lime treated soil Linear shrinkage of 2% lime treated soil Linear shrinkage of 4% lime treated soil N/A Soil Lime:RHA 1:3 Lime:RHA 1:4 A 2.12 2.15 N/A N/A B 3.44 3.24 N/A N/A C 3.0 6 13 A 3 N/A N/A N/A B N/A N/A N/A N/A C 3 N/A N/A A 5.66 22.9 9 16 B 5.66 10 9 N/A C N/A N/A 36 A N/A N/A N/A N/A B 3 N/A N/A N/A C N/A N/A N/A A 3 2.63 3 4.88 B 3 4.04 9 N/A C 7 7.30 10.33 A N/A N/A N/A N/A B 4 N/A N/A N/A C N/A N/A N/A No lime saving could occur. Additive is not tested. LimesRHA Lime:RHA 1:2 1:1 176 Table 5.4 ^^.Additives Soils^v^ Ratios of strength at 7 days to strength at 90 days of soils treated with 8% content of various additives. Cement Cement:RHA 1:1 Cement:RHA 1:2 Cement:RHA 1:3 Cement:RHA 1:4 A .65 - .56 .55 .55 B .54 - .44 .40 .58 C .68 .81 .78 .70 - Table 5.5 Ratios of strength at 28 days to strength at 90 days of soils treated with 8% content of various additives. Cement Cement:RHA 1:1 Cement:RHA 1:2 Cement:RHA 1:3 Cement:RHA 1:4 A .93 - .74 .74 .74 B .89 - .72 .70 .79 C .85 .85 .90 .86 - ^•v. Additives Soils^-^. 177 Table 5.6 Ratio of RHA required to cement saved or identical economic cost ratio of cement to RHA. Level of Achievements Soil Cement:RB7 . Cement:RHA Cement:RHA 1:1 1:2 1:3 Cement:RHA 1:4 A 2.44 5 N/A B 2.29 2.71 N/A 10 45 A 4.01 N/A N/A B 2.81 2.65 N/A N/A N/A A 4.04 N/A N/A B 4.04 9 N/A 5.55 9 A N/A N/A N/A B N/A N/A N/A N/A N/A A 4.04 N/A N/A B N/A N/A N/A 4.04 6.65 A N/A N/A N/A B N/A N/A N/A N/A N/A UCS of 2% cement treated soil C UCS of 4% cement treated soil C Plasticity index of 2% cement treated soil C Plasticity index of 4% cement treated soil C Linear shrinkage of 2% cement treated soil C Linear shrinkage of 4% cement treated soil C N/A 5.66 7 4 15 3 15 N O cement saving could occur. Additive is not tested. 178 Table 5.7a Progressive total of loads applied 50 500 5,000 50,000 Table 5.7b Progressive total of loads applied 50 500 5,000 50,000 Table 5.7c Progressive total of loads applied 50 500 5,000 50,000 Deflection per load as number of load applications increases at point eH on the grid of untreated pavement. No. of loads applied Deflection due to loads applied (mm) Deflection due to one load application (mm) 50 450 4,500 45,000 3.12 4.25-3.12 6.97-4.25 8.95-6.97 0.062 0.0025 0.0006 0.0004 Deflection per load as number of load applications increases at point eH on the grid of 1.5% cement treated soil. No. of loads applied Deflection due to loads applied (mm) Deflection due to one load application (mm) 50 450 4,500 45,000 1.30 2.23-1.30 2.53-2.23 2.96-2.53 0.026 0.002 6.66 x 10~ 5 9.55 x IO" 6 Deflection per load as number of load applications increases at point dG on the grid of the 3% content of 1:1 cement-RHA treated soil. No. of loads applied Deflection due to loads applied (mm) Average deflection due to one load application (mm) 50 450 4,500 45,000 2.04 2.55-2.04 2.82-2.55 8.95-6.97 0.040 0.0011 6 x IO -5 2 x 10 -6 179 Chapter VI EXPERIMENTAL INVESTIGATIONS USING GRANULATED BLAST FURNACE SLAG (GBFS) 6.1 Scope of Chapter This chapter covers the experimental research used to determine the behaviour of granulated blast furnace slag in relation to its use in soil stabilisation. It sets the objectives of this research, describes the materials used and details the programme and procedures of testing. It also gives the results of all the various tests used. 6.2 Objectives of Research The main objectives of the research reported in this chapter have been as follows: a) To examine the influence of granulated blast furnace slag, as a single additive to soils on various properties of a range of soils. b) To study the effects of lime-GBFS and cement-GBFS additives on the properties of soils. 180 6.3 Materials 6.3.1 Blast Furnace Slag (GBFS) The slag used was a sample of granulated blast furnace slag produced in Port Kembla, NSW, and delivered in 200 litre drums to the Department of Civil and Mining Engineering, University of Wollongong. The specific gravity of the sample was 2.86 and the grading was as follows: % passing 2.36mm 100 % passing 425pm % passing 75pm % passing 13.5pm 50 5 2 The chemical analysis of the sample was as follows: Si02 31.7% A1203 Fe203 CaO MgO Na20 k20 Loss on ignition 14.0% 2.6% 40.5% 5.80% 0.18% 0.42% 1.04% 181 6.3.2 Cement 'Kandos' commercial grade, ordinary portland cement was used conforming to Australian Standards (AS1315) as specified in section 4.3.2. 6.3.3 Lime 'Blue Circle' commercial grade, hydrated lime was used, conforming to Australian Standards (AS1672) as specified in section 4.3.3. 6.3.4 Soils Four different soils were selected for stabilisation and tested in this investigation. soils A, B, C and D. These soils are designated as Description and properties of these soils have been given in Chapter 4 (section 4.3.4 and Table 4.1) . 6.4 Testing regime GBFS varies according to the iron content of the ore, the proportions and constituents of fluxing stone and coke fed into the furnace solidification of and the the liquid conditions slag. of cooling and The variations are 182 reflected in the physical and chemical composition of GBFS with particular emphasis on the ratio of lime to silica and the sulphur content. The relative contents of these materials affect the pozzolanic reaction of GBFS with lime and cement. Consequently, it was decided that testing be carried out, in a sequence similar to that in Chapter 4 (section 4.4), to determine the: i) Reactivity of GBFS (ie, the optimum ratio of lime or cement to GBFS). ii) Effect of lime, GBFS and cement individual additives on the engineering properties of soils A,B and C. iii) Effect of lime-GBFS and cement-GBFS additivies at their optimum and practical ratios on the properties of soils A,B and C. iv) Behaviour of GBFS, lime, cement, lime-GBFS and cement-GBFS stabilised soil D under the action of repeated dynamic loads. Testing was carried out in accordance with methods described in Chapter 3. 183 6.5 Optimum ratios of lime or cement to GBFS The unconfined compressive strength test was selected to investigate the degree of reactivity of GBFS in lime-GBFS and cement-GBFS compacted specimens and specifically to determine the optimum ratios of lime and cement to GBFS. Dry mixtures of lime-GBFS and cement-GBFS were prepared, proportioned by weight and mixed. The ratio of lime to GBFS and cement to GBFS was in the range of 1:1 and 1:10. Two series of compacted specimens were then prepared at OMC using standard compaction test equipment. All specimens were cured and tested in a manner similar to that specified in Chapter 4 (section 4.5). The results of the UCS tests on the lime-GBFS specimens are presented in Figure 6.1, whereas those of cement-GBFS specimens are presented in Figure 6.2. Figure 6.1 indicates that for both curing periods (28 and 90 days), the optimum ratio of lime to GBFS is the ratio 1:2 whereas Figure 6.2 shows that there is no optimum ratio of cement to GBFS. This result indicates that the strength of cement-GBFS specimens is dominated by the hydration reactions of cement rather than by the pozzolanic reaction between the released lime and the GBFS. 184 6.6 Treatment of soils with various additives Various additives, namely GBFS, lime, lime-GBFS, cement, cement-GBFS were used individually to stabilise the soils (A, B & C) . The various quantities of additives were 2%, 4%, 6% and 8% of the total weight of the dry soil and additive. The ratio of lime to GBFS for each quantity of additive was varied as 1:1, 1:2, 1:3 and 1:4. Although the ratio 1:2 was found to be the optimum ratio of lime to GBFS (section 6.5), the values 1:1, 1:3 and 1:4 were also considered to be within the practical range. The initial testing indicated that no optimum ratio of cement to GBFS occurs (section 6.5). In the test series the values 1:1, 1:2, 1:3 and 1:4 were considered to be within the practical range and were also used for comparison. 6.7 Testing of stabilised soils 6.7.1 Compaction characteristics The optimum moisture contents and the maximum dry densities of soils stabilised with various additives and various quantities (section 6.6) were determined in accordance with standard compaction test T120. The test results are presented in Tables 6.1 and 6.2. 185 6.7.2 Unconfined compressive strength Three series of specimens of soils stabilised with the various additions and various quantities (section 6.6) were prepared and compacted to their maximum dry densities at their OMC using the standard compaction test equipment. All specimens were then cured and tested in a manner similar to that described in Chapter 4 (section 4.7.2). The results of specimens cured for 7, 28 and 90 days are shown in Tables 6.3 and 6.4, whereas the 90 days test results are shown in Figures 6.3 and 6.4. 6.7.3 Linear shrinkage The linear shrinkage of all mixes was determined in accordance with test method T113 using materials collected from unconfined compressive strength crushed specimens which had been previously cured for 7 and 28 days. moulding and testing techniques were Preparation, identical to those specified in Chapter 4 (section 4.7.3). The results of the 7 and 28 days tests are presented in Tables 6.5 and 6.6, whereas the results of the 28 days curing period are shown in Figures 6.5 and 6.6. 186 6.7.4 Atterberg Limits Plastic limit, liquid limit and plasticity index of all mixes were determined in accordance with test methods T108 and T109 using compressive materials strength crushed collected specimens previously cured for 7 and 28 days. from unconfined which had been Preparation, curing and testing procedures were identical to those shown in Chapter 4 (section 4.7.4). Liquid limit, plastic limit and plasticity index of the various treatments after the curing periods of 7 and 28 days are given in Tables 6.5 and 6.6 where as the results of the plasticity index for the 28 days curing period are given in Figures 6.7 and 6.8. 6.7.5 Effect of delay in compaction on the strength of stabilised soils This part of the investigation was limited to some selected mixes. Its main role the effect of delay stabilised soils. was to determine the general trend of in compaction on the strength of Samples of dry soil A were mixed with cement and cement-GBFS additives. The ratio of cement to GBFS was varied as 1:2 and 1:4, whereas the quantity of additives used in each case was 8% of the total dry weight of the treated soil. 187 Samples of dry soil C also were mixed with lime and lime-GBFS additives. The ratio of lime to GBFS was varied as 1:1 and 1:3, whereas the quantity of additives used in each case was 8% of the total dry weight of the treated soil. Water was added and every mix was put in a covered metal container and maintained at its OMC during the delay periods. At the conclusion of the various delay periods (2 hours, 4 hours, 6 hours and 24 hours) the various mixtures were immediately compacted using the standard compaction test equipment. The speciemns were cured and tested in a way similar to that described in Chapter 4 (section 4.7.5). At the conclusion of the 90 days curing period the specimens were subjected to unconfined compression. The strength of these specimens is given in Tables 6.7 and 6.8. The losses in strength due to delays in compaction, expressed as percentage of strength of undelayed compaction specimens, also are given in Tables 6.7 and 6.8 and shown in Figures 6.9 and 6.10. 6.7.6 Effect of various additives on the shear strength parameters of soils The undrained triaxial compression test was carried out on selected stabilised mixes to determine whether or not the 188 increase in UCS of stabilised mixes was associated with an increase in cohesion, angle of internal friction or both. The tests were carried out in accordance with Australian Standards Test Method AS1289.F4.1. Samples of dry soil B were mixed with cement and cement-GBFS additives. The ratio of cement to GBFS was varied as 1:2 and 1:3. The quantities of additives in each case were 4% and 8% of total dry weight of the treated soil. Samples of dry soil C were mixed with lime and lime-GBFS additives. The ratio of lime to GBFS was varied as 1:1 and 1:3. The quantities of additives in each case were 4% and 8% of the total dry weight of the treated soil. Water was added and every mix was compacted at its OMC using standard compaction test equipment. Preparation, curing and testing of samples were identical to those described in Chapter 4 (section 4.7.6). Values of cohesion (C) and angle of internal friction (0) of the various mixes are given in Tables 6.9 and 6.10. 189 6.7.7 Effect of various additives on the CBR value of soils The CBR test in this part of the investigation was limited to some selected mixes. Its main role was to determine the general trend of the effect of various additives on the CBR property of soils and to confirm results derived from the UCS test. Dry samples of soil A and B were mixed with GBFS, lime and lime-GBFS additives. The ratio of lime to GBFS and cement to GBFS was varied as 1:2 and 1:3. The quantities of additives in each case were 4% and 8% of the total dry weight of treated soil. Cement at the rate of 2% of total dry weight of treated soil, also was used for comparison. Further, dry samples of soil C were prepared and mixed with GBFS, lime, lime-GBFS and cement-GBFS additives. The ratio of lime to GBFS and cement to GBFS, in this case, was varied as 1:1 and 1:2 whereas the quantities of additives in each case were 4% and 8% of total dry weight of treated soil. Cement at the rates of 4% and 8% of total dry weight of treated soil, also was used for comparison. Water was added and all mixes were compacted at their OMC in accordance with the standard procedures of the CBR test with the exception of using a special split CBR mould to 190 facilitate specimen extraction for the purpose of curing. All specimens were cured and tested in a manner similar to that described in Chapter 4 (section 4.7.7). The CBR values of the various mixes for the various curing times are presented in Tables 6.11 to 6.13, and the results of the 90 days curing period are shown in Figures 6.11 to 6.13. 6.7.8 Repeated dynamic load test The test in this part of the investigation was conducted on three pavements. Soil D stabilised with GBFS, lime-GBFS and cement-GBFS additives pavements. The ratio of lime to GBFS and cement to GBFS used was formed the base course of these 1:1, whereas the quantity of additives used was 8%, 3% and 3% respectively and expressed as percentage of the total dry weight of the treated soil. The sub-base of all pavements consisted of beach sand from the Illawarra region. Particle size distribution of sand was as given in section 4.7.8a. Placement of pavement materials, compaction of sub-base and base courses and assembling of test rig were carried out in a manner similar to that described in section 4.7.8a. 191 After the pavements had been constructed and the test rig assembled, zero readings were taken at the grid points at which deflections were to be measured. The pavements were covered by a damp cloth and cured for 7 days. At the conclusion of the curing period the GBFS and the lime-GBFS treated pavements were each subjected to 50,000 cycles of 42kN load applications, at a uniform rate of one load cycle per second. The cement-GBFS treated pavement was intended to be subjected to one million 42kN load applications, but because of a major breakdown in the test facility the test was concluded at 250,000 load applications. Deflection readings were taken at intervals during the load application for the three pavements. In total, 385 readings were taken of the deflections of the three pavements at various intervals during the tests and at various positions on the pavements. in a tabular The results of the deflections are given form in Tables 6.14 to 6.16. Figures 6.14 to 6.16 show the deflections of pavements after the various intervals at the cross sections of the maximum deflections. 6.7.9 Scanning Electron Microscopy It was considered that limited testing of some of the soil mixes would be sufficient for determining the morphology of the GBFS pozzolanic reaction products in soil stabilisation. 192 Samples of lime-GBFS treated Soil A and lime-GBFS treated Soil C were made available for examination in a Hitachi S450 Scanning Electron Microscope. The ratio of lime to GBFS in each case was 1:1 whereas the quantity of lime-GBFS additive was 8% of the total dry weight of the treated soil. Preparation, curing and examining of samples were identical to those described in Chapter 4 (section 4.7.9). Scanning electron micrographs of the lime-GBFS stabilised Soil A and lime-GBFS stabilised Soil C are shown in Figures 6.17 and 6.18. 