Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 VACUUM TECHNOLOGY 2293 HVET/RVET AUTOMATION Session #1 FLOW: TRANSITION FROM VISCOUS TO MOLECULAR FLOW 3 Session #1 Transition From Viscous to Molecular Flow Agenda Objectives • • • • • • • • Attendance Safety Topic Course Introduction Discussion: Viscous to Molecular Flow Learning Activity: AHVET Pumpdown Discussion: Rough Pumps Revisited Troubleshooting Introduction • • • • • • Analyze Man Caught in Vacuum Chamber case study Review the syllabus & other administrative stuff Review old VacTech news Why is Molecular Flow different than Viscous Flow? Learn High Vacuum pump-down procedure Review Rough Pumps, their function, and some features Discover what Troubleshooting is 4 1 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 A Simple Question WHAT IS SAFETY? 5 Safety is… Safety is the state of being relatively free from harm, danger or injury Harm, danger, and injury are the result of circumstances or conditions present in the workplace: Hazards, Exposure and Risk 6 6 2 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 A HAZARD IS A PHYSICAL CONDITION THAT COULD CAUSE HARM OR AN INCIDENT; AN UNSAFE CONDITION 7 7 EXPOSURE IS THE PHYSICAL STATE WHERE A PERSON OR A GROUP OF PEOPLE COULD BE HARMED BY A HAZARD 8 8 3 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Often quantitatively calculated as the probability of an incident x the severity (low, normal, high) RISK IS THE LIKELIHOOD, HIGH OR LOW, THAT A HAZARD WILL ACTUALLY CAUSE HARM. 9 9 May also be known as ‘consequence’. SEVERITY IS THE HARM THAT WOULD RESULT FROM AN INCIDENT DUE TO THE HAZARD. 10 10 4 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 What’s the Point? • Personnel heath and safety requires identification of Hazards. • The existence of hazards alone does not mean the situation is unsafe. Personnel must have Exposure to the hazard before it is a concern. • Even exposure does not create an unsafe situation. To be unsafe, the situation must be such that there is Risk the hazard will actually cause harm. • If there is risk of harm, the severity of the harm must be assessed and, if necessary, mitigated. 11 Man Caught in a Vacuum Chamber! • Extremely possible in large vacuum chambers • Asphyxiation • Decompression Sickness a/k/a “The Bends” • Countermeasures: – Confined Space Procedures 12 5 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 What happens when human skin is exposed to outer space? Don’t Try This at Home! 13 VACUUM TECHNOLOGY 2293 VACUUM ANALYSIS & TROUBLESHOOTING Significance, Characteristics, Features & Functionality LOGISTICS AND OTHER STUFF… 14 6 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 What you signed up for… • College Level coursework in Vacuum Technology • Objective: Prepare technicians for work in industries that rely on “high” vacuum processes (Nominally below 1 Torr; 1 mTorr by definition) • Vacuum enables many manufacturing processes, including: – – – – – – Semiconductor Microelectromechanical systems (MEMS) High-Performance Glass Optics Manufacture of “pure” metals Etc. 15 What we do here is Pretty Darn Close to Rocket Science! • By the end of the course, you will: • Skills Needed coming into class – Be conversant in high vacuum technology – High school algebra: no Calculus – Be able to explain the function and purpose of vacuum components – Understand how to write a lab report – Perform system calculations – Select components and materials for basic applications – Start developing skills to understand system performance and performance issues – Understand the Scientific Method – Excel/spreadsheet manipulation – Word/word processing & high school writing capability – Workplace problem-solving and teamwork – Prerequisite: 1292 class or equivalent experience 16 7 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 General Plan for Course Make Vacuum Week 1-5 Measure Vacuum Utilize Vacuum Week 6-10 Week 11-16 17 Your Normandale Instructors! John Lasswell Scott Holm-Hansen John.Lasswell@normandale.edu Scott.HolmHansen@normandale.edu Office – S1342/S1335 Hours: • One hour after class or by arrangement • Monday on ZOOM Office – S1342 Hours: • MTWR afternoons by arrangement • Phone 952-358-9238 4:00-5:00 Central Time • • Discussion Forum? Phone 952-358-9238 (leave a voicemail) Special Guests • • • • • Nancy Louwagie Ruth Robinson Tom Johnson Kim Klein And other notquite-ready for prime-time players, to be named later 18 8 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Our Success… EACH STUDENT CAN APPLY THE KNOWLEDGE AND SKILLS THEY HAVE LEARNED TO UNDERSTAND, OPERATE AND MAINTAIN THE VACUUM SYSTEMS THEY ARE RESPONSIBLE FOR. 19 Communicating with Your Instructors Option 1-Email Option 2-Phone Option 3-Scheduled Meeting 20 9 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Comms: Weekly D2L Announcement • Look Something like this • Published at 11:59 Monday evening before class • Links will connect you to all the stuff you should need for the week 21 Comms: E-mail From Your Instructor • • • Will come via your Normandale email address