EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 2 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL REVISION DESCRIPTION SHEET Rev. Para. 0 Revision Description For Review Hold No. Para. 1 2.3.1 Vendor supplied MSDS of MDEA 2 2.3.2 Vendor supplied MSDS of Antifoam 3 2.3.3 Vendor supplied MSDS of Corrosion Inhibitor 4 2.3.4 Vendor supplied MSDS of Caustic 5 2.3.5 Vendor supplied MSDS of Biocide 6 2.3.6 Vendor supplied MSDS of Scale Inhibitor 7 2.3.7 Vendor supplied MSDS of Oxygen Scavenger 8 2.3.8 Vendor supplied MSDS of Complex Product 9 4.5.4 5.4.3 Instrument Air Compressor loading and unloading pressure set points/lead/lag compressor loading and unloading pressure set points 10 4.11.3.1 4.11.3.2 4.11.3.3 7.2.6 Demineralized Water Package operating set point/alarm and trip set points 11 4.13.3.1 4.13.3.2 4.13.3.4 4.13.3.5 4.13.3.6 4.13.3.7 7.2.8 Steam Generation Package: operating set point/alarm and trip set points Description of Hold EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 3 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL CONTENTS SECTION I 1.1 1.2 1.3 1.4 OBJECTIVE ............................................................................. 11 ABBREVIATION ......................................................................... 11 UNITS OF MEASUREMENT ............................................................. 12 GENERAL DESCRIPTION ............................................................... 13 SECTION II 2.1 2.2 2.3 2.3.1 2.3.2 2.3.3 2.3.4 2.3.5 2.3.6 2.3.7 2.3.8 2.3.9 OVERVIEW OF SRU UPGRADE FACILITIES ........................ 20 PROCESS ................................................................................ 21 SRU Upgrade Facilities Overview ................................................... 21 Acid Gas Enrichment Unit (AGEU) .................................................. 21 Sulphur Recover Unit Process Description ......................................... 24 Tail Gas Treatment Unit (TGTU) .................................................... 26 Tail Gas Incinerator ................................................................... 29 Amine Drain System .................................................................. 31 NEW UTILITY FACILITIES.............................................................. 33 Instrument and Plant Air ............................................................. 33 Demineralised Water System ........................................................ 35 Sea Cooling Water System ........................................................... 37 Boiler Feed Water System ........................................................... 39 Steam Generation Package 6848-A-02A/B/C...................................... 41 Fuel Gas System ....................................................................... 44 Effluent and Waste Water Treatment Unit ........................................ 46 FIRE WATER & DELUGE SYSTEM ..................................................... 48 Fire Water System .................................................................... 48 Deluge System ......................................................................... 48 SECTION IV 4.1 4.1.1 4.1.2 4.2 4.2.1 HEALTH SAFETY AND ENVIRONMENT ............................ 15 HEALTH, SAFETY AND ENVIRONMENT (HSE) ....................................... 16 LEAKAGE OF ACID GAS ................................................................ 16 HAZARDS IN HANDLING CHEMICALS ................................................. 17 MDEA .................................................................................... 17 Antifoam ............................................................................... 17 Corrosion Inhibitor .................................................................... 17 Caustic .................................................................................. 17 Biocide .................................................................................. 17 Scale inhibitor ......................................................................... 17 Oxygen Scavenger ..................................................................... 17 Complex Product ...................................................................... 17 Hydrogen Sulphide .................................................................... 17 SECTION III 3.1 3.1.1 3.1.2 3.1.3 3.1.4 3.1.5 3.1.6 3.2 3.2.1 3.2.2 3.2.3 3.2.4 3.2.5 3.2.6 3.2.7 3.3 3.3.1 3.3.2 INTRODUCTION ...................................................... 10 PROCESS AND CONTROL DESCRIPTION.......................... 50 ACID GAS ENRICHMENT UNIT (AGEU) ............................................... 51 Equipment Specification ............................................................. 51 AGEU PROCESS DESCRIPTION & CONTROL ......................................... 58 SULPHUR RECOVERY UNIT ........................................................... 75 Equipment Details .................................................................... 75 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 4 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.2.2 4.2.3 4.2.4 4.3 4.3.1 4.3.2 4.3.3 4.4 4.4.1 4.4.2 4.5 4.5.1 4.5.2 4.5.3 4.5.4 4.6 4.6.1 4.6.2 4.6.3 4.7 4.7.1 4.7.2 4.8 4.8.1 4.8.2 4.8.3 4.9 4.9.1 4.9.2 4.9.3 4.10 4.10.1 4.10.2 4.11 4.11.1 4.11.2 4.11.3 4.12 4.12.1 4.12.2 4.12.3 4.13 4.13.1 4.13.2 4.13.3 Revamped Claus Unit Process Chemistry .......................................... 77 Revamped Claus Unit Process Description ......................................... 78 Sulphur Recovery Unit Process Control ............................................ 79 TAIL GAS TREATMENT UNIT .......................................................... 89 Tail Gas Treatment Unit Equipment Specification ............................... 89 Tail Gas Treatment Unit (TGTU) Process Description............................ 92 Tail Gas Treatment Unit Control Description ..................................... 94 INCINERATOR ......................................................................... 102 Equipment Specification ............................................................ 102 Process Description and Control ................................................... 103 INSTRUMENT AIR PACKAGE.......................................................... 107 Instrument Air Compressor Package ............................................... 107 Instrument Air Dryer Package ...................................................... 108 Instrument Air Package Description ............................................... 109 Instrument Air Package Control Description ..................................... 110 EFFLUENT & WASTE WATER TREATMENT ......................................... 112 Equipment Specification ............................................................ 112 Effluent and Waste Water Treatment Process Description .................... 116 Effluent & Waste Water Treatment Control Description ....................... 118 LP FUEL GAS .......................................................................... 123 Equipment Specification ............................................................ 123 Fuel Gas System Process Description.............................................. 123 SEA COOLING WATER SYSTEM ...................................................... 125 Equipment Specification ............................................................ 125 Sea Cooling Water System Process Description .................................. 126 Sea Cooling Water Control .......................................................... 127 Electrochlorination Package ........................................................ 128 Equipment Specification ............................................................ 128 Electro Chlorination System Description ......................................... 131 Electro chlorination Package Control ............................................. 132 NGL-4 SEA WATER FILTERS.......................................................... 133 Equipment Specification ............................................................ 133 NGL-4 Sea Water Filters S-8840A/B Description ................................. 134 DEMINERALISED WATER SYSTEM ................................................... 134 Equipment specification ............................................................ 134 Demineralised Water System Process Description............................... 138 Demineralised Water System Control description ............................... 141 BOILER FEED WATER DEAERATOR SYSTEM ........................................ 144 Equipment specification ............................................................ 144 Boiler Feed Water De-aerator Description ....................................... 146 Boiler Feed Water Deaerator Control Description ............................... 148 STEAM GENERATION PACKAGE ..................................................... 151 Equipment Specifications ........................................................... 151 Steam Generation Package Process Description ................................. 154 Control Description .................................................................. 165 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 5 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.14 4.14.1 4.14.2 4.14.3 4.14.4 4.14.5 4.14.6 4.14.7 4.14.8 CHEMICAL INJECTION SYSTEMS ..................................................... 177 Antifoam Injection Package 9103-A-11 ........................................... 177 Caustic Injection Package 9103-A-13.............................................. 179 Corrosion Inhibitor Injection Package 9103-A-12 ................................ 181 Complex Product Injection Package 6834-A-09 .................................. 184 Oxygen Scavenger Injection Package 6834-A-09................................. 187 Biocide Injection Package 6932-A-06.............................................. 189 Scale Inhibitor Injection Package 6932-A-07 ..................................... 192 Catalyst Injection Package 9101-A-01............................................. 195 SECTION V 5.1 5.2 5.3 5.3.1 5.4 5.4.1 5.4.2 5.4.3 5.4.4 5.4.5 5.4.6 5.5 5.5.1 5.6 5.6.1 5.6.2 5.7 5.7.1 5.7.2 5.7.3 5.7.4 5.7.5 5.7.6 5.8 5.8.1 5.8.2 5.9 5.9.1 PRE-REQUISITE FOR START-UP ................................... 198 GENERAL .............................................................................. 199 INTERFACE ACTIVITIES............................................................... 200 START-UP OF UTILITIES.............................................................. 202 Start-up Sequence ................................................................... 202 Instrument Air/Plant Air System ................................................... 202 Pre Start-up Checks.................................................................. 202 Instrument Air compressor Start-up ............................................... 203 Start-up permissive conditions: .................................................... 204 Instrument Air Dryer start-up ...................................................... 208 Instrument Air Dryer Start-up Checks ............................................. 208 Dryer Start ............................................................................ 208 Nitrogen system ...................................................................... 211 Lining up of Nitrogen from existing system to the New Distribution Header 211 Drinking water system ............................................................... 212 Lining up of Drinking Water to existing network ................................ 212 Lining up of Drinking Water to DMW Package .................................... 212 Effluent & Waste Water Treatment system ...................................... 213 Lining up of Waste Water Degasser 6922-V-07 ................................... 213 Lining up of Sour Water Stripper 6922-C-01...................................... 214 Lining up of Stripper Overhead Circulation Pump 6922-P-11A/B ............. 215 Lining up of Sour Water Stripper overhead Sour Gas ........................... 215 Pressurising Waste Water Degasser 6922-V-07 with Nitrogen ................. 215 Lining up of Sour Water Stripper Reboiler ........................................ 216 Flare system .......................................................................... 217 Start-up of LP Flare System ........................................................ 217 LP ACID GAS FLARE SYSTEM......................................................... 218 Fuel Gas System ...................................................................... 219 Line-up Fuel Gas from the Existing 1st Stage Booster Compressor 6701-K-10/20/30 in NGL-3 .......................................................... 219 5.10 Sea cooling water system ........................................................... 220 5.10.1 Pre-start up checks .................................................................. 220 5.10.2 Initial Starting and Lining Up of Sea Cooling Water ............................. 221 5.11 Electro Chlorination Package Start-up ............................................ 221 5.11.1 Normal start-up of Electro Chlorination Plant: .................................. 222 5.12 Chemical Injection System ......................................................... 224 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 6 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.12.1 5.12.2 5.12.3 5.12.4 5.12.5 5.12.6 5.12.7 5.12.8 5.13 5.13.1 5.13.2 5.13.3 5.14 5.14.1 5.14.2 5.15 5.15.1 5.15.2 5.15.3 5.15.4 5.15.5 5.15.6 5.15.7 5.15.8 5.15.9 5.16 5.17 Complex Product Injection Package (6834-A-09) ................................ 224 Oxygen Scavenger Injection Package (6834-A-09)............................... 225 Biocide Injection Package (6932-A-06)............................................ 226 Scale Inhibitor Injection Package (6932-A-07) ................................... 227 Catalyst Injection Package (9101-A-01)........................................... 228 Antifoam Injection Package (9103-A-11) ......................................... 229 Corrosion Inhibitor Injection Package (9103-A-12) .............................. 230 Caustic Injection Package (9103-A-13)............................................ 231 Demineralized Water System ....................................................... 231 Demineralized Water Unit Start-up ............................................... 231 Demineralized Water Unit Sequence .............................................. 235 Neutralization Pit .................................................................... 238 Boiler Feed Water Deaerator system .............................................. 241 Lining up of Steam Condensate Flash Drum 6834-V-05 ......................... 241 Lining up of BFW Deaerator Package 6834-A-08 ................................. 242 Steam Generation Package Start-up .............................................. 243 Checks for Start-up .................................................................. 243 Water Filling .......................................................................... 244 Fuel Gas Line-up ..................................................................... 245 FD Fan Start-up....................................................................... 245 Burner Start-up ....................................................................... 246 Boiler Normal Start-up .............................................................. 250 Start-up from Cold Condition (Manual Mode) .................................... 251 Start-up from Hot Condition........................................................ 254 Going On Line......................................................................... 254 LEAK CHECKING OF SYSTEMS ....................................................... 255 PURGING............................................................................... 256 SECTION VI 6.1 6.2 6.3 6.3.1 6.3.2 6.3.3 6.3.3.1 6.3.3.2 6.3.4 6.4 SECTION VII 7.1 7.1.1 7.1.2 7.1.3 7.1.4 7.1.5 START-UP OF PLANT .............................................. 258 GENERAL .............................................................................. 259 START-UP SEQUENCE ................................................................ 259 START-UP OF PROCESS .............................................................. 260 Start-up of Incinerator 9101-F-14.................................................. 260 Start-Up of Acid Gas Enrichment Unit ............................................ 267 Start-Up of Sulphur Recovery Unit................................................. 283 Start-up of Reaction Furnace (9101-F-01) Burner ............................... 283 Heating Up the System .............................................................. 290 Start-up of Tail Gas Treatment Unit .............................................. 304 RAMP UP OF PLANT LOAD ........................................................... 319 OPERATION & MONITORING ...................................... 320 PROCESS PLANT OPERATION AND MONITORING .................................. 321 Acid Gas Enrichment Unit ........................................................... 321 Sulphur Recovery Unit ............................................................... 326 Tail Gas Treatment Unit ............................................................ 331 Instrumentation ...................................................................... 337 Process On-Stream Analysis and Testing .......................................... 337 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 7 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7.1.6 7.2 7.2.1 7.2.2 7.2.3 7.2.4 7.2.5 7.2.6 7.2.7 7.2.8 Tail Gas Incinerator .................................................................. 339 UTILITIES .............................................................................. 341 Instrument Air & Plant Air .......................................................... 341 Effluent & Waste Water Treatment ............................................... 343 Fuel gas system....................................................................... 345 Sea Cooling Water System .......................................................... 345 Electro Chlorination Package....................................................... 346 DM Water Package ................................................................... 348 Boiler feed water system ........................................................... 351 Steam Generation .................................................................... 353 SECTION VIII START-UP AFTER EMERGENCY SHUTDOWN .................... 357 8.1 8.2 8.3 8.4 8.5 GENERAL .............................................................................. 358 Tail Gas Incinerator Restart ........................................................ 358 Acid Gas Enrichment Unit Restart ................................................. 358 Sulphur Recovery Unit Restart ..................................................... 359 TGTU Restart ......................................................................... 359 SECTION IX 9.1 9.1.1 9.1.2 9.1.3 9.1.4 9.2 9.2.1 9.2.2 9.2.3 9.2.4 9.2.5 9.2.6 9.2.7 PROCESS ............................................................................... 362 Incinerator ............................................................................ 362 Acid Gas Enrichment Unit ........................................................... 362 Sulphur Recovery Unit ............................................................... 364 Tail Gas Treating Unit ............................................................... 365 UTILITIES .............................................................................. 366 Instrument air package.............................................................. 366 Effluent & Waste Water Treatment Unit ......................................... 368 Electro Chlorination Package....................................................... 368 Chemical Injection Packages ....................................................... 369 DM Water Package ................................................................... 376 Boiler Feed Water System .......................................................... 376 Steam Generation Package ......................................................... 377 SECTION X 10.1 10.1.1 10.1.2 10.1.3 10.1.4 10.2 10.2.1 10.2.2 10.2.3 10.2.4 10.2.5 10.2.6 10.2.7 10.2.8 TROUBLE SHOOTING OPERATIONS.............................. 361 PLANNED SHUTDOWN ............................................. 380 Planned Shutdown - Process ........................................................ 381 TGTU Shutdown ...................................................................... 381 SRU Shutdown ........................................................................ 384 Acid Gas Enrichment Unit Shutdown .............................................. 386 Incinerator Shutdown................................................................ 387 UTILITIES .............................................................................. 389 Steam Generation Package Shutdown ............................................ 389 Boiler Feed Water System Shutdown .............................................. 390 DM water package Shutdown ....................................................... 391 Chemical Injection System Shutdown ............................................. 392 Electro Chlorination Package Shutdown .......................................... 395 Sea cooling water Shutdown ....................................................... 396 Fuel Gas system Shutdown.......................................................... 396 Effluent & Waste Water Unit Shutdown .......................................... 397 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 8 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10.2.9 Instrument air Shutdown ............................................................ 398 SECTION XI 11.1 11.2 11.2.1 11.2.2 11.2.3 11.2.4 11.3 11.3.1 11.3.2 11.3.3 11.3.4 11.3.5 11.3.6 11.3.7 11.3.8 11.3.9 11.4 11.4.1 11.4.2 11.4.3 11.4.4 11.4.5 11.4.6 SECTION XII 12.1 12.2 12.2.1 12.2.2 12.3 12.4 12.4.1 12.4.2 12.4.3 12.4.4 12.4.5 12.4.6 12.4.7 12.4.8 12.5 EMERGENCY SHUTDOWN ......................................... 400 GENERAL .............................................................................. 401 PROCESS ............................................................................... 403 Acid Gas Enrichment Unit ........................................................... 403 Sulphur Recovery Unit ............................................................... 411 Tail Gas Treatment Unit ............................................................ 423 Incinerator ............................................................................ 430 UTILITIES .............................................................................. 432 Steam Generation System .......................................................... 432 Boiler Feed Water System .......................................................... 434 DM water system ..................................................................... 437 Chemical Injection System ......................................................... 439 Electro Chlorination System ........................................................ 444 Sea Cooling Water System .......................................................... 444 Fuel Gas System ...................................................................... 445 Effluent Waste Water System ...................................................... 446 Instrument Air Compressors ........................................................ 450 Utility Failure ......................................................................... 450 LP Steam Failure ..................................................................... 451 Sea Cooling Water Failure .......................................................... 451 Instrument Air Failure ............................................................... 452 Power Failure ......................................................................... 452 Boiler Feed Water Failure .......................................................... 452 Fuel Gas Failure ...................................................................... 452 MAINTENANCE ...................................................... 454 General ................................................................................ 455 PREVENTIVE MAINTENANCE ......................................................... 455 Process ................................................................................ 455 UTILITIES .............................................................................. 470 SHUTDOWN MAINTENANCE .......................................................... 485 Catalyst Loading & special procedures ........................................... 485 SRU 1st Stage & 2nd Stage Converters/Hydrogenation Reactor................. 486 Catalyst Activity & Life Expectancy ............................................... 497 Catalyst Preparation ................................................................. 499 Catalyst Management................................................................ 501 SRU Converter Catalyst Rejuvenation: ............................................ 502 SRU Converter Catalyst Stripping .................................................. 503 TGTU Hydrogenation Reactor Catalyst Oxidation: .............................. 505 Hydrogenation Reactor Sulphiding in Series with the SRU ..................... 510 Combustion Air Blower 9102-K-11A lube oil replacement...................... 512 SECTION XIII ANNEXURE ........................................................... 513 13.1 13.2 13.3 PFD/P&ID .............................................................................. 514 HEAT AND MATERIAL BALANCE ..................................................... 514 CAUSE AND EFFECT DIAGRAM....................................................... 514 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 9 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 13.4 13.5 DESIGN BASIS ......................................................................... 514 MSDS ................................................................................... 514 SECTION XIV REFERENCE DOCUMENTS .......................................... 515 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 10 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION I INTRODUCTION EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 11 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 1.1 OBJECTIVE The purpose of this Operating & Maintenance Manual (O&M) is to provide guidance to the operators for safe and efficient operation of the Utilities and Processing Facilities at the SRU Upgrade Facilities at Mesaieed. This O&M Manual provides detailed guidance on the start-up, shut-down and safe operation of the Utilities and Processing Facilities at SRU Upgrade Facilities. 