6.7.10 Powder X-ray Diffraction Analysis X-ray diffraction patterns were determined for the soil mixes used in the preceding Scanning Electron Microscopy examination. Preparation, curing and testing of specimens were carried out in a way similar to that specified in Chapter 4 (section 4.7.10). The X-ray diffraction patterns determined for the lime-GBFS treated soils A and C are shown in Figures 6.19 and 6.20. 193 T A B L E 6.1a ADDITIVE Compaction characteristics of lime, G B F S and LimeG B F S stabilised soil A OMC (%) (%) MDD gm/cm 3 LIME 0% 2% 4% 6% 8% LIME.GBFS 1:1 13.00 14.50 16.00 16.50 17.00 1.83 1.82 1.77 1.74 1.73 0% 2% 4% 6% 8% 13.00 14.50 15.50 16.00 16.50 1.83 1.82 1.79 1.77 1.77 0% 2% 4% 6% 8% LIME:GBFS 1:3 13.00 14.50 15.00 15.75 16.00 1.83 1.82 1.81 1.79 1.79 0% 2% 4% 6% 8% LIME:GBFS 1:4 13.00 14.50 14.90 15.50 15.00 1.83 1.82 1.82 1.80 1.80 0% 2% 4% 6% 8% 13.00 14.50 14.50 14.70 14.70 1.83 1.82 1.82 1.82 1.83 0% 2% 4% 6% 8% 13.00 14.00 14.50 14.70 14.70 1.83 1.84 1.84 1.85 1.85 LIME.GBFS 1:2 GBFS 194 T A B L E 6.1b ADDITIVE Compaction characteristics of lime, G B F S and lime-GBFS stabilised soil B OMC (%) (%) MDD gm/cm 3 LIME 0% 2% 4% 6% 8% LIME:GBFS 1:1 15.00 16.00 16.50 17.00 18.00 1.82 1.81 1.78 1.75 1.73 0% 2% 4% 6% 8% 15.00 15.50 16.00 16.50 17.50 1.82 1.82 1.81 1.78 1.77 0% 2% 4% 6% 8% LIME:GBFS 1:3 15.00 15.50 16.00 16.00 17.00 1.82 1.83 1.82 1.82 1.82 0% 2% 4% 6% 8% LIME:GBFS 1:4 15.00 16.00 16.00 16.00 16.00 1.82 1.82 1.83 1.83 1.84 0% 2% 4% 6% 8% 15.00 15.50 16.00 16.00 16.00 1.82 1.82 1.83 1.84 1.84 0% 2% 4% 6% 8% 15.00 15.50 15.50 15.70 15.70 1.82 1.83 1.84 1.84 1.85 LIME:GBFS 1:2 GBFS 195 T A B L E 6.1c ADDITIVE Compaction characteristics of lime, G B F S and lime-GBFS stabilised soil C OMC (%) (%) MDD gm/cm 3 LIME 0% 2% 4% 6% 8% 22.00 23.00 24.00 24.50 25.00 1.32 1.32 1.31 1.30 1.29 22.00 22.50 23.00 23.00 23.00 1.32 1.32 1.32 1.31 1.31 22.00 22.00 22.50 22.50 23.50 1.32 1.32 1.32 1.32 1.32 0% 2% 4% 6% 8% 22.00 22.00 22.00 21.50 20.00 1.32 1.32 1.32 1.32 1.33 0% 2% 4% 6% 8% 22.00 22.00 21.00 20.50 20.00 1.32 1.32 1.32 1.32 1.33 LIME:GBFS 1:1 0% 2% 4% 6% 8% LIME:GBFS 1:2 0% 2% 4% 6% 8% LIME:GBFS 1:3 GBFS 196 T A B L E 6.2a ADDITIVE Compaction characteristics of cement, G B F S and cement-GBFS stabilised soil A (%) OMC (%) MDD gm/cm 3 CEMENT 0% 2% 4% 6% 8% CEMENT:GBFS 1:1 13.00 14.00 14.50 15.50 16.50 1.83 1.85 1.85 1.85 1.85 13.00 14.00 14.50 15.00 15.70 1.83 1.83 1.84 1.85 1.85 0% 2% 4% 6% 8% CEMENT:GBFS 1:3 13.00 14.00 14.50 14.50 14.70 1.83 1.83 1.84 1.84 1.84 0% 2% 4% 6% 8% CEMENT:GBFS 1:4 13.00 14.00 14.50 14.50 14.70 1.83 1.83 1.84 1.85 1.85 0% 2% 4% 6% 8% 13.00 14.30 14.70 14.70 14.90 1.83 1.83 1.83 1.84 1.84 0% 2% 4% 6% 8% 13.00 14.00 14.50 14.70 14.70 1.83 1.84 1.84 1.85 1.85 0% 2% 4% 6% 8% CEMENT:GBFS 1:2 GBFS 197 TABLE 6.2b ADDITIVE Compaction characteristics of cement, GBFS and cement-GBFS stabilised soil B OMC (%) (%) MDD gm/cm 3 CEMENT 0% 2% 4% 6% 8% CEMENT:GBFS 1:1 15.00 15.50 16.50 17.00 17.50 1.82 1.82 1.84 1.84 1.84 15.00 15.50 16.00 16.50 17.00 1.82 1.83 1.84 1.84 1.84 15.00 15.50 16.00 16.00 16.50 1.82 1.83 1.84 1.84 1.85 15.00 15.50 16.00 15.70 15.70 1.82 1.83 1.84 1.84 1.85 0% 2% 4% 6% 8% 15.00 15.50 16.50 15.70 15.70 1.82 1.83 1.84 1.85 1.85 0% 2% 4% 6% 8% 15.00 15.50 15.50 15.70 15.70 1.82 1.84 1.85 1.85 1.85 0% 2% 4% 6% 8% CEMENT:GBFS 1:2 0% 2% 4% 6% 8% CEMENT.GBFS 1:3 0% 2% 4% 6% 8% CEMENT:GBFS 1:4 GBFS 198 T A B L E 6.2c ADDITIVE Compaction characteristics of cement, G B F S and cement-GBFS stabilised soil C (%) OMC (%) MDD gm/cm 3 CEMENT 0% 2% 4% 6% 8% CEMENT:GBFS 1:1 22.00 23.00 24.50 25.00 26.00 1.32 1.34 1.35 1.39 1.40 22.00 22.00 23.00 24.00 25.00 1.32 1.33 1.34 1.37 1.37 22.00 22.00 22.50 23.00 23.50 1.32 1.33 1.34 1.36 1.36 0% 2% 4% 6% 8% 22.00 22.00 22.00 22.50 23.00 1.32 1.33 1.33 1.34 1.34 0% 2% 4% 6% 8% 22.00 22.00 21.00 20.50 20.00 1.32 1.32 1.32 1.32 1.33 0% 2% 4% 6% 8% CEMENT:GBFS 1:2 0% 2% 4% 6% 8% CEMENT:GBFS 1:3 GBFS 199 TABLE 6.3a U C S (MPa) of lime, GBFS and lime-GBFS stabilised soil A. ADDITIVE (%) 7 CURING (DAYS) 90 28 LIME 0% 2% 4% 6% 8% LIME:GBFS 1:1 0.33 0.43 0.46 0.43 0.41 0.33 0.55 0.76 0.73 0.70 0.33 0.69 1.00 0.95 0.90 0% 2% 4% 6% 8% 0.33 0.41 0.46 0.48 0.40 0.33 0.44 0.72 0.79 0.79 0.33 0.54 0.86 0.95 0.90 0.33 0.39 0.50 0.67 0.57 0.33 0.43 0.57 0.85 0.85 0.33 0.46 0.75 0.92 0.94 0% 2% 4% 6% 8% LIME:GBFS 1:4 0.33 0.39 0.39 0.39 0.57 0.33 0.40 0.47 0.56 0.80 0.33 0.44 0.51 0.61 0.70 0% 2% 4% 6% 8% 0.33 0.36 0.39 0.39 0.35 0.33 0.38 0.39 0.50 0.51 0.33 0.40 0.51 0.58 0.67 0% 2% 4% 6% 8% 0.33 0.34 0.36 0.38 0.40 0.33 0.36 0.37 0.38 0.41 0.33 0.36 0.36 0.39 0.40 LIME:GBFS 1:2 0% 2% 4% 6% 8% LIME:GBFS 1:3 GBFS 200 TABLE 6.3b ADDITIVE U C S (MPa) of lime, GBFS and lime-GBFS stabilised soil B. (%) 7 C U R I N G (DAYS) 28 90 LIME 0% 2% 4% 6% 8% 0.26 0.32 0.34 0.28 0.27 0.26 0.40 0.42 0.38 0.36 0.26 0.50 0.57 0.50 0.45 0% 2% 4% 6% 8% 0.26 0.30 0.32 0.32 0.30 0.26 0.37 0.39 0.35 0.36 0.26 0.44 0.55 0.53 0.44 0.26 0.28 0.30 0.31 0.31 0.26 0.30 0.32 0.35 0.36 0.26 0.34 0.40 0.50 0.51 0% 2% 4% 6% 8% LIME:GBFS 1:4 0.26 0.27 0.28 0.29 0.29 0.26 0.30 0.30 0.29 0.33 0.26 0.32 0.32 0.36 0.38 0% 2% 4% 6% 8% 0.26 0.26 0.26 0.26 0.31 0.26 0.26 0.26 0.28 0.32 0.26 0.29 0.28 0.30 0.35 0% 2% 4% 6% 8% 0.26 0.26 0.26 0.27 0.28 0.26 0.26 0.26 0.27 0.28 0.26 0.26 0.26 0.27 0.29 LIME-.GBFS 1:1 LIME:GBFS 1:2 0% 2% 4% 6% 8% LIME:GBFS 1:3 GBFS 201 TABLE 6.3c ADDITIVE U C S (MPa) of lime, GBFS and lime-GBFS stabilised soil C. (%) 7 C U R I N G (DAYS) 90 28 LIME 0% 2% 4% 6% 8% LIME:GBFS 1:1 0.21 0.25 0.34 0.43 0.41 0.21 0.30 0.41 0.51 0.50 0.21 0.33 0.44 0.56 0.55 0% 2% 4% 6% 8% 0.21 0.22 0.25 0.30 0.30 0.21 0.25 0.30 0.36 0.37 0.21 0.28 0.35 0.42 0.43 0.21 0.22 0.24 0.27 0.27 0.21 0.26 0.29 0.34 0.34 0.21 0.28 0.32 0.37 0.38 0% 2% 4% 6% 8% 0.21 0.22 0.24 0.26 0.28 0.21 0.24 0.27 0.30 0.32 0.21 0.25 0.29 0.33 0.35 0% 2% 4% 6% 8% 0.21 0.21 0.23 0.23 0.24 0.21 0.21 0.23 0.24 0.25 0.21 0.21 0.23 0.25 0.25 LIME:GBFS 1:2 0% 2% 4% 6% 8% LIME:GBFS 1:3 GBFS 202 TABLE 6.4a ADDITIVE U C S (MPa) of cement, GBFS and cement-GBFS stabilised soil A (%) 7 CURING (DAYS) 90 28 CEMENT 0% 2% 4% 6% 8% CEMENT:GBFS 1:1 0.33 1.26 1.75 2.45 3.00 0.33 1.95 2.70 3.50 4.30 0.33 2.00 3.15 4.00 4.60 0.33 0.60 1.41 1.41 1.58 0.33 0.80 1.69 1.95 1.96 0.33 1.00 2.15 2.35 2.50 0.33 0.45 0.85 0.92 1.00 0.33 0.50 1.10 1.25 1.37 0.33 0.59 1.43 1.50 1.64 0.33 0.42 0.75 0.90 0.99 0.33 0.45 0.90 1.20 1.35 0.33 0.45 0.90 1.30 1.62 0% 2% 4% 6% 8% 0.33 0.39 0.47 0.75 0.85 0.33 0.40 0.49 0.75 0.95 0.33 0.40 0.71 1.10 1.32 0% 2% 4% 6% 8% 0.33 0.34 0.36 0.38 0.40 0.33 0.36 0.37 0.38 0.41 0.33 0.36 0.36 0.38 0.40 0% 2% 4% 6% 8% CEMENT:GBFS 1:2 0% 2% 4% 6% 8% CEMENT:GBFS 1:3 0% 2% 4% 6% 8% CEMENT:GBFS 1:4 GBFS 203 TABLE 6.4b ADDITIVE U C S (MPa) cement, G B F S and cement-GBFS stabilised soil B. (%) 7 C U R I N G (DAYS) 28 90 CEMENT 0% 2% 4% 6% 8% CEMENT:GBFS 1:1 0.26 0.43 0.62 0.90 1.40 0.26 0.67 1.02 1.50 2.30 0.26 0.74 1.15 1.70 2.57 0.26 0.30 0.52 0.62 0.75 0.26 0.42 0.73 0.82 1.02 0.26 0.50 0.85 1.00 1.20 0.26 0.33 0.40 0.60 0.61 0.26 0.38 0.50 0.65 0.75 0.26 0.42 0.54 0.75 0.95 0.26 0.33 0.41 0.50 0.51 0.26 0.33 0.41 0.51 0.55 0.26 0.33 0.42 0.60 0.65 0% 2% 4% 6% 8% 0.26 0.27 0.28 0.29 0.40 0.26 0.30 0.35 0.47 0.50 0.26 0.30 0.37 0.47 0.55 0% 2% 4% 6% 8% 0.26 0.26 0.26 0.27 0.28 0.26 0.26 0.26 0.27 0.28 0.26 0.26 0.26 0.27 0.28 0% 2% 4% 6% 8% CEMENT:GBFS 1:2 0% 2% 4% 6% 8% CEMENT:GBFS 1:3 0% 2% 4% 6% 8% CEMENT:GBFS 1:4 GBFS 204 TABLE 6.4c ADDITIVE U C S (MPa) of cement, GBFS and cement-GBFS stabilised soil C. 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Additive % Time elapsed Since mixing 90 days U C S (MPa) loss in strength % 8% CEMENT 0.00 hours 2.00 hours 4.00 hours 6.00 hours 4.60 3.22 2.34 1.47 0.00 30.00 49.00 68.00 0.00 hours 2.00 hours 4.00 hours 6.00 hours 1.64 1.24 1.05 0.67 0.00 24.00 36.00 59.00 0.00 hours 2.00 hours 4.00 hours 6.00 hours 1.32 1.05 0.84 0.56 0.00 20.00 34.00 57.50 8%CEMENT:SUVG1:2 8%CEMENT:SLAG1:4 212 T A B L E 6.8 Additive % Effect of delay in compaction on the U C S of lime and lime-GBFS stabilised soil C Time elapsed since mixing 90 days U C S (MPa) loss in strength % 8 % LIME 0.00 hours 2.00 hours 4.00 hours 6.00 hours 24.00 hours 0.55 0.52 0.51 0.51 0.48 0.00 5.45 7.27 7.27 12.72 0.00 hours 2.00 hours 4.00 hours 6.00 hours 24.00 hours 0.43 0.41 0.39 0.37 0.36 0.00 4.65 9.30 13.95 16.27 0.00 hours 2.00 hours 4.00 hours 6.00 hours 24.00 hours 0.35 0.32 0.30 0.30 0.30 0.00 8.57 14.28 14.28 14.28 8%LIME:SLAG1:1 8%LIME:SLAG1:3 213 T A B L E 6.9a Effect of lime and lime-GBFS additives on the shear strength parameters of Soil B. ADDITIVES Lime 7 DAYS CURING 0% 4% 8% 0 (degrees) C (MPa) 28 D A Y S C U R I N G 0 (degrees) C (MPa) 19.00 29.00 32.00 0.08 0.10 0.16 19.00 32.00 37.00 0.08 0.13 0.21 Lime: GBFS 1:1 19.00 25.00 31.00 0.08 0.10 0.10 7.00 25.00 34.00 0.08 0.10 0.12 Lime: GBFS 0% 4% 8% 1:3 0% 4% 8% 19.00 22.00 26.00 0.08 0.08 0.10 19.00 24.00 27.00 0.08 0.10 0.10 T A B L E 6.9b Effect of lime and lime-GBFS additives on the shear strength parameters of Soil C. 7 DAYS CURING ADDITIVES Lime 0% 4% 6% Lime-.GBFS 1:1 0% 4% 8% Lime:GBFS 28 DAYS CURING 0 (degrees) C (MPa) 0 (degrees) C (MPa) 7.00 30.00 28.00 0.08 0.16 0.23 7.00 35.00 33.00 0.08 0.17 0.22 7.00 20.00 28.00 0.08 0.11 0.14 7.00 22.50 33.00 0.08 0.12 0.18 7.00 12.00 20.00 0.08 0.10 0.11 7.00 14.00 22.00 0.08 0.11 0.13 1:3 0% 4% 8% 214 T A B L E 6.10 Effect of cement and cement-GBFS additives on the shear strength parameters of soil B. 7 DAYS CURING ADDITIVES Cement 0% 4% 6% CementGBFS 1:2 0% 4% 8% CementGBFS 28 D A Y S C U R I N G 0 (degrees) C (MPa) 0 (degrees) C (MPa) 19.00 36.50 44.00 0.08 0.11 0.16 19.00 47.00 50.00 0.08 0.19 0.29 19.00 28.00 29.00 0.08 0.13 0.14 19.00 47.00 48.50 0.08 0.23 0.25 19.00 24.00 26.00 0.08 0.10 0.12 19.00 38.00 46.50 0.08 0.18 0.23 1:3 0% 4% 8% 215 T A B L E 6.11 Effect of various additives and curing time on the C B R of stabilised soil A. CBR 28 Days 90 Days 55 75 72 55 81 76 55 69 80 55 71 84 0% 4% 8% 55 65 70 55 67 79 0% 4% 8% 55 60 65 55 62 66 0% 2% 55 102 55 110 55 80 99 55 80 105 55 70 101 55 70 98 ADDITIVES (%) LIME 0% 4% 8% LIME:GBFS1:2 0% 4% 8% LIME.GBFS 1:3 GBFS CEMENT CEMENT:GBFS1:2 0% 4% 8% CEMENT:GBFS1:3 0% 4% 8% 216 T A B L E 6.12 Effect of various additives and curing time on the C B R of stabilised soil B. ADDITIVES (%) LIME CBR 28 Days 90 Days 30 40 37 30 43 41 30 38 45 30 41 50 0% 4% 8% 30 36 42 30 36 43 0% 4% 8% 30 35 40 30 36 42 0% 2% 30 99 30 100 30 56 100 30 60 105 30 49 100 30 60 102 0% 4% 8% LIME.GBFS 1:2 0% 4% 8% LIME:GBFS1:3 GBFS CEMENT CEMENT:GBFS1:2 0% 4% 8% CEMENT:GBFS1:3 0% 4% 8% 217 T A B L E 6.13 Effect of various additives and curing time on the C B R of stabilised soil C. CBR 28 Days 90 Days 19 31 55 19 32 60 19 27 32 19 30 35 0% 4% 8% 19 25 32 19 27 35 0% 4% 8% 19 23 28 19 24 30 19 32 51 19 35 56 19 20 36 19 22 46 19 20 30 19 22 36 ADDITIVES (%) LIME 0% 4% 8% LIME:GBFS1:1 0% 4% 8% LIME:GBFS1:2 GBFS CEMENT 0% 2% 8% CEMENT:GBFS1:1 0% 4% 8% CEMENT:GBFS1:2 0% 4% 8% 218 TABLE 6.14 No. of Load Applications Permanent deformations of 3 % content of 1:1 Cement:GBFS treated pavement (mm) Row/Column a b c d e f g 5000 50000 250000 E 1.80 0.10 1.35 -0.70 0.78 -1.40 1.00 0.80 2.20 1.15 1.50 1.00 1.00 2.75 2.00 -0.20 0.02 -0.25 0.57 0.00 0.27 5000 50000 250000 F 1.72 1.76 2.17 0.70 1.28 1.57 1.42 2.10 2.80 1.28 1.55 2.15 2.05 2.22 2.50 0.21 1.31 1.51 0.17 1.30 1.42 G 1.37 1.87 1.87 0.51 1.16 1.24 0.89 1.66 2.60 1.00 0.99 1.09 1.80 2.07 2.04 1.25 1.75 0.50 -0.52 0.35 0.72 H 1.31 1.16 0.50 1.07 0.95 1.70 2.42 2.32 2.72 1.70 1.32 1.87 1.55 2.30 2.15 -0.57 5.15 0.73 5.01 0.03 5.81 I 0.40 0.38 0.12 -1.10 -1.20 0.30 0.45 0.38 0.45 3.98 2.75 1.26 1.85 1.36 1.83 -0.40 0,83 0.18 0.00 -1.52 0.18 5000 50000 250000 5000 50000 250000 5000 50000 250000 219 TABLE 6.15 No. of Load Applications 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 Permanent deformations of 3 % content of 1:1 lime:GBFS treated pavement (mm) Row/Column a b c d e E 0.30 -0.70 -0.70 -0.85 0.39 0.60 0.65 0.70 1.51 2.23 3.25 3.83 1.50 2.02 2.36 2.53 3.00 3.22 3.80 4.29 1.15 1.35 1.51 1.65 0.30 0.34 0.80 -0.32 F 0.40 0.50 1.30 0.68 0.00 1.02 -0.50 1.55 2.89 3.43 4.00 4.30 2.09 3.43 3.66 3.77 2.29 3.48 3.11 4.52 1.30 2.75 2.99 3.27 0.50 0.91 0.95 -1.05 0.41 0.58 0.54 1.11 0.90 1.51 -1.16 1.71 4.00 5.18 5.38 5.55 2.89 3.63 4.00 4.30 3.50 4.70 5.12 5.65 1.00 1.28 1.90 2.33 0.36 0.60 1.00 -0.55 0.60 0.80 1.00 0.96 0.30 1.00 -0.50 1.44 3.36 4.00 5.09 5.55 3.11 4.15 4.26 4.72 3.89 4.53 4.99 6.00 1.40 1.65 2.65 3.05 0.60 0.73 0.80 0.00 0.70 0.80 1.10 1.35 1.30 2.80 2.80 3.17 2.30 3.18 3.40 3.62 0.66 0.90 1.00 1.10 0.20 0.28 0.25 -0.47 G H I 0.20 0.75 0.00 -0.40 0.20 0.28 0.00 -0.80 f g 220 TABLE 6.16 No. of Load Applications 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 50 500 5000 50000 Permanent deformations of 8 % G B F S treated pavement (mm) Row/Column a b c d e f g E 1.10 0.80 1.65 0.00 -0.44 0.15 -0.40 0.40 0.83 1.88 2.58 3.08 1.99 2.13 3.24 5.39 2.36 4.02 4.96 6.76 1.75 0.85 2.65 3.45 -0.18 0.32 0.32 0.51 F 0.30 -0.30 1.70 0.48 1.33 3.10 0.60 2.43 4.15 -0.22 2.69 5.08 2.25 1.18 4.38 4.88 3.63 3.83 4.63 6.63 1.45 2.94 3.45 3.35 -0.04 0.06 0.56 0.66 G 0.35 0.45 2.10 2.20 0.95 1.67 1.74 2.75 1.87 2.82 4.97 5.42 2.41 3.58 5.11 5.21 3.44 4.26 5.26 6.26 1.10 2.45 3.80 3.70 -0.08 -0.05 0.38 0.40 H -0.05 0.25 0.20 -0.45 -0.05 1.09 2.13 3.05 2.85 5.10 5.38 5.55 3.30 5.40 6.00 6.40 4.35 5.70 6.20 6.70 1.20 1.20 2.80 3.30 0.00 0.00 0.10 0.25 0.50 1.20 1.10 0.60 0.44 1.53 1.22 1.38 0.74 1.72 2.10 2.42 0.53 2.03 3.90 3.38 0.50 1.50 2.60 3.41 1.45 0.40 0.20 0.30 0.12 1.32 0.67 0.92 I W> 221 CO z LU o co Q O • LU Q. 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CC UJ CC L U < IO h- -J 235 FIG.6.17 - Scanning electron micrograph of the fracture surface of Soil A stabilised with 8% content of 1:1 lime-GBFS additive after 7 days accelerated curing 236 FIG.6.18 - Scanning electron micrograph of the fracture surface of Soil C stabilised with 8% content of 1:1 lime-GBFS additive after 7 days accelerated curing 237 f !• ra >\™ /. <-» - <JSJ t <n> J a-« a-n O-«J . g-bs 9-U VS • » • * 0-3 i O'K fl'SS % 0-3 z ars a-is r <rv s r\> l ri> m* «..-.-\>3—\ - rtf 6-Slr • D-» t-C"^" o-o — = ^ . • 0-3r T3 03 (0 •H iH •H rQ CD > • o-iy (0 •rH •P +•> a-o> cn•H o-K < TJ Q-1C us 0-JE OSJ o-ve o-tr 0-5 (TIE rot ra rn o-iz m> «•-? f^P)) •CT°0 ^ l ^ ^ O ^ 73 ra rH •rH CM cn 0 w c O •H 4-1 1 rH 0 CD 3 OD CO g 0 •rH c U -H TJ 0) 0) +J rH 4-> +J .« (fl (0 rH rH a 0} 4H rH 0 c 0 <D U +J O +J c rd •H o-n o-i: t^yxmo) *Q?S u« 1-H SMI J'll I'll 0 5i 31^\0 >o> •H T3 <#> r00 rH > (0 rC a) rH +J +J 1 •H MH X ,5 ra o-fi / 0 u (fl •P (fl SH >1 4-1 c ra M-l o U T3 o-n rn \ ( 501 (Tl g. oi «i 0 7 •) S 6 H 238 o-s> rrt 1 r« a-a •OMJ • a-*.? *0?S »•« r vis "y < J O-iS |-0-K •• a-ts - ra a-as i . .* -»_ o-vt rl* Tl CU tn m f . art •H (13 ot* <r2> • <riv rQ > ra -H P P tn -H •a J VJ> 0?S • V.t O-lf r« o-ss o-»c •ott rlt VIS ta •H •H UJ c 0 CM •rH Di W CQ rH O 3 4H I O 0 Q) CIS Oil '00^ r ws «'« OUZ CK rH r H TJ 0) d) •) -52 < CH 0"lZ m >c. •9-1! Oil o-ti I'll 0'5I 0 51 o-vt 71^\y\\oro>\ g C -H • 0'tl - J:I . <rn P •• ra •H ra »H Ou ra Pd. a) UH iH >1 Cu O 03 ra O 4H W0 O T ) •H P TJ <c #> r00 O 03 >i n ra -P co ra .C 03 C " SH P P 0 I -H <4H x 5 <a o o-oi ^ * „X 0". SO ol u 01 • III l'*i H CM Chapter VII DISCUSSION AND ANALYSIS OF RESULTS CONCERNING GBFS 7.1 GBFS as a single additive to soils 7.1.1 Effect of GBFS additive on compaction characteristics of soil It can be observed from Table 6.1 that when GBFS is added to soils A, B and C, the maximum dry density of these soils is increased. This can be explained by the fact that the addition of GBFS to soils A, B and C has significantly improved the grading of these soils (see Table 7.1) and reduced the porosity of their compacted specimens (as shown in Appendix B). The effect of addition of GBFS to soils A, B and C on their OMC is related to the comparative fineness of GBFS and the soils. As shown in Table 6.1 when GBFS is added to the soils A, B and C the OMC of soil C decreases whereas the OMC of soil A and soil B increases. This is due to the fact that GBFS is coarser than soil C and hence it decreases the particle surface area of this soil and subsequently decreases the water demand in compaction. Conversely, GBFS is finer that soil A and soil B and hence it increases the 240 particle surface area of these soils increases the water demand in compaction. and subsequently The increase in OMC is more pronounced in the case of coarser soil (soil A) where the increase in fineness due to the addition of GBFS is more significant. GBFS as a single additive to soils, therefore, can be utilised in improving the workability of wet soils (ie, gravel, sand soils). it can also be used in improving the grading and increasing the density of soils and subsequently favourably affecting the strength properties of treated soils. 