Message to either a Partial Class Group or Individual Reasons: – – • For your information For some action on your part (response may be requested) Recommended: Set up automatic notification to an email address you look at frequently 22 10 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Comms: Announcements From Your Instructor • Message for entire class • Recommended: Set up automatic notification to an email address you look at frequently You will get an email message like this https://normandale.learn.minnstate.edu/d2l/Notifications/Settings?ou=4148064 23 Course Materials You Supply NCC Supplies via Online • • Optional Textbook: Introduction to Vacuum Technology – – – – – – David Hata – ISBN-13: 978-0-13-045018-0 • • • • • • • • • Paper Black/Blue Pen Red Pen Highlighter – the colors of choice Internet Connected Computer Printer Office Suite software apps Camera and Microphone Ability to deliver document deliverables in PDFs Weekly: • Slide Deck Handout Study Guide Handout Reading Material Links Video Links Available Monday12:59 pm Quiz – Available after class to start of next class • Experimental Equipment 24 11 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Resource: If you can find it… • The Third Edition (not the blue cover version) • This text is the closest that the NCC faculty have found that relates to the purpose of this course. • Good long-term Reference • May be available on Amazon (new) or eBay (used) • https://kipdf.com/modern-vacuum-practice2007-nigel-s-harris-mcgraw-hill2007_5ad30c6b7f8b9a886c8b4587.html 25 Lessons: In-Class Lecture/Discussion • Topic Orientation allows a certain amount of material to be presented • Primarily intended as an opportunity to discuss the topic as opposed to being a lecture • Managed digression is acceptable • Death by PowerPoint potential… 26 12 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Lessons: Study Guide Preview It! Pink Text = Hidden when Printing Read It! Hyperlinked to documents in D2L Outline Class Notes Only from 2 or 3 every week Automate personalized SG 27 Lesson Homework: Read It! Assignment • Developing the skill of getting information from information published by others is important. • This information is a record of what has been observed…but not of the present or future – What can that mean to us? 28 13 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Homework: Read It! Assignment • • • The patron of the Normandale VACT program, Phil Danielson and his wife , gifted his published articles on vacuum technology to the program on his death These can be found at: https://www.normandale.edu/dep artments/stem-andeducation/vacuum-and-thin-filmtechnology/vacuum-technologyresources--the-danielsoncollection/articles Assignments relevant to the topic under consideration will be made. 29 Lesson Homework: Read It! Assignment • Other Materials – Operator and Maintenance Data – Papers by Others – Etc. 30 14 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Lessons: Study Guide Watch It! Figure It! Typically about 1 hour of video content Typically about 1 hour of video content Typically about 1 hour of video content Information about the Lab Activity 31 Lesson Homework: Online Activities -Videos Benefits for Students Benefits to Teachers • • • • • • • Create a more engaging sensory experience than using print materials alone Provide a go-to resource that can be watched from anywhere Increase knowledge retention Can assist the learning of any subject Increase digital literacy and communication • • • • • Increase student engagement Offer flexibility to pause, rewind, etc. Create a flipped classroom Facilitate remote learning Analytics Opportunities for student feedback and assistance Changes the role of teachers from lecturers to facilitators 32 15 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Lesson Homework: Online Activities PhET – University of Colorado • https://phet.colorado.edu/e n/simulations/filter?subjects =physics,chemistry,math&typ e=html&sort=alpha&view= grid Wisc-Online – Wisconsin Technical College System • https://www.wisconline.com/learn/naturalscience/chemistry • https://www.wisconline.com/learn/naturalscience/physics General Idea: Provide additional focus on a particular technical subject You will need to: • Establish an account with each of these (they are free) • Make sure your computer will allow the animations provided. • If you use your work computer, work with your IT department if there are issues 33 Lessons: Study Guide Lab Information Partial Information about the Lab Activity Memo Report Practice writing. Do your best. You are not expected to be Shakespere 34 16 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Turn in your homework to the appropriate Drop Box • Scan your homework into a single pdf file. • Multiple pdf & jpeg files can be accommodated but are a pain • See the announcements for pdf software that you can use from your phone. • Other formats? Let’s discuss! • You only need to turn in the Homework • Turn in study guides to the correct drop box • Only the last submission is graded (so relying