1.2 ABBREVIATION AG Acid Gas AGEU Acid Gas Enrichment Unit AGRU Acid gas removal unit ATM Atmospheric BCS Boiler control system BFW Boiler Feed Water BMS Burner Management System BSR Beavon Sulphur Recovery BTEX Benzene, Toluene, Ethyl Benzene, Xylene CCR Central Control Room DCC Desuperheater/Contact Condenser DCS Distributed Control System DMW Demineralised Water ECP Electro Chlorination Package ESD Emergency Shutdown FD Forced Draft FV Flow Control Valve F&G Fire and Gas HAZOP Hazard & Operability Study HCV Hand Control Valve HMI Human Machine Interface HP High Pressure HSE Health, Safety and Environment ICSS Integrated Control and Safety System ITR Inspection and Test Report KOD Knock Out Drum LCP Local Control Panel LCS Local Control Station LEL Lower Explosive Limit LER Local Equipment Room LOR Local Off Remote EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 12 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 1.3 LP Low Pressure LPM litres per minute LV Level Control Valve MCC Motor Control Centres MDEA Methyl Di Ethanol Amine MMS Machine Monitoring System MP Medium Pressure MSDS Material Safety Data Sheet NGL Natural Gas Liquids O&M Operation & Maintenance PFD Process Flow Diagram P&ID Piping and Instrument Diagram PIL Petrofac International Limited PPE Personal Protective Equipment PSV Pressure Safety Valve PV Pressure Control Valve QP Qatar Petroleum RGG Reducing Gas Generator SRU Sulphur Recovery Unit TGTU Tail Gas Treatment Unit TLV Threshold Limit Value TV Temperature Control Valve TSV Temperature Safety Valve UCP Unit Control Panel UEL Upper Explosive Limit UPS Uninterrupted Power Supply VFD Variable Frequency Drive UNITS OF MEASUREMENT Sm3/hr 3 Standard cubic meter per hour Nm /hr Normal cubic meter per hour m³/hr Cubic meter per hour l/hr Litres per hour T/hr Tonnes per hour mg/l Milligram per Litre Kg/hr Kilograms per hour Bar (a) Bar absolute Bar (g) Bar gauge EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 13 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL mbar Milli bar Ppb Parts Per Billion ppmv Parts Per Million by Volume ppmw Parts Per Million by Weight M Meters Mm 2 1.4 Milli meters m Square meters Kcal/hr Kilo calories per hour kW Kilo Watt GENERAL DESCRIPTION The primary objective of the Sulphur Recovery Upgrade project is to comply with State Environmental Regulations. The objective is met by upgrading the existing Sulphur Recovery Facilities at NGL-3, in Mesaieed, to achieve a minimum sulphur recovery of 99.5% during normal operation. The upgrade of the SRU includes routing additional sour gas streams from other NGL plants (NGL-1, 2 and 4) to SRU unit along with NGL-3 AGRU 1 & 2 acid gases. New Process systems that are included in this upgrade project are: • Acid Gas Enrichment Unit (AGEU) • Tail Gas Treating unit (TGTU) • Tail Gas Incinerator • Existing SRU is upgraded. New utility systems that are included in this upgrade project are: • Instrument Air and Plant Air System • Nitrogen System • Drinking Water System • Oily Water Drain System • Effluent & Waste Water Treatment System • Flare System • LP Fuel Gas System • Sea Cooling Water System • Demineralised Water System • Boiler Feed Water Deaerator System EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL • Steam Generation System • Electrical Power System • Control and Safety System Rev.: 0 Date: 03/09/2012 Page: 14 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 15 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION II HEALTH SAFETY AND ENVIRONMENT EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 16 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 2.1 HEALTH, SAFETY AND ENVIRONMENT (HSE) This safety section briefs about the safety features of the Sulphur Recovery Upgrade facilities at Mesaieed which provide safety systems to protect personnel, environment and assets from the threats of production hazards. The safety of the plant facilities is maintained at a minimum risk level by adopting the following safety design aspects: 1. Avoiding Exposure to Potential Hazards 2. Minimising the Potential (frequency) for Hazardous occurrences (release of Hydrocarbons, Hydrocarbon Flammable Gases and any other abnormal hazardous event) 3. Containing and Minimising the Consequence (Fire, Explosion and Toxic Gas releases) of the Hazards 4. Providing the Means of Escape and Evacuation from such Hazards 5. Proving a Safe Working Environment for the Plant Personnel. 2.2 LEAKAGE OF ACID GAS While starting up of Acid Gas System that contains H2S & CO2, it is necessary to take special precautions as follows: 1. Area around the specific area is barricaded to prevent personnel approaching the worksite. 2. Personnel carrying out this operation have to take Work Permit and be aware of the hazards associated with Nitrogen (N2), Carbon Di-oxide (CO2) and Hydrogen Sulphide (H2S). 3. Wear appropriate Personal Protective Equipment (PPE). 4. As far as possible, the system to be entered is purged using N2/water prior to opening. This also negates the threat of elemental sulphur and associated corrosion and cracking. 5. Pyrophoric fire prevention measures are put in place (including availability of relevant portable fire extinguishers). 6. Personnel involved in the operation should wear Breathing Apparatus (BA) sets. 7. Check H2S concentration frequently after wedge open the flange. 8. Purging using N2 is continued as necessary. 9. When H2S concentration is NIL, the ‘All Clear’ is given and normal work activities can recommence. 10. Ensure O2 supply by circulating fresh air through the equipment prior to making vessel entry. 11. Follow PTW of QP. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 17 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 2.3 HAZARDS IN HANDLING CHEMICALS 2.3.1 MDEA Refer the Vendor supplied MSDS in Section XIII (Annexure) 2.3.2 Antifoam Refer the Vendor supplied MSDS in Section XIII (Annexure) 2.3.3 Corrosion Inhibitor Refer the Vendor supplied MSDS in Section XIII (Annexure) 2.3.4 Caustic Refer the Vendor supplied MSDS in Section XIII (Annexure) 2.3.5 Biocide Refer the Vendor supplied MSDS in Section XIII (Annexure) 2.3.6 Scale inhibitor Refer the Vendor supplied MSDS in Section XIII (Annexure) 2.3.7 Oxygen Scavenger Refer the Vendor supplied MSDS in Section XIII (Annexure) 2.3.8 Complex Product Refer the Vendor supplied MSDS in Section XIII (Annexure) 2.3.9 Hydrogen Sulphide Accidental Release Measures 1. Personal Precautions: Keep unnecessary personnel away. Ensure adequate ventilation. Do not touch or walk through spilled material. 2. Methods of containment: Stop the flow of material, if this is without risk. Eliminate all ignition sources (no smoking, flares, sparks or flames in immediate area). Prevent entry into waterways, sewers, basements or confined areas. 3. Methods for cleaning up: Avoid dust formation. Vacuum or sweep up material and place in a disposal container. 4. It is likely that the liquid in the system may contain pyrophoric iron sulphide. Even after steam-out/water washing, this may ignite when drying out in the presence of air. Therefore, water connections for flushing should be readily available EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 18 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Hazards Identification 1. Health Hazards: • Hydrogen Sulphide is a highly toxic gas, rapidly causing death when inhaled in high concentrations. Even at low concentrations irritation of the eyes, nose and throat are possible. The following table illustrates the hazard of varying concentrations: • TLV for prolonged exposure: 10 ppm • Slight symptoms after several hours exposure: 70-150 ppm • Maximum Concentrations that can be inhaled for one hour without serious effects: 170-300 ppm • Dangerous after exposure of 30 minutes to one hour: 400-700 ppm • Fatal in 30 minutes: 700 ppm and above • Skin absorption has been reported but is not considered significant • Hydrogen Sulphide can be recognized by its “rotten egg” odour. However its odour should never be used as a means of detection because exposure even to low concentrations may dull the sense of smell • Acute toxicity: The greatest danger from the inhalation of hydrogen sulphide is from its acute effects; it is not cumulative in action • Exposure to moderate concentrations causes headache, dizziness, nausea and vomiting in that order. Continued exposure may cause loss of consciousness, respiratory failure and death if the gas concentration is high enough. In exposures to high concentrations, loss of consciousness may occur rapidly and respiratory failure may follow a few minutes later. After severe exposures to hydrogen sulphide the individual may regain consciousness after several hours of treatment but he may show evidence of permanent severe brain damage. Persons having a significant exposure to hydrogen sulphide may develop a complete and permanent loss of the sense of smell thus destroying any ability to detect the presence of hydrogen sulphide 2. Chronic Exposure Prolonged exposure to low concentrations of Hydrogen Sulphide has an irritant effect on the mucous membranes, eyes and the respiratory tract. Eye effects have been reported at concentrations of 20 ppm or below. First-Aid Measures 1. General Principles: in case of exposure to hydrogen sulphide the patient should be removed to fresh air as quickly as possible. The rescuer must be certain that he is adequately protected against breathing the gas. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 19 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 2. Contact with skin and mucous membranes: Skin absorption is very low. Skin discoloration is possible after contact with liquid hydrogen sulphide. If such skin contact is suspected, the area should be thoroughly washed. 3. Contact with eyes: Eye contact with liquid and gas will cause painful irritation. In case of eye contact keep patient in darkened room; apply ice compresses; put ice on forehead. Send for physician. Eye irritation caused by exposure to hydrogen sulphide requires treatment by a physician, preferably an eye specialist. 4. Inhalation: A worker who has been overcome by hydrogen sulphide must be carried at once into uncontaminated atmosphere. If breathing has stopped, mouth to mouth resuscitation should be started immediately. If Oxygen inhalation apparatus is available, Oxygen should be administered by a competent person. Keep the patient quiet and warm. Call a physician immediately. Do not give anything by mouth to an unconscious patient. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 20 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION III OVERVIEW OF SRU UPGRADE FACILITIES EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 21 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.1 PROCESS 3.1.1 SRU Upgrade Facilities Overview The following facilities are part of the Sulphur Recovery Upgrade Project: • New Acid Gas Enrichment Unit (AGEU) • New Tail Gas Treating Unit (TGTU) • New Tail Gas Incinerator • Existing SRU upgrade/modification • Existing SRU upgrade - The SRU plant is upgraded to process the acid gas flow from the two AGRU trains, along with the acid gas streams from NGL 1/2/4 units. • Utilities System Upgrade: Sea Water Cooling System, Boiler Feed Water System, Steam Generation System, Instrument/Plant Air System, Fuel Gas System, Waste Water System, Electrical Power System, Control & Safety System. AGEU & TGTU are provided with common Amine System. Proprietary Amine solvent (Dow Ucarsol HS-103) has been selected for this purpose. 3.1.2 Acid Gas Enrichment Unit (AGEU) Lean acid gas enters the unit at a temperature of 53°C and a pressure of 0.55 barg. This stream is cooled in an Acid Gas Coolers (9103-E-101A/B), before passing to the Lean Acid Gas KO Drum (9103-V-14). The Lean Acid Gas KO Drum allows bulk removal of any condensed/entrained liquid from upstream. The liquid level in the Lean Acid Gas KO Drum is controlled by pumping the liquid via the Acid Gas KO Drum Return Pumps (9103-P-14A/B) to the existing MDEA storage tank. Alternatively, the sour water can be routed to the sour water stripper, via a normally closed isolation valve. Vapour leaves the Lean Acid Gas KO Drum and fed to the Acid Gas Amine Absorber (9103-C-11), at the bottom. The vapour passes upwards through a trayed bed in contact with a lean amine solution. The counter current contact with the amine solution essentially removes all the H2S and some of the mercaptans and part of the CO2 from the vapour stream. If any BTEX exists in the lean acid gas, it is expected that 80-90% will slip directly to the Incinerator. Treated gas leaving the top of the absorber (9103-C-11) goes to the Incinerator (9101F-14). The rich amine solution, containing absorbed acid gas, is combined with solvent from the Tail Gas Amine Absorber (9102-C-12). It is removed from the column by the Acid Gas Rich Amine Pump (9103-P-12A/B). This stream is then heated in the Lean/Rich Exchanger, before it is fed to the Amine Regenerator (9103-C-12). The rich amine flow rate is controlled to maintain the level in the Acid Gas Amine Absorber. The amine regeneration facilities required for the Acid Gas Enrichment and Tail Gas Treatment Units are shared with the use of a common solvent. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 22 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL In the Amine Regenerator, the rich solution is stripped counter currently with vapours generated by the Amine Regenerator Reboiler. The bottom of the column is maintained at a temperature by regulating the LP steam flow rate into the Regenerator Reboiler (9103-E-13). The stripping action in the lower section removes and releases the contaminants from the solution, such as the acid gases, mercaptans and residual dissolved hydrocarbons. The stripped vapours are cooled in the Regenerator Condenser (9103-E-12), and the Regenerator Condenser Trim Cooler (9103-E-16), by regulating air flow by fans in Regenerator Condenser and adjusting the flow rate of Sea water to the Regenerator Condenser Trim Cooler. Any water and amine in the overhead stream is condensed and collects in the Regenerator Reflux Drum (9103-V-12). The reflux flow rate is controlled by maintaining the liquid level in the Regenerator Reflux Drum. Acid gas from the Regenerator Reflux Drum passes overhead to the Sulphur Recovery Unit. Hot lean amine solution from the Regenerator is pumped to the Amine Surge Tank (9103-T-11) by the Hot Lean Amine Pump (9103-P-17 A/B). The Lean/Rich Exchanger (9103-E-11), Lean Amine Cooler (9103-E-14) and Lean Amine Trim Cooler (9103-E-15) cool the solution prior to the Amine Surge Tank. The lean solution from the Amine Surge Tank is pumped to the Acid Gas Amine Absorber and the Tail Gas Amine Absorber via the Lean Amine Pump (9103-P-13A/B). A slipstream is taken off after the pump and returns to the surge tank through the Lean Amine Filter (9103-S-11), Carbon Filter (9103-S-12) and the Fines Filter (9103-S-13). The filters remove particulate matter from the stream as well as hydrocarbons that accumulate in the Amine solution. The Amine Surge Tank (9103-T-11) receives the recycle flow from the filter circuit and the regenerator. It has the capacity to hold the whole system inventory at shut down. The Amine Surge Tank is maintained at a slightly positive pressure, however not high enough to be able to float on the flare header to maintain pressure and stop ingress of Oxygen. Therefore it is provided with Nitrogen blanketing to prevent air ingress and to minimise the risk of solution degradation. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 1 – Acid Gas Enrichment Unit Rev.: 0 Date: 03/09/2012 Page: 23 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 24 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.1.3 Sulphur Recover Unit Process Description The acid gas stream from the gas treating plant enters the Acid Gas KO Drum (9101-V04) where acid water is knocked out and pumped to Amine Sump (9103-V-14). The gas stream flows to exchanger (9101-E-06) for preheating before entering the Reaction Furnace (9101-F-01), where the acid gas is burnt by the high intensity burner with a controlled amount of air. Air is supplied by an electrically driven blower (9101-K01A/B) & preheated by exchanger (9101-E-05). The products of the combustion are cooled in passing through the tube section of the Waste Heat Boiler (9101-E-07) where a 24 barg steam is generated in the shell side. Gases and any condensed liquid sulphur from the Waste Heat Boiler flow to the Sulphur Condenser (9101-E-01) where the gases are cooled and the additional sulphur is condensed. The gases then passes through the Auxiliary Burner (9101-F-02) where they are reheated by burning a split stream of acid gas (or fuel gas) with air, before entering the first Claus Converter (9101-V-01). In this converter the gases flow downwards through a bed of CR 4/8 mm activated alumina, top loaded with a layer of AM 4/8 catalyst. In the converter, additional elemental sulphur is produced and carried over in vapour phase by the hot gases. The exothermic Claus reaction results in a temperature increase through the adiabatic converter. The hot gases leaving the first converter are cooled in the Sulphur Condenser (9101-E-02) by generating 5 barg steam, the condensed sulphur flows to the Sulphur Degassing Pit (9101-T-01/01Z) through Sultraps. The gases from the Sulphur Condenser (9101-E-02) flow through a coalescer equipped with SS wire mesh pads for the removal of any entrained sulphur. The gases then passes through the second stage auxiliary burner (9101-F-03) where they are reheated by burning a split stream of acid gas (or fuel gas) with air, before entering the second Claus Converter (9101-V-02), loaded with a more active catalyst CRS 31 and a layer of AM 4/8 mm catalyst on the top of the bed. The Final Condenser (9101-E-04) ensures cooling of the process gases by preheating the boiler feed water which is used in the Waste Heat Boiler (91 01-E-07) and the two LP steam producing 1st stage & 2nd stage condenser (9101-E-01 & 9101-E-02). The process gases from Final Condenser passes through a Final Separator (9101-V-05) to achieve complete removal of liquid sulphur drops from the process gases. A coalescer is provided in Final Separator (9101-V-05). From final separator, the process gas is routed to Incinerator (9101-F-14), where all remaining sulphur compounds are burnt to sulphur dioxide. Incineration is achieved by burning fuel gas with a slight excess of air at a temperature of 800°C. The incinerated gas is disposed of to the atmosphere via stack (9101-X-11). The sulphur produced in the process is extracted from all sulphur condensers through sultraps and is routed to the Sulphur Degassing Pit (9101-T-01). The sulphur is degassed through AQUISULF sulphur degassing process. The degassed sulphur is then transferred to the Storage Tank 9101-T-02 by Sulphur Transfer Pumps (9101-P-04A/B). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 2 - Sulphur Recovery Unit Rev.: 0 Date: 03/09/2012 Page: 25 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 26 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.1.4 Tail Gas Treatment Unit (TGTU) The purpose of the Tail Gas Treating Unit is to reduce the hydrogen sulphide concentration in the tail gas to a level corresponding to >99.5% total sulphur recovery. All residual hydrogen sulphide is oxidised to sulphur dioxide before it is released to the atmosphere. The BSR/Amine process consists of a Beavon Sulphur Recovery (BSR) reducing or hydrogenation section and a selective amine section. The process uses the BSR technology to reduce all sulphur compounds in the SRU tail gas to hydrogen sulphide. This section includes water condensation and separation upstream of the amine section with a caustic circulation system to protect against SO2 breakthrough, which degrades the amine and causes severe corrosion. The amine section uses an amine solution to remove most of the hydrogen sulphide from the treated sulphur plant tail gas while minimising the co-absorption of carbon dioxide. The Claus tail gas from the Final Sulphur Condenser 9101-E-04 is fed to the Reducing Gas Generator (RGG). The purpose of the Reducing Gas Generator is to generate reducing gases (H2 and CO). This is achieved by the combustion of fuel gas with a substoichiometric quantity of air. The production of reducing gases is regulated by controlling the flow of the fuel gas and air. Air flow is set by the outlet temperature of the Reducing Gas Generator 9102-F-01 whilst the fuel gas flow rate is set to be a fixed proportion of the air flow. LP steam is fed to the Reducing Gas Generator to suppress the formation of carbon. The flow rate of the steam is ratio-controlled according to the fuel gas flow rate. The tail gas from the Final Sulphur Condenser is mixed with the hot combustion products in the Reducing Gas Generator to ensure a temperature that will favour the desired reactions in the Hydrogenation Reactor (9102-V-01). The Hydrogenation Reactor contains a fixed bed Cobalt/Molybdenum (CoMo) catalyst. The reactions are exothermic resulting in a temperature rise across the reactor. The gas is cooled by the generation of LP steam in the Reactor Effluent Cooler. The tail gas is then desuperheated and the excess water removed in the Desuperheater/Contact Condenser (9102-C-01). This tower contains an upper packed section, a chimney tray and a lower section containing packing and bubble cap trays. In the lower packed section of the tower (Desuperheater section), tail gas is contacted with a circulating stream of a mildly caustic water solution. This removes sulphur dioxide and cools the tail gas down. The Desuperheater Circulation Pump (9102-P11A/B) pumps the caustic water solution from the bottom of the tower to the top of the packing. Water make up is provided to the lower (Desuperheater) section, under level control, from the top (Contact Condenser) section circulation. The solution is maintained at an alkaline pH of around 9.0 to protect against SO2 breakthrough from the reactor. SO2 causes corrosive conditions in the Desuperheater EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 27 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Contact Condenser and the Amine Absorber, and degrades the amine. The pH of the circulating liquid is monitored by a continuous analyser and controlled by periodic, manual addition of fresh caustic solution. An intermittent bleed from this section removes accumulated contaminants from the circuit. The desuperheated gas and water vapour then passes through the (wash) bubble cap trays and the chimney tray into the upper (Contact Condenser) packed section. Here the gas is cooled by direct contact with a circulating water stream. The water is pumped by the Cooling Water Circulation Pump from the chimney tray, through the Contact Condenser Cooler where it is cooled, and back to the top of the tower. The water that is condensed in this section is slightly sour. Some is used as make up on demand to the lower Desuperheater section and the remainder is taken off under level control and sent to effluent treatment. The condensed water loop is kept separate from the water in the desuperheater circulation loop to avoid contamination with salt products that may be formed in the Desuperheater section. The tail gas leaves the Desuperheater Contact Condenser (9102-C-11) at a temperature of approximately 40°C and is sent to the Tail Gas Amine Absorber (9102-C-12) which uses a lean amine solution to remove the hydrogen sulphide from the tail gas, whilst minimising the co-absorption of carbon dioxide. The gas enters at the bottom of the absorber and passes through a packed bed counter current to the lean amine solution that preferentially absorbs H2S. The lean amine solution is supplied from the Amine Regenerator. The Tail Gas Rich Amine Pump (9102-P-16 A/B) pumps the rich solvent solution from the bottom of the Tail Gas Amine Absorber (9102-C-12) to the Acid Gas Amine Absorber (9103-C-11) before it is regenerated in the Amine regenerator (9103-C-12). The amine regeneration facilities required for the Acid Gas Enrichment and Tail Gas Treatment Units are shared with the use of a common solvent. The H2S that is stripped from the rich amine solution in the Amine Regenerator is fed to the Sulphur Recovery section, thus closing the recycle loop around the SRU and TGTU sections. Treated gas from the Tail Gas Amine Absorber passes to the Incinerator along with that from the Acid Gas Amine Absorber and from the Sulphur Pit. The incinerator is designed to incinerate all sulphur compounds in the streams under normal operation. It is also used to incinerate additional streams while the TGTU is bypassed or during start-up or abnormal operating conditions. The flue gas is released to the atmosphere through the Stack (9101-X-11). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 28 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 3 - Tail Gas Treatment Unit FV-1314 XV-1331 LV-1305 FV-1304 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 29 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.1.5 Tail Gas Incinerator An Incinerator is provided to thermally oxidise all possible sulphur compounds to SO2 in off gas effluents from the Acid Gas Amine Absorber, Tail Gas Amine Absorber, SRU tail gases and vent gases from the sulphur Degassing Package. Moreover all BTEX content of off gas effluent is also destructed. To ensure complete combustion of these sulphur compounds the Incinerator's combustion chamber temperature is maintained at a temperature of about 817°C by burning fuel gas supplied with combustion air in the unit's burner. Combustion air is supplied from 2 x 100% Incinerator Air Blowers (9101-K-12 A/B). The flows of fuel gas and combustion air are each measured by flow and then ratio controlled to ensure the correct amount of excess air is always maintained in the Incinerators combustion chamber to allow the oxidation of the sulphur compounds in the tail and vent gases to take place. An Oxygen analyser located in the Incinerator outlet combustion gases ducting monitors the excess O2 in the Incinerators combustion gases. Adjustments may be made to the fuel gas to air ratio controller to ensure the correct excess of O2 (3% by Mol) is seen in the stack gases. A SOX/NOX analysers, located part way up the Incinerator Stack (9101-X-11), monitors the Incinerator stack gases for SOX/NOX content. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 4 - Tail Gas Incinerator Rev.: 0 Date: 03/09/2012 Page: 30 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 31 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.1.6 Amine Drain System Amine drained from pumps and other equipment during times of maintenance and plant overhaul, is collected in the Amine Sump. The Amine Sump Pump must be started manual by operations in order to transfer the amine to the Amine System via the Amine Sump Filter. A differential pressure indicator across the filter monitors the filter pressure drop. In the event that the amine sump pump is not manually stopped when the low level alarm is activated then a low low level switch will stop the pump to prevent loss of suction damage to the pump. To prevent air ingress into the amine sump a small flow of Nitrogen is introduced into the amine sump and allowed to pass out of the sump to the atmosphere through carbon canister. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 5 - Amine Sump and Pump Rev.: 0 Date: 03/09/2012 Page: 32 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 33 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.2 NEW UTILITY FACILITIES 3.2.1 Instrument and Plant Air The new air compressor package consists of the following: 1. Two Air Compressors (6837-K-02A/B) having a capacity of 900 Nm3/hr (dry basis) 2. One air compressor discharge drum, (6837-V-10) is provided • Two Instrument Air Dryer packages, (6837-A-03/04) running at 2 X 50%, each dryer capacity is 300 Nm3/hr (dry basis) • One Instrument Air Receiver (6837-V-11) with storage capacity to provide instrument air for a period of 20 minutes following a compressor trip The new Air System will supply instrument and plant air with the following supply battery limit conditions for both instrument and plant air: Design Operating Pressure bar (g) 9.7 7.0 Temperature (°C) 85 55/60 The new instrument and plant air headers are connected to the existing NGL-3 instrument and plant air headers respectively through cross over connection lines with (manual isolation valves) for operation flexibility. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 34 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 6 – Plant/Instrument Air System EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 35 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.2.2 Demineralised Water System The supply of fresh water to the new DMW Package is taken from existing Drinking Water Storage Tanks (6834-T-01 A/B) by means of new Drinking Water Feed Pumps (6834-P-23 A/B, one operating, one standby). Each pump is designed for a flow of 10 m3/h and supplies fresh water to the following users: • Demineralised Water Package • Cross connection to the existing fresh water network • Utility water to utility stations, safety showers and eye wash stations. The Demineralised Package is based on ion exchange technology (similar to the existing DMW Package) and consists of two identical trains. The following equipment items are envisaged to form part of the package: • Two Cation Exchangers • Two Anion Exchangers • Two Demineralised-Water Regeneration Pumps • two Demineralised-Water Recirculation Pumps • One Hydrochloric Acid (HCL) Storage Tank • There HCL Injection Pumps • One Caustic (NaOH) Storage Tank • Three NaOH Injection Pumps • One Neutralisation Pit • One Neutralisation Pump The DMW Package operates continuously and automatically and thus requires minimum operator intervention. The package includes the necessary control and safety devices. The Demineralised Water from the DMW Package is routed to Demineralised Water Storage Tank (6834-T-08). Capacity of Demineralised Water Storage Tank is 83 m3. Centrifugal type, DMW Feed Pumps (6834-P-24A/B one running, one standby) are used to supply demineralised water at 3.7 barg pressure and ambient temperature, from DMW Storage Tank to the: • Steam Condensate Flash Drum (6834-V-05) • Amine Surge Tank (9103-T-11) • Make-up water to Cooling Water Circulation Pump (9102-P-12 A/B) • Start-up water to Stripper Overhead Circulation Pump (6922-P-11 A/B) • Make-up water to Amine Regenerator Reflux Drum (9103-V-12) • Existing DMW Network System (for operational flexibility, normally no flow). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 36 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 7 – Demineralized Water System EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 37 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.2.3 Sea Cooling Water System Two Seawater Cooling Pumps 6932-P-04A/B are installed on a new jetty and take suction from the sea. The pumps are vertical-shaft, constant speed centrifugal pumps and are electric motor driven. The seawater cooling pumps have a design capacity of 1600 m3/h (each) at a discharge pressure of 5.0 barg. One pump is normally running, while the other is on standby. Each pump is capable of supplying a normal flow of 1200 m3/h to users for SRU upgrade. The water enters the pump through a suction pipe (stilling tube) to reduce turbulence. A coarse mesh bar suction screen is installed at each pump to prevent seaweed and other debris from entering the seawater supply system. From the common discharge of seawater cooling pumps, seawater stream flows via a new dedicated 24” main supply header to the new Filtration Package Unit (6932-S02A/B). The self cleaning rotary type Seawater Filters (one in operation and one on standby) are capable of removing particle sizes greater than 1000 microns from seawater and each unit is designed for a flow of 1600 m3/h. The filtered water from filters is routed to the heat exchangers located in AGEU/TGTU and other users. The filter skid comprises: • Two Rotary Filters (6932-S-02A/B) and motors • The 2 x 100% filters are equipped with an automatic back-flushing mechanism which operates on intermittent basis A small portion of the main seawater (cooling water) flow is diverted downstream of the filters to provide seawater supply for the Electro Chlorination Unit (6932-A-05). The Electro Chlorination Unit generates sodium hypochlorite solution. The sodium hypochlorite solution is injected into Sea Cooling Water Pumps suction lines to control growth of marine organisms in the Sea Cooling Water System. There is one dedicated new Electro Chlorination Unit. In addition, a dedicated Biocide Injection Unit (6932-A-06) for effective control of growth of marine organisms and a dedicated Scale Inhibitor Injection Unit (6932-A-07) to prevent formation of mineral scales in the Sea Cooling Water system are also provided for existing as well new Sea Cooling Water Systems. The new Cooling Water System is a once through system and the seawater returned from the SRU upgrade facilities is discharged into existing Seawater Observation Sump (6932-X-01) which has a retention capacity of 60 m3. From the sump the seawater overflows to the sea. To prevent fouling the temperature of cooling water from each exchanger outlet should not exceed the maximum allowable temperature limit of 45°C. A tie in to the existing NGL-3/4 seawater supply system is also provided to supply seawater from the new Sea Water Pumps. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 38 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 8 – Sea Cooling Water System To Existing Sea Cooling Water System 6932-S-02A/B Cooling Water Filters 9103-E-101 Acid Gas Cooler 9103-E-15 Lean Amine Trim Cooler 9103-E-16 Regenerator Condenser Trim Cooler 9102-E-13A/B Contact Condenser Trim Cooler 6848-T-02 Boiler Blow Down Pit Steam Generation Package Acid Gas Enrichment Unit 6932-A-05 M M Electro Chlorination Package Sea Cooling Water Pumps 6932-P-04A 6932-A-06 Biocide Injection Package 6932-T-01 Local Chemical Drain Pit 6932-P-04B 6932-A-07 Scale Inhibitor Injection Package Tail Gas Tr. Unit To Observation Sump 6932-X-01 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 39 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.2.4 Boiler Feed Water System Boiler Feed Water (BFW) is required for the generation of MP and LP steam in the gas fired water Steam Generators (6848-A-02 A/B/C). The Boiler Feed Water, consists of a mixture of LP steam condensate and Demineralised Water make-up. The Boiler Feed Water system includes the following equipment: Description Steam condensate Flash Drum Deaerator Feed Pumps Equipment Tag No. 6834-V-05 6834-P-20A/B Steam Condensate Cooler 6834-E-02 Boiler Feed Water Deaerator Package 6834-A-08 Boiler Feed Water Pumps BFW Chemical Injection Package • O2 Scavenger Injection Pumps • Complex Product Injection Pumps 6834-P-22 A/B/C 6834-A-09 The Boiler Feed Water passes through a Steam Condensate Flash Drum 6834-V-05 where the flash steam cools down the inventory to 102°C to prevent cavitations in Deaerator Feed Pumps. The DMW Condensate is pumped by the Deaerator Feed Pumps to the heating section of a Thermal Deaerator where all the free carbon dioxide and the oxygen up to 5 ppb are removed by heating and scrubbing the water with the LP saturated steam at 0.2 barg pressure. The extracted dissolved gases such as O2, CO2 and water vapour are discharged through restriction orifice (68-RO-1305) to atmosphere. A dose of Oxygen Scavenger is injected into the hold up section of the Deaerator to completely eliminate the residual oxygen from the water. The capacity of the holding section in the Deaerator is equivalent to 20 minutes. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 40 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 9 – Boiler Feed Water System EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 41 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.2.5 Steam Generation Package 6848-A-02A/B/C The MP steam boiler package 6834-A-02A/B/C includes three boilers, two operating and one stand-by. Each boiler has a nominal steam generating capacity of 45 T/h. The Boiler Feed Water enters the external Economizer 6848-E-01A, which is a finned tubes heat exchanger (water/flue gas). The feed water is heated by the flue gas thermal heat in the flue gas path. In case sour fuel gas is used, the boiler feed water is sent to a preheating water circuit installed inside the water drum, before going to the Economiser 6848-E-01A. This is to avoid acid condensation inside the flue gas duct. From the Economizer outlet, the feed water enters into the boiler upper drum called “Steam Drum” 6848-V-02A. Boiler functioning relies on “steam/water natural circulation”, with evaporating rising circuits formed by the hottest tubes of boiler evaporating bank. Remaining tubes acts as downcomers, which feed the rising circuits. In the boiler evaporating tubes, the mixture of saturated water & steam is produced. Then through the steam drum internal separators, the saturated steam is separated from the saturated water droplets. The steam then passes through the steam header and reaches the temperature and pressure controlling stations. The pressure is controlled by a pressure control valve 68-PV-1524 and the temperature is controlled by water injection type Desuperheater 6848-X-03A. The combustion air for the boiler is supplied by a Forced Draft Fan 6848-K-02A, driven by an electric motor. At the inlet of the FD Fan 6848-K-02A, a Grid Filter 6848—03A, a Sand Filter 6848-S-02A and a silencer 6848-X-06A are provided. Downstream of this, the modulating inlet control damper is provided. At the outlet the air passes through a duct that delivers air to wind box. The combustion air measuring device 68-FE-1526 is provided in this duct. Air is supplied to the burners through the wind box. When the combustion takes place, the high temperature flue gas pass through the boiler furnace, enclosed by water cooled tubes. The flue gases at the end of the combustion chamber, turn to 180° and pass through the evaporative convective section. The convective section is located on the right side of the furnace. The flue gases then pass through the Economizer and reach the stack. A Flue Gas Recirculation Fan 6848-K-03A, which takes suction from the flue gas Economizer downstream duct and discharges to the combustion air measuring device 68-FE-1526 provided in combustion air duct, is provided. In order to meet the specified low emissions target, at high boiler load, the burners can be operated in flue gas recirculation mode, the combustion air is mixed with a proper flue gas flow rate (about 15% of nominal flow rate). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 42 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The steam generator is provided with one burner, designed to burn both sour and sweet fuel gas. The burner is designed to have a turndown of 10:1. Burner is provided with a pilot which is of high energy type. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 43 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL XV-1527 TV-1522 PV-1523 Fig. 10 – Steam Generation System EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 44 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.2.6 Fuel Gas System LP fuel gas is required for • New Steam Generation Boilers 6848-A-02A/B/C The main normal LP fuel gas supply for the new MP Steam Boiler Package (6848-A-02A/B/C) and Waste Water Degasser (6922-V-07) blanketing is supplied from the first stage suction of the existing Booster Compressors (6701-K-10120/30) in NGL-3. In addition, two back up sources are provided; the first is the fuel gas from (6103-K-01 A/B) with a second backup from existing 30” line to Point B. The new fuel gas supply system will consist of a letdown station, Fuel Gas KO Drum (6236-V-05), and a supply header to the Steam Boilers and Waste Water Degasser. The source pressure from the take-off point is let down to 7 barg through the pressure control valve 62-PV-1301A before entering the LP Fuel Gas KO Drum. The source pressure of the fuel gas from 6103-K-01 A/B is 20 barg whilst that of feed gas from the 30” line is 45 barg. The former is let down to 7 barg through the pressure control valve 62-PV-1301 B and the latter via 62-PV-1302. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 45 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 11 – Fuel Gas System PV-1303 Hydro Carbon Gas Flare Header To LP Flare To Steam Boiler Package 6848-A-02A/B/C XV-1301 PV-1301A From 1st Stage Booster Compressor (6701-K-10/20/30) Suction Header To LP Hydrocarbon Flare Header E-19 LP Fuel Gas KO Drum 6236-V-05 XV-1302 PV-1301B Backup Supply Fuel Gas from 6103-K-01A/B XV-1303 PV-1302 To Flare Header Backup Supply Fuel Gas from 30" Existing Line EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 46 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3.2.7 Effluent and Waste Water Treatment Unit The sour water resulting from the new facilities added as part of the SRU Upgrade Project contains high levels of dissolved sulphides which need to be removed before the waste water can be discharged to the marine environment. The acceptable levels of sulphides is 0.1 mg/l (0.1 ppmw) and to achieve this the sour water is treated in the sour water treatment system. Sour water from various sources is collected in the Degassing Drum, which provides over 20 minutes of hold-up for the waste water. The flow of waste water from Desuperheater/Contact Condenser (9102-C-11) is continuous at a rate of 8.7 m3/h whilst all other sources are intermittent. The sour water from the degasser is continuously pumped under flow control by Waste Water Degasser Pumps (6922-P08A/B) to the Sour Water Stripper Unit for treatment. In the event the Sour Water Treatment System is unavailable due to a process upset, provision exists for manually routing the degasser liquids directly to the Observation Sump (6922-X-04). A balance line between Degassing Drum and Sour Water Stripper 6922-C-01 means that the pressure in the Degassing Drum floats on the stripper operating pressure (i.e. 1.0 barg). A nitrogen supply line is provided to maintain pressure in the drum if it falls below a certain minimum as liquids are pumped out. The sour water from degasser drum is filtered in 6922-S-06 and then preheated in Sour Stripped Water Exchanger 6922-E-01 before feeding to Sour Water Stripper 6922-C-01. The Sour Water Stripper operates at 1.0 barg and has an upper section and a lower tray section. The sour water is stripped by the vapours generated from the Sour Water Stripper Reboiler 6922-E-04. The Reboiler utilises LP steam to heat the sour water that comes from the bottom of the Sour Water Stripper to 126⁰C. The condensed steam from the Reboiler is sent to the LP Condensate system through level control. Reflux for the column is provided by a pump-around system. Water is taken from below tray 33 pumped by Stripper Overheads Circulation Pumps 6922-P-11A/B under flow control, cooled in Stripper Overheads Cooler 6922-E-03 and then returned to the top tray. The stripper overhead acid gases are routed to the AGEU (upstream of 9103-V-14). In the event of high column pressure, excess gases are diverted to LP Acid Gas flare. The stripped water from the stripper is pumped under level control cascaded to a flow controller via Stripped Water Pump 6922-P-10A/B to the Sour/Stripped Water Exchanger 6922-E-01 to preheat the feed to the stripper. The water is then routed to the Stripper Water Cooler 6922-E-02 where it is cooled to 55°C before discharge to the Observation Sump. An analyser is provided in the line to the Observation Sump to monitor the sulphide content of the stripped water stream. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 47 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 12 – Waste Water Treatment Unit Balance Line LP Fuel Gas from 6236-V-05 PV 1315A PV-1307 Waste Water from Cooling Water Circulation pumps 9102-P-12A/B PV 1315B Sour Gas to TGTU To LP Acid Gas Flare XV 1312 PV 1307 Pressurised drain from 9102-P-12A/B Stripper Overheads Cooler 6922-E-03 XV 1313 M LV-1325 Water for Startup Sour Water from Regenerator Reflux Drum 9103-P-11A/B Corrosion Inhibitor NC Waste Water Degasser 6922-V-07 FV 1316 FV 1314 Waste Water Stripper 6922-C-01 Stripper Overheads Circulation Pumps 6922-P-11 A/B TV 1327 Sour Water Stripper Reboiler 6922-E-04 Waste Water Degasser Pumps 6922-P-08A/B Sour Water Filter 6922-S-06 Sour Stripped Water Exchanger 6922-E-01 Desuperheater FV 1315 6922-X-01 From LP Steam Reboiler Condensate Drum 6922-V-09 LV 1327 LP Condensate Stripped Water Pumps 6922-P-10A/B Stripped Water Cooler 6922-E-02 M FV 1317 Stripped Water to Observation Sump 6922-X-04 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 48 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL 3.3 FIRE WATER & DELUGE SYSTEM 3.3.1 Fire Water System The fire water ring main for the new Process facilities is connected to the existing 12” ring main and tie-in provided at two existing fire water ring mains 12”-6533-FW-001C12T & 12”-6533-FW-002-C12T. The fire water ring main for the new Utilities is connected to the existing 12” ring main and tie-in provided at two existing fire water ring mains 12”-6533-FW-006-C121 & 12”-6533-FW-107-C120. Fire water ring main is buried with minimum 1 meter cover. Ring main block valves are post indicator type and accessible from surface. Fire hydrants and monitors are located at 1.5 m from road. If the distance is shorter, a crash barrier is provided. The fire hydrants and monitors are located at 15 m from plant/equipment/buildings they intended to protect. All fire hydrants face the plant equipment. Fire hydrants are 4-way outlet hydrant valves with (1000 LPM) inbuilt pressure regulating device. Each hydrant is provided with 6” riser pipe bib nosed 3” branch inlet and 2.5” instantaneous hose connection. Monitors are suitable for manual operation with locking facilities in both horizontal and vertical planes. It is capable of 360° horizontal movement and elevation 75° above and 30° below the horizontal. 3.3.2 Deluge System Deluge Skid is used in the new facilities as per details below. Deluge Skid No. 91-DV-1711 Deluge Valve Size 4” Equipment protected Hydrogenation Reactor (9101-V-11) Acid Gas Cooler (9103-E-101) 91-DV-1712 8” Lean Acid Gas KO Drum (9103-V-14) Acid Gas Amine Absorber (9103-C-11) Deluge valves are activated by: • Automatically activated upon fire detection via F&G System/fusible plug loop • Manually locally activated by hand lever through HCV/Push button at safe distance • Manually/remotely activated from F&G console. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 49 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL LC NC Air Vessel 6 Lit. Capacity LO Fig. 13 – Deluge Valve Typical Installation EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 50 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION IV PROCESS AND CONTROL DESCRIPTION EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 51 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.1 4.1.1 ACID GAS ENRICHMENT UNIT (AGEU) Equipment Specification Acid Gas Coolers Equipment Tag No. Process Medium (Shell/Tube) 9103-E-101A/B Acid Gas/Sea Water Design Pressure Shell Side, barg 6.2 Design Pressure Tube Side, barg 8.0 Design Temperature Shell Side, (Max./Min.), °C 175/0 Design Temperature Tube Side, (Max./Min.),°C 85/0 Operating Pressure Shell/Tube Side, barg 0.51/1.7 Operating Temperature, Shell Side (In/Out) °C 63/53 Operating Temperature, Tube Side (In/Out) °C 35/41.76 Design Duty, kW Material of Construction, Shell/Tube 164 SS316L/Titanium Grade 2 Lean Acid Gas KO Drum Equipment Tag No. 9103-V-14 Tower Diameter/Height, mm 3000/7000 Process Medium Acid Gas Design Pressure, barg 3.5/FV Design Temperature, °C (Max./Min.) 175/0 Operating Pressure, barg Operating Temperature, °C Material of Construction, Shell/Internals 0.38 53 CS/SS316L Acid Gas KO Drum Return Pump Equipment Tag No. Process Medium 3 9103-P-14A/B Sour Water Capacity, m /hr (Normal/Rated) 5/6.7 Driver Type Motor Rated Power, kW Suction Pressure, bar(a) (Rated/Max.) 7.5 1.66/5.23 Discharge Pressure, bar(a) 5.0 Operating Temperature, °C 49 Design Temperature, °C (Max./Min.) Material of Construction - Casing/Impeller 85/0 A351-CF8M/SS316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 52 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Acid Gas Amine Absorber Equipment Tag No. 9103-C-11 Tower Diameter, mm 4100 Tower Height, mm 20040 Tray Nos. 10 Process Medium Acid Gas/MDEA Design Pressure, barg (Max./Min.) 3.5/FV Design Temperature, °C (Max./Min.) 175/0 Operating Pressure, Top/Bottom, barg Operating Temperature, Top/Bottom, °C Material of Construction, Top section Material of Construction, Bottom section Material of Construction, Internals 0.19/0.38 46/58.1 CS+SS316L CLAD CS SS316L Acid Gas Rich Amine Pumps Equipment Tag No. Process Medium 3 Capacity, m /hr (Normal/Rated) Driver Type Rated Power, kW Suction Pressure, bar(a) (Rated/Max.) 9103-P-12A/B Rich Amine 682/750.2 Motor 195 1.99/6.1 Discharge Pressure, bar(a) 8.5 Operating Temperature, °C 56 Design Temperature, °C (Max./Min.) Material of Construction Casing/Impeller 85/0 A351-CF8M/SS316L Lean/Rich Amine Exchanger Equipment Tag No. Process Medium 9103-E-11A/B Rich Amine/Lean Amine Design Pressure Lean Amine Side, barg 14.3 Design Pressure Rich Amine Side, barg 13.6 Design Temperature (Max./Min.)°C Operating Pressure Lean/Rich Amine Side bar(g) 150/0 5.8/5.32 Operating Temperature, Lean Amine Side (In/Out) °C 129/85 Operating Temperature, Rich Amine Side (In/Out) °C 55/101 Design Duty, kW 34669 Material of Construction, Plates SS 316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 53 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Amine Regenerator Equipment Tag No. 9103-C-12 Tower Diameter, mm 5650 Tower Height, mm 24450 Tray Nos. 24 Design Pressure, barg (Max./Min.) 7.0/FV Design Temperature, °C (Max./Min.) 175/0 Operating Pressure, Top/Bottom, bar(a) 2.21/2.44 Operating Temperature, Top/Bottom, °C 118/131 Material of Construction, Top section Material of Construction, Bottom section Material of Construction, Internals CS+SS316L CLAD CS SS316L Hot Lean Amine Pumps Equipment Tag No. Process Medium 3 Capacity, m /hr (Normal/Rated) Driver Type Rated Power, kW Suction Pressure, bar(a) (Rated/Max.) 9103-P-17A/B Lean Amine 717/789 Motor 195 2.84/8.9 Discharge Pressure, bar(a) 7.8 Operating Temperature, °C 131 Design Temperature, °C (Max./Min.) Material of Construction Casing/Impeller 150/0 A351-CF18M/SS316L Regenerator Condenser Cooler Equipment Tag No. Type Process Medium 9103-E-12 Forced Draft Air Cooler Acid Gas No. of Fans 12 Fan Power, kW/Fan 22 Design Pressure, barg 7.0/FV Design Temperature (Max./Min.)°C 175/0 Operating Pressure bar(a) 2.18 Operating Temperature, (In/Out) °C 118/54 Design Duty, kW 18574 Material of Construction, Header & Tubes Alloy 825 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 54 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Regenerator Condenser Trim Cooler Equipment Tag No. Process Medium (Shell/Tube) 9103-E-16 Acid Gas/Sea Water Design Pressure Shell Side barg (Max./Min.) 8.0/FV Design Pressure Tube Side barg (Max./Min.) 8.0/FV Design Temperature Shell Side(Min./Max.) °C 150/0 Design Temperature Tube Side (Min./Max.) °C 85/0 Operating Pressure Shell/Tube Side, barg 1.07/5.0 Operating Temperature, Shell Side (In/Out) °C 54/49 Operating Temperature, Tube Side (In/Out) °C 35/42 Design Duty, kW Material of Construction Shell/Tube 271 SS316L/Titanium Grade-2 Regenerator Reflux Drum Equipment Tag No. Process Medium 9103-V-12 Acid Gas Drum Diameter, mm 1500 Drum Height, mm 4520 Design Pressure, barg (Max./Min.) 7.0/FV Design Temperature, °C (Max./Min.) 175/0 Operating Pressure, barg Operating Temperature, °C Material of Construction 1.02 49 SS316 Regenerator Reflux Drum Pumps Equipment Tag No. Process Medium Capacity, m3/hr (Normal/Rated) Driver Type Rated Power, kW Suction Pressure, bar(a) (Rated/Max.) Discharge Pressure, bar(a) Operating Temperature, °C Design Temperature, °C (Max./Min.) Material of Construction, Casing/Impeller 9103-P-11A/B Regenerator Reflux Liquid 26.15/31.4 Motor 22 2.27/8.6 8.41 49 85/0 A351-CF8M/SS316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 55 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Regenerator Reboiler Condensate Pot Equipment Tag No. Process Medium Drum Diameter, mm Drum Height, mm Operating Pressure, barg Operating Temperature, °C Design Pressure, barg (Max./Min.) Design Temperature, °C (Max./Min.) Material of Construction 9103-V-13 Condensate 2100 4100 4.5 155 7.0/FV 185/0 CS Regenerator Reboiler Equipment Tag No. Process Medium Design Pressure, Shell Side, barg Design Pressure, Tube Side barg Design Temperature, Shell side °C Design Temperature, Tube side °C Operating Pressure, Shell, Side barg Operating Pressure, Tube Side barg Operating Temperature, Shell side °C Operating Temperature, Tube side °C Design Duty, kW Material of Construction, Shell side Material of Construction, Tube side 9103-E-13 Amine 7.0/FV 7.0/FV 150/0 185/0 1.356 4.5 130 159 48413 CS SS316L Lean Amine Cooler Equipment Tag No. 9103-E-14 Process Medium Lean Amine Design Pressure, barg, (Max./Min.) 14.3/FV Design Temperature °C 175/0 Operating Pressure barg 4.3 Operating Temperature °C 85 Design Duty, kW Material of Construction 30318 Header/Tubes Alloy 825 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 56 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Lean Amine Trim Cooler Equipment Tag No. Process Medium 9103-E-15 Lean Amine Design Pressure, Lean Amine Side, barg 14.3 Design Pressure, Sea Water Side, barg 8.0 Design Temperature Lean Amine Side °C 90/0 Design Temperature Sea Water Side °C 85/0 Operating Pressure Lean Amine Side barg 5.30 Operating Pressure Sea Water (In/Out) Side barg 2.6 Operating Temperature, Lean Amine Side (In/Out) °C 54/45 Operating Temperature, Sea Water Side (In/Out) °C 35/45 Design Duty, kW 6821 Material of Construction, Plates Titanium SB265 Amine Surge Tank Equipment Tag No. Process Medium Size (ID/Height), mm Design Pressure, barg (Max./Min.) 9103-T-11 MDEA 1100/5500 0.075/-0.005 Design Temperature, °C (Max./Min.) 85/0 Operating Pressure, barg 0.02 Operating Temperature, °C 45 Material of Construction CS Lean Amine Pumps Equipment Tag No. Process Medium 3 Capacity, m /hr, Normal/Rated Driver Type Rated Power, kW Suction Pressure, bar(a) (Rated/Max.) 9103-P-13A/B Lean Amine 835/919 Motor 240 1/1.59 Discharge Pressure, bar(a) 7.50 Operating Temperature, °C 45 Design Temperature, °C 85 Material of Construction, Casing/Impeller A351-CF8M/SS316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 57 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Lean Amine Filter Equipment Tag No. Process Medium 9103-S-11 Lean Amine Operating Pressure, barg 2.8 Clean Pressure drop, bar 0.1 Max. Allowed Pressure drop, bar, dirty 0.7 Operating Temperature, °C 45 Design Temperature, °C Design Pressure, barg 3 85/0 9.4 Flow rate, m /hr 184 Material of Construction CS Activated Carbon Filter Equipment Tag No. Process Medium 9103-S-12 Lean Amine Operating Pressure, barg 2.1 Clean Pressure drop, bar 0.3 Max. Allowed Pressure drop, bar 0.7 Operating Temperature, °C 45 Design Temperature, °C 85/0 Design Pressure, barg 9.4 Flow rate, m3/hr 184 Material of Construction CS Fines Filter Equipment Tag No. Process Medium 9103-S-13 Lean Amine Operating Pressure, barg 1.4 Clean Pressure drop, bar 0.1 Max. Allowable Pressure drop, bar 0.7 Operating Temperature, °C 45 Design Temperature, °C Design Pressure, barg 3 85/0 9.4 Flow rate, m /hr 184 Material of Construction CS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 58 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Amine Sump Equipment Tag No. Process Medium Vessel size (ID/T/T) mm 9103-V-10 MDEA 4200/8500 Design Temperature, °C (Max./Min.) 175/0 Design Pressure, barg (Max./Min.) 7.0/FV Operating Temperature, °C Ambient Operating Pressure, barg 0.05 Material of Construction CS Amine Sump Pump Equipment Tag No. Process Medium 3 Capacity, m /hr (Normal/Rated) Driver Type 9103-P-15 Amine 11.8 Motor Rated Power, kW Suction Pressure, bara, Max./Rated Operating Temperature, °C Design Temperature, °C (Max./Min.) Material of Construction, Casing/Impeller 15 8.4/1.03 20 175/0 A351-CF8M/SS316L Amine Sump Filter Equipment Tag No. Process Medium Size (ID/T/T), mm Design Temperature, °C Design Pressure, barg 3 9103-S-14 Amine 308/920 175/0 17.7 Flow rate, m /hr 10 Material of Construction CS 4.1.2 AGEU PROCESS DESCRIPTION & CONTROL 4.1.2.1 Acid Gas Enrichment Unit Process Chemistry The function of the amine solvent is: To enrich the week acid gas stream from the upstream gas sweetening units in an Acid Gas Amine Absorber so that the H2S content of the acid gas is increased to a point that will make the gas easier to process in the downstream SRU. The H2S in the acid gases from the upstream gas sweetening unit are absorbed by amine solvent in the Acid Gas Amine Absorber. Similarly the H2S gases produced in the EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 59 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL TGTU are absorbed by amine in the Tail Gas Amine Absorber. The combined rich amines from both the absorber are routed to the Amine Regenerator where the H2S is stripped from the amine by heating. The stripped gases from the regenerator system are routed to SRU. Hydrogen Sulphide, H2S or HSH is a weak acid and ionizes in water to form hydrogen ions and sulphide ions. H+ + SH- HSH Since it is a weak acid, only a small fraction of the HSH will ionize. Ethanolamines are weak bases and ionize in water to form amine ions and hydroxyl ions: (CH3)z (CH3)z (CH2OHCH2)x NHy + H2O Where for MDEA x = 2, y = 0, z = 1 (CH2OHCH2)x NHy+1 + OH- When H2S dissolves into the solution containing the amine ions, it will react to form a weakly bonded salt of the acid and the base. (CH3)z (CH3)z (CH2OHCH2)x NHy+1 + SH(CH2OHCH2)x NHyS The sulphide ion is thus absorbed by the amine solution. This salt formation reaction does not go to completion. As the arrow indicates, and equilibrium level of sulphide ion, SH- remains in the sour gas stream. The overall reaction can be summarized by the following equation: (CH3)z (CH3)z (CH2OHCH2)x NHy + H2S (CH2OHCH2)x N HyS Operating variables are adjusted to favour the forward reaction (absorption process) and conversely, adjusted to favour the reverse reaction (regeneration process). 