Soran-University Faculty of engineering Chemical department Viscometer Prepared By Supervised By Huda Muslih Qadir proff. Ibtisam kama M.Widad and M.Maryam Table of Contents Introduction ................................................................................ 2 Materials , Equipment’s .............................................................. 4 procedure .................................................................................... 5 Calculation.................................................................................. 6 Data ............................................................................................ 7 Result .......................................................................................... 8 Discussion ................................................................................. 8 Conclusion .................................................................................. 9 Reference .................................................................................. 10 Table Of Figure Figure 1 4 Figure 2 4 Figure 3 4 Figure 4 4 Figure 5 4 Figure 6 4 Figure 7 6 Figure 8 6 1 Aim In this experiment we are going to use a viscometer for different liquids to find time for each liquid Measuring viscosity be viscometer Introduction A viscometer is a tool that is used to measure the viscosity of a material. By measuring the viscosity, the viscometer is able to quantify the thickness or the amount of internal friction of a material. During the test, the fluid material and the test equipment are brought into contact with one another and the drag is used in the viscosity calculation. Viscometers are instruments that measure the fluid flow and viscosity of liquids. The viscosity of a liquid can affect its performance, whether this is pumping or piping it, or how it performs for dipping and coating. What is Viscosity? Viscosity is the measure of how resistant a material is to motion when you apply force to it. For example, if you squeeze a tube of toothpaste, how easily does the contents There is a formula for measuring viscosity: Viscosity = sheer stress/shear rate. 2 Kinematic Viscosity Kinematic viscosity is the ratio of - absolute (or dynamic) viscosity to density - a quantity in which no force is involved. Kinematic viscosity can be obtained by dividing the absolute viscosity of a fluid with the fluid mass density like ν=μ/ρ Dynamic Viscosity Dynamic viscosity is the force needed by a fluid to overcome its own internal molecular friction so that the fluid will flow. The units of dynamic viscosity are: Force / area x time The Pascal unit (Pa) is used to describe pressure or stress = force per area This unit can be combined with time (sec) to define dynamic viscosity. 3 Materials. Crude Kerosene, Water Equipment’s Graduation cylinder Funnel Viscometer Thermometer Stopwatch Pycnometer Figure 1 Figure 4 Figure 3 Figure 2 Figure 5 F i g u r e 1 Figure 6 4 Procedure (about what were we doing from lab) First we need to prepare the laboratory balance, and the number on balance must be zero. We bring the pycnometer and by laboratory balance we weight it, and should be empty when measuring on the balance and we will get the weight of the pycnometer in grams We found weight (mass) for each liquid for each liquids by this equation: First brought the viscometer Then we put some of the water in the graded cylindar Then we put the water in the viscometer a little bit and blow it on one side to rise on the side to the specified location We pushed and we use our breath to pushed harder to in order the liquid rise up to upper mark and the liquid rise up over the upper mark The are two things of the viscometer • Upper mark indicating where sample is moved to by suction • Lower marl representing original position which sample returns to when suction force is released We should reduce the liquid point that is more than the right point It can not be one level We stop pushing the liquid get to the lower mark After that We find the time by viscometer 5 Figure 7 Figure 8 Calculation : Volume of pycnometer :50mL Temperature:21℃ 11.75+12.25+12.34 𝜇 water = 3 =12.11s 15.67+15.34+15.43 t c.kerosene = 3 =15.4 𝜇 c.kerosene =? P water =? Pc.kerosene =? 6 For density: (m)liquids =∆𝑚 − 𝑒𝑚𝑝𝑡𝑦 𝑚𝑎𝑠𝑠 𝑜𝑓 𝑝𝑦𝑐𝑛𝑜𝑚𝑒𝑡𝑒𝑟 ∆𝒎 𝒈 No m empty gr M liquid gr P 𝒈𝒓 𝒄𝒎𝟑 water 83.5 33.3 50.2 1.004 Crude 73.1 33.3 39.8 0.796 kerosene V =C .t …………………………… (1) 𝜇 V = ………………………………..(2) 𝑝 From (1) and (2) we found : 𝑝 2𝑡 2 𝜇2 = 𝜇1 𝑝 1𝑡1 ………………….(3) We use this equationto find viscosity crude kerosene : 𝑝 2𝑡 2 𝜇2 = 𝜇1 𝜇 𝑝 1𝑡1 1 P 1 t1 𝜇2 𝜇2 is viscosity of water =0.89 mpa.s is density of water p2 is flow time of water t2 is viscosity of crude kerosene is density of crude kerosene is flow time of water 0.89∗0.796∗15.48 1.004∗12.11 = 0.902 mpa.s Data 𝒈𝒓 liquid density ( water 1.004 𝒄𝒎𝟑 ) time (s) dynamic viscosity (mpa.s) 12.11 s 0.89 mpa.s 7 crude kerosene 0.796 15.48 s 0.902 mpa.s 8 Result In this data above we found viscosity of crude kerosene and also need a density both a material by pycnometer we need of them Some people put have a time even time was a different after that we find the average time We can find them by ostwald viscometer, To determine the relative viscosity of given liquid using Ostwald’s viscometer appear that viscosity kurde kerosene more than water because when density is increase the viscosity is decrease Discussion What is the relationship between viscosity and temperature What are the effects of temperature on viscosity In fluids the property of viscosity is due to the cohesive force or. intermolecular forces of attraction. More these forces more will be these molecules denying to flow. Hence more is the resistance to flow ,which results more viscosity. Now if u increase the temperature of any liquids the viscosity decreases. But if u consider gases then it's viscosity increases with increase in temperature, which has a cause. In case of liquids,with increase in temperature viscosity decreases But in case of gases vicsosity increases with increase in temperature There are two kinds of viscosity commonly reported, kinematic and dynamic. Dynamic viscosity is the relationship between the shear stress and the shear rate in a fluid. The Kinematic viscosity is the relationship between viscous and inertial forces in a fluid. 9 What are the error in viscometer? The error associated from misalignment towards the unbounded sides of the capillary (left to right) can be quite severe if the surface tension of the fluid (or lack thereof due to surface contaminates on the capillary cell walls) allow sample to "leak" out of the flow cell. Conclusion At this test we learned that how to determine the Measuring viscosity be viscometer We find the time by viscometer and find density by pycnometer, A viscometer ) is an instrument used to measure the viscosity of a fluid. For liquids with viscosities which vary with flow conditions We have compared between the speed of water oil and soap and we’ve realized that the speed of water is more than oil and soap and the speed of oil is more than the soap . 10 Reference : • https://www.machinerylubrication.com/Read/29451/a natomy-of-viscometer • https://www.corrosionpedia.com/definition/6089/visco meter • https://www.quora.com/What-is-the-relationshipbetween-viscosity-and-temperature • https://www.azom.com/amp/article.aspx?ArticleID=10 036 11