on me to understand what is a complete submission is somewhat hazardous) 35 Dreadful Things Quizzes Exam • • • • One Final - ±1-1/2 hours • • • • • Expect one most weeks They may pop up in class Open book – notes – homework – friends (if any) Quizzes start after class and are due by the next class No extensions One do-over I must grade written answers; this will happen after the due date These should not be too hard • • • Always Cumulative Open book – notes – homework This should be somewhat challenging 36 17 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Earning Your Grade Study Guide a/k/a Homework • 60% of grade • Do Collaborate • Due by the next class session • Give yourself a reasonable time limit Quizzes Final Exam • 30% of grade • Open book, open note • Don’t collaborate • One do-over • Due by the next class session • One-hour limit • 10% of grade • During class time, finals week • 2-hour limit 37 Per Time Investment Class Session • Class Time – ±3-4 hours/week • Homework – 4+ hours/week – – – – – Reading Assignments Problems Lab Analysis On-line activities Quizzes 38 18 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Policies and Procedures – Questions? • • • • • • ADA D2L Attendance Weather Events Other Events Late Assignments • Incomplete Grades • Academic Dishonesty • Other Dubious Behavior 39 Good Telepresence Etiquette! CLASS • Keep Camera On! Don’t hide with your camera off all the time • Sit sort of close to the camera! • Talk once in awhile without being prompted! • Be judicious about using “mute” 40 19 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Professionalism • How we should work together! • Route to maximizing Boogie Factor! 41 VACUUM TECHNOLOGY 2293 VACUUM ANALYSIS & TROUBLESHOOTING Significance, Characteristics, Features & Functionality FLOW: THE TRANSITION FROM VISCOUS TO MOLECULAR FLOW 42 20 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Impact of the Light Bulb on Vacuum Technology • No, not Thomas Edison – 1802: Humphry (Henry) Davy & Davy Electric Arc Lamp – 1840: Henry de la Rue – platinum filament in an evacuated tube – 1850-1878: Joseph Swan – Improved filaments in Better Vacuums – 1874: Woodward and Evans – Arc Lamp in Nitrogen-filled globes • Edison: – 1878-patent application for improved electric lights – 1879-purchase of Woodward/Evans patent; patent for carbon filament (similar to Swan) – 1880-Commercial production of light bulbs begins • Vacuum Technology transitions from a scientific curiosity to an industrial process for mass production 44 Edison’s Advances • Device Combination – Geissler Pump in Rough/Backing Mode (higher volumetric flow rate, pump to about 0.1 Torr pressure) – Sprengel Pump in continuous exhaustion mode (pump to 1 mPa/7.5x10-6 Torr pressure) – McLeod Gauge (measure to 10-6 Torr) • Also: – Control of Mercury Flow – Automation of Mercury Delivery to 100 pumps – Removal of Residual Gasses during lamp processing 45 21 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Edison Pump System Schematic Diagram These devices have complex tubing that could be diagrammed in more detail 46 How was Low of a Pressure Needed? • Eliminate as much oxygen as possible to reduce oxidation (corrosion): – Chemical reaction rates tend to double every 10 degrees temperature rise – Filament temperatures are in the range of 2800-2900 0F • Eliminate as much gas as possible to reduce filament cooling due to the gas – Cooling will affect the color and intensity of light – Backfilling with Nobel gasses that don’t chemically react or Halogens which prevent filament condensation except on the filament are exceptions under the correct conditions. 47 22 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Interesting but off task. WHAT HAPPENS WHEN THE PRESSURE OF A GAS IS REDUCED? 48 VACUUM TECHNOLOGY 2293 VACUUM ANALYSIS & TROUBLESHOOTING Learning Activity/Scott Holm-Hansen OPERATING THE HVET 90 23 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 High Vacuum System Components VC P1 • • • • • • • • • VC – Vacuum Chamber V1 – Roughing Valve P1 – Roughing Pump G1 – Roughing Gauge V2 – Venting Valve V3 – High Vac Valve V4 – Foreline Valve P2 – High Vac Pump G2 – High Vac Gauge P2 92 Key Turbo Operating Information • Crossover Pressure – 200 mTorr – Production systems often need to pump down to 75 mTorr before crossing over • Base Pressure – ±0.005 mTorr (5x10-6 Torr) 93 24 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 HVET – High Vacuum Equipment Trainer • • • • Small footprint allowing ease of transporting Open system design allows students to easily see all system components A variety of gauges were used to compare different gauge technologies Gauges have local displays to show pressures at point of use 94 VC – Vacuum Chamber • • The vacuum chamber is where high vacuum processes take place The HVET has a plastic bell jar for easy viewing of experiments. Plastic material eliminates risk of implosion or shattering. 