4.1.2.2 Acid Gas Enrichment Unit Process Description Lean acid gas enters the unit at a temperature of 53°C and a pressure of 0.55 barg. This stream is cooled in Acid Gas Coolers (9103-E-101A/B), before passing to the Lean Acid Gas KO Drum (9103-V-14). The Acid Gas Coolers (9103-E-101A/B) are cooled by sea cooling water. The outlet temperature of the Acid Gas Coolers (9103-E-101A/B) is maintained at 49°C. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 60 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The Lean Acid Gas KO Drum allows bulk removal of any condensed/entrained liquid from upstream. The liquid level in the Lean Acid Gas KO Drum is controlled by pumping the liquid through the Acid Gas KO Drum Return Pumps (9103-P-14A/B) to the existing MDEA storage tank. Alternatively, the sour water can be routed to the sour water stripper, through a normally closed isolation valve. Vapour leaves the Lean Acid Gas KO Drum and fed to the Acid Gas Amine Absorber (9103-C-11), at the bottom. The vapour passes upwards through a trayed section in contact with a lean amine solution. The counter current contact with the amine solution essentially removes all the H2S and some of the mercaptans and part of the CO2 from the vapour stream. If any BTEX exists in the lean acid gas, it is expected that 80-90% will slip directly to the Incinerator. The Acid Gas Amine Absorber (9103-C-11) consists of 10 numbers of valved trays. The feed gas enters below the bottom of the bottom tray. The lean amine enters over the top of the top tray. Lean amine flow to the Acid Gas Amine Absorber is controlled by the flow controller 91-FIC-1501; set point for the controller 91-FIC-1501 is calculated in the block 91-FFY1502 by multiplying the acid gas/lean amine ratio set point (0.02) provided through 91-HIC-1502, with the pressure and temperature compensated acid gas flow (91-FY1502). 91-FIC-1501 regulates the lean amine flow to the acid gas amine absorber via the control valve 91-FV-1501. Acid gas amine absorber (9103-C-11) top pressure is controlled at 0.2 barg by the pressure controller 91-PIC-1502. The pressure is maintained through the pressure control valve 91-PV-1502 located in the treated gas line to the Incinerator. Rich amine from the Tail Gas Amine Absorber enters at the bottom of the column. Treated gas leaving the top of the absorber (9103-C-11) goes to the Incinerator (9101-F-14). The rich amine solution, containing absorbed acid gas, is combined with solvent from the Tail Gas Amine Absorber (9102-C-12). It is removed from the column by the Acid Gas Rich Amine Pump (9103-P-12A/B). This stream is then heated in the Lean/Rich Exchanger, before it is fed to the Amine Regenerator (9103-C-12). The rich amine flow rate is controlled to maintain the level in the Acid Gas Amine Absorber. The amine regeneration facilities required for the Acid Gas Enrichment and Tail Gas Treatment Units are shared with the use of a common solvent. The Amine Regenerator 9103-C-12 consists of 24 numbers of valved trays and one chimney tray. The rich amine enters over the top of the 3rd tray from the top. The rich amine flow is controlled by the flow controller 91-FIC-1520B. The pressure of the Regenerator is controlled by supplying nitrogen through a pressure controller 91-PIC1539. The Regenerator Reboiler vapours enter the bottom of the vessel. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 61 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The Reboiler is heated by LP Steam which is drawn from the steam distribution header. Steam flow to the Regenerator Reboiler is controlled by 91-FIC-1503 which regulates the control valve 91-FV-1503. Set point-1 (SP1) for the steam flow control is received from the calculation block 91-FFY-1503A which multiplies the rich amine flow controller 91-FIC-1520A output and manually provided set ratio (118.5) between steam and rich amine through 91-HIC-1503. Set point-2 (SP2) is received from the output of the Regenerator overhead temperature controller 91-TIC-1510. During normal operation SP1 take precedence and when the temperature of the Regenerator over head reaches more than 118°C SP2 will take precedence. In the Amine Regenerator, the rich solution is stripped counter currently with vapours generated by the Amine Regenerator Reboiler. The bottom of the column is maintained at a temperature by regulating the LP steam flow rate into the Regenerator Reboiler (9103-E-13). The stripping action in the lower section removes and releases the contaminants from the solution, such as the acid gases, mercaptans and residual dissolved hydrocarbons. The stripped vapours are cooled in the Regenerator Condenser Cooler (9103-E-12), and the Regenerator Condenser Trim Cooler (9103-E-16), by regulating air flow by fans in Regenerator Condenser Cooler and adjusting the flow rate of Sea water to the Regenerator Condenser Trim Cooler. Any water and amine in the overhead stream is condensed and collects in the Regenerator Reflux Drum (9103-V-12). The liquid collected from the Regenerator Reflux Drum is pumped by the Regnerator Reflux Drum Pumps 9103-P-11 A/B back to the Regenerator. There is a provision to send the liquid to the Waste Water Degasser 6922-V-07. The reflux flow rate is controlled by maintaining the liquid level in the Regenerator Reflux Drum. Acid gas from the Regenerator Reflux Drum passes overhead to the Sulphur Recovery Unit. Hot lean amine solution from the Regenerator is pumped to the Amine Surge Tank (9103-T-11) by the Hot Lean Amine Pump (9103-P-17 A/B). The Lean/Rich Exchanger (9103-E-11), Lean Amine Cooler (9103-E-14) and Lean Amine Trim Cooler (9103-E-15) cool the solution prior to the Amine Surge Tank. The lean solution from the Amine Surge Tank is pumped to the Acid Gas Amine Absorber and the Tail Gas Amine Absorber via the Lean Amine Pump (9103-P-13A/B). A slipstream is taken off after the pump and returns to the surge tank through the Lean Amine Filter (9103-S-11), Activated Carbon Filter (9103-S-12) and the Fines Filter (9103-S-13). The filters remove particulate matter from the stream as well as hydrocarbons that accumulate in the Amine solution. The Amine Surge Tank (9103-T-11) receives the recycle flow from the filter circuit and the Regenerator. It has the capacity to hold the whole system inventory at shut down. The Amine Surge Tank is maintained at a slightly positive pressure, however not high enough to be able to float on the flare header to maintain pressure and stop ingress of Oxygen. Therefore it is provided with Nitrogen blanketing to prevent air ingress and to minimise the risk of solution degradation. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 62 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL All the amine drains from the unit is collected in the Amine Sump 9103-V-10. The collected amine is pumped to the Amine Surge Tank through the amine filters. The amine sump is blanketed with nitrogen at a slightly positive pressure. 4.1.2.3 Acid Gas Enrichment Unit Process Control 4.1.2.3.1 Lean Acid Gas Knock Out Drum Level Control Lean acid gas knock out drum (9103-V-14) level is maintained by ON/OFF gap controller 91-LIC-1501 which controls the acid gas KO drum return pumps (9103-P-14 A/B) & the discharge line control valve 91-LV-1501. 91-LIC-1501 controls the ON/OFF of Acid Gas Knock Out Drum Return Pumps and discharge line valve by sending the signal 0% or 100%. High level of the level controller 91-LIC-1501 starts the duty Acid Gas Knock Out Drum Return Pump & opens the level control valve 91-LV-1501. Low level of the controller closes the level control valve 91-LV-1501 and stops the duty Acid Gas Knock Out Drum Return Pump. Acid Gas Knock Out Drum Return pumps ON or OFF can be done by the controller only when the pumps are in auto mode which is selected through the switch (91-HS-1562 & 91-HS-1563). Controller Tag 91-LIC-1501 Control Description Unit Lean Acid Gas KO Drum level control % Alarm Low High 12 37 • High high level alarm (91-LAHH-1502) in Lean acid gas KO drum closes the acid gas block valve 91-XV-1501 • Low low level alarm (91-LALL-1503) in Lean acid gas KO drum trips the acid gas return pumps (9103-P-14A/B) and closes the on/off valve 91-XV-1503 located at the liquid outlet line from acid gas KO drum (downstream of the control valve 91-LV-1501) • Acid Gas KO Drum Return Pumps discharge control valve 91-LV-1501 closes on instrument air failure 4.1.2.3.2 Acid Gas Absorber Top Pressure Control Acid gas amine absorber (9103-C-11) top pressure is controlled by the pressure controller 91-PIC-1502. The pressure is maintained through the pressure control valve 91-PV-1502 located in the treated gas line to the Incinerator. Alarm Controller Tag Control Description Unit Operating Set Point Low High 91-PIC-1502 Amine absorber top pressure control bar(g) 0.2 NA NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 63 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Acid gas amine absorber top pressure control valve 91-PV-1502 opens on instrument air failure. 4.1.2.3.3 Acid Gas/Lean Amine Flow Ratio Control Acid gas flow to the acid gas amine absorber (9103-C-11) is measured by 91-FT-1502. Lean amine flow to the Acid Gas Amine Absorber is controlled by the flow controller 91-FIC-1501; set point for the controller 91-FIC-1501 is calculated in the block 91-FFY-1502 by multiplying the acid gas/lean amine ratio set point (0.02) provided through 91-HIC-1502, with the pressure and temperature compensated acid gas flow (91-FY-1502). 91-FIC-1501 regulates the lean amine flow to the acid gas amine absorber via the control valve 91-FV-1501. Control Loop Controller Tag 91-FIC-1501 Control Description Lean amine flow to absorber Unit 3 m /hr Alarm Operating Set Point Low High 487 390 536 • High high level alarm (91-LAHH-1504) in Acid Gas Amine Absorber bottom closes the lean amine ON/OFF valve 91-XV-1504 located at the downstream of 91-FV-1501. • Lean amine flow control valve 91-FV-1501 to acid gas amine absorber closes on instrument air failure. 4.1.2.3.4 Acid Gas Amine Absorber Level Control Rich amine solution from the TGTU Tail Gas Amine Absorber combines with the rich amine at the bottom section of the Acid Gas Amine Absorber. The master level controller 91-LIC-1505 controls the rich amine level at the bottom of the Acid Gas Amine Absorber by controlling the cascaded slave rich amine flow controller 91-FIC-1520B, which regulates the Acid Gas Rich Amine Pumps (9103-P12A/B) discharge flow to Amine Regenerator 9103-C-12 via Lean/Rich Amine Exchanger 9103-E-11A/B through the control valve 91-FV-1520 located at the inlet of the Amine Regenerator 9103-C-12. Controller Tag • Control Description 91-LIC-1505 Absorber level control 91-FIC-1520B Rich amine flow to Amine Regenerator Alarm Unit Operating Set Point Low High % 50 12 86 m3/hr 635 500 NA High high level alarm (91-LAHH-1504) in Acid Gas Amine Absorber bottom activates the ESD Level-2 shutdown EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 64 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Low low level alarm (91-LALL-1516) in Acid Gas Amine Absorber bottom trips the Acid Gas Rich Amine Pumps (9103-P-12A/B) • Rich amine flow control valve 91-FV-1520 to Amine Regenerator closes on instrument air failure. 4.1.2.3.5 Acid Gas Rich Amine Pumps Minimum Flow Control Acid Gas Rich Amine Pumps (9103-P-12A/B) discharge flow is measured by 91-FT-1508 and minimum flow to Acid Gas Amine Absorber bottom is controlled by 91-FIC-1508. The controller 91-FIC-1508 controls the pump minimum flow control valve 91-FV-1508 to Acid Gas Amine Absorber bottom. Controller Tag 91-FIC-1508 Control Description Acid Gas Rich Amine Pump minimum flow Alarm Unit Operating Set Point Low High m3/hr 375 330 NA • Low low flow alarm (91-FALL-1510) set at 300 m3/hr in 9103-P-12A/B discharge, trips the Acid Gas Rich Amine Pumps 9103-P-12A/B • Pump minimum flow control valve 91-FV-1508 opens on instrument air failure. 4.1.2.3.6 Rich Amine to Regenerator Temperature Control Rich amine solution leaving the Lean/Rich Amine Exchanger (9103-E-11-A/B) temperature is maintained by the temperature controller 91-TIC-1513. Temperature controller 91-TIC-1513 is located at hot rich amine outlet leaving the exchanger. The output from this controller resets the control valve 91-TV-1513 on the hot lean amine solution bypass line around the Lean/Rich Amine Exchanger. Controller Tag 91-TIC-1513 Control Description Rich Amine to Amine Regenerator temperature Control Alarm Unit Operating Set Point Low High °C 104 99 109 Hot lean amine bypass control valve 91-TV-1513 locks on instrument air failure. 4.1.2.3.7 Amine Regenerator Overhead Pressure Control Amine regenerator overhead pressure is controlled by the pressure controller 91-PIC1539. The pressure is maintained through the pressure control valve 91-PV-1539 by controlling the nitrogen supply to the Regenerator. 91-PIC-1539 opens the Nitrogen control valve 91-PV-1539 on falling pressure in the Regenerator over head to Regenerator Condenser Cooler. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 65 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Controller Tag 91-PIC-1539 Control Description Amine Regenerator top pressure control Unit Bar g Operating Set Point 1.2 Alarm Low 0.95 High 1.4 Amine Regenerator 9103-C-12 top pressure nitrogen control valve 91-PV-1539 opens on instrument air failure. 4.1.2.3.8 Amine Regenerator Level Control The master level controller 91-LIC-1510 maintains the bottom level of Amine Regenerator by controlling the cascaded slave lean amine flow controller 91-FIC-1530, which regulates the Hot Lean Amine Pumps (9103-P-17A/B) discharge flow to Lean Rich Amine Exchanger through the control valve 91-FV-1530 located at the outlet of Lean Amine Trim Cooler 9103-E-15. Controller Tag Control Description 91-LIC-1510 Amine Regenerator bottom level control 91-FIC-1530 Lean amine flow to 9103-T-11 Alarm Unit Operating Set Point Low High % 50 17 82 m3/hr 669 NA NA • Low low level alarm (91-LALL-1517) in Amine Regenerator bottom trips the Hot Lean Amine Pumps (9103-P-17A/B) and closes the Hot Lean Amine ON/OFF valve 91-XV-1507 to Lean Rich Exchanger • High high level alarm (91-LAHH-1509) in Amine Regenerator bottom activates the ESD level-2 shutdown • Lean amine outlet flow control valve 91-FV-1530 to Amine Surge Tank closes on instrument air failure 4.1.2.3.9 Hot Lean Amine Pumps Minimum Flow Control Hot lean amine pumps (9103-P-17A/B) discharge flow is measured by 91-FT-1512 and pumps minimum flow to Amine Regenerator bottom is controlled by 91-FIC-1512. Output of the controller 91-FIC-1512 controls the pump minimum flow control valve 91-FV-1512. Controller Tag 91-FIC-1512 Control Description Hot Lean Amine Pump min flow Alarm Unit Operating Set Point Low High m3/hr 250 220 NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 66 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Hot Lean Amine Pumps 9103-P-17A/B discharge flow low low alarm (91-FALL-1509) set at 200 m3/hr will activate the tripping of 9103-P-17A/B. • Pump minimum flow control valve 91-FV-1512 opens on instrument air failure. 4.1.2.3.10 Regenerator Condenser Cooler Control Temperature of the acid gas flow from the Amine Regenerator overhead is controlled by cooling the fluid to Tmax=54°C in summer and not less than Tmin=49°C in winter using one fixed speed fan (on/off) control, and another two VSD controlled fans working simultaneously. The Regenerator Condenser Cooler outlet temperature is measured by 91-TT-1516 and received by the temperature controller 91-TIC-1516. The output of this controller sends the control signal to control the three fans. In auto mode, the temperature controller maintains the cooler outlet temperature at Tset= (54°C + 49°C)/2=52°C by changing the VSD rates of the following cooler fans: • 9103-EM-12AB • 9103-EM-12AC • 9103-EM-12BB • 9103-EM-12BC • 9103-EM-12CB • 9103-EM-12CC • 9103-EM-12DB • 9103-EM-12DC The fixed speed fan (9103-EM-12AA/BA/CA/DA) operates on gap control set point between the values Tmax=54°C & Tmin=49°C. This scheme will be applicable for all the 4 bays simultaneously. Details of control tags are tabulated below: Sl. # Motor No. Control Tag Remarks 1 9103-EM-12AA 91-HS-1512 Fixed speed fan 2 9103-EM-12AA 91-SY-1513 VSD 3 9103-EM-12AA 91-SY-1552 VSD 4 9103-EM-12BA 91-HS-1553 Fixed speed fan 5 9103-EM-12BB 91-HS-1554 VSD 6 9103-EM-12BC 91-HS-1555 VSD 7 9103-EM-12CA 91-HS-1556 Fixed speed fan 8 9103-EM-12CB 91-HS-1557 VSD EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 67 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Motor No. Control Tag Remarks 9 9103-EM-12CC 91-HS-1558 VSD 10 9103-EM-12DA 91-HS-1559 Fixed speed fan 11 9103-EM-12DB 91-HS-1560 VSD 12 9103-EM-12DC 91-HS-1561 VSD High high vibration alarm of each fan trips the respective fan motors. 4.1.2.3.11 Regenerator Condenser Trim Cooler Outlet Temperature Control 91-TIC-1502 located at the outlet of the Regenerator Condenser Trim Cooler, maintains the outlet temperature of the acid gas condensate to Regenerator Reflux Drum. The temperature controller adjusts the bypass control valve 91-TV-1502 and maintains the Regenerator Condenser Trim Cooler outlet temperature 91-TT-1502. Controller Tag 91-TIC-1502 Alarm Control Description Unit Operating Set Point Low High Regenerator Condenser Trim Cooler Outlet Temperature °C 49 44 54 Regenerator Condenser Cooler 9103-E-12 outlet temperature control valve 91-TV-1502 to reflux drum opens on instrument air failure. 4.1.2.3.12 Regenerator Reflux Drums Level Control Bottom level in the Regenerator Reflux Drum level is maintained by controlling the reflux return to the Amine Regenerator via Reflux Drum Pumps 9103-P-11A/B. Regenerator reflux drum bottom level is controlled by the master controller 91-LIC1506 cascaded with the reflux pumps discharge flow slave controller 91-FIC-1531, which regulates the control valve 91-FV-1531 located in the reflux inlet to Amine Regenerator. Controller Tag Control Description 91-LIC-1506 Regenerator reflux drum level control 91-FIC-1531 Reflux to amine regenerator Alarm Unit Operating Set Point Low High % 50 16 80 m3/hr 26 NA NA • Low low level alarm (91-LALL-1518) in Regenerator Reflux Drum trips the Reflux Drum Pumps (9103-P-11A/B) • High high level alarm (91-LAHH-1507) in Regenerator Reflux Drum closes the DM water ON/OFF valve 91-XV-1517 to Regenerator Reflux Drum EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 68 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Reflux flow control valve 91-FV-1531 to Amine Regenerator opens on instrument air failure. • 4.1.2.3.13 Regenerator Reflux Drums Condensate Control Condensate flow to the Regenerator Reflux Drum bottom is measured by 91-FT-1521 and controlled by 91-FIC-1521. Condensate flow is controlled through the control valve 91-FV-1521. Controller Tag Control Description 91-FIC-1521 Regenerator reflux drum condensate flow control Alarm Unit Operating Set Point Low High m3/hr 0.6 0.4 0.8 • ESD valve 91-XV-1517 located at the upstream of the control valve 91-FV-1521 closes on high high level alarm 91-LAHH-1507 of Regenerator Reflux Drum • Condensate flow control valve 91-FV-1521 closes on instrument air failure. 4.1.2.3.13 Regenerator Reflux Drums Pressure Control A split range pressure controller 91-PIC-1503 is provided to maintain the pressure of Regenerator Reflux Drum (9103-V-12) by controlling the following valves: • Acid gas control valve 91-PV-1503B (0-50%) to acid gas KO drum 9101-V-04 • Acid gas control valve 91-PV-1503A (50-100%) to LP Acid Gas Flare On rising pressure 91-PIC-1503 first opens the acid gas to Acid Gas KO Drum control valve 91-PV-1503B; further increase in pressure causes the pressure controller to open the vent valve 91-PV-1503A to release gases to the LP Acid Gas Flare. Fig. 14 – 91-PIC-1503 Controller Output The above drawing shows the split range operation of 91-PV-1503A & 91-PV-1503B. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 69 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Alarm Controller Tag Control Description Unit Operating Set Point Low High 91-PIC-1503 Regenerator Reflux Drum pressure bar(g ) 1 0.787 1.2 • ESD valve 91-XV-1516 located at the acid gas to Acid Gas KO Drum control valve downstream • Control valve 91-PV-1503B closes on ESD-Level-0, Level-1 & Level-2 shutdown • Regenerator Reflux Drum 9103-V-12 pressure control valve 91-PV-1503A to LP flare opens on instrument air failure • Regenerator Reflux Drum 9103-V-12 pressure control valve 91-PV-1503B to Acid Gas KO Drum closes on instrument air failure. 4.1.2.3.14 Regenerator Reflux Pumps Minimum Flow Control Regenerator Reflux Pumps (9103-P-11A/B) discharge flow is measured by 91-FT-1505 and minimum flow to Amine Regenerator is controlled by 91-FIC-1505. Output of the controller 91-FIC-1505 controls the pump minimum flow control valve 91-FV-1505. Controller Tag Control Description 91-FIC-1505 Regenerator Reflux Drum pumps to Regenerator Alarm Unit Operating Set Point Low High m3/hr 20 17.6 NA • Low low flow alarm (91-FALL-1506) set at 16 m3/hr trips the Regenerator Reflux Pumps 9103-P-11A/B • Pump minimum flow control valve 91-FV-1505 opens on instrument air failure. 4.1.2.3.15 Sour Water Flow Control to Waste Water Degasser Sour water flow from the discharge of Regenerator Reflux Drum Pumps (9103-P-11A/B) to the Waste Water Degasser (6922-V-07) is measured by 91-FT-1532 and sends the signal to the flow controller 91-FIC-1532. 91-FIC-1532 regulates the flow to Waste Water Degasser via the control valve 91-FV1532. Control Loop: Controller Tag 91-FIC-1532 Control Description Sour water flow to Waste Water Degasser Alarm Unit Operating Set Point Low High m3/hr 0.17 NA NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 70 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • ESD valve 91-XV-1575 located at the downstream of the sour water flow control valve 91-FV-1532 closes on activation of waste water degasser level (69-LI-1311) high high alarm • Sour water flow control valve 91-FV-1532 closes on instrument air failure. 4.1.2.3.16 Amine Regenerator Reboiler Temperature Control Temperature in the amine regenerator is to be maintained to allow for optimum H2S stripping from the rich amine. Temperature control is achieved by controlling the steam flow to the Regenerator Reboiler. Steam flow to the Regenerator Reboiler is controlled by 91-FIC-1503 which regulates the control valve 91-FV-1503. Set point-1 (SP1) for the steam flow control is received from the calculation block 91-FFY-1503A which multiplies the rich amine flow controller 91-FIC-1520A output and manually provided set ratio (118.5) between steam and rich amine through 91-HIC-1503. Set point-2 (SP2) is received from the output of the Regenerator overhead temperature controller 91-TIC-1510. During normal operation SP1 take precedence and when the temperature of the Regenerator over head reaches more than 118°C SP2 will take precedence. Controller Tag Control Description 91-FIC-1503 Steam to Regenerator Re-boiler 91-TIC-1510 Amine Regenerator (9103-C12) overhead 91-FIC-1520A Rich amine flow control Alarm Unit Operating Set Point Low High Kg/hr 72410 65816 80442 °C 118 113 123 m3/hr 635 500 NA • ESD valve 91-XV-1505 located on the upstream of 91-FV-1503 closes on activation of amine regenerator bottom level 91-LI-1509 high high alarm set at 50% • Steam control valve 91-FV-1503 to reboiler closes on instrument air failure. 