7.1.2 Effect of GBFS additive on the strength properties of soils 7.1.2a Effect on UCS It has been observed from Table 6.3 and Figure 6.3 that GBFS as a single additive to soils A, B and C increases the UCS of these soils. This can be attributed to reduction in porosity and increase in density of the compacted specimens of these treated soils. It can also be observed from Tables 6.3 that the UCS of GBFS treated soils A and B may not result in strength changes with the variation of curing time. This implies that strength development reactions had not taken place between these soils and any constituent of 241 GBFS during the various curing times. However, the slight increase in UCS of GBFS treated soil C with the increase in curing time may indicate a reaction between this heavy clay soil and the free lime in the GBFS. 7.1.2b Effect on CBR Tables 6.11 to 6.13 and Figures 6.11 to 6.13 show that the CBR values of treated soils A, B and C increase with the increase in the quantity of GBFS additive. This could be attributed to the decrease in compressibility caused by the increase in density and the decrease in porosity of these treated soils (see section 7.1.1). Unlike the UCS test results, the CBR values of all treated soils exhibited a slight increase with increase in curing time. However, this may not be meaningful in an engineering context in the light of precision, accuracy and repeatability of the test. 7.1.3 Effect of GBFS additive on the Atterberg limits and linear shrinkage of soils. Atterberg limits and linear shrinkage tests have exhibited some scattered results as shown in Table 6.5. Liquid limit and plastic limit of GBFS treated soil A show a very slight increase with the increase of GBFS quantity whereas liquid 242 limit and plastic limit of GBFS treated soil B do not vary from those of untreated soil. Tables 6.5a and 6.5b indicate that GBFS has no significant effect on the plasticity and linear shrinkage of low cohesion soils (ie soil A & soil B) whereas Table 6.5c shows that GBFS as a single additive to soils has a remarkable effect on the plasticity and linear shrinkage of cohesive soils (ie soil C) . Table 6.5c shows that plastic limit of GBFS treated soil C increases with the increase of GBFS quantity whereas liquid limit, plasticity index and linear shrinkage decrease with the increase in GBFS quantity. These effects are due to the partial replacement of high plastic particles of soil C with the low plasticity GBFS particles. The effects could also be attributed to the action of free lime in the GBFS on the clay particles which may explain the slight reduction in plasticity index of GBFS treated soil occuring with curing time. This is consistent with the findings for UCS tests in section 7.1.2a. Although the effects of GBFS on the plasticity and linear shrinkage of cohesive soils are remarkable, they are inferior to those which occur by the addition of lime or cement to these soils. For example, the linear shrinkage of 8% GBFS treated Soil C is almost comparable to the linear shrinkage achieved by the 243 addition of 1% lime or 1% cement to this soil (see Figures 6.5c and 6.6c). From Figures 6.7c and 6.8c, it can also be deduced that the addition of 6-7% GBFS to soil C is required to achieve the plasticity index achieved by the addition of 1% cement or 1% lime to the soil. The use of GBFS as a single additive to soils to modify their plasticity and shrinkage properties is, therefore, not efficient. 7.1.4 Effect of GBFS additive on the behaviour of soils under the action of repeated dynamic load. The various measurements of deflections for both pavements (the untreated soil D and the 8% GBFS treated soil D) shown in Tables 4.15 and 6.16 reveal that: i) For any point on the grid, where measurements were taken, the deflection increased with the increase in number of load applications. ii) As the number of total load applications to the pavements increased, the actual deflection per single load applied decreased, indicating stiffness had increased (see Table 7.2). that pavement 244 iii) The maximum values of deflection for the various number of load cycles occurred close to the wheel contact area and particularly under the wheel edge. iv) For any number of load cycles the deflections at almost all measuring points on the grid for the GBFS treated pavement were less than the corresponding deflection for the untreated pavement. The maximum value of deflection for the GBFS treated pavement after 50,000 load cycles was less than the maximum deflection for the untreated pavement GBFS treated pavement). pavement and 8.95mm value of (6.7mm for 8% for untreated This signifies the positive role of GBFS in improving the stiffness of a soil and reducing its compressibility by increasing the density and reducing porosity as was indicated in section 7.1.1. 7.2 Lime-GBFS Additives 7.2.1 Effect of lime-GBFS additives on compaction characteristics of soils It can be observed from Table 6.1 that when 1:1 lime-GBFS additive is added to the soils A, B and C, the maximum dry density of these soils is decreased. dominant effect gravity = 2.35). of the light weight This is due to the of lime (specific As the quantity of GBFS in the additive 245 increases, the maximum dry density of the treated soils increases. This is due to the fact that GBFS is heavier than lime (specific gravity = 2.86) and GBFS tends to improve the particle size distribution of the treated soils and reduce the porosity of the compacted specimens (see Table 7.1 and Appendix B) . Table 6.1 also shows that when lime-GBFS additives are added to soil A and soil B, the OMC of these soils increases. This is more pronounced as the quantity of GBFS in the additive is decreased. This implies that the increase in OMC is dominated by the hydration effect of lime rather than by the quantity of water required to wet the increased surface area of the soil particles. Table 6. lc shows that the OMC of treated soil C increases due to the addition of 1:1 lime-GBFS. This can be attributed to the dominant effect of lime hydration. However, as the quantity of GBFS in the additive increases, the effect of GBFS, again, becomes more dominant than the effect of lime and tends to decrease the OMC of treated soil C due to the fact that GBFS is coarser than this soil (see Table 7.1) and hence it decreases its particle surface area. Lime-GBFS additives, therefore, can be utilised for improving the workability of wet soils (gravel, sand etc.). They also can be used as mechanical stabilisers for improving the grading and increasing the density of soils, 246 which may favourably affect the strength properties of treated soils. 7.2.2 Effect of lime-GBFS additives on the strength properties of soils 7.2.2a Effect on UCS A perusal of Table 6.3 shows that: i) For a given quantity of additive, as GBFS in the additive decreases, the strength at all ages for all treated soils increases. treated soils additive. was The highest strength for all achieved by using 1:1 lime-GBFS This is not consistent with the case of lime-GBFS specimens (section 6.5.3) and implies that lime reacts more readily with soils than with GBFS. sufficient quantity of lime A (initial consumption of lime, ICL) may be consumed in increasing the pH value of soils to a stage (pH = 12.4) at which reactions take place between the lime and the clay minerals and other pozzolans to produce hydrated calcium silicate and calcium aluminate gels. ii) As the curing time increases, the strengths of treated soils increase which implies that pozzolanic reactions take place over a long time. 247 For all additives, the strength of treated soil increases with increasing quantity of additive, up to a peak value,then decreases with the continuous increase in the quantity of additive, similar to that in the case of lime stabilisation. The quantity of additive, at which a peak value of strength occurs, tends to increase additive. with decreasing amount of lime in the This conforms to the previous finding that lime reacts more readily with soil than with GBFS. For all soils tested, the lime-GBFS additives were not able to achieve the highest strength achieved by lime additive. This is more pronounced in the case of soil C which, as a heavy clay, is very suitable to lime stabilisation. This denotes that lime-GBFS additives are more efficient in modifying the strength of non cohesive soils than they are in modifying the strength of cohesive soils. Figure 6.3 shows that the UCS of soils treated with 4% content of 1:1, 1:2 and 1:3 lime-GBFS additives are greater than stabilisation. pozzolan, in those of 2%, 1.3% and 1% lime This signifies the role of GBFS, as a the stabilised soils. strength development of lime-GBFS The effectiveness of this role will be examined further in section 7.2.7. 248 7.2.2b Effect on CBR From Tables 6.11 to 6.13 and Figures 6.11 to 6.13, it can be observed that: i) For all additives, the CBR of all treated soils increases with increasing quantity of additive and/or curing time. ii) For a given quantity of additive, as the amount of GBFS in the additive decreases, the CBR value of all treated soil increases. iii) In the case of soil C, which as a heavy clay is very suitable to lime stabilisation, the lime-GBFS additives were not able to achieve the highest CBR value achieved by lime additive. This, also, is consistent with the findings for UCS in section 7.2.2a. However, the 1:2 lime to GBFS additive, at an additive quantity of 8%, was able to achieve higher CBR values than those achieved by 2.6% lime in the case of soil A and soil B. This implies once more that: a) lime-GBFS additives are more suitable for modifying the strength of non cohesive soils than they are for modifying the strength of cohesive soils. 249 b) GBFS is a pozzolan and has a role in the strength development of lime-GBFS soil stabilisation. The observations described in (i) and (ii) are consistent with the findings for UCS in section 7.2.2a. 7.2.3 Effect of delay in compaction on the strength of lime-GBFS treated soils It can be seen from Table 6.8 that delay in compaction of lime and lime-GBFS treated soils decreases the strength of these mixes. This is more pronounced as the time elapsed since mixing is increased. The results presented in Table 6.8 have also shown that in lime and lime-GBFS stabilisation, the losses in strength due to delay in compaction were not great and almost equal. This implies that the rate of reaction in lime-GBFS stabilisation is relatively slow and somewhat similar to lime stabilisation. respect of Accordingly, the time constraints in compaction, including delays caused by plant breakdown, etc, and the effect of rain are not so critical. These observations are consistent with the findings for lime-RHA additives which are explained in Chapter 5 (section 5.2.3) . 250 7.2.4 Effect of lime-GBFS additives on the shear strength parameters of soils It has been observed, as shown in Table 6.9, that in almost all cases, the shear strength parameters (cohesion and angle of internal friction) of the soil increase with increasing quantity of additive and/or decreasing amount of GBFS in the additive. For a given proportion of lime to GBFS, as the quantity of additive increases, observed in an all cases. increase in the parameters is It can also be seen that the cohesion and angle of internal friction of soil B stabilised with 8% content of 1:1 lime-GBFS were higher than those with 4% lime additive. In the case of soil C, the cohesion and angle of internal friction achieved by 8% content of 1:1 lime-GBFS additive were somewhat similar to those achieved by 4% lime additive. These observations are consistent with the findings for UCS and CBR in section 7.2.2a and 7.2.2b. Table 6.9 also shows that shear strength parameters increase with increasing curing time. This confirms the belief that GBFS is a pozzolan and its reaction with lime takes place over a long time. As shear strength of a soil is determined by its parameters and effective normal stress (ie r = C +rntan 0), it can 251 easily be seen that the above mentioned observations are applicable to the effect of lime-GBFS additives on the shear strength of soils. As previously stated, these observations conform to the findings for CBR and UCS which are, more or less, measures of the combined effects of cohesion and internal friction of a soil. Accordingly, it can be stated that the increase in strength {UCS, CBR and shear strength) due to lime-GBFS stabilisation is caused by the increase in both the angle of internal friction and cohesion of the stabilised soil. The reasons behind this increase were discussed in Chapter 5 (section 5.2.4). 7.2.5 Discussion of the results of the XRD analysis of lime-GBFS stabilised soils A comparison of the XRD chart of lime-GBFS treated Soil A, as shown in Figure 6.19, with the XRD chart of the untreated soil (Figure 4.25) reveals that the peaks pattern in both cases are almost similar with the exception of the presence of Calcite (CaC03) in the treated sample. This was identified by the existence of several peaks at d spacings of 2.285, 2.095, 1.913 and 1.875 A°. The XRD chart of lime-GBFS treated Soil C, as shown in Figure 6.20, has also indicated the presence of Calcite in the treated soil. This can be identified by the peaks shown at d spacings of 3.035, 2.285, 2.095, 1.913 and 1.875 A°. 252 It was also shown that the treated soil retained some details of the original structure of the untreated soil (ie, Quartz) whereas some other details such as Kaolinite disappeared. The XRD charts of lime-GBFS treated Soils A and C have not indicated the existence of any form of calcium silicate hydrate or calcium aluminate hydrate. Possible existence of such compounds could be hindered by the presence of Calcite in the samples. The presence of Calcite could be attributed to the effect of atmospheric carbon dioxide on the thin dispersion of the fine material. The XRD analysis has proved inconclusive in providing information on the nature of the hydration products of the lime-GBFS soil stabilisation. 7.2.6 Discussion of the results of the SEM examination of lime-GBFS stabilised soils The scanning electron micrograph of the fracture surface of the lime-GBFS treated Soil A as shown in Figure 6.17 reveals a rough texture with few cracks and microporosities. This indicates that the surface of the treated soil retained some details of the surface of the untreated soil (see Figure 4.21). However, these cracks and microporosities are smaller in number and size than those shown for untreated soil in Figure 4.21. 253 Figure 6.17 also reveals a considerable crystalline reaction product, presumably calcium silicate hydrate, which can be seen at the bottom left of the micrograph. Few other patches of amorphous reaction products can be seen covering some areas and filling some of the microporosities in the fracture surface. The micrograph of the lime-GBFS treated Soil C as shown in Figure 6.18 amorphous reveals a massive components which and even distribution of are presumably the non crystalline reaction products. The description of the features of both micrographs given in this section are some what subjective. Consequently, speculations on the origin of strength and other properties when based Hence, on this observation the SEM proved identifying the hydration have inconclusive products limited in of validity. comparing lime-GBFS and soil stabilisation. 