Surface and Coatings Technology 125 (2000) 45–48 www.elsevier.nl/locate/surfcoat Laser cladding of turbine blades L. Shepeleva a, *, B. Medres a, W.D. Kaplan a, M. Bamberger a, A. Weisheit b a Department of Materials Engineering, TECHNION - Israel Institute of Technology, Technion City, 32000 Haifa, Israel b Institute fur Werkstoffkunde und Werkstofftecknik, Agricolastrabe 6, D-38678 Clausthal-Zellefreld, Germany Abstract A comparative study of two different techniques for the application of wear-resistant coatings for contact surfaces of shroud shelves of gas turbine engine blades (GTE ) has been conducted. Wear-resistant coatings were applied on In713 by laser cladding with direct injection of the cladding powder into the melt pool. Laser cladding was conducted with a TRUMPF-2500, CW-CO 2 laser. The laser cladding was compared with commercially available plasma cladding with wire. Both plasma and laser cladded zones were characterized by optical and scanning electron microscopy. It was found that the laser cladded zone has a higher microhardness value (650–820 HV ) compared with that of the plasma treated material (420–440 HV ). This is a result of the significant reduction in grain size in the case of laser cladding. Unlike the plasma cladded zones, the laser treated material is free of micropores and microcracks. © 2000 Elsevier Science S.A. All rights reserved. Keywords: Laser cladding; Plasma cladding; Shroud shelve; Turbine blade 1. Introduction The operational stability of turbine blades with shroud shelves depends on the wear resistance of the shroud shelves. [1,2]. It is known that during operation, as a result of dynamic contact as well as vibration and heat, the contact surfaces of shroud shelves undergo intensive wear. This leads to the formation of a gap between them and, as a result, increases the amplitude of alternating loads on the blade critical cross-section [2]. Thus, the wear of the blade shroud shelves’ contact area determines the overall service life of the GTE [2,3]. To increase the service life of turbine blades with shroud shelves, plasma cladding of cobalt stellites supplied in the form of wire is used. These materials exhibit sufficiently high tribological properties [1,3]. In spite of a significant increase in wear resistance for cladded blades (compared with non-cladded blades) plasma cladding technology has some essential drawbacks: $ plasma cladding is performed manually, and does not provide the required uniformity of the coating; $ the layer contains cracks and pores both at the layer– substrate interface and in its entire volume; $ the plasma cladded layer has a sharp boundary with * Corresponding author. the substrate, where high stress concentration leads to the formation of cracks and pores under loading; and $ plasma cladding increases the hardness of the coating by 20– 40 HV above that of the substrate. These limitations can be overcome by applying coating techniques, such as laser cladding [3–5]. This paper presents a comparison between the microstructure and properties of plasma cladding in which the clad material is supplied via a wire, and laser cladding with direct injection of cladded powder into the melt pool. 2. Experimental methods Commercially available blades with plasma cladding were investigated, as well as wear-resistant coatings produced by laser cladding, using the method of direct injection of cladding powder into the melt pool. All tests were performed with alloy In713. Laser cladding was conducted with a TRUMPF-2500 CW-CO laser operated at a laser power density in the 2 range of 2.8×104–3.6×104 W/cm2 and scanning velocities of 0.5–0.7 cm/s. The powder feed rate was 0.015– 0.02 g/s. Both plasma and laser cladding zones were 0257-8972/00/$ - see front matter © 2000 Elsevier Science S.A. All rights reserved. PII: S0 2 5 7- 8 9 7 2 ( 9 9 ) 0 0 60 3 - 9 46 L. Shepeleva et al. / Surface and Coatings Technology 125 (2000) 45–48 Fig. 1. SEM micrograph of the plasma cladded zone and its interface with the substrate. Fig. 3. (a) SEM micrograph of a laser cladded substrate region. (b) EDS line-scan analysis of the major elemental distribution across the laser clad–substrate interface. Fig. 2. EDS line-scan analysis of the major elemental distribution across the plasma clad–substrate interface characterized by optical and scanning electron microscopy (SEM ). 