Abstract The 3-point bend test is a standard test used to study the flexural properties of materials when subjected to loads. For this experiment, three specimens of different materials (a carbon fiber nylon composite, a glass carbon fiber composite, and basswood) were subjected to a 3-point bend test to gather data on the stress and strain experienced by the materials. This data was then used to calculate the maximum shear stress, flexural strain at failure, modulus of rupture, flexural modulus, standard deviation of the stress, and the standard deviation of the strain. It was hypothesized that the rank of the materials from highest flexural modulus to lowest flexural modulus would be the carbon fiber nylon composite, the basswood, and then the glass fiber nylon composite. Our data, however, disproved this hypothesis, with the carbon fiber nylon composite being the highest, followed by the glass fiber nylon composite, and then the basswood with the lowest. Possible reasons for this incorrect hypothesis could be the quality of the lab equipment, human error, or the fact that the equations used come from the ASTM D790 document, which contains the standard for flexural properties of unreinforced and reinforced plastics and electrical insulating materials, while one of the materials is wood. ii Table of Contents Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Experimental Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Materials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Testing Methodology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 2 3 Results and Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Calculation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Discussion and Errors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 5 8 Conclusion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 iii Introduction Understanding how, why, and when materials fail is imperative for designing any engineering structure. One important aspect of this understanding comes from flexural testing. Uniaxial tension and compression tests may not provide all of the information needed about a material’s behavior. As a material bends or flexes, the combination of forces and loads it is subjected to becomes complex and can experience tension, compression, and shear all at once [1]. The 3-point bend test is one method of flexural testing and allows for all of these forces to be taken into consideration. Because of this, bend testing is often used to see how materials will react to realistic loading situation, especially if a material will be used in a support structure [1]. In a 3-point bend test, a rectangular cross-section of a material rests on two supports and is loaded midway between the supports with a loading nose [2]. The specimen is then deflected until either rupture occurs or a maximum strain of 5% is reached, whichever occurs first [2]. From this test, material properties such as flexural stress, strength, strain, and modulus and modulus of rupture can be calculated [2]. This data can be useful for quality control and specification purposes [2], and, in wooden samples, instigating the effect of parameters that might influence the properties of the material, such as moisture content, temperature, knot size and location, or slope of the grain [3]. The objective of this experiment is to conduct a flexural test, using the 3-point bend test method, on wooden beam and composite specimens and determine the flexural strength, maximum shear stress at failure, flexural strain at failure, modulus of rupture, and flexural modulus. The materials of the three specimen used in this experiment will be basswood, a glass fiber nylon composite, and a carbon fiber nylon composite. Before the 3-point bend test was performed, a hypothesis was formed regarding the flexural modulus of the materials. The flexural modulus, also call the modulus of elasticity in bending, is the ratio, within the elastic limit, of stress to corresponding strain. Based on available data on the materials, the material with the highest flexural modulus will be the carbon fiber nylon composite [4], followed by the basswood [5], followed by the glass fiber nylon composite with the lowest flexural modulus [6] . 1 Experimental Methods Materials The materials utilized in this flexural test were a glass fiber nylon composite, a carbon fiber nylon composite, and one wooden beam composed of basswood. These specimens are pictured below in Figure 1. Figure 1: Labeled specimen used in the experiment. The initial dimensions of length and width were measured using a Vernier caliper. The measurements for width and thickness were taken at 3 different points near the midpoint on each specimen. Next, the specimen dimensions measured were averaged for approximate dimensions that were the input into the software. All the measurements were taken using mm and are shown in Figure 2 and Table 1 below. 2 Figure 2: Dimensions of the specimen. Table 1: Average Specimen Dimensions Dimension (mm) Carbon Fiber Glass Fiber Basswood Width Thickness 12.59 3.19 12.56 3.21 9.43 9.43 Testing Methodology The mechanical test frame utilized for the tensile testing is the Instron 1321 Servohydraulic Test System with a 100kN load cell that was fitted with a 3-point bend test fixture. A specimen was then centered horizontally on the supports of the 3-point bend test fixture as exemplified in the Figure 3. The span of the support was 65 mm. 3 Figure 3: Specimen centered on the supports. Once the specimen was accurately placed, the average dimensions that were previously measured were then entered into the computer software. The machine was then turned on to begin the load application of 3mm/min. While the load was applied, the computer recorded the load and displacement data. The experiment concluded once the specimen bent and failed. This procedure was repeated for the other two test specimens. 4 Results and Discussion Calculation The data collected from the experiment was formatted into a spreadsheet for each material specimen recording the load and the amount of elongation experienced by the specimen at each time step of 0.1 seconds. To compare each material specimen, the results were used to calculate the bending stress strain curve for each material. Using the equation below to calculate bending, or flexural, stress: σf = 3P L 2bd2 (1) Where σf is the flexural stress, P is the load applied to the specimen measured in Newtons, L is the support span in mm, b is the width of the beam in mm, and d is the thickness of the beam in mm. For the Basswood beam specimen, the width and the thickness were both measured to be 9.43 mm. The value for L, the support span, was 65 mm. Therefore, using Equation (1) from above for a 50 N applied load, the flexural stress can be calculated to be 5.81 MPa as seen below. σf = 3(50)(65) = 5.81M P a 2(9.43)(9.43)2 (2) To calculate flexural strain the following equation was used f = 6Dd L2 (3) Where f is flexural strain, D is the deflection or extension measured in mm, L is the support span in mm, and d is the thickness of the beam in mm. Equation (1) for bending stress and Equation (3) for bending strain were obtained from source [2] and were used to produce the stress-strain curve which can be seen in Figure 4. 