7.2.7 Effect of lime-GBFS additives on the Atterberg limits and linear shrinkage of soils A perusal of Table 6.5 reveals that: Liquid limit and plastic limit of lime-GBFS treated soils increase with the increase of additive quantity with one 254 notable exception where the very high liquid limit of soil C decreases with the increase in additive quantity. However, the plasticity index and linear shrinkage of all treated soils decrease with the increase in additive quantity. These effects are more pronounced as the amount of GBFS in the lime-GBFS is decreased. These effects could be referred to the combined action of the partial replacement of plastic soil particles with the GBFS particles of, relatively, low plasticity and ion exchange between the lime and the clay minerals of soils. Table 6.5 also shows that liquid limit, plastic limit, plasticity index and linear shrinkage of treated soils after a curing period of 28 days are almost equal to those after a curing period of 7 days. This can be explained by the fact that the reactions responsible for reducing plasticity and shrinkage (ie cation exchange) occur during a short period of time and mostly in the first 7 days of the curing time, and that GBFS does not react with soils as was discussed in section 7.1.2. A perusal of Figures 6.5 and 6.7 reveals that lime-GBFS additives could not attain the results achieved by 4% lime additive. Hence, their use to modify the plasticity and shrinkage of soils could be restricted to a lower level of achievement. However, their limited role in this context 255 (ie to replace 2-3% lime additive in modifying plasticity and shrinkage of soils) could be justified by the amount of lime saving they can achieve. The observations presented in this section are almost identical to the findings for lime-RHA additives as discussed in Chapter 5 (section 5.2.7). 7.2.8 Implications of lime savings Figure 6.3a indicates that the UCS of 2% lime treated soil A can be achieved by 3.6% content of 1:2 lime-GBFS additive (ie, 1.2% lime + 2.4% GBFS). The lime saving is therefore equal to 2-1.2 = 0 . 8 % and the ratio of GBFS required to lime saved is 2.4/0.8 = 3. not economically Therefore 1:2 lime-GBFS additive is feasible to replace the 2% lime stabilisation unless the cost of lime is equal to or greater than 3 times the cost of GBFS. Table 7.3 has been derived in a similar manner utilising Figures 6.3, 6.5 and 6.7 and applying the same calculations for the various values of UCS, shrinkage and plasticity for each case of soil treatment. From Table 7.3, it can be deduced that: 256 i) 1:1 lime-GBFS additive tends to be the most economical additive of all lime-GBFS additives tested. These additives tend to be less economical as the quantity of GBFS in the additive increases. ii) Lime-GBFS additives are more efficient in stabilising non cohesive soils (soil A and soil B) than in stabilising clays. iii) All of the tested lime-GBFS additives are not recommended for replacing 4% lime in stabilising soils. iv) 1:1 lime-GBFS can not be recommended for replacing 2% lime in modifying strength, plasticity and shrinkage of clays (soil C) unless the cost of lime is 6-7 times the cost of GBFS. However, this economic cost ratio tends to decrease as the treated soil tends to be coarser (identical cost ratios for increasing the strength of soil A and soil B are 2.25 and 4.68 respectively). 7.2.9 Effect of lime-GBFS additive on the behaviour of soils under the action of repeated dynamic load The results of the laboratory tests used in this research indicate that lime-GBFS additives, particularly that of proportion 1:1, can be used in soil stabilisation to modify workability, strength, plasticity and shrinkage of soils. 257 To find whether or not the behaviour of these treatments under the action of repeated dynamic loads is consistent with the finding for the various laboratory tests, it was decided to compare the pavements having 2% lime treated soil D and 3% content of 1:1 lime-GBFS treated soil D with the control pavement of untreated soil D. The various measurements of surface deflections of the three pavements, shown in Tables 4.15, 4.16 and 6.15, reveal that: i) For any point on the grid, where measurements were taken, the surface deflection of the three pavements increased with the increase in number of load applications. ii) As the number of total load applications to the pavements increases, the actual deflection per single load applied decreases, indicating that the pavement stiffness has increased ( see Table 7.4.). iii) The maximum deflections for the various number of load cycles occur close to wheel contact area and particularly under the wheel edge (ie, point eH on the grid) for all cases. iv) For any number of load cycles the deflection, at any point on the grid, of the lime-GBFS treated pavement 258 was less than the deflection of the untreated pavement. This indicates that lime-GBFS additive increases the stiffness and reduces the compressibility of soils. The deflection of the lime-GBFS treated pavement after any number of load applications was less than the deflection of the lime treated pavement at all points on the grid. The maximum value of deflection of lime-GBFS treated pavement after 50,000 load cycles was less than the maximum value of deflection of the lime treated pavement (7.2mm for 2% lime treated pavement and 6.0mm for 3% content of 1:1 lime-GBFS treated pavement). This signifies the positive role of GBFS, as a pozzolan in lime-GBFS additive, for improving the stiffness of a soil and reducing its compressibility and is consistent with the findings for strength in sections 7.2.2 and 7.2.4. Perusal of Figures 4.14, 4.15 and 6.15 reveals that, for all pavements, there were downward movements of all points on the grid where measurements were taken, and the permanent deformations of the three pavements were caused by the densification of the pavements rather than by any shear failure of these pavements (see also Figures 4.20, 4.21 and 6.18). 259 vii) A visual assessment of the surface of all pavements showed that no fatigue cracks or shrinkage cracks were developed and the pavements were intact and sound at the conclusion of the test. In general the observations derived from the results of the repeated dynamic load test have demonstrated that 1:1 lime-GBFS additive is effective and efficient in improving the behaviour of soils under the action of repeated loads. The observations desribed in (i) to (vii) are almost identical to the findings for lime-RHA additives as shown in Chapter 5 (section 5.2.9). 7.3 Cement-GBFS Additives 7.3.1 Effect of various cement-GBFS additives on compaction characteristics A perusal of Table 6.2 reveals that when cement-GBFS additives are added to soils A, B and C, the maximum dry density and the optimum moisture content of these soils increase. pronounced decreased. The increase in OMC of the treated soils is more as the This quantity implies of GBFS in the that the increase dominated by the hydration reactions of cement. additive in OMC is is In the case 260 of soils A and B, additional water is required for wetting the increased surface area of the soil particles due to the addition of GBFS (GBFS is finer than both soils, as shown in Table 7.1). The increase in maximum dry densities of all treated soils was mainly due to the partial replacement of soil with heavier cement-GBFS additives (specific gravity for 1:1 to 1:4 proportions are 3.0, 2.95, 2.93 and 2.916 respectively. The increase in dry densities could also be influenced by the improvement in grading and the reduction in porosity of all treated additives. soils due to the additon of cement-GBFS The porosity values were calculated by a method similar to that specified in section 5.1.1 and 5.2.1 and are presented in Appendix B. Cement GBFS additives, therefore, can be used to enhance the workability of wet soils. They can also be used for improving the grading, reducing porosity and increasing the density of soils which may affect favourably the strength properties of these soils. 7.3.2 Effect of cement GBFS additives on the strength properties of soils 7.3.2a Effect on UCS It has been observed, as shown from Table 6.4, that: 261 For a given quantity of additive, as cement content in the additive increases the strength, of treated soils, increases consistent with the case of cement-GBFS specimens (section 6.5.3). This implies that the strength development is dominated by the hydration reactions of cement rather than by the pozzolanic V reactions of the GBFS. For all additives there is continuous increase in strength of treated soils, with increasing quantity of additive. No peak value of strength was observed. This is consistent with the findings stated above. As curing time increases the strength of treated soils increases. The rates of strength development of soils (A and B) treated with cement-GBFS additives are slightly slower than those of cement treated soils. Rates of strength development, as ratios of 28 days strength to 90 days strength, for various treated soils are derived from Table 6.4 and presented in Table 7.5. From this Table, it can be seen that GBFS is acting somewhat as a weak retarder and hence may not have a significant effect on the workability of cement-GBFS soil stabilisation. This effect will be further examined in the later discussion on the effect of delay in compaction on strength of treated soils (section 7.3.3) . 262 iv) From Figure 6.4c, for example, it can be seen that the UCS of soil C treated with 4% content of 1:1, 1:2 and El:3 cement-GBFS additives are greater than those of 2% content of 1:3 and 1% cement treatment of soil C. This indicates that GBFS has a role in strength development of cement-GBFS soil stabilisation. The effectiveness of this role is investigated in section 7.3.7. 7.3.2b Effect on CBR The results presented in Table 6.11 to 6.13 and Figures 6.11 to 6.13 show that: i) For a given quantity of additive, as the amount of GBFS in the additive decreases, the CBR value of all treated soil increases. ii) For all additives, the CBR of treated soils increases with increasing quantity of additive and no peak value is observed. iii) As the curing time increases, the CBR of all treated soil increases. iv) In the case of soil C, which as an organic clay is not suitable for cement stabilisation, the 1:1 cement-GBFS additive, at an additive quantity of 8%, was able to 263 achieve a higher CBR value than that achieved by 4% cement treatment (see Figure 6.13). This clearly indicates that cement can be partially replaced by GBFS and that GBFS has a role in the strength development of cement-GBFS stabilisation of organic clays. The effectiveness of this role in the stabilisaton of soil A and soil B and the implication of cement saving in these cases cannot be derived from the CBR values as some of these values are greater than 100 and considered meaningless in accordance with the discussion of the appropriateness of the test in section 3.4.4. The observations described in (i) to (iii) are consistent with the findings for UCS in section 7.3.2a. 7.3.3 Effect of delay in compaction on the strength of cement-GBFS treated soils The results presented in Table 6.7 show that a loss in strength occurs if the compaction of cement or cement-GBFS treated soil is delayed. The loss in strength is more pronounced as the time elapsed since mixing is increased. The delay in compaction of cement treated soil A was critical, resulting in 30% to 70% loss of strength due to 2-6 hours delay in compaction. However, this loss in 264 strength was additives. reduced slightly by using cement-GBFS The decrease in the loss of strength is more pronounced as the amount of GBFS in the additive is increased. This could be attributed to the fact that GBFS acts as a weak retarder in slowing the rate of strength development 7.3.2a). of cement-GBFS treated soils (see section The loss in strength due to delay in compaction of cement-GBFS treated soil is 16% - 30% less than that of cement treated soil. respect of Accordingly, the time constraints in compaction, including delays caused by plant breakdown, etc, and the effects of rain are less critical. These observations are consistent with the findings for lime-RHA, cement-RHA and lime-GBFS additives as described in sections 5.2.3, 5.3.3 and 7.2.3. 7.3.4 Effect of cement-GBFS on the shear strength parameters of soils It has been observed, as shown in Table 6.10, that the shear strength parameters friction) of quantity of the (cohesion treated soil and increase additive, curing time and/or amount of cement in the additive. stated that angle the increase in of with internal increasing increasing the Accordingly, it can be strength of cement-GBFS stabilised soil is influenced by the increase in both its cohesion and angle of internal friction. 265 This is consistent with the findings for lime-RHA, cement-RHA and lime-GBFS additives as discussed in Chapter 5 and 7 (sections 5.2.4, 5.3.4 and 7.2.4). 7.3.5 Effect of cement-GBFS additives on the Atterberg limits and linear shrinkage of soils It can be observed, as shown from Table 6.6, that: i) Liquid limit and plastic limit of cement GBFS treated soils increase with the increase of additive quantity with one notable exception where the very high liquid limit of soil C decreases with increase of additive quantity. ii) The plasticity index and linear shrinkage of all treated soils decrease with the increase in additive quantity. amount of These effects are more pronounced as the GBFS in the cement-GBFS additive is decreased. iii) It can also be seen from Table 6.6 that liquid limit, plastic limit and plasticity index of treated soils (A, B and C) after a curing period of 28 days vary slightly from those after a curing period of 7 days. 266 iv) The linear shrinkage of treated soils A and B tends to increase slightly with the increase in curing time due to the prolonged hydraulic reactions of GBFS stimulated by the effect of cement. An inspection of Figures 6.6 and 6.8 reveals that, with respect to linear shrinkage and plasticity index, cement-GBFS cannot attain the results achieved by 4% cement additive (except for the linear shrinkage of treated soil C) . Hence their use to modify the plasticity and shrinkage of soils could be restricted to this level of cement replacement. However, their limited role has to be justified by the amont of cement saving they can achieve. The observations described in (i, ii and iii) are consistent with the findings for lime-GBFS additives as discussed in section 7.2.6. 7.3.6 Implications of cement saving Figure 6.4c indicates that the UCS of 2% cement treated soil C can be achieved by 3.1% content of additive (ie, 1.55% cement + 1.55% GBFS). 1:1 cement-GBFS The cement saving is therefore, equal to 2-1.55 = 0.45% and the ratio of GBFS required to cement saved is 1.55/0.45 = 3.44. Therefore 1:1 cement-GBFS additive is not economically feasible to replace the 2% cement additive in stabilising soil C unless the total cost of cement is equal to or greater than 3.44 times 267 the total cost of GBFS (ie, material, mixing and separate storage costs). Table 7.6 has been derived in a similar manner, utilising Figures 6.4, 6.6 and 6.8 and applying the same calculations for the various values of strength, plasticity index and linear shrinkage for each case of soil treatment. From Table 7.6, it can be deduced that: i) 1:1 cement-GBFS is the most economical additive of all cement-GBFS additives used. These additive tend to be less economical as the quantity of GBFS in the additive increases. ii) 1:2, 1:3 and 1:4 cement-GBFS additives are not efficient and can not be recommended to be used in soil stabilisation. iii) 1:1 cement-GBFS additive is not efficient in modifying plasticity and shrinkage properties of low cohesion soils nor is it efficient in modifying the strength of crushed rocks (gravel-sand-silt, soils). iv) 1:1 cement-GBFS additive can be recommended for replacing 2-4% cement additive in modifying the strength, plasticity and shrinkage of clays provided 268 that the cost of cement is equal to, or greater than, 2-4 times the cost of GBFS. v) 1:1 cement-GBFS additive also can be recommended for replacing 2% cement additive in modifying the strength of sand-silt soils provided that the cost of cement is equal to or greater than five times the cost of GBFS. 7.3.7 Effect of cement-GBFS on the behaviour of soils under the action of repeated dynamic load In section 7.3.2a and 7.3.2b it was found that GBFS acted as a pozzolan and cement-GBFS has soil a role in strength stabilisation. development To inspect of the effectiveness of this role in improving the behaviour of soils under the action of repeated dynamic loads, it was decided to compare the pavements containing 1.5% cement treated soil D and 3% content of 1:1 cement-GBFS treated soil D with the control pavement of untreated soil D. The various measurements of surface deflection for the three pavements, shown in Tables 4.15, 4.18 and 6.14 reveal that: i) For any point on the grid, where measurements were taken, the surface deflection in all three pavements increased with applications. the increase in number of load 269 ii) As the number of total load applications to the pavements decreased, the actual deflection per single load applied decreased, indicating that the stiffness had increased (see Table 7.7). iii) The maximum deflection for the various number of load cycles occurred close to wheel contact area (ie, point eH and dH on the grid). iv) For any number of load cycles, the values of deflection, at any point on the grid, of the cement-GBFS treated pavement were less than the values of deflection indicates that of the untreated cement-GBFS pavement. additive This increases the stiffness and reduces the compressibility of soils. v) The maximum deflection of the 3% cement-GBFS treated pavement after 250,000 load cycles was equal to 2.3mm. This was less than the maximum deflection of the 1.5% cement treated pavement after 50000 load cycles, which was equal to 2.96mm. This signifies the role of GBFS in cement-GBFS additive in increasing the density and stiffness and reducing the compressibility of soils. vi) Figure 6.16 reveals that most of the points on the 3% 1:1 cement-GBFS treated pavement, where measurements were taken, exhibited a downward movement and the 270 deflection was caused by the densification pavement rather than by any shear failure. consistent with the findings for all of the This is treated and untreated pavements as discussed in sections 5.2.9 and 7.2.9. vii) A visual assessment of the surface of the 3% content of 1:1 cement-GBFS treated pavement showed that no fatigue cracks or shrinkage cracks were developed and the pavement was intact and sound at the conclusion of the test. In general, the observations derived from the results of the repeated dynamic load test have demonstrated that 1:1 cement-GBFS additive is an effective and efficient stabiliser in improving the behaviour of soil under the action of repeated dynamic loads. The observations described in this section are almost similar to the findings of lime-GBFS additives as described in section 7.2.9. 