4.1.2.3.17 Regenerator Re-Boiler Condensate Pot Level Control Regenerator Reboiler condensate is collected in the Condensate Pot (9103-V-13). Level of the Condensate Pot is measured by 91-LT-1508 and controlled by throttling the control valve 91-LV-1508 to LC distribution header via 91-LIC-1508. Controller Tag 91-LIC-1508 Control Description Regenerator Re-boiler Condensate Pot level Alarm Unit Operating Set Point Low High % 50 12 86 Reboiler condensate control valve 91-LV-1508 will close on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 71 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.1.2.3.18 Lean Amine Cooler Temperature Control Temperature of the lean amine from the Lean/Rich Exchanger (9103-E-11) is controlled by cooling the fluid to Tmax=54°C in summer and not less than Tmin=45°C in winter using three fans: one fixed speed fan (on/off) control, and another two VSD controlled fans working simultaneously. The Lean Amine Cooler 9103-E-14 outlet temperature is measured by 91-TT-1518 and controlled by the temperature controller 91-TIC-1518. The output of this controller sends the control signal to control the three fans. In auto mode, the temperature controller maintains the cooler outlet temperature T set= (54°C + 45°C)/2=50°C by changing the following VSD rates: (9103-EM-14AB/AC/BB/BC/CB/CC/DB/DC/EB/EC/FB/FC/GB/GC/HB/HC/IB/IC/JB/JC) The fixed speed fan (9103-EM-14AA/BA/CA/DA/EA/FA/GA/HA/IA/JA) operates on gap control set point between the values Tmax=54°C & Tmin=45°C. This scheme will be applicable for all the 10 bays simultaneously. Details of control tags are tabulated below: Sl. # Motor No. Control Tag Remarks 1. 9103-EM-14AA 91-HS-1514 Fixed speed fan 2. 9103-EM-14AB 91-SY-1515 VSD 3. 9103-EM-14AC 91-SY-1558 VSD 4. 9103-EM-14BA 91-HS-1519 Fixed speed fan 5. 9103-EM-14BB 91-SY-1520 VSD 6. 9103-EM-14BC 91-SY-1521 VSD 7. 9103-EM-14CA 91-HS-1522 Fixed speed fan 8. 9103-EM-14CB 91-SY-1523 VSD 9. 9103-EM-14CC 91-SY-1524 VSD 10. 9103-EM-14DA 91-HS-1525 Fixed speed fan 11. 9103-EM-14DB 91-SY-1526 VSD 12. 9103-EM-14DC 91-SY-1527 VSD 13. 9103-EM-14EA 91-HS-1528 Fixed speed fan 14. 9103-EM-14EB 91-SY-1529 VSD 15. 9103-EM-14EC 91-SY-1530 VSD 16. 9103-EM-14FA 91-HS-1531 Fixed speed fan 17. 9103-EM-14FB 91-SY-1532 VSD 18. 9103-EM-14FC 91-SY-1533 VSD 19. 9103-EM-14GA 91-HS-1534 Fixed speed fan 20. 9103-EM-14GB 91-SY-1535 VSD EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 72 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Motor No. Control Tag Remarks 21. 9103-EM-14GC 91-SY-1536 VSD 22. 9103-EM-14HA 91-HS-1537 Fixed speed fan 23. 9103-EM-14HB 91-SY-1538 VSD 24. 9103-EM-14HC 91-SY-1539 VSD 25. 9103-EM-14IA 91-HS-1540 Fixed speed fan 26. 9103-EM-14IB 91-SY-1541 VSD 27. 9103-EM-14IC 91-SY-1542 VSD 28. 9103-EM-14JA 91-HS-1543 Fixed speed fan 29. 9103-EM-14JB 91-SY-1544 VSD 30. 9103-EM-14JC 91-SY-1545 VSD High high vibration alarm of each fan trips the respective fan motors. 4.1.2.3.19 Lean Amine Trim Cooler Outlet Temperature Control 91-TIC-1509 located at the outlet of the Lean Amine Trim Cooler (9103-E-15) maintains the outlet temperature of the lean amine to Amine Surge Tank (9103-T-11). The temperature controller 91-TIC-1509 adjusts the control valve 91-TV-1509 located in the bypass line of Lean Amine Trim Cooler maintains the lean amine outlet temperature. Controller Tag 91-TIC-1509 Alarm Control Description Unit Operating Set Point Low High Lean amine Cooler to amine surge tank °C 45 40 50 Lean amine cooler bypass control valve 91-TV-1509 closes on instrument air failure. 4.1.2.3.20 Lean Amine Surge Tank Pressure Control A split range pressure controller 91-PIC-1526 is provided to maintain the vapour space of the tank under a slightly positive pressure. On rising pressure in the tank, 91-PIC1526 closes (0-50%) the nitrogen flow to tank via the control valve 91-PV-1526A, on further increase in pressure the pressure controller 91-PIC-1526 opens (50-100%) the vent valve 91-PV-1526B to release gases to the atmosphere. Controller Tag 91-PIC-1526 Control Description Lean amine surge tank (9103-T-11) pressure Alarm Unit Operating Set Point Low High bar(g) 0.02 0.01 0.03 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 73 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 15 – 91-PIC-1526 Controller Output The above drawing shows the split range operation of 91-PV-1526A & 91-PV-1526B. • Amine Surge Tank 9103-T-11 nitrogen line control valve 91-PV-1526A closes on instrument air failure. • Amine Surge Tank 9103-T-11 control valve control valve 91-PV-1526B opens on instrument air failure. 4.1.2.3.21 Lean Amine Pumps Minimum Flow Control Lean amine pumps (9103-P-13A/B) discharge flow is measured by 91-FT-1511 and minimum flow to Amine Surge Tank is controlled by 91-FIC-1511. Output of the controller 91-FIC-1511 throttles the pump minimum flow control valve 91-FV-1511. Control Loop: Controller Tag 91-FIC-1511 Control Description Lean Amine Pumps discharge Alarm Unit Operating Set Point Low High m3/hr 375 330 NA Low low flow (91-FALL-1515) alarm set at 300 m3/hr trips the Lean Amine Pumps 9103-P-13A/B. 4.1.2.3.22 Amine Sump Pressure Control A split range pressure controller 91-PIC-1527 is provided to maintain the vapour space of the tank under a slightly positive pressure. On rising pressure in the tank, 91-PIC1527 closes (0-50%) the nitrogen flow to tank via the control valve 91-PV-1527A, on further rising pressure, the pressure controller 91-PIC-1527 opens (50-100%) the vent valve 91-PV-1527B to release gases to the atmosphere. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 74 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The below drawing shows the split range operation of 91-PV-1527A & 91-PV-1527B: Fig. 16 – 91-PIC-1527 Controller Output Control Loop: Controller Tag 91-PIC-1527 Control Description Amine Sump pressure control Alarm Unit Operating Set Point Low High bar(g) 0.05 0.027 0.07 • Amine sump 9103-V-10 nitrogen line control valve 91-PV-1527A closes on instrument air failure • Amine Sump 9103-V-10 nitrogen control valve 91-PV-1527B opens on instrument air failure. 4.1.2.3.23 Lean Amine Pumps Flow to Filter Lean Amine Pumps (9103-P-13A/B) discharge flow to Lean Amine Filter (9103-S-11) is controlled by 91-FIC-1507. Output of the controller 91-FIC-1507 resets the control valve 91-FV-1507. Controller Tag 91-FIC-1507 Alarm Control Description Unit Operating Set Point Low High Lean Amine Pumps to Lean Amine Filter m3/hr 155.6 125 NA Lean Amine Pumps 9103-P-13A/B flow control valve 91-FV-1507 to filter closes on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 75 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.2 4.2.1 SULPHUR RECOVERY UNIT Equipment Details Process Air Blowers Equipment Tag No. Process Medium Rated Capacity (Dry Base), kg/hr 9101-K-01A/B Air 29478 Inlet Pressure, bar(a) 1.01 Inlet Temperature, °C 43 Discharge Pressure, bar(a) 1.90 Discharge Temperature, °C 49 Design Temperature, °C 120 Drive Type Motor Sulphur Degassing Pumps Equipment Tag No. Pump Type 9101-P-03A/B Vertical Centrifugal Process Medium 3 Liquid Sulphur Capacity, m /hr (Normal/Rated) 130/130 Suction Pressure, bar(a), Rated/Max. 1.0/1.61 Discharge Pressure, bar(a) Operating Temperature, °C, Normal/Max. Design Temperature, °C Driver Type 8.6 140/160 185 Motor Rated Power, kW Material of Construction, Casing/Impeller 45 Duplex SS Sulphur Product Pumps Equipment Tag No. Pump Type 9101-P-04A/B Vertical Centrifugal Process Medium 3 Liquid Sulphur Capacity, m /hr (Normal/Rated) 130/130 Suction Pressure, bar(a), Rated/Max. 1.0/1.61 Discharge Pressure, bar(a) Operating Temperature, °C, Normal/Max. Design Temperature, °C Driver Type Rated Power, kW Material of Construction, Casing/Impeller 8.6 140/160 185 Motor 45 Duplex SS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 76 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sulphur Tank Pumps Equipment Tag No. 9101-P-15A/B Process Medium Liquid Sulphur 3 Capacity, m /hr (Normal/Rated) 7.4/8.14 Suction Pressure, bar(a), Rated/Max. 0.9/2.5 Discharge Pressure, bar(a) 9.6 Operating Temperature, °C, Normal/Max. 160 Design Temperature, °C 185 Driver Type Motor Rated Power, kW Material of Construction, Casing/Impeller 11 A216WCB Sulphur Degassing Pit Equipment Tag No. 9101-T-01B Size, (L/W/D), mm 10800/7000/3000 Process Medium Operating Temperature, °C, Normal/Min. Liquid Sulphur 140/127 Operating Pressure, bar(g) ATM Design Temperature, °C 185 Design Pressure, bar(g) 0.02/-0.005 Material of Construction Reinforced Concrete Sulphur Degassing Pumps Equipment Tag No. Pump Type 9101-P-09A/B Vertical Centrifugal Process Medium 3 Liquid Sulphur Capacity, m /hr (Normal/Rated) 130/130 Suction Pressure, bar(a), Rated/Max. 1.0/1.61 Discharge Pressure, bar(a) Operating Temperature, °C, Normal/Max. Design Temperature, °C Driver Type Rated Power, kW Material of Construction, Casing/Impeller 8.6 140/160 185 Motor 45 A 995 1B/A 995 1B EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 77 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sulphur Product Pumps Equipment Tag No. Pump Type 9101-P-10A/B Vertical Centrifugal Process Medium 3 Liquid Sulphur Capacity, m /hr (Normal/Rated) 130/130 Suction Pressure, bar(a), Rated/Max. 1.0/1.61 Discharge Pressure, bar(a) Operating Temperature, °C, Normal/Max. Design Temperature, °C Driver Type 8.6 140/160 185 Motor Rated Power, kW Material of Construction, Casing/Impeller 45 Duplex SS Catalyst Tank Equipment Tag No. 9101-T-09 Size, (ID/Ht), mm 700/1000 Process Medium Catalyst Design Temperature, °C 85 Design Pressure, bar(g) ATM Catalyst Metering Pumps Equipment Tag No. Process Medium 9101-P-11A/B Catalyst Design Temperature, °C 85 Design Pressure, bar(g) 2.0 Drive Motor Rated Power, kW 0.55 Steam Ejector Equipment Tag No. 3 4.2.2 9101-X-03 Capacity, Nm /hr 500 Design Temperature, °C 185 Differential Pressure, bar 0.1 Revamped Claus Unit Process Chemistry The function of a SRU is to process H2S rich acid gases to produce liquid elemental Sulphur. The sulphur recovery Claus process combines 2 mols of H2S with 1 mol. of SO2 to form elemental sulphur. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 78 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL In the modified Claus process some of the H2S rich acid gas is burnt with the correct amount of Oxygen (from air) to oxidise one third of the H2S to SO2: Main Reactions: H2S + 3/2O2 —> SO2 + H2O This reaction produces a high enough temperature to trigger the Claus reaction thermally: 2H2S + SO2 —> 3S + 2H2O The Claus reaction is continued at progressively lower temperatures in the two catalytic stages where the remaining H2S then combines with the SO2 & produce elemental Sulphur. 4.2.3 Revamped Claus Unit Process Description The acid gas stream from the gas treating plant enters the Acid Gas KO Drum (9101-V04) where acid water is knocked out and pumped to Amine Sump 9103-V-10 by the Acid Water Pumps 9101-P-01A/B. The gas stream flows to Acid Gas Preheater (9101-E06) for preheating before entering the Reaction Furnace (9101-F-01), where the acid gas is burnt by the high intensity burner with a controlled amount of air. Air is supplied by an electrically driven Process Air Blower (9101-K-01A/B) & preheated by Air Preheater (9101-E-05). The products of the combustion are cooled in passing through the tube section of the Reaction Furnace Boiler (9101-E-07) where a 24 bar(g) steam is generated in the shell side. Gases and any condensed liquid sulphur from the Reaction Furnace Boiler flow to the Reaction Furnace Condenser (9101-E-01) where the gases are cooled and the additional sulphur is condensed. The gases then passes through the 1st Stage Auxiliary Burner (9101-F-02) where they are reheated by burning a split stream of acid gas (or fuel gas) with air, before entering the 1st Stage Converter (9101-V-01). In this converter the gases flow downwards through a bed of CR 4/8 mm activated alumina, top loaded with a layer of AM 4/8 catalyst. In the converter, additional elemental sulphur is produced and carried over in vapour phase by the hot gases. The exothermic Claus reaction results in a temperature increase through the adiabatic converter. The hot gases leaving the first converter are cooled in the 1st Stage Condenser (9101-E-02) by generating 5 barg steam, the condensed sulphur flows to the Sulphur Degassing Pit (9101-T-01/01B) through Sultraps. The gases from the Sulphur Condenser (9101-E-02) flow through a coalescer equipped with SS wire mesh pads for the removal of any entrained sulphur. The gases then passes through the 2nd Stage Auxiliary Burner (9101-F-03) where they are reheated by burning a split stream of acid gas (or fuel gas) with air, before entering the 2nd Stage Converter (9101-V-02), loaded with a more active catalyst CRS 31 and a layer of AM 4/8 mm catalyst on the top of the bed. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 79 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The Last Condenser (9101-E-04) ensures cooling of the process gases by preheating the Boiler Feed Water which is used in the Reaction Furnace Boiler (9101-E-07) and the two LP steam producing Reaction Furnace Condenser (9101-E-01) & 1st Stage Condenser (9101-E-02). The process gases from Last Condenser passes through a Final Separator (9101-V-05) to achieve complete removal of liquid sulphur drops from the process gases. A coalescer is provided in Final Separator (9101-V-05). From final separator, the process gas is routed to Tail Gas Treatment Unit, where the hydrogen sulphide concentration in the tail gas is reduced to a level corresponding to >99.5% total sulphur recovery. The sulphur produced in the process is extracted from all sulphur condensers through sultraps and is routed to the Sulphur Degassing Pits (9101-T-01/9101-T-01B). The sulphur is degassed through AQUISULF sulphur degassing process. The degassed sulphur is then transferred to the Sulphur Storage Tank 9101-T-02 by Sulphur Product Pumps (9101-P-04A/B & 9101-P-10A/B). 4.2.4 Sulphur Recovery Unit Process Control 4.2.4.1 Pipe Separator Level Control The acid gas stream from NGL-3 AGRU-1 & 2 enters the pipe separator where the acid gas is routed to the top of the separator to AGEU acid gas coolers and the bottom liquid is drained to amine drain distribution header. Level in the vessel is maintained by regulating the control valve 91-LV-1053, in the pipe separator bottom to amine drain distribution header through 91-LIC-1053. Control Loops: Controller Tag 91-LIC-1053 Alarm Control Description Unit Operating Set Point Low High Pipe separator level control % 50 14 98 • Low low level alarm (91-LALL-1054) set at 33% in the pipe separator closes the liquid outlet block valve 91-XV-1109. • Pipe separator level control valve 91-LV-1503 to amine drain distribution header closes on instrument air failure. 4.2.4.2 BFW Pre-heater Temperature Control Temperature of the heated water outlet from the BFW pre heater is monitored by 91-TT-1091 and controlled by 91-TIC-1091. Temperature control is achieved by regulating the LP steam flow control valve 91-FV-1057 to BFW Preheater by 91-FIC-1057. The MASTER temperature controller 91-TIC-1091 is cascaded with SLAVE steam flow controller 91-FIC-1057. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 80 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Controller Tag Control Description Alarm Unit Operating Set Point Low High 91-TIC-1091 BFW Preheater outlet temperature °C 120 115 125 91-FIC-1057 LP steam flow to BFW Preheater Kg/hr 860 775 947 LP steam control valve 91-FV-1057 closes on instrument air failure. 4.2.4.3 Last Condenser Outlet Tail Gas Control Tail gas from the Last Condenser is routed to the Incinerator through 91-XV-1097 during start-up and during normal operation tail gas is routed to TGTU through 91-XV1098. This diversion is achieved by activating the selector switch 91-HS-1052A. This opens the valve 91-XV-1098, when 91-XV-1098 is fully open the valve 91-XV-1097 closes. This ensures that at least one path is fully open for the tail gas to pass through without pressuring the upstream reaction furnace. • High high pressure alarm 91-PAHH-1055 set at 0.73 barg opens the valve 91-XV1097 to Incinerator and closes the valve 91-XV-1098 to RGG • ESD valve 91-XV-1097 opens on instrument air failure • ESD valve 91-XV-1098 closes on instrument air failure 4.2.4.4 New Sulphur Degassing Pit Level Control New Sulphur Degassing Pit (9101-T-01B) level is measured by 91-LT-1051 which sends the signal to the level controller 91-LIC-1051. Level control is achieved by regulating the control valve 91-LV-1051 to the sulphur storage tank (9101-T-02). Controller Tag 91-LIC-1051 Alarm Control Description Unit Operating Set Point Low High Sulphur Degassing Pit level % 50 17 80 • Low low level alarm 91-LALL-1052 set at 10% trips the Sulphur Degassing Pumps (9101-P-09A/B) and Sulphur Product Pumps (9101-P-10A/B) • Sulphur Degassing Pit level control valve 91-LV-1051 closes on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 81 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.2.4.5 Combustion Control for 1st Stage Auxiliary Burner During normal operation the Air/Acid Gas ratio controller maintains the temperature of the process gas and when the acid gas flow decreases, the temperature of the process gas is maintained by the Air to Fuel gas ratio controller. Selection of this controller can be either manual through 91-HS-1028A or automatically when the temperature 91-TICA-1007 of the 1st stage burner outlet reduces below the desired set point (210°C). This reduction in temperature stops the acid gas flow in the 1st stage auxiliary burner. Acid gas flow to 1st stage auxiliary burner is controlled by 91-FIC-1019 and fuel gas flow is controlled by 91-FIC-1020, set point for both the controllers is provided by 91-TICA1007 via selector switch 91-HS-1028A. 91-FIC-1019 commands the acid gas flow valve 91-FV-1019 and 91-FIC-1020 commands the fuel gas control valve 91-FV-1020. Ratio set point (air/fuel gas) and (air/acid gas) is provided via 91-HIC-1018A and 91-HIC-1018B, respectively. Combustion air flow is controlled by 91-FIC-1018. Set point for the controller is provided by air/acid gas or air/fuel gas ratio calculation as per selection through 91-HS-1028B and output of the combustion air flow controller 91-FIC-1018 directly commands the air damper valve 91-FV-1018. Controller Tag Control Description Alarm Unit Operating Set Point Low High °C 230 210 250 st 91-TICA-1007 1 Stage Auxiliary Burner temperature 91-FIC-1019 acid gas flow Sm3/hr 281.939 111 332 comb air flow 3 Sm /hr 908.768 NA 981 3 159.635 8 170 91-FIC-1018 91-FIC-1020 fuel gas flow Sm /hr EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 82 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The schematic diagram for 1st stage auxiliary burner temperature control is shown below: Fig. 17 – 1st Stage Auxiliary Burner Temperature Control EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 83 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 1st Stage Auxiliary Burner combustion air flow (91-FI-1133) low low alarm set at 253 Sm3/hr, acid gas flow (91-FI-1134) low low alarm set at 105 Sm3/hr and Fuel gas Flow (91-FI-1135) low low alarm set at 7 Sm3/hr activates the following: • 4.2.4.6 • Closure of Fuel gas block valves 91-XV-1028 and 91-XV-1031. • Opening of fuel gas vent valve 91-XV-1132 • Closure of fuel gas control valve 91-FV-1020 • Closure of acid gas control valve 91-FV-1019 • Closure of combustion air control valve 91-FV-1018 • 1st stage combustion air damper/control valve 91-FV-1018 opens on instrument air failure • 1st stage acid gas control valve 91-FV-1019 closes on instrument air failure • 1st stage fuel gas control valve 91-FV-1020 closes on instrument air failure. Combustion Control for 2nd Stage Auxiliary Burner During normal operation the Air/Acid Gas ratio control maintains the temperature of the process gas flowing through the catalytic converter and then to sulphur condenser. When the Acid gas flow decreases, the temperature of the process gas is maintained by the Air to Fuel gas ratio controller. The selection of this controller can be either manual through 91-HS-1029A or automatically when the temperature 91-TIC-1019 reduces below the desired set point (210°C). This reduction in temperature stops acid gas flow and introduce fuel gas flow in the 2nd stage Auxiliary burner. Acid gas flow to 2nd Stage Auxiliary Burner is controlled by 91-FIC-1026 and the fuel gas flow is controlled by 91-FIC-1027. Set point for both the controllers is provided by 2nd Stage Auxiliary Burner temperature controller 91-TIC-1019 via selector switch 91-HS-1029A. Output of the controller 91-FIC-1026 commands the acid gas flow control valve 91-FV-1026 and Output of the controller 91-FIC-1027 commands the fuel gas control valve 91-FV-1027. Ratio set point (air/fuel gas) and (air/acid gas) is provided by operator via 91-HIC1025A and 91-HIC-1025B, respectively. Combustion air flow is controlled by 91-FIC-1025. Set point for the controller is provided by air/acid gas or air/fuel gas ratio calculation as per selection through 91-HS-1029B. Output of the combustion air flow controller 91-FIC-1025 commands the air damper valve 91-FV-1025. Controller Tag Control Description Alarm Unit Operating Set Point Low High °C 210 190 230 nd 91-TICA-1019 2 stage auxiliary burner temperature EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 84 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Controller Tag 91-FIC-1026 91-FIC-1025 91-FIC-1027 • Control Description Acid gas flow combustion air flow fuel gas flow Alarm Operating Set Point Low High 3 Sm /hr 155.382 80 175 3 Sm /hr 519.541 NA 523 3 159.635 8 170 Unit Sm /hr 2nd stage burner combustion air flow (91-FI-1136) low low alarm set 180 Sm3/hr, acid gas flow (91-FI-1137) low low alarm set at 76 Sm3/hr and Fuel gas Flow (91-FI1138) low low alarm set at 7 Sm3/hr activates the following: • closure of Fuel gas block valves 91-XV-1031 and 91-XV-1133 • opening of fuel gas vent valve 91-XV-1134 • closure of fuel gas control valve 91-FV-1027 • closure of acid gas control valve 91-FV-1026 • closure of combustion air control valve 91-FV-1025 • 2nd stage combustion air damper/control valve 91-FV-1025 closes on instrument air failure. • 2nd stage acid gas control valve 91-FV-1026 closes on instrument air failure • 2nd stage fuel gas control valve 91-FV-1027 closes on instrument air failure EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 85 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The schematic diagram for 2nd stage auxiliary burner temperature control is shown below: Fig. 18 - 2nd Stage Auxiliary Burner Temperature Control 9101-V-02 2 X Air Ratio HIC 1025B Acid Gas SP FY 1025B PV FIC PV 1026 nd Stage Converter Selector MV HS 1029A TICA 1019 FT 1026 Acid Gas to 2nd Stage Burner FV-1026 SP FIC PV 1027 MV FT 1027 Fuel Gas to 2nd Stage Burner FV-1027 PV Air Ratio HIC Fuel Gas 1025A X FY 1025A HS 1029B Selector FT 1025 Combustion Air to 2nd Stage Burner PV Comp PT 1002 TT 1004 SP FY 1025 FIC 1025 MV FV-1025 9101-F-03 2nd Stage Auxiliary Burner EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 86 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.2.4.7 Combustion Control for Reaction Furnace Combustion temperature in the Reaction Furnace is maintained by controlling the ratio of fuel gas, combustion air flow rates during start-up and by acid gas, combustion air flow rates during normal operations. Fuel gas flow to reaction furnace is controlled by 91-FIC-1009 which commands the fuel gas control valve 91-FV-1009. Secondary combustion air flow to reaction furnace is controlled by 91-FIC-1002B; Set point for the controller is calculated in the block 91-FY-1009 by multiplying fuel gas flow with AIR/FG ratio, which is manually provided via 91-HIC-1009. Secondary air flow is regulated by 91-FV-1002B. Trim air (make-up) flow is controlled by 91-FIC-1003; set point for the controller is provided by analyzer controller 91-AIC-1001 which measures the H2S/SO2 ratio (4:1). 91-FIC-1003 throttles the damper 91-FV-1003. Air selection to the reaction furnace is done by 91-HS-1142 (Secondary air during start-up and trim air during normal operations). Acid gas flow to the reaction furnace is measured by 91-FT-1001 which determines the quantity of combustion air to the reaction furnace. Pressure, temperature Compensated acid gas flow to reaction furnace is indicated by 91-FI-1001A. Acid gas analyzer value in the reflux drum is measured by 91-AI-1502. 91-HIC-1001 bias range (80%-120%) is manually provided as (Main air flow)/(total air flow) * 100. Main combustion air flow is controlled by 91-FIC-1002, and set point for the main combustion air flow controller is calculated in the block 91-FFY-1001A as: 2.38*(91-AI1502/100)* (91-FI-1001A)*(91-HIC-1001)/100. 91-FFY-1001B a bias block receives the remote set point from 91-FFY-1001A, which adds or subtracts the bias value received from the selector/auto trigger switch 91-HS-1142. When the manipulated variable received by 91-HS-1142 is >=80%, then it adds 1.25% of 91-FIC-1002 set point at each 30sec to the bias block 91-FFY-1001B and when the manipulated variable received by 91-HS-1142 is <=20%, then it subtracts 1.25% of 91-FIC-1002 set point at each 30 sec to the bias block 91-FFY-1001B. Controller Tag 91-FIC-1009 91-FIC-1002 91-FIC-1002B 91-FIC-1003 • Control Description Fuel gas flow Main comb air flow Sec comb air flow Trim air flow Alarm Operating Set Point Low High 3 Sm /hr 357.802 330 380 3 Sm /hr 21124.6 18437 22534 3 Sm /hr 5744.1 NA NA 3 2057.59 NA NA Unit Sm /hr Reaction Furnace combustion air damper/control valve 91-FV-1002, 91-FV1002B and 91-FV-1003 closes on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 87 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Reaction furnace 9101-F-01 acid gas control valve 91-FV-1019 closes on instrument air failure. • Reaction furnace 9101-F-01 fuel gas control valve 91-FV-1009 closes on instrument air failure. • Reaction furnace combustion air flow low low alarm (91-FI-1129) set at 16722 sm3/hr, acid gas flow low low alarm (91-FI-1140) set at 10912 sm3/hr and fuel gas flow low low alarm (91-FI-1130) set at 64 sm3/hr activates the tripping of reaction furnace, 1st stage auxiliary burner and 2nd stage auxiliary burners. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 88 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The schematic representation of Reaction Furnace control is shown below: Fig. 19 – Reaction Furnace Combustion control EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 89 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.3 4.3.1 TAIL GAS TREATMENT UNIT Tail Gas Treatment Unit Equipment Specification Combustion Air Blowers Equipment Tag No. Process Medium Rated Capacity, kg/hr, Rated/Normal/ Turndown 9102-K-11A/B Air 3175/2886/606 Design Temperature, °C 150 Inlet Pressure, bara 1.01 Discharge Pressure, bara 1.55 Drive Type Diver Power, kW Material of Construction, Impeller Motor 145 SS Grade 15-5PH Reducing Gas Generator Equipment Tag No. 9102-F-11 Size (ID/T/T), mm 1500/4300 Operating Pressure, barg 0.44 Operating Temperature, °C 290 Design Temperature, Metal/Refractory, °C 340/1800 Design Pressure, barg 5 Material of Construction, Shell CS Hydrogenation Reactor Equipment Tag No. 9102-V-11 Size (ID/T/T), mm 3100/6100 Design Temperature, Metal/Refractory, °C 340 Design Pressure, barg 3.5 Operating Pressure, barg 1.45 Operating Temperature, Inlet/Outlet °C Material of Construction, Shell 290/327 CS, Refractory lined EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 90 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Reactor Effluent Cooler Equipment Tag No. Process Medium 9102-E-11 Process Gas Design Pressure, Shell Side, barg 7.0/FV Design Pressure, Tube Side, barg 7.0 Design Temperature, Shell Side, °C 185/0 Design Temperature, Tube Side, °C 340/0 Operating Pressure, Shell Side barg 6.0 Operating Pressure, Tube Side, barg 0.38 Operating Temperature, Shell Side, LP BFW/ LP Steam, °C 105/159 Operating Temperature, Tube Side (In/Out) °C 320/178 Design Duty, kW Material of Construction, Shell & Tube 2152 CS Start-up Gas Steam Ejector Equipment Tag No. 9102-X-11 Design Temperature, °C 225 Design Pressure, barg 7.0 Motive Fluid LP Steam Steam Inlet Pressure, barg 4.5 Steam Inlet Temperature, °C 159 Material of Construction CS Desuperheater/Contact Condenser Equipment Tag No. 9102-C-11 Size (ID X T/T), mm 2900/3400 X 27470 Design Temperature, °C 193/0 Design Pressure, barg 3.5/FV Operating Pressure, Top/Bottom, barg Operating Temperature, Top/Bottom, °C Material of Construction, Shell/Internal 0.18/0.30 42/82 CS/SS316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 91 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Cooling Water Circulation Pumps Equipment Tag No. 3 Capacity, m /hr (Normal/Rated) Suction Pressure, bar(a) (Rated/Max.) 9102-P-12A/B 210.6/252.7 2.8/6.4 Discharge Pressure, bar(a) 8.4 Operating Temperature, °C 71 Design Temperature, °C (Max./Min.) 150/0 Driver Type Motor Rated Power, kW Material of Construction, Casing/Impeller 75 A351-CF8M/SS316L Desuperheater Circulation Pumps Equipment Tag No. 3 Capacity, m /hr (Normal/Rated) Suction Pressure, bar(a) (Rated/Max.) 9102-P-11A/B 240 1.5/5.1 Discharge Pressure, bar(a) 5.6 Operating Temperature, °C 80 Design Temperature, °C (Max./Min.) 150/0 Driver Type Motor Rated Power, kW Material of Construction, Casing/Impeller 55 A351-CF8M/SS316L Wash Water Filter Equipment Tag No. 9102-S-15 Size (ID/T/T), mm 736/2080 Design Temperature, °C Design Pressure, barg 3 150/0 9.6 Flow rate, m /hr 240 Operating Temperature, °C 82 Operating Pressure, barg 4.5 Clean Pressure Drop, bar 0.1 Max. Allowed Pressure Drop, bar 0.7 Size of particles to be removed, microns 5 Material of Construction CS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 92 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Contact Condenser Cooler Equipment Tag No. 9102-E-12 Tube Side Design Pressure, barg 12.4 Tube Side Design Temperature, °C 150/0 Operating Pressure bar(a) 6.0 Operating Temperature, In/Out, °C 73/40 Design Duty, kW (Summer/Winter) 4593/7985 Material of Construction, Tubes Alloy 825 Contact Condenser Trim Cooler Equipment Tag No. 9102-E-13A/B Design Pressure Shell Side, barg 12.4 Design Pressure Tube Side, barg 9.55 Design Temperature Shell Side, (Min./Max.), °C 150/0 Design Temperature Tube Side (Min./Max.)°C 85/0 Operating Pressure Shell/Tube Side barg 3.95/1.7 Operating Temperature, Shell Side, (In/Out), °C 54/40 Operating Temperature, Tube Side (In/Out) °C 35/45 Design Duty, kW 3387 Material of Construction, Shell/Tube SS316L/Titanium Grade-2 Blowdown Pit Equipment Tag No. Size, (L/W/H), m Design Pressure, barg 4.3.2 9102-T-01 1/1/1 0 Design Temperature, °C 185 Material of Construction Concrete Tail Gas Treatment Unit (TGTU) Process Description The Tail Gas Treating Unit reduces the hydrogen sulphide concentration in the tail gas to a level corresponding to >99.5% total sulphur recovery. All residual hydrogen sulphide is oxidised to sulphur dioxide before it is released to the atmosphere. The BSR/Amine process consists of a Reducing Gas Generator section, Hydrogenation section, Desuperheater/Contactor section and a selective amine absorption section. The process uses the BSR technology to reduce all sulphur compounds in the SRU tail gas to hydrogen sulphide. This section includes water condensation and separation upstream of the amine section with a caustic circulation system to protect against SO2 breakthrough, which degrades the amine and causes severe corrosion. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 93 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The amine section uses an amine solution to remove most of the hydrogen sulphide from the treated sulphur plant tail gas while minimising the co-absorption of carbon dioxide. The Claus tail gas from the Final Separator 9101-V-05 is fed to the Reducing Gas Generator (RGG) 9102-F-11. The purpose of the Reducing Gas Generator is to generate reducing gases (H2 and CO). This is achieved by the combustion of fuel gas with a substoichiometric quantity of air. The production of reducing gases is regulated by controlling the flow of the fuel gas and air. Air flow is set by the outlet temperature of the Reducing Gas Generator 9102-F-11 while the fuel gas flow rate is set to be a fixed proportion of the air flow. LP steam is fed to the Reducing Gas Generator to suppress the formation of carbon. The flow rate of the steam is ratio-controlled according to the fuel gas flow rate. The tail gas from the Final Separator 9101-V-05 is mixed with the hot combustion products in the Reducing Gas Generator to ensure a temperature that will favour the desired reactions in the Hydrogenation Reactor (9102-V-11). The Hydrogenation Reactor contains a fixed bed Cobalt/Molybdenum (CoMo) catalyst. The reactions are exothermic resulting in a temperature rise across the reactor. The gas is cooled by the generation of LP steam in the Reactor Effluent Cooler 9102-E-11. The tail gas is then desuperheated and the excess water removed in the Desuperheater/Contact Condenser (9102-C-11). This tower contains an upper packed section, a chimney tray and a lower section containing packing and bubble cap trays. In the lower packed section of the tower (Desuperheater section), tail gas is contacted with a circulating stream of a mildly caustic water solution. This removes sulphur dioxide and cools the tail gas down. The Desuperheater Circulation Pump (9102-P11A/B) pumps the caustic water solution from the bottom of the tower to the top of the packing. Water make up is provided to the lower (Desuperheater) section, under level control, from the top (Contact Condenser) section circulation. The solution is maintained at an alkaline pH of around 9.0 to protect against SO2 breakthrough from the reactor. SO2 causes corrosive conditions in the Desuperheater Contact Condenser and the Amine Absorber, and degrades the amine. The pH of the circulating liquid is monitored by a continuous analyser and controlled by periodic, manual addition of fresh caustic solution. An intermittent bleed from this section removes accumulated contaminants from the circuit. The desuperheated gas and water vapour then passes through the (wash) bubble cap trays and the chimney tray into the upper (Contact Condenser) packed section. Here the gas is cooled by direct contact with a circulating water stream. The water is pumped by the Cooling Water Circulation Pump from the chimney tray, through the Contact Condenser Cooler 9102-E-12 and Contact Condenser Trim Cooler 9102-E-13A/B where it is cooled, and back to the top of the tower. The water that is condensed in this section is slightly sour. Some is used as make up on demand to the lower Desuperheater section and the remainder is taken off under level control and sent to EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 94 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL effluent treatment. The condensed water loop is kept separate from the water in the Desuperheater circulation loop to avoid contamination with salt products that may be formed in the Desuperheater section. The tail gas leaves the Desuperheater Contact Condenser (9102-C-11) at a temperature of approximately 40°C and is sent to the Tail Gas Amine Absorber (9102-C-12) which uses a lean amine solution to remove the hydrogen sulphide from the tail gas, while minimising the co-absorption of carbon dioxide. The gas enters at the bottom of the absorber and passes through a trayed section counter current to the lean amine solution that preferentially absorbs H2S. The lean amine solution is supplied from the Lean Amine Pumps 9103-P-13A/B. The Tail Gas Rich Amine Pump (9102-P-16 A/B) pumps the rich solvent solution from the bottom of the Tail Gas Amine Absorber (9102-C-12) to the Acid Gas Amine Absorber (9103-C-11) before it is regenerated in the Amine regenerator (9103-C-12). The amine regeneration facilities required for the Acid Gas Enrichment and Tail Gas Treatment Units are shared with the use of a common solvent. The H2S that is stripped from the rich amine solution in the Amine Regenerator is fed to the Sulphur Recovery section, thus closing the recycle loop around the SRU and TGTU sections. Treated gas from the Tail Gas Amine Absorber passes to the Incinerator along with that from the Acid Gas Amine Absorber and from the Sulphur Pit. 4.3.3 Tail Gas Treatment Unit Control Description 4.3.3.1 Controls for RGG Combustion Air Blower (9102-K-11A/B) 4.3.3.1.1 Surge Protection The basic objectives of the surge protection system are: • To prevent surge-induced compressor damage and process upsets without sacrificing energy efficiency • To maintain selected process-limiting variables within safe or acceptable range • To achieve these objectives, the anti surge controller manipulates the position of a blow-off valve and IGV (inlet pressure control) 4.3.3.1.2 Anti surge Protection The regulation of the combustion air blower valves is implemented on the CCC Antisurge controller. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 95 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL CCC receives the following signals from the compressor skid (9102-K-11A/B) to perform the pressure and anti-surge regulation: Sl. # 9102-K-11A Tag No. 9102-K-11B Tag No. Service 1. 91-PT-1452 91-PT-1712 Discharge air pressure 2. 91-TT-1454 91-TT-1714 Discharge air temperature 3. 91-FT-1452 91-FT-1712 Discharge air flow 4. 91-PT-1454 91-PT-1714 Compressor inlet air pressure 5. 91-TT-1455 91-TT-1715 Compressor inlet air temperature 6. 91-PT-1456 91-PT-1716 Discharge air pressure after check valve 7. 91-ZT-1453 91-ZT-1713 IGV valve position transmitter 8. 91-ZT-1451 91-ZT-1711 Blow-off valve position transmitter 9. 91-II-1470 91-II-1730 Main motor current signal Note: 9102-K-11A controls are discussed in the following section. After processing all the above signals, CCC controls the IGV 91-PCV-1453 and blow-off valve 91-FCV-1451. CCC also provides trip signal 91-XS-1464 for excessive surge to ESD to stop the compressor. When the blower is started IGV 91-PCV-1453 receives a minimum opening signal from CCC which is a pre-set value on CCC and the blow-off valve 91-FCV-1451 remains open. When the compressor is loaded, CCC modulates the IGV 91-PCV-1453 and blow-off valve 91-FCV-1451 to maintain the discharge air pressure constant. 4.3.3.1.3 IGV 91-PCV-1453 The regulation system of compressor IGV valve 91-PCV-1453 is of the constant pressure type. After the loading of compressor the pressure regulation loop stabilizes and the IGV 91-PCV-1453 opens or closes only when the air required by the machine varies, so as to maintain the discharge pressure of the blower within the set-point defined. 4.3.3.1.4 Blow-off Valve 91-FCV-1451 The anti-surge regulation loop provides to regulate the blow-off valve 91-FCV-1451 by a continuous calculation of the discharge pressure 91-PT-1452 and discharge flow 91-FT-1452. When the flow is higher than the pressure the result of the calculation closes the blow-off valve. When the pressure is higher than the flow the result of the calculation opens the blow-off valve. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 96 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.3.3.2 Reducing Gas Generator Controls 4.3.3.2.1 Hydrogenation Reactor I/L Temperature Control The Hydrogenation Reactor inlet temperature is controlled through 91-TIC-1307 by adjusting the air and the fuel Gas flow rates to the Reducing Gas Generator. The Hydrogenation Reactor inlet temperature is controlled by 91-TIC-1307, output of the controller 91-TIC-1307 is directly fed to the combustion air flow controller 91-FIC1304 as a set point and output of the controller 91-FIC-1304 regulates the air flow damper 91-FV-1304. Fuel gas flow is controlled by 91-FIC-1311; set point for the fuel gas controller is derived in the block 91-UY-1304 by multiplying the air flow with AIR/FG ratio set value provided from 91-HIC-1304 (Range: 0.09 to 0.15). Output of the controller 91-FIC-1311commands the fuel gas control valve 91-FV-1311. If the Hydrogenation Reactor inlet temperature increases, then controller 91-TIC-1307 shall first decrease the Set point of combustion air flow controller 91-FIC-1304, which in turn decrease the set point of fuel gas controller 91-FIC-1311 and vice versa. 4.3.3.2.2 Steam Flow Control LP steam is injected directly in to the RGG burner in a ratio of steam to fuel gas to suppress the formation of soot. Steam flow to RGG is measured by 91-FT-1310 which is fed as a process variable to the steam flow controller 91-FIC-1310, set point for the controller is calculated by multiplying the process variable from 91-FIC-1311(FG flow) with the STEAM/FG ratio manually provided via 91-HIC-1311(2.0:1.0). Output (0-100%) of the controller 91-FIC-1310 directly commands the control valve 91-FV-1310. Alarm Control Loop Unit Operating Set Point Low High 91-TIC-1307 Hydrogenation reactor I/L temperature °C 290 285 295 91-FIC-1304 RGG comb air flow Sm3/hr 2371.6 2134 2609 3 Sm /hr 263.7 237 290 kg/hr 400 360 440 Controller 91-FIC-1311 RGG fuel gas flow 91-FIC-1310 RGG quench steam flow EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 97 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 20 - Reducing Gas Generator Temperature Control 9102-V-11 SP PV X Hydrogenation Reactor FIC 1304 MV Comp FY 1304 FT 1304 TIC 1307 PT 1304 FV-1304 PV Fuel Gas Ratio HIC Air 1304 MV X UY 1304 FIC SP 1311 PV FT 1311 Fuel Gas to RGG FV-1311 X HIC 1311 SP UY 1311 PV SP FIC PV 1310 MV FT 1310 Steam to RGG Tail Gas TT 1304 Combustion Air to RGG Steam Ratio Fuel Gas TT 1307 FV-1310 9102-F-11 Reducing Gas Generator EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 98 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.3.3.3 Reactor Effluent Cooler Controls 4.3.3.3.1 Reactor Effluent Cooler Level Control Hydrogenated process gases from the Hydrogenation Reactor are cooled in the Reactor Effluent Cooler (9102-E-11) and generates LP steam in the shell side of the cooler. The water level in the Reactor Effluent Cooler is maintained by level controller 91-LIC1302 by monitoring the level through 91-LT-1302, level control is achieved by controlling the boiler feed water inlet to the Reactor Effluent Cooler through the control valve 91-LV-1302. Controller Tag Control Description 91-LIC-1302 Reactor Effluent Cooler level Control Alarm Unit Operating Set Point Low High % 85 81 92 • Low low level alarm (91-LALL-1309) set at 76% in reactor effluent activates the RGG (9102-F-11), TGTU and SRU shutdown • BFW inlet to reactor effluent control valve 91-LV-1302 opens on instrument air failure. 4.3.3.3.2 Reactor Effluent Cooler Outlet Tail Gas Control In normal operation tail gas from the Reactor Effluent Cooler will be routed to Contact Condenser but during start-up tail gas is diverted to the Incinerator. This diversion of tail gas is accomplished by activating the selector switch 91-HS1303A. This opens the valve 91-XV-1332 (tail gas going to the Contact Condenser) and when it is fully open the valve 91-XV-1331 will close (tail gas going to the incinerator). This ensures that at least one path is fully open for the tail gas to pass through without pressuring the upstream reducing gas generator RGG. 4.3.3.4 4.3.3.4.1 Desuperheater/Contact Condenser Controls Desuperheater/Contact Condenser Column Bottom Level Control The Desuperheater Circulation Pump (9102-P-11A/B) takes suction from the Desuperheater/Contact Condenser (9102-C-11) bottom and circulates water to the column through Wash Water Filter (9102-S-15). The Desuperheater/Contact Condenser column bottom level is maintained by the level controller 91-LIC-1307, regulating the level control valve 91-LV-1307, which controls slip stream of water flow from the Cooling Water Circulation Pumps (9101-P-12A/B) to the bottom section of the column as top up water. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 99 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Controller Tag 91-LIC-1307 Control Description Desuperheater/Contact Condenser column bottom level Alarm Unit Operating Set Point Low High % 50 22 93 • Low low level alarm (91-LALL-1306) in Desuperheater/Contact Condenser column bottom trips the Desuperheater Circulation Pumps 9102-P-11A/B • Desuperheater/Contact Condenser column bottom level control valve 91-LV-1307 opens on instrument air failure. 4.3.3.4.2 Circulating Water Return Flow to Desuperheater Control The Desuperheater Circulation Pump (9102-P-11A/B) takes suction from the column (9102-C-11) bottom and circulates water to the column through Wash Water Filter (9102-S-15). Flow from the Wash Water Filter to the column bottom is maintained by the flow controller 91-FIC-1314 which regulates the flow control valve 91-FV-1314. Controller Tag 91-FIC-1314 Alarm Control Description Unit Operating Set Point Low High Circulating water return to Desuperheater m3/hr 199 179 219 • Low low flow alarm (91-FALL-1306) set at 30 m3/hr in circulating water return to de super heater trips the de super heater circulation pumps 9102-P-11A/B • Circulating water return to de super heater flow control valve 91-FV-1314 opens on instrument air failure. 4.3.3.4.3 Desuperheater/Contact Condenser Top Level Control The cooling water circulation in the Contact Condenser top section is carried out by Cooling Water Circulation Pump (9101-P-12A/B). The Contact Condenser (9102-C-11) top level is maintained by the level controller 91-LIC-1305 through the level control valve 91-LV-1305, which controls the excess water flow from the Cooling Water Circulation Pumps discharge to the Waste Water Degasser (6922-V-07). Controller Tag Control Description 91-LIC-1305 Desuperheater/Contact Condenser top level Alarm Unit Operating Set Point Low High % 50 32 90 • Low low level alarm (91-LALL-1304) in Desuperheater/Contact Condenser column top trips the Cooling Water Circulation Pump 9102-P-12 A/B • Desuperheater/Contact Condenser column top level control valve 91-LV-1305 closes on instrument air failure EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 100 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.3.3.4.4 Desuperheater/Contact Condenser Top Circulating Water Flow Control Cooled circulating water return from the Contact Condenser Trim Cooler (9102-E13A/B) flows to top of the de-super heater/contact condenser column (9102-C-11) is measured by 91-FT-1307 and controlled by the flow controller 91-FIC-1307 which regulates the flow control valve 91-FV-1307. Controller Tag Control Description 91-FIC-1307 Desuperheater/ Contact Condenser top CW • 4.3.3.4.5 Alarm Unit Operating Set Point Low High m3/hr 197 177.3 216.7 Desuperheater/Contact Condenser column top cooling water control valve 91-FV1307 opens on instrument air failure Desuperheater/Contact Condenser Top Pressure Control In normal operation Desuperheater/Contact Condenser column (9102-C-11) tail gas flows to the Tail Gas Amine Absorber 9102-C-12 but during start-up, flow will be diverted to the Incinerator and the tail gas pressure is maintained by the pressure controller 91-PIC-1308 by monitoring the pressure transmitter 91-PT-1308 located in the start-up bypass line to Incinerator. If the pressure increases then the control valve 91-PV-1308 opening will increase to pass more gas to the Incinerator (9101-F-14). Alarm Controller Tag Control Description Unit Operating Set Point Low High 91-PIC-1308 Desuperheater/ Contact Condenser column top pressure bara 1.19 NA NA • 4.3.3.4.6 Desuperheater/Contact Condenser column top pressure control valve 91-PV-1308 to incinerator opens on instrument air failure Contact Condenser Cooler Temperature Control Temperature of the circulating water from the Cooling Water Circulation Pumps (9102-P-12-A/B) is controlled by cooling the fluid to 54°C (maximum temperature) in summer and not less than 40°C (minimum temperature) in winter using three fans: one fixed speed fan (on/off) control (column 1), and another two VSD controlled fans working simultaneously (in column 2 & 3). The contact condenser cooler outlet temperature is measured at outlet of Contact Condenser Trim Cooler by 91-TT-1301 and received by the temperature controller 91-TIC-1301. The output of this controller sends the control signal to control the three fans and also to control the bypass control valve 91-TV-1301 of Contact Condenser Trim Cooler. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 101 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL In auto mode, the temperature controller shall follow up the cooler outlet temperature changes by changing the VSD (9102-EM-12AB/AC/BB/BC) rates to maintain the temperature set point-1 = (54°C + 40°C)/2=47°C. The fixed speed fan (9102-EM-12AA/BA) will operate on gap control set point between the values Tmax=54°C & Tmin=42°C. The temperature control valve will be used only in case the cooler outlet temperature goes to pre-determined temperature T=42°C, then the control valve shall open gradually to maintain the cooler temperature and keep it around the set point-2 (42°C). 4.3.3.5 Tail Gas Amine Absorber Controls 4.3.3.5.1 Tail Gas Absorber Level Control The tail gas from the Desuperheater/Contact Condenser (9102-C-11) enters at the bottom of Tail Gas Amine Absorber 9102-C-12. Bottom level in the Tail Gas Amine Absorber (9102-C-12) is maintained by controlling the rich amine flow from the bottom of the column to Acid Gas Amine Absorber (9103-C-11) through 9103-P-16A/B. Tail gas absorber bottom level is controlled by 91-LIC-1308; Tail Gas Rich Amine Pumps 9102-P-16A/B discharge flow to Acid Gas Amine Absorber is measured by 91-FT-1325 and controlled by the flow controller 91-FIC-1325; set point for the SLAVE flow controller 91-FIC-1325 is received from the tail gas absorber MASTER level controller 91-LIC-1308. Output of the flow controller 91-FIC-1325 directly controls the control valve 91-FV-1325 in the Tail Gas Rich Amine Pumps 9102-P-16A/B discharge flow to the acid gas amine absorber. Controller Tag Control Description 91-LIC-1308 Tail Gas Amine Absorber bottom level 91-FIC-1325 Rich amine flow to 9103-C11 Alarm Unit Operating Set Point Low High % 50 11 82 m3/hr 136 NA NA • High high level alarm (91-LAHH-1310) in Tail Gas Amine Absorber bottom closes the lean amine inlet valve 91-XV-1310 to Tail Gas Amine Absorber • Low low level alarm (91-LALL-1301) in Tail Gas Amine Absorber bottom trips the Tail Gas Rich Amine Pumps (9102-P-16A/B) and closes tail gas rich amine valve 91-XV-1309. • Rich amine flow control valve 91-FV-1325 to Acid Gas Amine Absorber closes on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 102 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.3.3.5.2 Lean Amine to Tail Gas Amine Absorber Flow Control Lean amine solution from Lean Amine Pumps (9103-P-13A/B) and tail gas from Desuperheater/Contact Condenser (9102-C-11) enters the Tail Gas Amine Absorber (9102-C-12). Lean amine flow to the absorber is measured by 91-FT-1301 and controlled by 91-FIC-1301. Output of the flow controller directly regulates the lean amine flow control valve 91-FV-1301. Controller Tag 91-FIC-1301 Alarm Control Description Unit Operating Set Point Low High Lean amine flow to Tail Gas Amine Absorber m3/hr 135 110 148.5 • High high level alarm (91-LAHH-1310) in Tail Gas Amine Absorber bottom closes the lean amine inlet valve 91-XV-1310 to Tail Gas Amine Absorber located on the downstream of 91-FV-1301. • Lean amine inlet valve 91-XV-1310 closes on activation of ESD-0, ESD-1 and ESD-2 shutdown. 4.3.3.5.3 Tail Gas Rich Amine Pumps Minimum Flow Control Tail Gas Rich Amine Pumps (9102-P-16A/B) minimum flow to Tail Gas Amine Absorber bottom is controlled by 91-FIC-1303. Output of the controller 91-FIC-1303 controls the fail open control valve 91-FV-1303. Controller Tag 91-FIC-1303 • 4.4 4.4.1 Control Description Tail Gas Rich Amine Pump min flow Alarm Unit Operating Set Point Low High m3/hr 31.25 27.5 NA Tail Gas Rich Amine Pump discharge flow Low low alarm (91-FALL-1305) set at 25 m3/hr trips the Tail Gas Rich Amine pumps (9102-P-16A/B). INCINERATOR Equipment Specification Incinerator Air Blowers Equipment Tag No. Process Medium Rated Capacity, ACMH 9101-K-12A/B Air 63,402 Design Temperature, (Min./Max.), °C 0/52 Drive Type Motor Driver Power, kW Material of Construction, Impeller 94 Corten Steel EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 103 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Incinerator Equipment Tag No. 9101-F-14 Size, (OD/L), m 3.886/17.374 Process Medium Tail Gas/Air/Fuel Gas Design Temperature, shell, °C 343 Design Pressure, barg 3.8 Burner Model Size Quantity Duty GSLF-24J 82” 1 32.2 MW-H Turndown 5:1 Pilot Type AR/GS-1 Design Temperature, shell, °C 343 Design Pressure, barg 3.8 Incinerator Stack Equipment Tag No. Process Medium 9101-X-11 Flue Gas Shell OD/Height, m 2.438/110 Design Temperature, (Shell/Refractory), °C 343/1538 Design Pressure, barg Internal Lining 4.4.2 Process Description and Control 4.4.2.1 Tail Gas Incinerator Process Description ATM. YES, L.W. Castable An Incinerator 9101-F-14 is provided to thermally oxidise all possible sulphur compounds to SO2 in off gas effluents from the Acid Gas Amine Absorber 9103-C-11, Tail Gas Amine Absorber 9102-C-12, SRU tail gases and vent gases from the Sulphur Degassing Pit 9101-T-01/01B. Moreover all BTEX content of off gas effluent is also destructed. To ensure complete combustion of these sulphur compounds the Incinerator's combustion chamber temperature is maintained at a temperature of about 800°C by burning fuel gas supplied with combustion air in the unit's burner. Combustion air is supplied from 2 x 100% Incinerator Air Blowers (9101-K-12 A/B, One Operating and One Standby). The Blowers are driven by VFD motors. Each Blower is provided with an Air Intake Stack with Bird Screen, Sand Filter and Rain Hood. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 104 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fuel gas to the Incinerator is supplied from the existing Fuel Gas network. A tapping is taken from the existing fuel gas line 6”-6536-FG-101-C12P and fuel gas is supplied to the Incinerator 9101-F-14 and Reducing Gas Generator 9102-F-11. The flows of fuel gas and combustion air are each measured by flow and then ratio controlled to ensure the correct amount of excess air is always maintained in the Incinerator combustion chamber to allow the oxidation of the sulphur compounds in the tail and vent gases to take place. An Oxygen Analyser 91-AE-1051 located in the Incinerator outlet combustion gases Stack 9101-X-11 monitors the excess O2 in the Incinerator combustion gases. Adjustments may be made to the fuel gas to air ratio controller to ensure the correct excess of O2 (3% by Mol) is seen in the stack gases. A sulphur dioxide analyser AE-1052, located at the Incinerator Stack (9101-X-11), monitors the Incinerator stack gases for SO2 content. A NOX analyser 91-AE-1053, located at the Incinerator Stack (9101-X-11), monitors the Incinerator stack gases for NOX content. 