5 350 300 Carbon Fiber Fiberglass Stress (MPa) 250 Basswood 200 150 100 50 0 0 0.02 0.04 0.06 0.08 0.1 0.12 Strain Figure 4: The bending stress vs strain graph. From the stress and strain curve, the flexural stress and strain at failure can be collected. To obtain the maximum shear stress the following equation was used 3P (4) 4bd Where P is the applied load in Newtons, b is the width of the beam in mm, and d is the thickness of the beam in mm. To find the modulus of rupture Equation (5) was used to first find Mmax , which is required to solve Equation (6) for modulus of rupture. Pmax L Mmax = (5) 4 Where Mmax is the maximum moment, Pmax is the maximum applied load before failure in Newtons, and L is the support span in mm. Taking the calculated value for Mmax , modulus of rupture was found using Equation (6) τmax = σ= Mmax c I (6) Where Mmax is the maximum moment, c is the distance from the neutral axis, and I is the moment of inertia of the cross-sectional area of the beam. This value of σ, or 6 modulus of rupture, was compared to the maximum bending stress for each specimen seen in Figure 4 and confirmed to be the same value. The last value calculated for this experiment was the flexural modulus using the following equation EB = L3 m 4bd3 (7) where EB is the modulus of elasticity in bending or the flexural modulus, L is the support span in mm, m is the slope of the linear section of the stress strain curve, b is the width of the beam in mm, and d is the thickness in mm. The calculated values can be found in Table 2. Table 2: Calculated Result Values Values and Units Glass Fiber Carbon Fiber Basswood Maximum Shear Stress (MPa) Flexual Strain at Failure (mm/mm) Modulus of Rupture (MPa) Flexural Modulus (MPa) Standard Deviation of Stress (MPa) Standard Deviation of Strain (MPa) 5.51 0.0254 223.19 1532929 72.68 0.0080 7.80 0.0207 318.06 2745621 99.59 0.0069 3.06 0.0680 42.13 5197.99 11.86 0.033 The standard deviations for stress and strain were calculated using Equation (8) from source [2] s s= (ΣX 2 − nX̂ 2 ) (n − 1) (8) where s is the estimated standard deviation, X is the value at a single point, n is the number of data points being considered, and X̂ is the mean of values in the set of points. This equation can be used to find the standard deviation for any calculated values within a larger data set. 7 Discussion and Errors The material with the highest flexural modulus was the carbon fiber composite followed by the glass fiber composite. The basswood had the lowest flexural modulus. This differs from the hypothesis developed at the beginning of the experiment in that the hypothesis conjectured that the glass fiber would have the lowest flexural modulus instead of the basswood. One possible source of error were the calculations conducted using the raw data. The equations that were used came from the ASTM D790 (Source [2]) which is the standard test methods for flexural properties of unreinforced and reinforced plastics and electrical insulating materials. This could have contributed to the significantly lower flexural modulus for the basswood because it is a wood which is neither a plastic nor an electrical insulating material. The physical flexural response of all three materials was similar. The carbon fiber composite, the glass fiber composite, and the basswood all warped under the stress of the load until they reached their yielding point, where they then experienced a fracture at the point the load was being applied as exemplified in Figure 5. One difference between the materials is that the basswood specimen compressed slightly at the point of the load before beginning to bend. Figure 5: Fractured materials. It should also be noted that the calculated values for the modulus of rupture was 8 similar in value to the automated result values from the computer generated data. Meanwhile, the flexural modulus calculated values had a much larger difference in comparison to the automated result values from the computer generated data. This error can be attributed to calculation errors resulting from human error or due to the precision, or lack thereof, of the computer software/testing machine. The automated result values that were computer generated from the software are listed in Table 3 below. Table 3: Automated Result Values Values and Units Modulus of Rupture (MPa) Flexural Modulus (MPa) Glass Fiber Carbon Fiber 226.4 20477 9 318.3 29290 Basswood 43.25 2460 Conclusion This experiment was conducted to test the flexural strengths of three different material specimens. The three-point bend test was used to calculate the flexural stress and the flexural strain of each specimen, maximum shear stress at failure, the modulus of rupture, and the flexural modulus. From these calculations, it was concluded that the carbon fiber nylon composite had the highest maximum shear stress, modulus of rupture, and flexural modulus, and the lowest flexural strain at failure while the basswood had the lowest maximum shear stress, modulus of rupture, and flexural modulus, and the highest flexural strain at failure. The hypothesis stated that the material with the highest flexural modulus would be be the carbon fiber nylon composite, followed by the basswood, followed by the glass fiber nylon composite. Based on results previously discussed, however, the order was actually the carbon fiber nylon composite, followed by the glass fiber nylon composite, followed by the basswood. The reason for this difference is likely due to calculation errors, quality of lab equipment, or, as previously discussed, the equation used to solve for the flexural modulus. 10 References [1] “What is Bend Testing?” Instron. [2] “Standard Test Methods for Flexural Properties of Unreinforced and Reinforced Plastics and Electrical Insulating Materials,” ASTM International , 2010. [3] “Standard Test Methods for Mechanical Properties of Lumber and Wood-Base Structural Material,” ASTM International , 2010. [4] Plasticomp, “Product Data Sheet for Complet LCF30-PA6,” 2014. [5] “American Basswood Wood,” MatWeb Material Property Data. [6] PlastiComp, “Product Data Sheet for Complet LGF30-PA6,” 2014. 11