271 Table 7.1 soil Effect of G B F S additive on the grading of soils sieve size Grading of soil Grading of GBFS % passing % passing Grading of soil + 8% GBFS % passing Grading of max density curve % passing A 19mm 9.5mm 4.75mm 2.36mm 425pm 75pm 13.5pm 100 73 36 22 15 8 4 100 100 100 100 50 5 2 100 75 41 28 17 7.5 3.5 100 70 50 35 15 6 3 B 4.75mm 2.36mm 425pm 75pm 13.5^m 100 85 43 24 17 100 100 50 5 2 100 86 43.5 22.5 15.5 100 90 30 13 5 2.36mm 425pm 75pm 13.5pm 100 95 71 53 100 50 5 2 100 91 66 49 100 42 18 8 C 272 Table 7.2 Deflection per load as number of load increases at point of maximum deflection on the grid (ie point eH) of the 8 % G B F S treated pavement Progressive total of loads applied N o of loads applied Deflection due Average deflection loads applied (mm) due to one load application (mm) 50 500 5,000 50,000 50 450 4,500 45,000 4.35 5.70-4.35 6.20-5.70 6.70-6.20 .087 0.003 1.11 x10-4 1.11 X10-5 273 Table 7.3 Ratio of G B F S required to lime saved or identical economic cost ratio of lime to G B F S Level of achievement Soil lime.GBFS 1:1 lime.GBFS 1:2 lime:GBFS 1:3 lime:GBFS 1:4 2.25 4.68 3 NA NA NA NA NA C 6.6 6.6 13.69 U C S of 4 % lime treated A soil B NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA C NA 6.7 4.0 NA 50 7.55 Plasticity index of 4 % A NA NA NA NA lime treated soil B NA NA NA NA C NA NA NA Linear shrinkage of 2% A B lime treated soil NA NA NA NA 30 NA 5.69 6.86 9.0 Linear shrinkage of 4 % A NA NA NA NA B NA NA NA NA C NA NA NA U C S of 2 % lime treated A soil B C Plasticity index of 2 % lime treated soil A B C lime treated soil —NA Additive is not tested N o lime could be saved NA NA 274 Table 7.4a Deflection per load as number of load applications increases at point eH on the grid of the pavement containing 3 % lime-GBFS treated soil D Progressive total of load applications No. of load applications Deflection due to load applications (mm) 50 450 4,500 45,000 50 500 5,000 50,000 Table 7.4b 3.89 4.53 - 3.89 4.99 - 4.53 6.00 - 4.99 No. of load applications Deflection due to load applications (mm) 50 500 5,000 50,000 50 450 4,500 45,000 5.95 6.90 - 5.95 7.12-6.90 7.20-7.12 Average deflection due to one load application (mm) 0.119 .002 4.88x10-5 1.77x10-6 Deflection per load as number of load applications increases at point eH on the grid of the untreated pavement Progressive total of load applications No. of load applications Deflection due to load applications (mm) 50 500 5,000 50,000 .0778 .0014 .0001 2.24x10-5 Deflection per load as number of load applications increases at point eH on the grid of the pavement containing 2 % lime treated soil D Progressive total of load applications Table 7.4c Average deflection due to one load application (mm) 50 450 4,500 45,000 3.12 4.15-3.12 6.97 - 4.25 8.95 - 6.97 Average deflection due to one load application (mm) .062 .0025 .0006 .0004 275 Table 7.5 Ratio of U C S at 28 days to U C S at 90 days for soils treated with 8 % content of cement and cement-GBFS additives Additives Cement CementGBFS 1:1 CementGBFS 1:2 CementGBFS 1:3 .93 .89 .857 .85 .784 .73 .835 .68 .90 .83 .84 .92 Soils A B C 276 Table 7.6 Ratio of G B F S required to cement saved or identical economic cost ratio of cement to G B F S Level of achievement Soil Cement.GBFS Cement.GBFS Cement:GBFS Cement.GBFS 1:1 1:2 1:3 1:4 U C S of 2 % cement treated soil A B C 19 4.64 3.44 NA NA 3.42 NA NA 1.41 NA NA U C S of 4 % cement treated soil A B C NA NA 1.58 NA NA NA NA NA NA NA NA Plasticity index of 2 % cement treated soil A B C 5.20 NA 4.12 9.79 NA 21.58 6.07 NA 21.95 7.92 NA Plasticity index of 4 % cement treated soil A B C NA NA 1.98 NA NA NA NA NA NA NA NA Linear shrinkage of 2 % A cement treated soil B C NA NA 3.15 NA NA 20.27 30 NA 9.0 NA NA Linear shrinkage of 4 % A cement treated soil B C NA NA 2.27 NA NA NA NA NA NA NA NA NA — N o cement saving could occur Additive is not tested 277 Table 7.7a Deflection per load as number of load applications increases at point eH on the grid of the untreated pavement Progressive total of load applications 50 500 5,000 50,000 Table 7.7b 50 500 5,000 50,000 Average deflection due to one load application ( m m ) 50 450 4,500 45,000 3.12 4.25-3.12 6.97 - 4.25 8.95 - 6.97 .062 .0025 .0006 .0004 No. of load applications Deflection due to load applications (mm) Average deflection due to one load application ( m m ) 50 450 4,500 45,000 1.30 2.23 -1.30 2.53 - 2.23 2.96 - 2.53 0.26 .002 6.66x10-5 9.55x10-6 Deflection per load as number of load applications increases at point d H on the grid of the pavement containing 3 % content of 1:1 cementG B F S treated soil D Progressive total of load applications 5,000 50,000 250,000 Deflection due to load applications (mm) Deflection per load as number of load applications increases at point eH on the grid of the pavement containing 1.5% cement treated soil D Progressive total of load applications Table 7.7c No. of load applications No. of load applications Deflection due to load applications (mm) Average deflection due to one load application (mm) 5,000 45,000 200,000 1.70 1.87-1.7 2.3 -1.87 3.4x10-4 3.77x10-6 2.15x10-6 278 Chapter VIII DISCUSSION OF ECONOMIC FEASIBILITY OF THE APPLICATIONS OF RHA AND GBFS TO SOIL STABILISATION 8.1 Introduction Chapters 4 to 7 report the studies of a number of additives, involving RHA and GBFS, for soil stabilisation. Technical performance details have been specified where possible, and indications of the type of situation in which these additives might or might not be appropriate are presented. However, it must be emphasized that an Engineer's choice between alternative additives cannot be made solely on the basis of technical considerations. RHA and GBFS additives may suffer unreasonably in competition with lime and cement additives because consumers are usually geared to the preferred use of primary materials. This preference for primary supplies is not due to the inferiority of by-products (ie, RHA and GBFS) but could result from the prejudice, habit and the maintenance of status of industry ingrained in our materials use practice. The use of RHA and GBFS additives in soil stabilisation, therefore, may not be justified unless RHA and GBFS are available in large quantities at a particular location at low competitive cost. This cost may constitute the major 279 factor in deciding which of the technically and socially acceptable alternatives should be used. Section 8.2 to 8.10 present the comparative costs of RHA, GBFS, lime and cement used in this research and investigate the economic feasibility of using RHA and GBFS additives in soil stabilisation in NSW. 8.2 Availability Of RHA The major rice growing area is primarily centred in the Riverina area, where the Ricegrowers Co-Operative Limited produces an annual crop of close to one million tonnes of paddy rice, resulting in 160,000 tonnes of rice hulls. Smaller quantities of rice hulls, of the order of 6,000 tonnes/year Burdekin and delta, 1,000 tonnes/year, Queensland and the are produced Northern in the Territory, respectively. Currently, approximately 20,000 tonnes/year of rice hulls from the Riverina area are burnt in controlled combustion furnaces at Griffith producing around 1,000 tonnes/annum of low carbon (grey ash) and 3,000 tonnes/annum of high carbon (black ash) rice hull ash (no controlled burning of the Queensland and Northern Territory rice hulls is currently in operation). The ashes are produced under strict quality control to comply with exacting requirements of the steel 280 and refractory industries which comprise the major market. As a result of this strict quality control, the ashes currently attract high revenue. At present 60% of the rice hulls from the Riverina are disposed of by field burning. It is planned (52) to install incineration or power generation facilities at all mills (Echuca, Deniliquin, Griffith) within Coleambally, five years, which Leeton, should Yenda and ensure that, progressively, up to 30,000 tonnes/annum of low carbon ash will become available. This ash, which would normally be used as landfill, as a soil ameliorant for sandy soils or as a substitute for lime in soils, should become available locally at low cost. Currently, the grey ash is sold at $250/tonne whereas the black ash which was used in this research is sold at $380/tonne F.O.T. Ex Biocon, Griffith. The price of black ash, therefore, is approximately equal 2.5 times the price of lime or cement at any place in NSW, particularly at Finley RTA Works Office, NSW (the closest RTA Works Office to Griffith) where lime and cement are currently delivered in bags and bulk at $130-150/tonne. 281 8.3 Economic feasibility of RHA as a single additive to Soils It was stated in section 5.1.2a and 5.1.2b that RHA, technically, is not suitable to impart significant strength to soils. However, it was also stated in section 5.1.3 that RHA cannot be recommended to be used in modifying the plasticity and shrinkage properties of soils unless the cost of lime or cement is 5-6 times the cost of RHA. This condition could not be met as shown in the previous section which indicates beyond any question that RHA used in this research cannot, currently, be recommended to be used in replacement of lime or cement in soil stabilisation in NSW. 8.4 Economic feasibility of Lime-RHA additives to Soils It has been shown in Section 5.2.8 that 1:1 lime-RHA additive tends to be the most economical additive of all lime-RHA additives tested in this research and that 1:1 lime-RHA additive is not recommended to be used in improving the strength of soils unless the price of lime is at least 3 times the price of RHA. It was also shown in section 5.2.7 that 1:1 lime-RHA additive can be recommended to be used in modifying the plasticity and shrinkage properties of soils provided that the cost of lime is at least 5-6 times the cost of RHA. 282 Section 8.2 clearly shows that both conditions, which enable 1:1 lime-RHA to be economically implemented in increasing the strength and modifying the stability of soils, are not met. plasticity and volume Consequently, it can be determined that 1:1 lime-RHA additive and subsequently all other lime-RHA additives are not, at present, economically feasible to be used in soil stabilisation in NSW. 8.5 Economic feasibility of Cement-RHA additives to Soil Section 5.3.7 has indicated that 1:1 cement-RHA additive tends to be the most economical additive of all cement-RHA additives tested additives can be in this research recommended for and that cement-RHA replacing 2% cement additive for increasing the strength of low cohesion soils provided that the cost of cement is equal to, or greater than, 2.4 times the cost of RHA. It was also shown in section 5.3.7 that the cost of cement should equal at least 4 times the cost of RHA to enable cement-RHA additive to be implemented, economically, in modifying the plasticity and shrinkage properties of soils or achieving a strength comparable to that achieved with 4% cement additive. The fact that the cost of cement is not 4 times the cost of RHA but rather 2.5 times less than the cost of RHA dictates 283 that cement-RHA additives cannot, at present, be recommended to be used in soil stabilisation in NSW. 8.6 Summary The current high cost of RHA in NSW has rendered this material unsuitable to be used as a single additive to soils or in combination stabilisation. with lime or cement in the soil However, Biocon is currently investigating larger furnaces that will produce grey ash at rate of up to 3 tonnes per hour or 15000 tonnes per annum. It is assumed that the cost of this grey ash will be as low as $50/tonne bulk ex. rice mill. This assumption suggests a role for grey ash in soil stabilisation particularly if it proved, after testing, to be a better soil stabiliser than black ash. 8.7 Availability of GBFS Iron and steel making has been a part of Australia's history and development since the first established at Mittagong, NSW in 1848. blast furnace was The scope and thrust of the slag industry has been significantly changed in the late 1980's with the construction of new granulation facilities at No. 2 and 5 Furnaces, Port Kembla and No.3 Furnace, Newcastle. These new facilities have taken the 284 process from the basic form which is still currently in use at No.4 Furnace, Port Kembla, which has minimal controls on flow rates, pressure, temperature, automatic dewatering and automatic sampling (55). The three steel production centres at Port Kembla, Newcastle and Whyalla generated more than 3.2 million tonnes of total iron and steel making slag in 1989 (54) of which Port Kembla works, as the largest steel making centre in Australia (4.0 million tonnes per annum) produced more than 420,000 tonnes of GBFS. This GBFS is currently marketed by Australian Steel Mill Services Pty Ltd, Port Kembla, NSW, and sold at $6.00 to $10.00 per tonne depending on the quantity of material ordered. This price is F.O.T. Ex Port Kembla and is approximately /14 times the cost of lime or cement ($130 $140 per tonne) at any place within a distance of 300km from Port Kembla. 8.8 Economic feasibility of GBFS as single additive to Soils Section 7.1.2a and section 7.1.3 indicate that GBFS as a single additive to soils has a remarkable effect on strength, plasticity and shrinkage properties of cohesive 285 soils. However, these sections also show that the effects of GBFS on the properties of soils are inferior to those occurring due to the addition of lime or cement additives to soils and that GBFS as a single additive to soils is not an efficient stabiliser unless the cost of lime or cement is between 6-9 times the cost of GBFS. This condition is met as is clearly shown in section 8.7. Hence GBFS as single additive to soils can be recommended for use in modifying strength, plasticity and shrinkage properties of cohesive soils in locations where the cost of GBFS does not exceed 140/6 = $23.33 (ie where haulage rate does not exceed 23.33 - 10.00 = $13.33 (per tonne). If x km is the haulage distance in excess of 40kms, then the haulage rate can be calculated by using the equation provided by RTA NSW: Haulage rate = 9.32 + 0.2612 x and therefore the haulage distance in excess of 40kms will equal to 15.35km. This indicates that GBFS as a single additive to soils can be recommended to be used in modifying strength, plasticity and shrinkage properties of cohesive soils in locations within a distance of 55kms from Port Kembla or similar GBFS production plant. 