4.4.2.2 4.4.2.2.1 Tail Gas Incinerator Process Control Incinerator Temperature control (91-TIC-1155) Normal operating temperature of the Incinerator is 817⁰C; the temperature in the Incinerator is controlled by modulating the flow of fuel gas and combustion air. Temperature in the Incinerator is measured by 91-TT-1155 and controlled by 91-TIC1155. The output of the controller 91-TIC-1155 is fed to a splitter 91-TY-1155A where the output is splitted into 0-50% which is fed to 91-TY-1155C for regulating the combustion air flow and 50-100% which is fed to 91-TY-1155B for regulating the fuel gas flow. 0-50% output of 91-TIC-1155 is scaled to 0-100% and is reversed in 91-TY-1155C (This is for regulating the temperature of Incinerator during normal operation by varying the speed of the air blower). This value is then fed to a high selector function block 91-FY1156C. The other input of 91-FY-1156C is received from 91-FY-1155A (This determines the quantity of combustion air required based on fuel gas flow). The combustion air flow rate from Air Blowers is measured in the common discharge line by 91-FT-1156. 91-FIC-1156 receives the PV from 91-FT-1156 and set point (SP) from 91-FY-1156C. The output (MV) of 91-FIC-1156 is then scaled to 4-20 mA. The scaled current signal is sent to VSD panel of Duty Air Blower for controlling its speed. The speed of the Air Blower determines the quantity of combustion air required. The main fuel gas flowing to the burner is measured by 91-FT-1155 and the PV is sent to 91-FIC-1155. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 105 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The set point for 91-FIC-1155 is derived from the temperature controller 91-TIC-1155. i.e. The output (MV) of 50-100% is scaled to 0-100% and is fed as SP through 91-TY1155B to 91-FIC-1155. The ratio set point is manually entered by operator via 91-HIC-1155A. The fuel gas flow value (PV) of 91-FIC-1155 is multiplied by ratio set point in function block 91-FY1155A. The ratio set point gives the correct ratio of air to fuel gas based on a manually determined composition. The multiplication factor is a manual entry and is based on the design composition of the feed gas. The output value of 91-FY-1155A is given to the selector function block 91-FY-1156C. The actual ratio of combustion air to fuel gas is displayed in function block 91-FY-1155A. Fuel gas flow control is achieved via 91-FIC-1155 by controlling 91-FV-1155 This reversed output and air/fuel ratio provided via 91-HIC-1155A is allowed to pass through the high demand selector 91-FY-1156C which provides the set point to combustion air flow controller 91-FIC-1156. Output of the controller modulates the combustion air flow by changing the Combustion air fan 9101-K-12A/B VFD set point. 50-100% output of 91-TIC-1155 is scaled to 0-100% in 91-TY-1155B, which provides the set point to the fuel gas controller 91-FIC-1155 and output of the controller 91-FIC1155 commands the fuel gas control valve 91-FV-1155. Controller Tag Control Description Unit 91-TIC-1155 91-FIC-1155 Operating Set Point Alarm Low NA NA High 850 NA Incinerator stack temp °C 800 3 Incinerator Fuel gas flow Sm /hr 2256.9 Incinerator combustion air 91-FIC-1156 Sm3/hr 46938.7 NA NA flow • High high temperature alarm (91-TAHH-1160) set at 900°C, low low combustion air flow alarm (91-FALL-1156B/C) set at 8383 Sm3/hr, low low fuel gas pressure alarm (91-PALL-1156) set at 0 barg and high high fuel gas pressure alarm (91-PAHH-1156) set at 4 barg at Incinerator • Closes the following valves: • Fuel gas block valve 91-XV-1555 to burner • Fuel gas block valve 91-XV-1557 to burner • Pilot gas block valve 91-XV-1558 to burner • Pilot gas block valve 91-XV-1560 to burner • Instrument air block valve 91-XV-1161 • Pilot air block valve 91-XV-1162 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 106 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • • Opens the following valves: • Fuel gas vent valve 91-XV-1158 • Pilot gas vent valve 91-XV-1159 Fuel gas supply control valve 91-FV-1155 to Incinerator furnace closes on instrument air failure. The schematic diagram for Incinerator temperature control is shown below: Fig. 21 - Incinerator Temperature Control Master TE 1155 TT 1155 TIC 1155 Incinerator 9101-F-14 X TY 1155B Slave MV SP 50-100% TY 1155A Split X 0-50% FY PV 1155A FIC 1155 PV X Burner TY 1155C FT 1155 HIC Fuel Ratio 1155A Air Combustion Air Fuel Gas to Incinerator FV 1155 Slave FT 1156A Combustion Air Fan PV FIC 1156 MV VFD FY-1156A 9101-K-12A Combustion Air Fan VFD 9101-K-12B FY-1156B > SP FY 1156C High Selector EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 107 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.5 INSTRUMENT AIR PACKAGE 4.5.1 Instrument Air Compressor Package 4.5.1.1 Equipment Specification Screw Compressors Tag No. 6837-K-02A/B Rotary, Dry Screw, 2 stage, Air-cooled Type No. of units Two (1 Working + 1 Standby) 3 Capacity, Nm /hr (Total) @52°C & 100% RH 900 Design Pressure, barg 8.6 Design Temperature, °C 52/0 Compressor Inlet Pressure, barg ATM Compressor Inlet Temperature, °C AMB (0-52) Compressor Outlet Pressure, barg 8 Driver Driver Power, kW Motor 200 Pre-cooler Tag No. 6837-E-03A Design Pressure, barg 11 Design Temperature, °C 260 Inter-cooler Tag No. 6837-E-03A Design Pressure, barg 3.7 Design Temperature, °C 180 After-cooler Tag No. 6837-E-03A Design Pressure, barg 13.7 Design Temperature, °C 200 After-cooler Tag No. 6837-E-04A Design Pressure, barg 10.5 Design Temperature, °C 160 Max. Capacity, L/S 650 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 108 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Discharge Air Receiver Tag No. 6837-V-10 Size, mm, (Dia x T/T) 2400 x 7200 Design Pressure, barg 9.7 Design Temperature, °C 85 Operating Pressure, barg 7 Operating Temperature, °C 60 Material of Construction CS 4.5.2 Instrument Air Dryer Package 4.5.2.1 Equipment Specification Air Dryer Tag No. Dryer Type 6837-A-03/04 Twin Tower, pressure swing absorption with heatless regeneration Capacity, Nm3/hr 300 Design Pressure, barg 9.7 Design Temperature, °C 85/0 Operating Pressure, barg 8 Operating Temperature, °C 60 Desiccant Type Activated Alumina/Molecular Sieve Pre-Filter Tag No. Size (Dia x L), mm 6837-S-07A/B & 6837-S-09A/B 190 x 621 Design Pressure, barg 9.7 Design Temperature, °C 85 Material of Construction Cast Aluminium Dryer Vessels Tag No. 6837-V-14A/B & 6837-V-15A/B Size (Dia x T/T), mm 550 x 1500 Design Pressure, barg 9.7 Design Temperature, °C 85 Material of Construction CS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 109 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL After-Filters Tag No. 6837-S-08A/B & 6837-S-10A/B Size (Dia x L), mm 190 x 621 Design Pressure, barg 9.7 Design Temperature, °C 85 Material of Construction Cast Aluminium Instrument Air Receiver Tag No. 4.5.3 6837-V-11 Size mm, (Dia x T/T) 3700 x 7400 Design Pressure, barg 9.7 Design Temperature, °C 85/0 Operating Pressure, barg 7.1 Operating Temperature, °C 60 Material of Construction CS Instrument Air Package Description The new air compressor package consists of the following: 1. Two (2x100%) single base frames mounted Air Compressors (6837-K-02A/B), each having a capacity of 900 Nm3/hr (dry basis). 2. Each Compressor is supplied with an individual After Cooler. 3. One air compressor discharge drum, (6837-V-10) is provided. 4. Two Instrument air dryer packages, (6837-A-03/04) running at 2X50%, each dryer capacity is 300 Nm3/hr (dry basis). 5. Pre and After Filters for each dryer. 6. One instrument air receiver (6837-V-11) with storage capacity to provide instrument air for a period of 20 minutes following a compressor trip. 7. Dew point analyzers are provided for individual dryer package. The compressors are air-cooled, oil free, rotary screw type and are sized 100% of duty. Both Compressors operate in Duty/Standby configuration (with automatic changeover of the standby unit compressor). The dryer consists of two 50% heater-less desiccant dryers each consisting of two vessels (one drying, one regenerating), a set of duplex pre and after filters. Each dryer is 50% of design capacity (Single Compressor supply). Compressors and Dryers have locally mounted instruments and junction boxes and operate from the UCP, with DCS and ESD remote monitoring, through TCP/IP. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 110 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Based on air demand only one compressor under normal conditions will be loaded, the second unit can start but will have load inhibitors to ensure only one unit is loaded. Each dryer has a sonic nozzle at the discharge header to ensure the protection against the greater flow. Each compressor is monitored and controlled by the Package Controller (UCP) which provides information to the ICSS. There is only a push button station available at each equipment station in the field (LCP). However this LCP still only communicates with the UCP which then sends signals to the DCS. All the signals are hardwired to UCP. The subsystems MCC, ESD and ICSS are hardwired to the UCP and linked also through a redundant modbus TCP/IP communication link. Compressor instrumentation and solenoids are all wired to junction boxes, the UCP system receives an external net air pressure signal and then starts, loads/unloads and stops the available compressor based on its own selecton routine. The ICSS supervises the system status via the UCP connected to the junction boxes shown in the Electrical Service Diagram. The new Air System will supply instrument and plant air with the following supply battery limit conditions for both instrument and plant air: Design Operating Pressure bar (g) 9.7 7.0 Temperature (°C) 85 55/60 The new instrument and plant air headers are connected to the existing NGL-3 instrument and plant air headers respectively through cross over connection lines with (manual isolation valves) for operation flexibility. 4.5.4 Instrument Air Package Control Description A. Loading/Unloading The compressor always starts to run in unloaded condition, up to first 20 seconds known as the load delay, this is to ensure the oil pressure is stabilised. After the load delay compressor will load unless either the operator manually selects to unload or there is no air demand. If there is no air demand the compressor runs unloaded and is said to be idle. To load the compressor the solenoid valve 68-XY-1401 shall be energized, similarly to unload the compressor solenoid valve 68-XY-1401 shall be de-energised and solenoid valve 68-XY-1403 shall be energised. When the compressor is in remote mode, loading/unloading of every compressor is based on the net air pressure signal 68-PT-1311. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 111 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL When the compressor is in local mode loading/unloading of every compressor is based on the compressor O/L pressure signal transmitter 68-PT-1406. If the air demand is low, i.e. when the pressure transmitter signal is above the load set point then UCP unloads the compressor and if the air demand is high, i.e. when the pressure transmitter signal is below the load set point then UCP loads the compressor. The loading/unloading set pressure in barg is given below: Compressor Control Loading Unloading Status Compressor A lead XX XX running Compressor B lag XX XX standby Note: XX – Loading and Unloading set points will be set at site while commissioning the Air Compressor. B. Lead/Lag Control in Remote Mode Only in Remote-Auto mode the compressors shall follow the Lead, Lag logic. The purpose of Lead/Lag control is to allow two compressors to operate at once, with one operating as LEAD and maintaining system pressure, and the other operating as LAG and loading only as necessary when system pressure drops. When air demand is lower or equal to the air generation from one compressor, only the Lead compressor gets loaded. When the air demand increases above the capacity of one compressor, the lag Compressors gets loaded in sequence as per demand requirements. C. Compressor Auto changeover Compressor auto change over occurs on the 2 following conditions: 1. If the stand-by compressor was selected in remote mode then after 24 hours of duty compressor usage stand-by compressor will start automatically. 2. Duty compressor failure will start the standby compressor immediately. If the failed compressor was loaded and the air demand is still required, the unit will go in to loaded mode straight away after the starting delay (20 seconds). D. Dry Air Purge When the compressor is in “standby mode”, solenoid 68-XY-1407 is activated and this opens the purge air line allowing a small flow of dry air protecting the compressor during stand-by, also immediately when the status stand-by is changed to duty, solenoid 68-XY-1407 is de-energised. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 112 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL E. Water Separators Level Control Inter cooler and after cooler water Separators level is maintained by level indicators (68-XI-1402 and 68-XI-1406) via opening or closing of valves 68-XY-1402 and 68-XY-1406 respectively. F. Instrument Air Header Pressure Control The pressure on the discharge line from the instrument air receiver is monitored by a transmitter 68-PT-1310; pressure on the discharge line of the plant air header is controlled by 68-PIC-1310. Decrease in the instrument pressure signal will tends to close the control valve 68-PCV-1310 in the plant air line. Controller Tag 68-PIC-1310 4.6 4.6.1 Inst air header pressure control Alarm Unit Operating Set Point Low High bar(g) 6 5.5 NA Control Description • Instrument Air pressure 68-PI-1312A/B/C/low low alarm set at 5 barg activates ESD Level-2 shutdown. • Instrument air pressure control valve 68-PCV-1310 closes on instrument air failure. EFFLUENT & WASTE WATER TREATMENT Equipment Specification Waste Water Degasser Equipment Tag No. Process Medium Size (ID/T/T), mm 6922-V-07 Waste/Sour Water 1500/4500 Design Temperature, °C 165/0 Design Pressure, barg 3.5/FV Operating Temperature, °C 73 Operating Pressure, barg 1 Material of Construction CS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 113 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Waste Water Degasser Pumps Equipment Tag No. 6922-P-08A/B Pump Type Horizontal, Centrifugal Process Medium Waste/Sour Water 3 Capacity, Normal/Rated, m /hr Shut off Pressure, bar(g) Suction Pressure, bar(a), Normal/Rated Discharge Pressure, bar(a) Design Temperature, °C Operating Temperature, °C Driver Type Rated Power, kW Material of Construction, Casing/Internals 8.62/9.48 14.6 0.99/4.66 8.8 95/0 73 Motor 15 Duplex SS/Duplex SS Sour Water Filter Equipment Tag No. 6922-S-06 Process Medium Sour Water Size (ID/T/T), mm 1500/4500 Design Throughput, m3/hr 9.48 Design Temperature, °C 95/0 Design Pressure, barg 14.6 Operating Temperature, °C 73 Operating Pressure, barg 7 Material of Construction CS Sour/Stripped Water Exchanger Equipment Tag No. Process Medium Design Pressure Shell Side (Stripped Water), barg Design Pressure Tube Side (Sour Water), barg Design Temperature Shell Side (Stripped Water), °C Design Temperature Tube Side (Sour Water), °C Operating Pressure Shell Side (Stripped Water), bar(a) Operating Pressure Tube Side (Sour Water), bar(a) Operating Temperature, Shell Side (Stripped Water), (In/Out) °C Operating Temperature, Tube Side (Sour Water), (In/Out) °C Design Duty, kW Material of Construction, Shell/Tube 6922-E-01 Sour/Stripped Water 11.3 14.6 160/0 160/0 6.80 7.4 126/104 73/96 276 CS/SS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 114 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sour Water Stripper Equipment Tag No. 6922-C-01 Design Pressure, barg (Max./Min.) 3.5/FV Design Temperature, °C (Max./Min.) 165/0 Process Medium Sour Water Max. Liquid Level, Top Section, mm 700 Max. Liquid Level, Bottom Section, mm 1200 Tray Nos. 38 Tower Diameter, mm 1000 Tower Height, mm 25000 Operating Pressure, bar(a) 1.20 Operating Temperature, °C, Top/Bottom Material of Construction, Top section Material of Construction, Bottom section Material of Construction, Internals 82.2/126.1 CS+SS316L CLAD CS SS316L Stripped Water Pumps Equipment Tag No. 6922-P-10A/B Pump Type Horizontal, Centrifugal Process Medium Stripped Water 3 Capacity, Normal/Rated, m /hr Shut off Pressure, bar(g) Suction Pressure, bar(a), Rated/Design Discharge Pressure, bar(a) Design Temperature, °C Operating Temperature, °C Driver Type Rated Power, kW Material of Construction, Casing/Internals 9.31/13.03 11.2 2.81/5.11 8.6 160/0 126 Motor 11 Duplex SS/Duplex SS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 115 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Stripper Overhead Circulation Pumps Equipment Tag No. 6922-P-11A/B Pump Type Horizontal, Centrifugal Process Medium Water 3 Capacity, Normal/Rated, m /hr Suction Pressure, bar(a), Rated/Max. Discharge Pressure, bar(a) Design Temperature, °C Operating Temperature, °C Driver Type 13.23/19.85 3.9/7 8.0 150/0 121 Motor Rated Power, kW 7.5 Material of Construction, Casing/Internals Duplex SS/Duplex SS Sour Water Stripper Reboiler Equipment Tag No. 6922-E-04 Process Medium Sour Water Design Pressure, Shell Side barg 7.0/FV Design Pressure, Tube Side barg 7.0/FV Design Temperature, Shell side °C 165/0 Design Temperature, Tube side °C 185/0 Operating Pressure, Shell, Side barg 1.40 Operating Pressure, Tube Side barg 3.5 Operating Temperature, Shell side °C 126.1 Operating Temperature, Tube side °C 147.7 Design Duty, kW 1803 kW Material of Construction, Shell side CS Material of Construction, Tube side SS316L Re boiler Condensate Drum Equipment Tag No. 6922-V-09 Process Medium Steam Condensate Size (ID/T/T), mm 800/2400 3 Design Throughput, m /hr 9.48 Design Temperature, °C 185/0 Design Pressure, barg 7/FV Operating Temperature, °C 155 Operating Pressure, barg 4.5 Material of Construction CS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 116 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Stripper Overhead Cooler Equipment Tag No. Type Process Medium 6922-E-03 Forced Draft Stripper Overhead Vapours Design Pressure, barg 11.1 Design Temperature, °C 150/0 Operating Pressure, barg 2.7 Operating Temperature, °C 121/55 Design Duty, kW 998 Material of Construction CS Number of Fans 2 Driver Type Motor Rated Power, kW 15 Stripped Water Cooler Equipment Tag No. Type Process Medium 6922-E-02 Forced Draft Stripped Water Design Pressure, barg Design Temperature, °C 130/0 Operating Pressure, bar(g) 5.7 Operating Temperature, °C 104/52 Design Duty, kW 630 Material of Construction CS Number of Fans 2 Driver Type Rated Power, kW 4.6.2 11.2 Motor 11 Effluent and Waste Water Treatment Process Description Sour water from various sources is collected in the Waste Water Degasser 6922-V-07, which provides over 20 minutes of hold-up for the waste water. The flow of waste water from TGTU Cooling Water Circulation Pumps 9102-P-12A/B is continuous at a rate of 8.7 m3/hr. The pressurised drain from Cooling Water Circulation Pumps 9102-P12A/B and the flow from Regenerator Reflux Drum Pumps 9103-P-11A/B are intermittent. The sour water from the Waste Water Degasser 6922-V-07 is continuously pumped under flow control by Waste Water Degasser Pumps (6922-P-08A/B) to the Sour Water Stripper 6922-C-01 for treatment. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 117 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL In the event the Sour Water Treatment System is unavailable due to a process upset, provision exists for manually routing the Waste Water Degasser liquids directly to the Observation Sump (6922-X-04). A balance line between Waste Water Degasser 6922-V-07 and Sour Water Stripper 6922-C-01 means that the pressure in the Waste Water Degasser 6922-V-07 floats on the Sour Water Stripper 6922-C-01 operating pressure (i.e. 1.0 barg). A nitrogen supply line is provided to maintain pressure in the Waste Water Degasser 6922-V-07 if it falls below a certain minimum as liquids are pumped out. The sour water from Waste Water Degasser 6922-V-07 is filtered in Sour Water Filter (6922-S-06) to remove particle size of 10 micron e.g. sand, pipe scale and salts and then preheated in Sour/Stripped Water Exchanger (6922-E-01) before feeding to Sour Water Stripper. The Sour Water Stripper operates at 1.0 barg and has an upper section and a lower tray section. The upper section is provided with temperature indication locally as well as in DCS. A differential pressure transmitter is also provided across trays 33 to 38 with indication in DCS. The middle section of the column is also provided with a temperature indication locally as well as in DCS. A differential pressure transmitter is also provided across trays 1 to 32 with indication in DCS. The bottom section of the column is provided with temperature and level indications locally as well as in DCS. The sour water is stripped by the vapours generated from the Sour Water Stripper Reboiler 6922-E-04. The Reboiler utilises LP steam to heat the sour water that comes from the bottom of the Sour Water Stripper to 126⁰C. The condensed steam from the Reboiler is sent to the LP Condensate system through level control. Reflux for the column is provided by a pump-around system. Water is taken from below tray 33 pumped by Stripper Overheads Circulation Pumps (6922-P-11A/B) under flow control, cooled in Stripper Overheads Cooler (6922-E-03) and then returned to the top tray. The stripper overhead acid gases are routed to the TGTU (upstream of Desuperheater/Contact Condenser, 9102-C-11). In the event of high column pressure, excess gases are diverted to LP Acid Gas Flare. The stripped water from the stripper is pumped under level control cascaded to a flow controller via Stripper Water Pump (6922-P-10A/B) to the Sour/Stripped Water Exchanger (6922-E-01) to preheat the feed to the stripper. The water is then routed to the Stripped Water Cooler (6922-E-02) where it is cooled to 55°C before discharge to the Observation Sump. An analyser is provided in the line to the Observation Sump to monitor the sulphide content of the stripped water stream. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 118 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.6.3 Effluent & Waste Water Treatment Control Description 4.6.3.1 Waste Water Degasser Pressure Control Waste Water Degasser (6922-V-07) pressure is maintained by the pressure controller 69-PIC-1307 by monitoring the pressure through 69-PT-1307 located at the top of the vessel. The pressure is maintained by regulating the pressure control valve 69-PV-1307 in the nitrogen line to the Waste Water Degasser. 69-PIC-1307 opens the nitrogen control valve 69-PV-1307 on falling pressure in the Waste Water Degasser. Controller Tag 69-PIC-1307 Control Description Waste Water Degasser top pressure Alarm Unit Operating Set Point Low High barg 1 0.8 1.2 • High high pressure alarm (69-PAHH-1311) set at 1.3 barg in Waste Water Degasser closes the nitrogen inlet valve 69-XV-1315 • High high level alarm (69-LAHH-1311) set at 77% in Degasser closes the nitrogen inlet valve 69-XV-1315 • Waste Water Degasser 6922-V-07 nitrogen pressure control valve 69-PV-1307 closes on instrument air failure. 4.6.3.2 Waste Water Degasser Level Control Waste Water Degasser (6922-V-07) level is monitored by 69-LT-1301 and controlled by 69-LIC-1301. Level in the Degasser is controlled by controlling the sour water outlet from Sour/Stripped Water Exchanger (6922-E-01). Master controller 69-LIC-1301 acts in cascade and provides the set point to sour water flow Slave controller 69-FIC-1314 which regulates the control valve 69-FV-1314 in the outlet of Sour/Stripped Water Exchanger 6922-E-01. Controller Tag Alarm Control Description Unit Operating Set Point Low High 69-LIC-1301 Waste Water Degasser level % 50 33 53 69-FIC-1314 Sour water to Stripper column m3/hr 8.2 7.4 9 • High high level alarm (69-LAHH-1311) set at 77% in Degasser closes the nitrogen inlet valve 69-XV-1315 and waste water valve 69-XV-1312 from the Cooling Water Circulation Pumps 9102-P-12A/B • Low low level alarm (69-LALL-1311) set at 20% in Degasser 6922-V-07 trips the Waste Water Degasser Pumps 6922-P-08A/B EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 119 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • 4.6.3.3 Sour water to Stripper column control valve 69-FV-1314 closes on instrument air failure. Sour Water Stripper Pressure Control A split range pressure controller 69-PIC-1315 is provided to maintain the top pressure of Sour Water Stripper (6922-C-01) by throttling the sour gas to TGTU control valve 69-PV-1315A (0-50%) and sour gas to LP acid gas flare drum control valve 69-PV-1315B (50-100%). On rising pressure 69-PIC-1315 first opens the sour gas to TGTU control valve 69-PV1315A; further increase in pressure causes the pressure controller to open the vent valve 69-PV-1315B to release gases to the LP Acid Gas Flare. Fig. 22 – 69-PIC-1315 Controller Output The above drawing shows the split range operation of 69-PV-1315A & 69-PV-1315B. • 69-XV-1313 located at the downstream of sour water stripper top pressure control valve 69-PV-1315A to TGTU closes on activation on ESD-0 and ESD-1 shutdown • Sour Water Stripper Column 6922-C-01 control valve 69-PV-1315A to TGTU closes on instrument air failure • Sour Water Stripper Column 6922-C-01 control valve 69-PV-1315B to LP flare opens on instrument air failure. Controller Tag Control Description 69-PIC-1315 Sour Water Stripper top pressure Alarm Unit Operating Set Point Low High bar(g) 1 0.8 1.2 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 120 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.6.3.4 Sour Water Stripper Bottom Level Control Stripped water from the bottom of the Sour Water Stripper 6922-C-01 is pumped via Stripped Water Pumps (6922-P-10A/B) to the Sour/Stripped Water Exchanger (6922-E01). Outlet from the Sour/Stripped Water Exchanger 6922-E-01 enters in to the Stripped Water Cooler (6922-E-02) and the cooled stripped water is sent to Observation and Buffer Sump. Sour Water Stripper (6922-C-01) bottom level is controlled by regulating the stripped water cooler outlet to the Observation and Buffer Sump. Sour Water Stripper ‘MASTER’ level controller 69-LIC-1306 acts in cascade and provides the set point to the Stripped Water Cooler outlet ‘SLAVE’ flow controller 69-FIC-1317 which regulates the flow control valve 69-FV-1317. Controller Tag 4.6.3.5 Alarm Control Description Unit Operating Set Point Low High 69-LIC-1306 Sour Water Stripper bottom level % 50 21 73 69-FIC-1317 Stripped Water Cooler outlet flow m3/hr 8 6 10 • Low low level alarm (69-LALL-1316) in Sour Water Stripper 6922-C-01 bottom trips the Stripped Water Pumps 6922-P-10A/B and closes the stripper outlet valve 69-XV-1339. • High high level alarm (69-LAHH-1316) Sour Water Stripper 6922-C-01 bottom trips the Waste Water Degasser Pumps 6922-P-08A/B and closes the Waste Water Degasser 6922-V-07 outlet valve 69-XV-1316. • Stripped Water Cooler 6922-E-02 outlet valve 69-FV-1317 to buffer sump closes on instrument air failure. Sour Water Stripper 6922-C-01 Top Level Control Water from the Stripper Overheads Cooler (6922-E-03) is circulated to the top of the Stripper through the Stripper Overhead Circulation Pumps (6922-P-11A/B). Stripper top level is maintained by controlling the start-up-water which is mixed with the circulated water from the Sour Water Stripper column at the suction of the Stripper Overheads Circulation Pumps (6922-P-11A/B). Stripper top level is monitored and controlled by 69-LIC-1325 which directly controls the control valve 6922-LV-1325 in the start-up-water line. Controller Tag Control Description 69-LIC-1325 Sour Water Stripper top level Alarm Unit Operating Set Point Low High % 50 30 74 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 121 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Low low level alarm (69-LALL-1315) in Sour Water Stripper top trips the Stripper Overhead Circulation Pump 6922-P-11A/B • Start-up water control valve 69-LV-1325 closes on instrument air failure. 