3. Results and discussion 3.1. Plasma cladding zone The plasma-cladding zone and its interface with the substrate are shown in Fig. 1. In this figure one can see that the plasma cladded zone is characterized by the presence of microcracks and pores, which might adversely affect the wear resistance of contact surfaces of blades [2]. The low content of Ni, which originates from the substrate, in the cladding is evident in Fig. 2. From Figs. 1 and 2 it can be concluded that the boundary between the clad and substrate is very sharp and contains a large quantity of microcracks and pores. The sharp boundary can be correlated with the processing characteristics — e.g. the relative size of the plasmaheating source compared with that of the wire and the 47 L. Shepeleva et al. / Surface and Coatings Technology 125 (2000) 45–48 Table 1 The microhardness at various locations in the laser cladded blades by various power densities Sample group 1 2 3 Laser treatment conditions ×104 ( W/cm2) Microhardness (HV ) Base Boundary Cladded layer 3.6 3.2 2.8 400 400 400 572 522 464 824 680–724 542 in the melt due to the intensive mixing. The low viscosity of the melt bath and the directional dendritic growth, which nucleated on the cold substrate, result in the crack- and pore-free interface [6 ] seen in Fig. 4. Table 1 presents the microhardness at various locations in the laser treated blades by various power densities. The microhardness for both interface and laser cladded zones increase as a function of laser radiation power density. The laser cladded zones reveal a significant grain refinement ( Fig. 5) which raises their microhardness values. Fig. 4. EDS line-scan analysis of concentration changes of basic elements of a laser cladded layer and substrate in interdendritic regions. substrate. Therefore, the melted wire, which spreads on the unmelted surface of the substrate, is not sufficiently overheated to ensure mixing and/or mutual dissolution of elements from both components. This is reflected in the concentration profiles seen in Fig. 2. The porosity seen in Fig. 1 results from gas entrapped in the high viscosity melt [6 ]. The microhardness of the plasma cladded layer is 420–440 HV. The microhardness of the substrate is 400 HV. 4. Conclusions 1. Laser cladding of the contact surfaces of shroud shelves by direct powder injection provides a cladding layer with a higher hardness than plasma treated surfaces. 2. Laser cladded zones, unlike the plasma treated surfaces, are free of microcracks and pores. 3. The laser cladded zone has a smooth interface with the substrate, which prevents stress concentration at the clad–substrate interface during operation. 3.2. Laser cladded Zone The laser cladded zone has a uniform microstructure with a smooth boundary between the cladded layer and the substrate ( Fig. 3(a) and (b)). The crack- and pore-free interface between the laser cladded zone and the substrate, at higher magnification, and the enrichment of the cladding with Ni from the substrate are evident in Fig. 4. The formation of a smooth interface by laser cladding can be explained by the fact that the laser beam causes significant heating of the injected powder and essential overheating of the molten surface of the substrate, and hence the hot particles melt on hitting the melt bath. The high temperatures prevail in the melt and the gradient in the surface tension throughout this melt pool result in dissolution of constituents from the substrate, and their distribution Fig. 5. SEM micrograph of a laser clad–substrate interface. 48 L. Shepeleva et al. / Surface and Coatings Technology 125 (2000) 45–48 Acknowledgement Dr. B. Medres and Dr. L. Shepeleva acknowledge the Center for Absorption in Science, Ministry of Immigrant Absorption State, Israel for its financial support. References [1] S.T. Kyshkin, A.V. Logunov et al., Scientific background for alloying of heat-resistant nickel alloys, Aviazionnie Materialy 00 (1987) 387. [2] A.I. Cosov, B.S. Medres et al., Laser alloying of contact surfaces of GTE blades, Aviazionaya Promishlennost Mag. 2 (1984) 8. [3] A.A. Soloviov, B.S. Medres et al., Laser alloying of GTE blades made of EP-109 alloy, Reports of 1st All-Union Conference on Laser Metallurgy and Laser-plasma Treatment, USSR, IMET, Academy of Sciences of the USSR, Moscow, 1984, p. 98. [4] W.M. Steen, Laser Material Processing, Springer-Verlag, 1991, p. 266. [5] M. Bamberger, W.D Kaplan, B. Medres, L. Shepeleva, Calculation of processes parameters for laser alloying and cladding, J. Laser Applications 10 (1) (1998) 29–33. [6 ] M. Boaz, M. Bamberger, G. Revesz, Laser alloying of a plasma sprayed WC/Co layer to enhance wear properties, Surf. Coat. Technol. 42 (1990) 175–186.