286 8.9 Economic feasibility of Lime-GBFS additives to Soils It has been shown in section 7.2.8 that 1:1 lime-GBFS additive tends to be the most economical additive of all lime-GBFS additives investigated in this research. also been recommended shown that 1:1 for replacing lime-GBFS additive 2% lime additive It has can be in modifying strength, plasticity and shrinkage of clays (soils) provided that the cost of lime is 6-7 times the cost of GBFS. This condition is satisfied at the place of production in Port Kembla and can also be met in any location within a distance of 55km from Port Kembla or similar production plant as was shown in section 8.8. Section 7.2.8 has also indicated that 1:1 lime-GBFS additive can be used for replacing 2% lime additive in increasing the strength of low cohesion soils provided that the cost of lime is 4.68 and 2.25 times the cost of GBFS depending on the nature of stabilised soils (4.68 times for sand-silt soils and 2.25 times for gravel-sand soils). In a way similar to that specified in section 8.8, it can be proved that these requirements can be satisfied in locations where hauling distance from Port Kembla or any other similar 287 GBFS production plant does not exceed 80-200km depending on nature of soils (80km for sand-silt soils and 200km for gravel-sand soils). 8.10 Economic feasibility of Cement-GBFS additives to Soils It has been shown in section 7.3.7 that 1:1 cement-GBFS additive is the most economical additive of all cement-GBFS additives used in this investigation. It has also been shown that 1:1 cement-GBFS additive can be recommended for replacing 2-4% cement additive in modifying strength, plasticity and shrinkage properties of clays provided that the cost of cement is equal to or greater than 2-4 times the cost of GBFS. It was also shown in section 7.3.7 that 1:1 cement-GBFS additives can be recommended for replacing 2% cement additive in modifying the strength of sand-silt soils provided that the cost of cement is equal to or greater than 4.65 times that the cost of GBFS. In a way similar to that specified in section 8.8, it can be proved that the economic requirements for the above stated applications can be satisfied and 1:1 cement-GBFS additive is economically feasible to be used in some soil stabilisation applications where hauling distance, of GBFS, does not exceed 80-230km depending on nature of soils and 288 purpose of stabilisation (230km for increasing strength and modifying plasticity and shrinkage of clays and 80km for increasing strength of sand-silt soils). 289 Chapter IX RECOMMENDED DESIGN PROCEDURES 9.1 Introduction The design of lime-pozzolan and cement-pozzolan additive stabilisation, as with other types of soil stabilisation, is largely a matter of selecting and proportioning materials to obtain the desired properties in the finished construction. The overall objective for the additive soil stabilisation is to determine an economical blend of soil and additive that yeilds a mix having sufficient workability, strength, durability and volume stability. When stabilising with cement or lime, the amount of lime or cement required obviously depends on the objectives of stabilisation and properties required. Decisions as to whether it would be advantageous to use RHA and GBFS, as single additives or in combination with lime or cement, must be taken with economy in mind. Since a given objective, such as a specified plasticity index, can be achieved by a variety of additives, the composition of the preferred mix may be chosen because of its economy. 290 Chapters 4 to 8 examined, technically and economically, the best ratios of lime or cement to RHA and GBFS produced in NSW. They also determined the amount of additives required to be added to four selected soils to obtain certain desired properties. Soil properties vary from point to point. The properties of RHA and GBFS also vary according indicated in section 4.4 and 6.4. that proportions and amounts of to many factors as These variations imply additives used in this investigation may not be appropriate to be implemented in every soil stabilisation work. This dictates that each individual problem must be analysed on its own merits before the design can be accomplished. The problem of choosing the proper additive may cause an inexperienced individual to become confused by the many alternatives available for use. For this reason, the following design procedures are suggested to be carried out before an attempt is made to choose an additive. 9.2 Mix design procedures of Lime-RHA Soil stabilisation The essential elements of the mix design procedures of lime-RHA soil stabilisation are listed below: 291 i) Define the objective of treatment and determine a specific value of the desired property (ie, CBR, UCS, Ip, etc.) using job specifications, pavement design or structural analysis. ii) Determine the minimum quantity of lime which achieves the desired specific value of soil property. A plot of lime content versus strength or any other desired property for three to four lime contents should be sufficient to enable a reasonable deduction of this minimum quantity of lime (see Figure 9.1a). iii) Plot this minimum quantity of lime as point M on the abscissa of Figure 9.1b. If there is any additional cost in involving RHA in the process of soil stabilisation (ie, additional equipment, men, etc.) this cost should be converted to an equivalent lime quantity, deduction from point M giving point N on the abscissa. iv) From point N draw a straight line of actual cost ratio, the slope of which corresponds to the ratio of cost of lime to the cost of RHA delivered to the site. 292 v) Determine the optimum ratio of lime to RHA by testing the UCS of lime-RHA pastes with at least three different proportions. The ratios of lime to RHA of 1:1, 1:2 and 1:3 are usually sufficient to enable an optimum ratio to be determined. vi) Consider the optimum ratio also to be the best economic ratio if RHA is needed to, significantly, improve soil. the particle size distribution of the Otherwise, the mix of best economic ratio can be considered as that mix which has a slightly higher lime content than that of the mix of optimum ratio. vii) From point 0 draw two straight lines representing the optimum ratio and the best economic ratio of lime to RHA. viii) Points above the line of actual cost ratio indicate the uneconomical additives. Hence the feasible quantities of RHA (as single additive to soils) are limited to the range indicated on the ordinate below point D, from which selection may be made by testing the specified property. The feasible lime-RHA mixtures are also limited to a fairly narrow range (ie, the triangular area 293 bounded by the lines of optimum ratio, best economic ratio and the actual cost ratio) from which selection may be made by testing directly the specified property. 9.3 Mix design procedures for Lime-GBFS, Cement-GBFS and Cement-RHA Soil stabilisation The design procedures for lime-GBFS, cement-GBFS and cement-RHA soil stabilisation are similar to those of lime-RHA specified in section 9.2. However, it must be emphasised that no optimum ratio of cement to GBFS and RHA can be determined. The ratio of 1:1 can be reasonably considered as the best economic ratio of these mixes. 294 FIG.9.1 - DETERMINATION OF THE COMPOSITION OF THE PREFERRED MIX IN A LIME-RHA SOIL STABILISATION >i +J u Specific value of desired property of soil CU o u a. o cn FIG.9.la TS CU U •rH CO CU Q c •H 99- 4% 6% 8% Lime additive (% of total dry weight) •rH CU >1 TJ (0 FIG.9.lb o -p o dP CU > •H +J •H TJ TJ rtJ < nc os 2% 4% 6% 8% Lime additive (% total dry weight) 295 Chapter X CONCLUSIONS Based on the preceeding experimental and economical investigations, the following conclusions have been drawn: 10.1 Conclusions concerning RHA as a single additive to Soils RHA improves the workability of wet soils. It increases the optimum moisture content and decreases the maximum dry density of these soils. RHA does not react chemically with soils or affect favourably behaviour their under unconfined the action compressive of repeated strength dynamic and loads. However, RHA tends to decrease the CBR of soils. RHA increases the liquid limit and plastic limit of soils. However, the very high liquid limit of heavy clays decreases due to the addition of RHA to these clays. RHA improves the volume stability of soils by decreasing their plasticity index and linear shrinkage. However, these decreases in plasticity and shrinkage are not comparable to those which occur by the addition of lime or cement to soils. 296 RHA can be recommended for replacing lime or cement in modifying the plasticity and shrinkage properties of soils provided that the cost of lime or cement is at least 5-6 times the cost of RHA. currently 2.5 times The cost of RHA produced in NSW is the cost of lime or cement and therefore, RHA cannot be recommended for replacing lime or cement in soil stabilisation in NSW unless significant decrease in cost of RHA can be achieved. 10.2 Conclusions concerning Lime-RHA additives Lime-RHA additives improve the workability of wet soils. They increase the optimum moisture content and decrease the maximum dry pronounced density as the of soils. quantity of These RHA in effects the are more additive is increased. 1:2 lime-RHA ratio is the optimum ratio associated with the highest strength of lime-RHA pastes. However, lime reacts more readily with soils than with RHA and hence the highest strength of all lime-RHA treated soils has been achieved by 1:1 lime-RHA additive. Lime-RHA additives increase the CBR, unconfined compressive strength and shear strength of soils. This is more 297 pronounced as either the curing time, the quantity of lime in the additive or the quantity of additive is increased. However, the unconfined compressive strength of treated soils increases with increasing quantity of additive, up to a peak value, then decreases with the continuous increase of the quantity of additive. The quantity of additive at which a peak value of unconfined compressive strength occurs, tends to increase with increasing amount of RHA in the additive. The increase in unconfined compressive strength, CBR and shear strength of lime-RHA soil stabilisation is caused by the increase in both the internal friction and cohesion of the stabilised soils. RHA acts as a pozzolan and has a role in strength development of lime-RHA soil stabilisation. However, the optimum increase in strength (CBR and unconfined compressive strength) achieved by lime-RHA additives is not comparable to the maximum increase in strength which occurs by the addition of lime to soils. Delay in compaction of lime and lime-RHA stabilised soils decreases the strength of these mixes. This is more pronounced as the time elapsed since mixing is increased. The rate of reaction in lime-RHA soil stabilisation is relatively slow and somewhat similar to lime stabilisation. The losses in strength of lime and lime-RHA stabilised soils 298 due to delay in compaction are, consequently, low and almost similar. Accordingly, the time constraints in respect of compaction are not so critical. Lime-RHA additives improve the volume stability of soils. They decrease the plasticity index and linear shrinkage and increase plastic These effects limit and liquid limit of these soils. are more pronounced as the quantity of additive and/or the amount of lime in the additive are increased. clays However, the very high liquid limit of heavy decreases with the increase in additive quantity and/or the amount of lime in the additive. Lime-RHA additives are more efficient for stabilising low cohesion soils than for stabilising clays. more efficient for increasing the They are also strength than for modifying the plasticity and shrinkage properties of soils. 1:1 lime-RHA additive tends to be the most economical additive of all lime-RHA additives used. It is an effective and efficient additive for improving the behaviour of soils under the action of repeated dynamic loads. 1:1 lime-RHA additive can be recommended for increasing the strength as well as for modifying the plasticity and shrinkage of soils, provided that the cost of lime is 3 times (for increasing the strength) and 5-6 times (for modifying the plasticity 299 and shrinkage) the cost conditions, currently, of RHA are not met respectively. These in NSW and lime-RHA additives are not economically feasible at this time for soil stabilisation in NSW. 10.3 Conclusions concerning Cement-RHA additives Cement-RHA additives improve the workability of wet soils. They increase the optimum moisture content and decrease the maximum dry pronounced density as the of soils. quantity of These RHA effects in the are more additive is increased. There is no optimum ratio of cement to RHA in cement-RHA pastes. The strength of these pastes increases with the increase of quantity of cement in the mix. Cement-RHA additives increase the CBR, Unconfined compressive strength and shear strength of soils. This is more pronounced as either the curing time, the quantity of cement in the increased. additive or the quantity of additive is The increase in unconfined compressive strength, CBR and shear strength of cement-RHA soil stabilisation is caused by the increase in both the internal friction and cohesion of the stabilised soils. 300 RHA as a pozzolan has a role in strength development of cement-RHA retarder soil in stabilisation. slowing down However, the strength it acts as a development and favourably affects the workability of these mixes. Delay in compaction of cement and cement-RHA stabilised soils decreases the strength of these mixes. The loss in strength is more pronounced as the time elapsed since mixing is increased. The loss in strength, due to delay in compaction, of cement-RHA stabilised soils is significantly less than that of cement stabilised soils. the amount of RHA in the This is more pronounced as additive is increased. Accordingly, the time constraints in respect of compaction of cement-RHA stabilised soils are not highly critical. Cement-RHA additives improve the volume stability of soils. They decrease the plasticity index and linear shrinkage and increase the plastic limit and liquid limit of these soils. These effects are more pronounced as the quantity of additive and/or the amount of cement in the additive are increased. clays However, the very high liquid limit of heavy decreases with the increase in additive and/or the amount of cement in the additive. quantity 301 Cement-RHA additives are more efficient for stabilising low cohesion soils than for stabilising clays. more efficient for increasing the They are also strength than for modifying the plasticity and shrinkage properties of soils. 1:1 cement-RHA additive tends to be the most economical mixture of all cement-RHA additives used. These additives tend to be less economical as the amount of RHA in the additive increases. 1:1 cement-RHA additive is an effective but not very efficient additive for improving the behaviour under the action of repeated dynamic loads. of soils It is also not efficient for replacing 4% cement additive in modifying the plasticity and shrinkage properties of soils. 1:1 cement-RHA additive can be recommended for replacing 2% cement additive in increasing the strength of low cohesion soils and modifying the plasticity and shrinkage properties of soils provided that the cost of cement is 2.4 times (for increasing the strength of low cohesion soils) and 4 times (for modifying the plasticity and shrinkage properties of soils) the cost of RHA. 1:1 cement-RHA additive can also be recommended for replacing 4% cement additive in increasing the strength of soils provided that the cost of cement is 4 times the cost of RHA. All of these cost requirements are 302 not, currently, met in NSW. additive and consequently investigated replacing Accordingly, 1:1 cement-RHA all other cement-RHA additives in this research cannot be recommended cement in soil stabilisation in NSW for unless significant decrease in cost of RHA can be achieved. 