95 25 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 V1 – Roughing Valve • • • The roughing valve isolates the roughing pump from the vacuum chamber The HVET uses an angle seat design with a manual handwheel Be sure to always fully open or close the valve 96 P1 – Roughing Pump • • The roughing pump removes gases from the vacuum chamber The HVET has a scroll pump with an ultimate pressure rating of Approximately 100 mTorr 97 26 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 G1 – Roughing Gauge • • The roughing gauge is useful for measuring pressure in the rough vacuum range The HVET uses a Capacitance Manometer/Pirani gauge combo for measuring down to the crossover pressure of 200 milliTorr 98 V2 – Venting Valve • • • The venting valve allows gas to return to the vacuum chamber bringing the pressure back to atmosphere The HVET has a simple quarter turn valve for this purpose The HVET vents with air from the atmosphere. It is preferred to vent with dry nitrogen as to minimize the amount of water vapor in the system 99 27 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 V3- High Vac Valve • • • The high vac valve isolates the high vac pump from the vacuum chamber The HVET uses a gate valve for this purpose The gate valve is the most popular choice for this application due to its high conductance 100 V4 – Foreline Valve • • • The foreline valve isolates the high vac pump from the roughing line The HVET uses an angle seat design with a manual handwheel Be sure to always fully open or close the valve 101 28 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 P2 – High Vac Pump • • • The high vacuum pump is used to remove gases from the vacuum chamber at pressures below the cross over pressure The HVET has a turbo pump for this purpose A turbo pump must be backed up by a roughing pump which is connected by the foreline 102 G2 – High Vac Gauge • • • The high vac gauge is useful for measuring pressures in the high vacuum range The HVET uses an Ion Gauge to measure the base pressure of the system <10-3 Torr The ion gauge can only be used in the high vacuum range. Be sure to shut it off before venting to atmosphere 103 29 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 High Vacuum Pump Down START BY ROUGH PUMPING THE TURBO PUMP DOWN (NOMINALLY 200 MTORR) VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 CLOSED P1 ON V3 CLOSED V4 OPEN P2 ON G2 OFF 106 High Vacuum Pump Down CLOSE FORELINE VALVE V4. ROUGH PUMP TO CROSSOVER PRESSURE (<200MT) VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 OPEN P1 ON V3 CLOSED V4 CLOSED P2 ON G2 OFF 107 30 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 High Vacuum Pump Down CLOSE ROUGH VALVE VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 CLOSED P1 ON V3 CLOSED V4 CLOSED P2 ON G2 OFF 108 High Vacuum Pump Down OPEN FORELINE VALVE VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 CLOSED P1 ON V3 CLOSED V4 OPEN P2 ON G2 OFF 109 31 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 High Vacuum Pump Down OPEN HIGH VAC VALVE VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 CLOSED P1 ON V3 OPEN V4 OPEN P2 ON G2 OFF 110 High Vacuum Pump Down TURN ON HIGH VAC GAUGE VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 CLOSED P1 ON V3 OPEN V4 OPEN P2 ON G2 ON 111 32 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 High Vacuum Venting TURN OFF HIGH VAC GAUGE VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 CLOSED P1 ON V3 OPEN V4 OPEN P2 ON G2 OFF 112 High Vacuum Venting CLOSE HIGH VAC VALVE VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 CLOSED P1 ON V3 CLOSED V4 OPEN P2 ON G2 OFF 113 33 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 High Vacuum Venting CLOSE FORELINE VALVE VC P1 P2 • • • • • • • • VC CLOSED V2 CLOSED V1 CLOSED P1 ON V3 CLOSED V4 CLOSED P2 ON G2 OFF 114 High Vacuum Venting OPEN VENT VALVE VC P1 P2 • • • • • • • • VC CLOSED V2 OPEN V1 CLOSED P1 ON V3 CLOSED V4 CLOSED P2 ON G2 OFF 115 34 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 VACUUM TECHNOLOGY 2293 VACUUM ANALYSIS & TROUBLESHOOTING Troubleshooting INTRODUCTION TO TROUBLESHOOTING 118 Troubleshooting is: • A systematic problem-solving process used to correct issues with complex systems • An iterative, trial-and-error process repeated until the issue is fixed. • Typically moves from common, known causes to the more complex diagnosis • A skill that needs to be practiced! Q: WHAT IS TROUBLESHOOTING? 119 35 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Troubleshooting Process • Gather Information • Describe the Problem • Determine the Most Probable Cause • Create a plan of action and test a solution • Implement the solution • Analyze the Results • Document the Process 120 • Safety is the state of being relatively free from harm, danger, or injury. • Edison was the person who transitioned vacuum technology from a curiosity to an industrial process • Theory is useful because it gives us clues on how to design and operate our equipment • Troubleshooting is both a skill and a process used to correct issues associated with complex processes 121 36 Session 1 - Transition from Viscous to Molecular Flow 1/12/2023 Fist to Five Vote How did Today Go? Terrible! Terrific! 122 37