10.4 Conclusions concerning GBFS as a single additive to Soils GBFS improves the workability of wet gravel-sand soils. It increases the optimum moisture content of these soils whereas it decreases the optimum moisture content of silts and clays. GBFS has no significant chemical reactions with soils. However, its mechanical porosity, increases stabilising the maximum effect reduces dry density and the affects favourably the stiffness and compressibility of soils. GBFS reduces the permanent deformation and improves the behaviour of soils under the action of repeated dynamic loads. It also increases the CBR and unconfined compressive strength of soils. The increase in unconfined compressive strength of cohesive soils is remarkable but inferior to those which occur by the addition of lime or cement to these soils. 303 GBFS has no significant effect on the liquid limit, plastic limit, plasticity index and linear shrinkage of low cohesion soils. Its effect on volume stability of heavy clays is remarkable. It increases the plastic limit and decreases the very high liquid limit, the plasticity index and the linear shrinkage of these heavy clays. However, these effects on plasticity and shrinkage properties are inferior to those which occur by the addition of lime or cement to these soils. GBFS, as a single additive to soils, can be recommended for modifying strength, plasticity and shrinkage properties of cohesive soils provided that the cost of lime or cement is 6-9 times the cost of GBFS. This condition can currently be met in NSW within a distance of 55km from Port Kembla or similar GBFS production plant. 10.5 Conclusions concerning Lime-GBFS additives 1:1 lime-GBFS additive improves the workability of wet soils. It increases the optimum moisture content and decreases the maximum dry density of soils. However, as the quantity of GBFS in the additive increases, the effect of GBFS gradually becomes more dominant than the effect of lime and tends to increase the maximum dry density and decrease 304 the optimum moisture content of treated soils, particularly clays. 1:2 lime:GBFS ratio is the optimum ratio associated with the highest strength of lime-GBFS pastes. However, lime reacts more readily with soil than with GBFS and hence the highest strength of all lime-GBFS treated soils has been achieved by 1:1 lime-GBFS additive. Lime-GBFS additives increase the CBR, unconfined compressive strength and the shear strength of soils. This is more pronounced as either the curing time, the quantity of lime in the additive or the quantity of additive is increased. However, the unconfined compressive strength of treated soils increases with increasing quantity of additive, up to a peak value, then decreases with the continuous increase in the quantity of additive. a peak value of The quantity of additive at which strength occurs tends to increase with increasing amount of GBFS in the additive. The increase in CBR, unconfined compressive strength and shear strength is caused by the increase in both the internal friction and cohesion of stabilised soils. GBFS, as a hydraulic cement or as a pozzolan, has a role in strength development However, the highest of lime-GBFS strength soil achieved stabilisation. by lime-GBFS 305 additives is not comparable to the maximum increase in strength which occurs by the addition of lime to soils. Delay in compaction of lime and lime-GBFS stabilised soils decreases the strength of these mixes. This is more pronounced as the time elapsed since mixing is increased. The rate of reaction in lime-GBFS soil stabilisation is relatively slow and somewhat similar to lime stabilisation. The losses in strength of lime and lime-GBFS stabilised soils due to delay in compaction are, consequently, low and almost similar. Accordingly, the time constraints in respect of compaction are not so critical. Lime-GBFS additives improve the volume stability of soils. They decrease the plasticity index and linear shrinkage and increase plastic limit and liquid limit of these soils. These effects are more pronounced as the quantity of additive and/or the amount of lime in the additive are increased. However, the very high liquid limit of heavy clays decreases with the increase in additive quantity and/or the amount of lime in the additive. Lime-GBFS additives are more efficient for stabilising low cohesion soils than for stabilising clays. 306 Lime-GBFS additives tend to be less economical as the amount of GBFS in the additive increases. the most used. reducing economical It is the an Hence, 1:1 lime-GBFS is additive of all lime-GBFS effective permanent and efficient deformation and additives additive for improving the behaviour of soils under the action of repeated dynamic loads. efficient However, all lime-GBFS for replacing additives 4% lime additive used in are not stabilising soils. 1:1 lime-GBFS additive can be recommended for replacing 2% lime additive in stabilising clays provided that the cost of lime is 6.7 times the cost of GBFS. It can also be recommended for replacing 2% lime in increasing the strength of low cohesion soils provided that the cost of lime is 2.25-4.68 times the cost of GBFS. These cost requirements are now satisfied in NSW in locations where hauling distance from Port Kembla or any other similar GBFS production plant does not exceed 55-200km depending on stabilisation the nature of soils and purpose of soil (55km for stabilising gravel-sand soils and 200km for stabilising sand-silt soils). 307 10.6 Conclusions concerning Cement-GBFS additives Cement-GBFS additives improve the workability of wet soils. They increase the optimum moisture content and maximum dry density of soils. The increase in optimum moisture content is more pronounced as the amount of cement in the additive is increased. There is no optimum ratio of cement to GBFS in cement-GBFS pastes. The strength of these pastes increases with the increase of amount of cement in the mix. Cement-GBFS additives increase the CBR, unconfined compressive strength and shear strength of soils. This is more pronounced as either the curing time, the quantity of cement in the increased. additive or the quantity of additive is The increase in unconfined compressive strength, CBR and shear strength of cement-GBFS soil stabilisation is caused by the increase in both the internal friction and cohesion of the stabilised soils. GBFS, as a hydraulic cement or as a pozzolan, has a role in strength development of cement-GBFS soil stabilisation. However the rates of strength development of cement-GBFS stabilised soils are slightly slower than those of cement stabilised soils. GBFS, therefore, acts as a weak retarder 308 and has no significant effect on the compaction working time of cement-GBFS stabilised soils. Delay in compaction of cement and cement-GBFS stabilised soils decreases the strength of these mixes. This is more pronounced as the time elapsed since mixing is increased. The loss in strength, due to delay in compaction, of cement, GBFS stabilised soils is slightly less than that of cement stabilised soils. This is more pronounced as the amount of GBFS in the additive is increased. Cement-GBFS additives improve the volume stability of soils. They decrease the plasticity index and linear shrinkage and increase the plastic limit and liquid limit of these soils. These effects are more pronounced as the quality of additive and/or the amount of cement in the additives are increased. However, the very high liquid limit of heavy clays decreases with the increase in additive quantity and/or the amount of cement in the additive. Cement-GBFS additives are not efficient for modifying the plasticity and shrinkage properties of low cohesion soils. 1:1 cement-GBFS additive is efficient for increasing the strength of soils and modifying the plasticity and shrinkage properties of clays. It is also an effective and efficient 309 additive in reducing the permanent deformation and improving the behaviour of soils under the action of repeated dynamic loads. 1:1 cement-GBFS additive can be recommended for replacing 24% cement additive in modifying strength, plasticity and shrinkage properties of clays provided that the cost of cement is equal to or greater than 2-4 times the cost of GBFS. 1:1 cement-GBFS additive can also be recommended for replacing 2% cement additive in modifying the strength of sand-silt soils provided that the cost of cement is equal to or greater than 4.65 times the cost of GBFS. These cost requirements can be met in NSW and 1:1 cement-GBFS additive can be recommended for the above stated applications in locations where hauling distance from Port Kembla or any similar GBFS production plant, does not exceed 80-230km depending on the nature of soil and purpose of stabilisation (230km for increasing the strengh and modifying the plasticity and shrinkage of clays and 80km for increasing the strength of sand-silt soils). 310 REFERENCES 1) Hawkes, H.E. and Webb, J.S. ,(1962) Geochemistry in Mineral Exploration, Harper and Row, New York. 2) Spense, R.J.S and Cook, D.J. (1983) Building Materials in Developing Countries, John Wiley and Sons, New York. 3) Ingles, O.G. and Metcalf, J.B. (1972) Soil Stabilisation Principles and Practices, Butterworths Sydney-Melbourne-Brisbane. 4) Ingles, O.G. (1978) "Soil Stabilisation The Next One Hundred Years", Symposium on Soil Reinforcing and Stabilising Techniques, Sydney, Australia, pp. 365-383. 5) Davidson, W.H. and Mullin, E.F. (1962) "Use of Fly Ash in Road Construction Proc. Australian Road in New South Wales", Research Board, 1:2, pp. 1085-1100. 6) National Association of Australian State Road Authorities (1979). The History and Challenge of Road Transport, Brickfield Hill, NSW, Australia. Kezdi, A. (1979) Stabilised Earth Roads, Elsevier Scientific Publishing Company, Amsterdam-Oxford- New York. Ingles, O.G. (1968) "Report on Survey of Use of Soil Stabilisation in Australia", Australian Road Research, J., 3. pp. 58-63. Cruickshank, J.W. (1977) "Stabilisation of Road Pavements - A Preliminary Survey", Road Research, J., 7. Australian pp. 41-42. Lee, I.K., Ingles, O.G. and White, W. (1983) Geotechnical Engineering, Pitman Publishing Inc, Marshfield, Massachusetts, USA. Lea, F.M. (1970) The Chemistry of Cement and Concrete, Edward Arnold (Publishers) Ltd, London. Yamanouchi, T. (1978) "Problems of the Development of Soil Stabilisation", Reinforcing and Stabilising Symposium on Soil Techniques, Sydney, Australia. Havelin, J.E. and Khan, F. (1951) "Hydrated LimeFlyash-Fine Aggregate", US Paten No. 2:554, 690. 14) Minnick, L.J. and Miller, R.H. (1952) "Lime-Flyash Compositions in Highways", Proc Highway Research Board, pp. 511-528. 15) Davidson, D.T., Sheeler, J.B. and Delbridge, N.G. (1958) "Reactivity of Four Types of Flyash with Lime", Highway Research Board, Bulletin No. 193, pp. 24-31. 16) Central Electricity Generation Board (1958) Pulverised Fuel Ash Information, Bulletins No. 4,5,6 and 7, London. 17) Bureau of Agricultural Economics (1983) "Situation and outlook, 1983, Rice, Australia", Government Publishing Service, Canberra, pp. 1-10. 18) Croft, J.B. (1964) "The Pozzolanic Reactivities of some New South Wales Flyashes and their Application to Soil Stabilisation", Australian Road Research Board, Proc. V2 (2), pp. 1144-1167. 19) Herzog, A. and Brock, R. (1964) "Some Factors Influencing the Strength of Soil-Lime-Flyash Mixtures", Australian Road Research Board, Proc V2(2), pp. 1226-1233. Department of Main Roads, NSW, (1978) "Stabilisation with Lime-flyash Mixture", Circular No. M&R 115, Sydney, Australia. Moulton, D., Seals, K., and Anderson, D. (1973) "Utilisation of Ash from Coal Burning Power Plants in Highway Construction", Highway Research Record, No. 430, pp. 26-39. Mehta, P.K. (1979) "Energy Resources and the Environment - A Review of the US Cement Industry", World Cement Technology, 9(5), pp. 144-160. Mehta, P.K. (1976) "Energy and Industrial Materials from Crop Residues", Resource Recovery and Conservation, pp. 223-238. Dave, N.G. (1981) "Pozzolanic Wastes and their Activation to Produce Improved Lime Pozzolana Mixtures", Second Australian Conference on Engineering Materials, University of New South Wales, Sydney, pp. 623-638. Hammond, A.A. (1976) "Evaluation of Bauxite-Waste for Cement Production in New Horizons in Construction Materials", Envo Publishing Co Inc, Vol 1, pp. 1159-163. 26) Lilley, A. (December 1979) "Cement Stabilised Materials", Civil Engineering, pp. 25-29. 27) Suwanvitaya, P. (1984) Properties and Behaviour of Rice Husk Ash-Lime Cement, Thesis (PH.D.) University of New South Wales. 28) Hough, J.H. and Bar, H.T. (1956) "Possible Uses for Waste Rice Hulls", Louisiana State University, Agricultural Experiment Station, Bulletin No. 507. 29) Rahman, M.A. (1986) "Effects of Rice Husk Ash on Geotechnical Properties of Lateric Soil", West Indian Journal of Engineering, Volume 11 No. 2, pp. 18-22. 30) Lazaro, R.C. and Moh, Z.C. (1976) "Stabilisation of Deltaic Clays with Lime-Rice Husk Ash Admixtures", Proceedings of Second South East Asian Conference on Soil Engineering, Singapore, pp. 215-223. 31) Subrahmanyam, M.S., Cheran, Lee Lih and Cheran,Lee So (December 1981) "Use of Rice Husk Ash for Soil Stabilisation", Gological Society Malaysia, Bulletin 14, pp. 143-151. Rajan, B.H., Subrahmanyam, H. and Sampath Kumar, T.S.(1982) "Research on Rice Husk Ash for Stabilising Black Cotton Soil", Highway Research Bulletin 17, pp. 61-75. Dussart, Jacques. (February 1979), "Blast Furnace and Steel Slags in France", The Australian I.M.M. Illawarra Branch, Utilisation of Steel Plant Slags Symposium, pp.25-34. Lee, A.R. (1974) "Blast Furnace and Steel Slag Production, Properties and Uses", Edward Arnold. Prandi, E. (1965) "Traitment au Laitier Granule des Materiaux Routieres", Ponts et Chaussees, Bull.Liais.Labs. Routieres,. Cohchi, M., Shiina, K. and Ohta, F., (1979) "Effective Prevention for Weathering Expansion Crack of Arc-Furnace Slag Concrete", The Cement Association of Japan, Volume 33, pp. 184-188. Sakai, M. and Miyamoto, M. (1979) "Experimental Study on the Properties of LD Converter Slag Concrete", Proc. of Japan Concrete Institute 1st Conference, pp. 185-188, 38) Hagga, Nobutake., Ohkawa, Yuichi., Michiokonno, Kawamoto, Takayuki., Mizoguchi, Ikuo., (June 1981) "Utilisation of Blast Furnace and Steel Slags in Road Construction", Nippon Steel Technical Report No. 17, pp. 73-89. 39) Kawamura, Mitsunori., Hasaba, Shigemasa, and Torri, Kazuyuki, "Effective Utilisation of Ld Converter Slag as a Soil Stabiliser", pp.285-296. 40) Hasaba, Shigemasa., Kawamura, Mitsunori. and Torri, Kazuyuki, (March 1982) "Reaction Products and Strength Charactaristics in the Stabilised Soil using Desulfurization By-Products and Blast Furnace Slag", Transactions of Japan Society of Civil Engineer, Volume 14, pp.251-253. 41) Bate, I.e. (November 1972) "Slag as a Road-Base and Stabiliser in Rhodesia", The Rhodesian Engineer, pp. 54-58. 42) Department of Main Roads, NSW, (December 1988), Accelerated Loading Facility Prospect Trial. Seminar on Results and Findings. 43) Hudson, Ken., (February 1989) "Stabilisation of Road Pavements France Autoroutes", New Zealand Concrete Construction, pp. 3-10. Shackel, B. (1975) "A Critical Assessment of Current Test Methods and Design Criteria for Stabilised Pavement Materials", Conference on stabilisation and compaction, University of New South Wales, Kensington, Australia. Shackel, B. (1975) "The Behaviour of Stabilised Soils under Simulated Traffic Loads", Proc. 7th Conference Australian Road Research Board, Vermont, Victoria, Volume 7, Part 7, pp. 18-37. Shackel, B. (1975) "Types of Repeated Loading Tests and Their Application to the Characterisation of Soils and Road Making Materials", Symposium On Repeated Loading of Soils With Particular Reference To Road, School Of Highway Engineering, Kensington, New South Wales, Australia. National Association of Australian State Road Authorities (1986) Guide to Stabilisation in Roadworks, Sydney, Australia. Natt, G. and Joshi, R. (1984) "Properties of Cement and Lime-flyash Stabilised Aggregate", Testing and Modeling Soils and Soil Stabilisers, Transportation Research Record 998, Washington, DC, pp. 32-40. 49) Rowe, G.H. (1985) "Laboratory Testing for Stabilisation", RRU Technical Recommendations TR7, Road Research Unit, National Roads Board, Wellington, New Zealand, pp. 5-11. 50) Indian Standard for Masonary Cement (IS4098). 51) South Africa National Institute for Transport and Research (1986) Cementitious Stabilisers in Road Constructions, Technical Recommendations for Highways Draft TRH13, Pretoria, South Africa, pp. 1-64. 52) Klatt, P. (1991) Private Communication. 53) Jones, D.E. (1990) "Industrial slag construction materials for the 1990's and beyond", Proc. 21st Engineering Nineties, Conference the Illawara on Materials Group, for Institution Engineers, Australia, University the of of Wollongong, NSW, Australia. 54) Jones, D.E. (1990) "In the beginning-slag", Seminar on slag products in the construction industry, Australasian Slag Association, pp. 1-12. Hanley, P.J. (1990) "Slag-towards 2000, Australian trend", Concrete for the Nineties, International Conference on the use of Flyash, Slag, Silica Fume and other silceous materials in concrete, Leura, Australia, pp. 1-11. Department of Main Roads, NSW (now known as the Roads and Traffic Authority, NSW) Materials Australia. Testing Manual, Volume (July 1, 1989). Sydney Appendix A METHOD OF OPERATION OF THE FATIGUE CONTROL PANEL USED IN THE REPEATED DYNAMIC LOAD TEST Fatigue Control Panel The panel is illustrated in Figure A.1 with each item numbered. Each item is then explained briefly* 1. Supply On/Off Switch A small toggle switch in the bottom lefthand corner of the control panel switches the mains supply to the fatigue control panel on and off. A red light indicates the supply is on. 2. Indicator A digital indicator displays the force applied to the jack load cell or the jack piston stroke* or an external feedback signal* It may Indicate either the peak values or the mean or static value* 3* Meter Selection Switch A three position toggle switch selects the meter to display load, external feedback or stroke* 6* Peak/Mean Selection Switch A three position toggle switch sets the meter display either positive or negative peaks, or the mean value* Note when reading static DC values the frequence switch. (7) should be switched to DC* 7* Meter Frequency Range Switch This control adjusts the tine constant of the meter and is used when the piston is measuring peak or mean oscillating values* It affects the rate of response of the meter* It should be switched to DC for reading static values* 84 Peak Reset Controls The peak indication may be reset manually or automatically* When the rotary switch is fully anti-clockwise the peak reading circuits are reset manually with the push button* As the switch is rotated clockwise the peak circuits are reset automatically at increasing frequency* 9, Monitor Sockets These 2mm terminals provide DC output signal of the value selected for indication of the meter* Full range of the transducer gives lOv DC. Minimum impedance of subsequent circuit 100k ohm* 10* Zero Controls Two calibrated multi-turn lockable potentiometers adjust the zero of the stroke and load indication and DC output signal* 11. DC Output Sockets Three sockets provide DC output signals of load and stroke., together with a signal earth connection. scale of the transducer. lOv equivalent to full Minimum impedance of subsequent circuit 100k ohm* 12. Control Selection Buttons Three push buttons set the jack to control either load or stroke or some other variable fed to the external feedback socket. Care must be exercised when changing from one control mode to another as a step may be applied to the specimen. 13, External Feedback Socket A co-axial socket beneath the external "contr selection button1* accepts the external feedback signal* This should be - i lOv may?mtim and any signal conditioning circuits must have flat frequency i response to 200Hz. Input impedance is 22k ohm and the feedback signal source should have a low impedance or errors will result. I ! 14. Mean Level Potentiometer The digital readout potentiometer controls i static or mean values. It can be switched so that 100% on the potentiometer is either full transducer range or 10Z of transducer range* The push buttons give tension (+va) or compression (-ve) sign* 15. Mean Level Potentiometer Range Switch This small toggle switch sets the mean level command potentiometer to 10S or 100Z full range. i i 16. Limit Load This switch is associated with control of stroke. When switched to limit the load applied by the machine to the load cell is limited to 0.5X (approximately) of full range* tension and compression. specimens* The limit operates in There will be some overshoot with very stiff If the specimen will be damaged with a 57, load it will be better use load control* 17. Valve Signal Indication A small edge meter gives an indication of signal on the servo valve* It may be used for observing performance or adjusting valve bias signal. 18. Valve Bias Adjustment A screw driver operated potentiometer adjusts valve bias signal. It may be used to set the system so that a particular command signal gives it the exact required valve. It is normally preset at the factory and does not require adjustment. 19. Gain Adjustment A screw driver operated control adjusts the control loop gain under load control and external feedback. Adjustment may be required as the gain of the system will vary with the specimen stiffness. The control loop gain for stroke control is adjusted on the jack electronic unit. 20. External Command Input A co-axial socket is provided for feeding external programme signals to the jack. The scaling of these signals is 10 volts DC for - full range. The input signal may be attenuated by the external programme attenuator control. Command signals may also be fed to a socket at the rear of the panel. 21. External Programme Attenuator A digital readout potentiometer may be used to attenuate the incoming externally generated programme. The i potentiometer reading gives percentages signal fed to the jack, i.e. 50Z on the potentiometer (50.0) means that half the incoming voltage is applied to the jack. 10 volts gives full transducer range* 22. Internal/External Command Selection A small toggle switch is used to select either the internal cyclic programme from the built-in function generator or as an alternative some external programme fed to the system through the co-axial input socket. ! ! - A 23. Oscillator Waveform Selection A rotary switch selects eitherjsine " triangular or square waveform, or ramp operation* 24* Stop/Run Switch When the switch is moved to "run" the oscillator outpu starts to go positive from zero* a; c « c o u Ai c o o fl) 3 6C «¥« « >J OM0 -l fa -U c o a to to c -H JJ © (0 o a i &4 25. Preset Switch When set to the preset position this toggle switch causes oscillator to stop when a preset count selected on the cycle counter is reached. 26. Frequency/Rate Oscillator frequency is set on a digital readout potentiometer and a decade selection switch. This selection switch gives the potentiometer the frequency ranges of 0 to 1 Hz, 0 to 10 Hz, or 0 to 100 Hz. The dial is also calibrated in rate .Z Range/Millisecond for use with the ramp facility. 27* Ramp hold Switch Enables the oscillator to produce ramp functions positive or negative going from zero. 28, Monitor Socket A 2mm socket marked monitor enables the output waveform of the oscillator to be displayed on an oscilloscope or similar device. Output - lOv DC. 29. Cycle Counter A six digit preset counter records either the number of completed cycles or the elapsed time. Counting occurs at 0 volts positive going. A preset number may be set on the counter by depressing the black button raising the red perspex cover and setting the finger wheels. When this preset number is reached the counter will stop the oscillator if the preset switch (25) is set to preset. Oscillator output will go to aero, but any mean value applied (14) will remain. 30. Counter Range Switch This switch gives counter scaling factors of 1 divided by 100 and also permits the selection of timing function which gives 1 count per second. An off opsition switches the counter off. Maximum counting rate on the xl range is 25 Hz and in excess of 100 Hz on the other two ranges. In normal use a maximum counter rate of about 5 Hz is recommended* 31. Reset Button This push button resets the counter and the divider circuits to zero and also.resets the trip circuits. 32. Stopped Light An amber light illuminates when the counter has stopped. 33, Tripped Light An amber light illuminates when the external trip circuits have operated. 34. External Trip Contacts When these 2mm terminals are shorted the command attenuator signal is set to zero. This trip is reset by the reset push button. A pair of contacts are brought to the rear panel and may be connected to hydraulic control circuit to stop the pump when the trip operates* Contacts are closed when tripped. 35. Oscillator/Pump Switch This toggle switch arranges that the trip circuit may either stop the oscillator or stop the oscillator and trip the pump. Procedure for Operation The following procedure is used to operate the loading panel. Figure A.2 shows the complete panel including supplies, and switches, 1* Start the cooling pumps in the Pump "House for the oil supply motors. 2* Switch the Dartec oil pumps on in the Pump House. 3* Switch the oil supply on in the Pump House. 4. Switch the electrical supply on to the fatigue panel. 5* Start the supply of oil to the low pressure pumps, 6* After approximately 20 seconds there will be an abrupt sound which indicates that the jack is now ready to operate. After sound switch on jack no. 1. 7. Switch on high pressure. 8. Take out any packing or obstructions between the wheel and frame and wheel and pavement. 9. The test is now ready to begin* Eor Static Loading (Refer to Figure A.1) 1. Switch supply on (1) 2. Switch (3) to load 3. Switch (7) to DC 4. Switch (8) to desired position. The position depends on how quickly a re reading is required. ,/yi, ... • -, . . _,,, j , *HVj/.ifimmw_,Vj, ,.,, -• ,. 1 TTPiy jEigure A . 2 - The complece operations panel for loading. I j 5. Switch (6) to mean • 6*. Calculate mean value required. For example if Che range of loading was from 10 kn Co 40 kn then mean value would be (10 + 40)/2 » 25 • 7*- Push load control button, (12) 8. Calculate command input required. 9. Switch (22) to internal. 10» Select command input required (21) 11. Switch (15) to 100Z, switch (14) to (-) for compression. 12. Select mean value required (14) As the mean value is increased the indicator display (2) will increase. The mean value (14) is increased until the static load required appears on the display (2). Once the load has been applied for the required duration, the load is released by returning (14) to zero. For Cyclic Loading 1* Switch supply on (1) 2* Switch (3) to load 3* Switch (7) to value desired to obtain peak or mean values. 4. Set (8) as for static loading. 5. Set (6) to mean initially. At a later stage during the running of the test + peak and - peak values may be desirable. All that is required is to set (6) to either + peak or • peak and depending on (8) the value is read. 6. Calculate mean value and command input required. 7. Select load control (12) 8. Switch (22) to internal. 9. Select (23) to wave form required. Sine wave used for test. 10. Select (24) to stop/zero. 11. Select Frequency required and set (26) accordingly. 12. Switch (15) to 100Z. 13. Switch (21) to required command input. 14. Switch (14) to (-) for compression, then turn dial to required mean value. This applies to the first load. 15. Switch (24) to run position and cyclic loading will commence. The counter (29) will count the number of cycles applied* 16. To unload, switch (24) to stop/zero and then return dial (14) to zero. Appendix B EQUIVALENT SPECIFIC GRAVITY AND CALCULATED POROSITY OF VARIOUS MIXES Equivalent specific gravity of the various additives used Proportion 1:1 1:2 1:3 1:4 Lime/GBFS 2.605 2.69 2.732 2.758 Cement/GBFS 3.00 2.953 2.93 2.916 Lime/RHA 2.07 1.976 1.93 1.902 Cement/RHA 2.465 2.24 2.127 2.06 - Additives Cement 3.14 Lime 2.35 RHA 1.79 GBFS 2.86 Equivalent specific gravity and calculated porosity of RHA and Lime/RHA stabilised Soil A Additive Specific Gravity Porosity Of Compacted Specimen (%) Lime/RHA 1:1 0% 4% 8% 2.93 2.895 2.861 37.50 38.86 39.53 Lime/RHA 1:2 0% 4% 8% 2.93 2.892 2.853 37.50 39.14 39.36 Lime/RHA 1:3 0% 4% 8% 2.93 2.89 2.85 37.50 39.10 39.65 Lime/RHA 1:4 0% 4% 8% 2.93 2.888 2.847 37.50 39.40 40.63 0% 4% 8% 2.93 2.88 2.838 37.50 39.58 41.50 RHA Equivalent specific gravity and calculated porosity of RHA and Lime/RHA stabilised Soil B Additive Specific Gravity Porosity Of Compacted Specimen (%) Lime/RHA 1:1 0% 4% 8% 2.86 2.828 2.7966 36.30 37.40 39.20 Lime/RHA 1:2 0% 4% 8% 2.86 2.8246 2.789 36.30 37.69 40.48 Lime/RHA 1:3 0% 4% 8% 2.86 2.822 2.785 36.30 37.63 40.39 Lime/RHA 1:4 0% 4% 8% 2.86 2.82 2.783 36.30 37.59 40.71 0% 4% 8% 2.86 2.817 2.774 36.30 37.52 40.52 RHA Equivalent specific gravity and calculated porosity of RHA and Lime/RHA stabilised Soil C Additive Specific Gravity Porosity Of Compacted Specimen (%) Lime/RHA 1:1 0% 4% 8% 2.83 2.80 2.769 53.30 55.00 56.30 Lime/RHA 1:2 0% 4% 8% 2.83 2.795 2.761 53.30 54.56 55.45 Lime/RHA 1:3 0% 4% 8% 2.83 2.794 2.758 53.30 55.26 55.76 Lime/RHA 1:4 0% 4% 8% 2.83 53.30 - - 0% 4% 8% 2.83 2.788 2.747 RHA 53.30 55.52 55.95 Equivalent specific gravity and calculated porosity of RHA and Cement/RHA stabilised Soil A Additive Cement/RHA 1:1 Specific Gravity 0% 4% 8% 2.93 — Porosity Of Compacted Specimen (%) 37.50 ~ Cement/RHA 1:2 0% 4% 8% 2.93 2.90 2.875 37.50 37.58 38.78 Cement/RHA 1:3 0% 4% 8% 2.93 2.898 2.865 37.50 37.88 39.61 Cement/RHA 1:4 0% 4% 8% 2.93 2.895 2.86 37.50 38.51 39.86 0% 4% 8% 2.93 2.88 2.838 37.50 39.58 41.50 RHA Equivalent specific gravity and calculated porosity of RHA and Cement/RHA stabilised Soil B Additive Cement/RHA 1:1 Specific Gravity 0% 4% 8% Porosity Of Compacted Specimen (%) 2.86 36.30 - — — " Cement/RHA 1:2 0% 4% 8% 2.86 2.835 2.810 36.30 37.21 39.50 Cement/RHA 1:3 0% 4% 8% 2.86 2.83 2.80 36.30 37.10 40.00 Cement/RHA 1:4 0% 4% 8% 2.86 2.828 2.796 36.30 37.76 40.27 0% 4% 8% 2.86 2.817 2.77 36.30 37.52 40.52 RHA Equivalent specific gravity and calculated porosity of RHA and Cement/RHA stabilised Soil C Additive Specific Gravity Porosity Of Compacted Specimen (%) Cement/RHA 1:1 0% 4% 8% 2.83 2.815 2.80 53.30 53.80 55.00 Cement/RHA 1:2 0% 4% 8% 2.83 2.80 2.783 53.30 53.93 55.08 Cement/RHA 1:3 0% 4% 8% 2.83 2.80 2.774 53.30 54.28 55.29 Cement/RHA 1:4 0% 4% 8% 2.83 53.30 - - 0% 4% 8% 2.83 2.788 2.747 RHA 53.30 55.52 55.95 Equivalent specific gravity and calculated porosity of GBFS and Cement/GBFS stabilised Soil A Additive Specific Gravity Porosity Of Compacted Specimen (%) Cement/GBFS 1:1 0% 4% 8% 2.93 2.933 2.935 37.50 37.26 36.96 Cement/GBFS 1:2 0% 4% 8% 2.93 2.931 2.932 37.50 37.20 37.20 Cement/GBFS 1:3 0% 4% 8% 2.93 2.93 2.93 37.50 37.20 36.80 Cement/GBFS 1:4 0% 4% 8% 2.93 2.929 2.928 37.50 37.50 37.10 0% 4% 8% 2.93 2.927 2.924 37.50 37.10 36.70 GBFS Equivalent specific gravity and calculated porosity of GBFS and Cement/GBFS stabilised Soil B Additive Specific Gravity Porosity Of Compacted Specimen (%) Cement/GBFS 1:1 0% 4% 8% 2.86 2.865 2.871 36.30 35.77 35.91 Cement/GBFS 1:2 0% 4% 8% 2.86 2.864 2.867 36.30 35.70 35.40 Cement/GBFS 1:3 0% 4% 8% 2.86 2.863 2.865 36.30 35.70 35.40 Cement/GBFS 1:4 0% 4% 8% 2.86 2.862 2.864 36.30 35.70 35.40 0% 4% 8% 2.86 2.86 2.86 36.30 35.60 35.30 GBFS Equivalent specific gravity and calculated porosity of GBFS and Cement/GBFS stabilised Soil C Additive Specific Gravity Porosity Of Compacted Specimen (%) Cement/GBFS 1:1 0% 4% 8% 2.83 2.837 2.844 53.30 52.70 51.80 Cement/GBFS 1:2 0% 4% 8% 2.83 2.835 2.839 53.30 52.70 52.10 Cement/GBFS 1:3 0% 4% 8% 2.83 2.834 2.838 53.30 53.00 52.70 Cement/GBFS 1:4 0% 4% 8% 2.83 53.30 - - 0% 4% 8% 2.83 2.8312 2.8324 GBFS 53.30 53.30 53.00 Equivalent specific gravity and calculated porosity of GBFS and Lime/GBFS stabilised Soil A Additive Lime/GBFS 1:1 Specific Gravity 0% 4% 8% 2.93 Porosity Of Compacted Specimen (%) 37.50 - _ ™ — Lime/GBFS 1:2 0% 4% 8% 2.93 2.92 2.91 37.50 38.00 38.40 Lime/GBFS 1:3 0% 4% 8% 2.93 2.922 2.914 37.50 37.70 38.20 Lime/GBFS 1:4 0% 4% 8% 2.93 2.923 2.916 37.50 37.70 37.20 0% 4% 8% 2.93 2.927 ,2.924 37.50 37.10 36.70 GBFS Equivalent specific gravity and calculated porosity of GBFS and Lime/GBFS stabilised Soil B Additive Specific Gravity Porosity Of Compacted Specimen (%) Lime/GBFS 1:1 0% 4% 8% 2.86 36.30 Lime/GBFS 1:2 0% 4% 8% 2.86 2.853 2.846 36.30 36.20 36.00 Lime/GBFS 1:3 0% 4% 8% 2.86 2.855 2.849 36.30 35.90 35.40 Lime/GBFS 1:4 0% 4% 8% 2.86 2.856 2.852 36.30 35.90 35.40 0% 4% 8% 2.86 2.86 2.86 36.30 35.60 35.30 GBFS Equivalent specific gravity and calculated porosity of GBFS and Lime/GBFS stabilised Soil C Additive Specific Gravity Porosity Of Compacted Specimen (%) Lime/GBFS 1:1 0% 4% 8% 2.83 2.821 2.812 53.30 53.20 53.40 Lime/GBFS 1:2 0% 4% 8% 2.83 2.824 2.818 53.30 53.20 53.10 Lime/GBFS 1:3 0% 4% 8% 2.83 2.826 2.822 53.30 53.20 52.80 Lime/GBFS 1:4 0% 4% 8% 2.83 53.30 0% 4% 8% 2.83 2.8312 2.8324 53.30 53.30 53.00 GBFS