4.6.3.6 Circulating Water Flow to Stripper Overhead Cooler Control Circulated water from the Sour Water Stripper (6922-C-01) top is pumped by Striper Overhead Circulation Pumps (6922-P-11A/B) to Stripper Overhead Cooler (6922-E-03). Circulated water flow to stripper overheads is measured by 69-FT-1316 and controlled by the flow controller 69-FIC-1316 which directly controls the flow control valve 69-FV-1316 located in the common discharge of 6922-P-11A/B. • 4.6.3.7 Controller Tag Control Description 69-FIC-1316 CW to Stripper Overhead Cooler Alarm Unit Operating Set Point Low High m3/hr 13.6 12.2 15 Circulating water flow control valve 69-FV-1316 to Stripper Overhead Condenser opens on instrument air failure Sour Water Stripper Reboiler Temperature Control Temperature control is achieved by controlling the steam flow to the stripper reboiler. LP steam flow to the Sour Water Stripper Reboiler 6922-E-04 is controlled by 69-FIC1315 which regulates the LP steam flow control valve 69-FV-1315. Set point for the steam flow control is received from the calculation block 69-UY-1315, where the sour water flow from 91-FIC-1314 is multiplied with manually set ratio (193) between LP steam and sour water which is provided via 69-HIC-1315. Controller Tag 69-FIC-1315 Control Description LP steam flow to the Stripper Reboiler Alarm Unit Operating Set Point Low High kg/hr 2154 1725 3015 • LP steam valve 69-XV-1314 located on the upstream of the control valve 69-FV1315 closes on activation of Waste Water Degasser pressure high high alarm set at 1.3 barg. • LP steam flow control valve 69-FV-1315 to reboiler closes on instrument air failure. 4.6.3.8 Stripper Reboiler Steam Temperature Control Temperature control of LP steam is achieved by passing the LP steam to Desuperheater (6922-X-01), where the temperature is maintained by injecting Boiler Feed Water. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 122 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL LP steam outlet temperature from the Desuperheater is monitored by 69-TT-1327 and controlled by 69-TIC-1327. Temperature Controller 69-TIC-1327 directly regulates the boiler feed water flow via 69-TV-1327 located at the inlet of De-super heater. Controller Tag 69-TIC-1327 • 4.6.3.9 Control Description LP steam temperature to the Stripper Reboiler Alarm Unit Operating Set Point Low High °C 148 NA 153 BFW control valve 69-TV-1327 to LP steam closes on instrument air failure Re-boiler Condensate Level Control LP condensate from the Sour Water Stripper Reboiler 6922-E-04 is collected in Reboiler Condensate Drum (6922-V-09). Condensate level is monitored by 69-LT-1327 and controlled by 69-LIC-1327. Condensate level is maintained by throttling the control valve 69-LV-1327 which regulates the condensate flow to the LP condensate header. Controller Tag 69-LIC-1327 • Alarm Control Description Unit Operating Set Point Low High Re-boiler Condensate Drum level % 50 17 75 Re boiler condensate control valve 69-LV-1327 to LP condensate header closes on instrument air failure 4.6.3.10 Stripper Overheads Cooler Temperature Control Circulating water from the Stripper Overheads Circulation Pumps (6922-P-11A/B) enters in to the Stripper Overheads Cooler (6922-E-03) where the water is cooled and passes to the Sour Water Stripper. Temperature of the circulating water to the Sour Water Stripper (6922-C-01) is monitored at the outlet of the Stripper Overheads Cooler by 91-TT-1315 and controlled by 69-TIC-1315. Temperature controller 69-TIC-1315 output controls the speed of the stripper overhead cooler fans VSDs at the same time. The temperature controller, 69-TIC-1315 regulates the speed of the sour water Stripper Overheads Cooler VSDs (6922-EM-03AA, 6922-EM-03AB) to maintain the temperature of circulation water to Sour Water Stripper. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 123 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Alarm Controller Tag Control Description Unit Operating Set Point Low High 69-TIC-1315 Stripper overheads cooler to sour water stripper °C 55 50 60 Details of control tags for VSD’s are tabulated below: S No. Motor-no Control Tag Remarks 1. 6922-EM-03AA 69-SY-1324 VSD 2. 6922-EM-03AB 69-SY-1329 VSD High high vibration alarm of each fan trips the respective fan motors 4.7 LP FUEL GAS 4.7.1 Equipment Specification LP Fuel Gas KO Drum Tag No. 6236-V-05 Size, mm, (Dia x T/T) 1100 x 2400 Design Pressure, barg 9.0 Design Temperature, °C Operating Pressure, (Normal/Max), barg Operating Temperature, °C Material of Construction 4.7.2 Fuel Gas System Process Description 4.7.2.1 Introduction 100/0 6/7 25-50 CS LP Fuel Gas is required for New Steam Generation Boiler Packages 6848-A-02A/B/C. 4.7.2.2 Process Description The new Fuel Gas requirements under the SRU upgrade project will be secured from two separate sources as follows. Source 1 Supply The main normal LP Fuel Gas supply for the new MP Steam Boiler Package (6848-A02A/B/C) is supplied from the first stage suction of the existing Booster Compressors (6701-K-10/20/30) in NGL-3. In addition, two back up sources are provided; the first is the fuel gas from 6103-K-01A/B with a second backup from existing 30” line (T-10). The new fuel gas supply system will consist of a letdown station, Fuel Gas KO Drum (6236-V-05) and a supply header to the steam boilers. The source pressure from the take-off point will be let down to 7 barg through the pressure control valve 62-PV- EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 124 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 1301A before entering the LP Fuel Gas KO Drum. The source pressure of the fuel gas from 6103-K-01 A/B is 20 barg whilst that of feed gas from the 30” line is 45 barg. The former is let down to 7 barg through the pressure control valve 62-PV-1301B and the latter via 62-PV-1302. Source 2 Supply LP fuel gas for SRU upgrade new users (Reducing Gas Generator 9102-F-11 and new Incinerator, 9101-F-14) will be sourced from the existing LP fuel gas header at NGL-3 as there is sufficient spare capacity available for there. 4.7.2.3 Operating and Control System The fuel gas for the LP fuel gas system is taken from the first stage suction of the Lean Gas Booster Compressors (6701-K-10/20/30), through 62-PV-1301A via pressure controller 62-PIC-1301 located in the top of the LP Fuel Gas KO Drum (6236-V-05). In the event of loss of lean gas supply from the Booster Compressors, the pressure controller 62-PIC-1301 signal is routed to 62-PV-1301B via soft valve selector 62-PY1301. In addition if there is an emergency shutdown of NGL Extraction unit (from where fuel gas is ultimately supplied) valve selector 62-PY-1301 is overridden and the signal from 62-PIC-1301 is automatically routed to 62-PV-1301B. This allows back up fuel gas taken from 6103-K-01A/B. The takeoff for the second back up supply is from 30" existing line (T-10) routed through 62-PV-1302 via pressure controller 62-PIC-1302. A fast acting pressure control valve 62-PV-1303 controlled by pressure controller 62-PC-1303 is provided on the overhead line from 6236-V-05 to route fuel gas to LP flare in the event the pressure in the KO drum continues to increase beyond the normal operating range. Alarm Controller Tag Control Description Unit Operating Set Point Low High 62-PIC-1301 LP fuel gas from existing Booster compressors bar g 7 5.3 7.8 62-PIC-1302 LP fuel gas to new SRU bar g 7 5.3 7.8 62-PIC-1303 Fuel gas to LP flare bar g 7 NA 7.8 • High high pressure alarm (62-PAHH-1304) set at 8.2 barg in LP fuel gas trips the boiler packages and closes the fuel gas inlet on/off valves 62-XV-1301, 62-XV-1302 and 62-XV-1303. • LP fuel gas inlet pressure control valves 62-PV-1301A, 62-PV-1301B and 62-PV-1302 close on instrument air failure. • Fuel Gas vent to LP flare pressure control valve 62-PV-1303 opens on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 125 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.8 4.8.1 SEA COOLING WATER SYSTEM Equipment Specification Sea Cooling Water Pumps Equipment Tag No. Pump Type Process Medium Capacity, m3/hr Suction Pressure, barg, Normal/Max. Discharge Pressure, barg Design Pressure, bar(g) Design Temperature, °C Operating Temperature, °C Driver Type Rated Power, kW Material of Construction, Casing/Internals 6932-P-04A/B Vertical, Centrifugal Sea Water 1600 0.07/0.25 5.0 8.0 85/0 35 Motor 340 Duplex SS/Duplex SS Sea Cooling Water Filters Equipment Tag No. Process Medium Size (ID/T/T), mm Design Throughput, m3/hr Design Temperature, °C Design Pressure, barg Operating Temperature, °C Operating Pressure, barg Material of Construction 6932-S-02A/B Sea Water 610/1016 1600 85/0 8 15-40 5 Duplex SS Local Biocide Drain Pit Equipment Tag No. 6932-T-06 Size (L/W/H), mm 1000/1000/1000 Design Temperature, °C Design Pressure, barg Material of Construction 85/0 0 Concrete Local Chemical Drain Pit Equipment Tag No. 6932-T-01 Size (L/W/H), mm 1000/1000/1000 Design Temperature, °C Design Pressure, barg Material of Construction 85/0 0 Concrete EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 126 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.8.2 Sea Cooling Water System Process Description Sea Cooling Water system is required to supply cooling water for the coolers in the SRU upgrade facilities. A part of sea cooling water is also supplied to existing sea water supply system. The Sea Cooling Water system includes two Sea Cooling Water Pumps (6932-P-04A/B, one operating and one standby), one Electro Chlorination Package (6932-A-05), one Biocide Injection Package (6932-A-06) and one Scale Inhibitor Injection Package (6932-A-07). Two Sea cooling Water Pumps 6932-P-04A/B are installed on a new jetty and take suction from the sea. The pumps are vertical-shaft, constant speed centrifugal pumps and are electric motor driven. The sea water cooling pumps have a design capacity of 1600 m3/h (each) at a discharge pressure of 5.0 barg. To meet the design flow requirements, one pump will be normally running, whilst the other is on standby. Each pump is capable of supplying a normal flow of 1200 m3/h to the users for SRU upgrade. The water enters the pump body through a suction pipe (stilling tube) shaped to reduce turbulence. A coarse mesh bar suction screen is installed at each pump to prevent seaweed and other debris from entering the sea water system. From the common discharge of seawater cooling pumps, seawater stream flows via a new dedicated 24” main supply header to the new filtration package unit (6932-S02A/B). The self cleaning rotary type Sea Water Filters (one in operation and one on standby) are capable of removing particle sizes greater than 1000 microns from seawater and each unit is designed for a flow of 1600 m3/h. The filtered water from filters is routed to the heat exchangers located in AGEU/TGTU another users. A small portion of the main seawater (cooling water) flow is diverted downstream of the filters to provide seawater supply for the Electro Chlorination Unit (6932-A-05). The Electro Chlorination unit generates sodium hypochlorite solution. The sodium hypochlorite solution is injected into Sea Cooling Water system. There is one dedicated new Electro Chlorination Unit. In addition, a dedicated Biocide Injection Unit (6932-A-06) for effective control of growth of marine organisms and a dedicated Scale Inhibitor Injection Unit (6932-A-07) to prevent formation of mineral scales in the Sea Cooling Water system are also provided for existing as well as new sea cooling water systems. The new cooling water system is a once through system and the sea water returned from the SRU upgrade facilities is discharged into existing Seawater Observation Sump (6932-X-01) which has a retention capacity of 60 m3. From the sump the seawater overflows to the sea. To prevent fouling the temperature of cooling water from each exchanger outlet should not exceed the maximum allowable temperature limit of 45°C. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 127 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL A tie in to the existing NGL-3/4 seawater supply system is also provided to supply seawater from the new seawater pumps. 4.8.3 Sea Cooling Water Control 4.8.3.1 Sea Cooling Water Pumps (6932-P-04A/B) The cooling water pumps can be started and stopped from the DCS by means of one of the hand switches 69-HS-1311/1322. The running status indication of the pumps is provided in the DCS. In addition, pump discharge low pressure alarms with indication in the DCS (69-PIA-1301/1303), a pressure transmitter (69-PT-1301/1303), and a sample connection (69-SC-013/014) are provided for each pump. The chlorination, biocide and scale inhibitor lines to the pumps are provided with flow indicators to monitor injection of these chemicals into the pump suction. The cooling water flow through each heat exchanger may be manually regulated by butterfly valves located upstream/downstream of the exchanger. The valves are within view of the respective process side temperature indicator locations. For operational flexibility a 18” crossover connection between sea cooling water pump discharge line 24”-6932-SW-259-A7A2 is provided to supply sea cooling water to NGL3/4. The crossover line contains two 18” butterfly valves which are normally closed. 4.8.3.2 Filtration System The Sea Cooling Water Filtration system comprises of two self cleaning rotary type Cooling Water Filters (6932-S-02A/B), one operating and one standby. Each filter is designed for a flow of 1600 m3/hr and is capable of removing particle sizes greater than 1000 microns. In addition each filter is equipped with an automatic back flushing mechanism which operates on an intermittent basis when filter cleaning is required. Across a cleaner seawater filter the normal pressure drop is 0.2 bar. During normal operation the filter will become dirty over a period of time and the pressure drop across it will increase. To ensure periodic cleaning of the online filter, a timer facility within the filter control panel automatically initiates the cleaning cycle after a preset interval and terminates it after a preset duration. The cleaning sequence involves the start of the cleaning gear and opening of the drain ON/OFF valve 69-XV-1340/1341. The former causes the debris trapped across the filter mesh to be loosened as the mesh rotates against static scrapers whilst the latter allows the loosened debris to be discharged back to the sea. The cleaning cycle lasts for approximately 90 seconds after which the drain ON/OFF valve closes and the cleaning gear stops by de-energising the contactor. In addition to the timer, a differential pressure transmitter (PDT-1309/1310) can also initiate the cleaning cycle when the filter pressure drop reaches a specified value (0.5 barg). After the completion of the cleaning sequence the timer is also reset. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 128 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The cleaning sequence may be stopped via hand switch (69-HS-1309/1310). In the event the cleaning gear is stuck, a common alarm 69-XA-1309/1310 is initiated. In addition a high high pressure drop alarm (69-PDAH-1309/1310) is also provided to alert the operator in the event of problems with the cleaning of the filter. The downstream isolation valves of both (operating and standby) filters are kept open at all the times during normal operation. The inlet isolation valve (MOV-1303/1304) of the standby filter is kept in closed position during normal operation. The selection of the operating filter must be made from the DCS via hand switches (HS-1309/1310). 4.8.3.3 Sea Cooling Water Outlet Pressure Control Sea Cooling Water Pumps (6932-P-04A/B) outlet is routed to Sea Cooling Water Filters (6932-S-02A/B) and the outlet pressure is maintained by the pressure controller 69-PIC-1306 by monitoring the pressure through 69-PT-1306 located in the common discharge of the Sea Cooling Water Pumps. The pressure is maintained by regulating the pressure control valve 69-PV-1306 in the cooling water drain line connected to the sea. 69-PIC-1306 opens the drain line control valve 69-PV-1306 on rising pressure in the outlet of Sea Cooling Water Pumps common discharge. Controller Tag 69-PIC-1306 • 4.9 4.9.1 Control Description Sea Cooling Water Pumps outlet pressure Alarm Unit Operating Set Point Low High barg 6 NA 6.5 Sea cooling water drain control valve 69-PV-1306 opens on instrument air failure ELECTROCHLORINATION PACKAGE Equipment Specification Electro Chlorination Package Equipment Tag No. 6932-A-05 Process Medium Sea Water Design Throughput, kg/hr Design Temperature, °C Design Pressure, barg 10 85/0 8 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 129 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Auto Backwash Filter Equipment Tag No. Process Medium Type Design Throughput, m3/hr Design Temperature, °C Design Pressure, barg 6932-S-03A/B Sea Water Auto Self Cleaning, Backwash type 14 85/0 6 Filtration Rate, Microns 500 Pressure Drop, Clean, bar 0.1 Pressure Drop, Dry, bar 0.22 Material of Construction, Body/Internal GRP/Monel Transformer Rectifier Equipment Tag No. Rating, kVA Power Supply 6932-RC-101A/B 52.7 415 V, 3ph, 50 Hz Output Voltage 44V DC Output Current 922 Amps DC Cooling Design Temperature, °C Air Natural Air Forced 85/0 Electrolyser Equipment Tag No. Type Capacity Per Cell, kg/hr Design Pressure, barg Design Temperature, °C Orientation Casing Anode Cathode 6932-G-01A/B Panchlor (Bi Polar) 10 6.0 85/0 Horizontal GRP with uPVC Lining Titanium Coated with Coating of Platinum group Mixed oxide Titanium EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 130 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Degassing Tank Equipment Tag No. Process Medium Capacity, m3/hr Design Temperature, °C Design Pressure, barg Residence Time, mins. Material of Construction 6932-T-02 Sea Water 5.0 80/0 Atmospheric + Fully Filled Liquid 15 Glass Reinforced Vinyl Ester Hydrogen Dilution Blowers Equipment Tag No. Process Medium 6932-K-01A/B Air 3 Capacity, m /hr 362 Design Temperature, °C 85/0 Design Pressure, mmWG 150 Motor Rating, kW 1.1 Material of Construction SS316L Dosing Pumps Equipment Tag No. Type 6932-P-05A/B Centrifugal 3 7.0/14.0 Design Temperature, °C 85/0 Capacity, m /hr, Continuous/Shock Dosing Design Pressure, barg 7.5 Motor Rating, kW 5.5 Material of Construction Titanium Acid Wash Tank Equipment Tag No. Type 6932-T-03 Vertical Process Medium HCl 3 2.0 Design Temperature, °C 80/0 Capacity, m Design Pressure, barg Working Pressure Material of Construction Atmospheric + Fully Filled Liquid ATM. Glass Reinforced Vinyl Ester EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 131 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Acid Wash Pump Equipment Tag No. 6932-P-06 Type Magnetic Drive Process Medium HCl 3 5.0 Design Temperature, °C 85/0 Capacity, m /hr, Continuous/Shock Dosing Design Pressure, barg 6.0 Motor Rating, kW 2.2 Material of Construction Poly Propylene Acid Bund Material of Construction 4.9.2 GRP Electro Chlorination System Description During normal operation the Electro Chlorination Unit supplies Sodium Hypochlorite that is injected into the suction lines of the Seawater Supply Pumps (6932-P-04A/B). The hypochlorite controls the growth of marine organisms in sea cooling water system. A small portion of the main sea cooling water flow to the new units of SRU is diverted downstream of the filters 6932-S-02A/B and this provides the sea water supply for the Electro Chlorination Unit 6932-A-05. The required flow of sea water is fed to each electrolyser module designed to produce 10kg/h of active chlorine. Direct current is passed through the sea water producing a sodium hypochlorite solution and hydrogen. The amount of active chlorine (sodium hypochlorite) produced, is directly proportional to the current passed through the cells. Hence, sea water is not normally varied. Any required reduction in active chlorine demand can be achieved by manually adjusting electrical current to the electrolysers at the local control panel. 4.9.2.1 Biocide and Scale Inhibitor Injection Packages During normal operation, the biocide from the Biocide Injection Package is directly injected into the hypochlorite injection line from Electro Chlorination Package just before the injection point into the Sea Cooling Water Pump Suction of existing (P-3001A/B/C & P-1618AR/BR/CR) and new 6932-P-04A/B sea cooling water systems. The injection is to be carried out at a concentration of 6.6 ppm three times daily for a 15 minute period. The biocide filling into the Biocide Storage Tank inside the package is a manual operation using flexible hose. During normal operation the scale inhibitor from the Scale Inhibitor Injection Package is injected into Sea Cooling Water Pump suction of existing (P-3001A/B/C & EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 132 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL P-1618AR/BR/CR) and new 6932-P-04A/B Sea Cooling Water Pumps. The injection is carried out continuously at a concentration of 1.5 ppm. The scale inhibitor filling into the storage tank inside the package is a manual operation using flexible hose. 4.9.3 Electro chlorination Package Control 4.9.3.1 Changeover of Auto Back Wash Filter Sea water is supplied to the skid at a rate of 14 m3/hr. 69-PCV-1463 maintains the system sea water pressure at 3.5 bar g from the inlet pressure of 5 bar (g). Sea water is filtered to 500 microns to supply to the electrolyser. An auto back wash filter (6932-S03A/6932-S-03B) is installed which operates on a duty/stand by basis, During the initiation of changeover/backwash the actuated discharge valve (69-XV1453/69-XV-1456) of duty filter will close, the actuated backwash valve of duty filter (69-XV-1452/69-XV-1455) will open and the actuated discharge valve (69-XV-1453/ 69-XV-1456) of stand by filter will open which ensures the filter changeover was happened. Following are the causes for filter change over to occur: Sl. # Tag No. 1. 69-PDI-1452 2. 3. 4. 4.9.3.2 Limit Unit Value DP across 6932-S-03A High-high barg 0.2 69-PDI-1453 DP across 6932-S-03B High-high barg 0.2 69-PI-1455 Filter common discharge Low-low barg 2.75 69-FI-1456 Service Electrolyser common I/L Low-low 3 m /hr 8.0 Changeover of Electrolyser Electrolyser stream (6932-G-01A/6932-G-01B) operates on duty/standby basis. Following are the causes for electrolyser changeover to occur: Sl. # I. Tag No. 69-FI-1451 Service Inlet flow to 6932-G01A Limit Low-low Unit Value 3 10 3 m /hr II. 69-FI-1452 Inlet flow to 6932-G01B Low-low m /hr 10 III. 69-PI-1455 Filter common discharge High-high barg 4.5 Also if the temperature difference between electrolyser upstream temperature (69TT-1451) and downstream of the individual electrolyser temperature (69-TT-1452/69TT-1453) is 5°C then controlled shutdown is initiated and the standby electrolyser unit is started. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 133 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL 4.9.3.3 Dosing Pumps Discharge Flow Control Dosing pumps (6932-P-05A/B) discharge flow is controlled via flow controller 69-FIC-1453. Dosing pump discharge flow rate is measured by magnetic flow transmitter 69-FT-1453 and controlled by 69-FIC-1453, set point is locally provided on the HMI. Output of 69-FIC-1453 directly commands the control valve 69-FV-1453. Controller Tag Control Description 68-FIC-1453 Dosing pumps discharge flow control Alarm Unit Operating Set Point Low High m3/hr 2 & 11 1.8 13.0 Note: The controller 68-FIC-1453 has 2 Set Points based on the Continuous Dosing and Shock Dosing. When continuously dosed, set point is 2m3/hr whereas for Shock Dosing, set point is 11m3/hr. 4.9.3.4 Acid Pumps Control The acid wash system is a manual system. To maintain the efficiency of the electrolyser streams, regular washing with dilute HCL is required to remove the hydroxide deposits. Following are the causes for tripping of Acid Wash Pump 6932-P-06: Sl. # 4.10 4.10.1 Tag No. Service Limit Unit Value 1. 69-LI-1454 Acid Wash Tank level Low-low mm 370 2. 69-AI-1451 Conductivity of acid wash solution High-high µS/cm 77000 NGL-4 SEA WATER FILTERS Equipment Specification Sea Water Filters Equipment Tag No. S-8840A/B Process Medium Sea Water Capacity, kg/hr, Min./Max. Design Temperature, °C Design Pressure, barg 138240/309760 85/0 7.0 Operating Temperature 40/15 Operating Pressure, barg 4 Material of Construction, Casing/Elements SA240UNS S31803/Duplex SS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 134 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.10.2 NGL-4 Sea Water Filters S-8840A/B Description Two Sea Water Filters S-8840A/B are installed in the existing sea water from cooling water supply line 8”-88-32-WR-0066-001W. The filter consists of a pressure containment body with inlet, outlet, drain/backwash outlet, PSV and vent connections. Filter Basket has been sized for the design flow conditions. Access to the filter basket is via the bolted cover at the top of the assembly. Sealing of the cover to the body is via a spiral wound gasket and stud bolts. A simple devit arm is provided to allow removal and support of the cover during maintenance operations. Across a clean Seawater Filter S-8840A/B the normal pressure drop is 0.2 bar. During normal operation the filter will become dirty over a period of time and the pressure drop across it will increase. The differential pressure transmitter (88-PDT-801) raises an alarm when the filter pressure drop reaches a specified value (0.4 bar). This means the filter needs cleaning and the clean filter is brought on line. 4.11 4.11.1 DEMINERALISED WATER SYSTEM Equipment specification DM Water Package Equipment Tag No. 6834-A-07 Process Medium DM Water 3 8.0 Design Temperature, °C 85/0 Design Pressure, barg 12.3 Capacity, m /hr Cationic Exchangers Bed Equipment Tag No. Process Medium ID, mm 6834-S-21A/B Fresh Water 600 3 Capacity, m /hr 3 Flow Rate, m /hr 10.5 7.0 Design Temperature, °C 85/0 Design Pressure, barg 12.3 Operating Temperature, °C 49 Operating Pressure, bar 4.0 Material of Construction, Casing/Elements CS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 135 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Anionic Exchangers Bed Equipment Tag No. Process Medium 6834-S-22A/B Fresh Water ID, mm 950 3 Capacity, m /hr 10.5 3 Flow Rate, m /hr 7.0 Design Temperature, °C 85/0 Design Pressure, barg 12.3 Operating Temperature, °C 49 Operating Pressure, bar 4.5 Material of Construction, Casing/Elements CS DM Water Recycle Pumps Equipment Tag No. Process Medium 6834-P-37A/B DM Water 3 Capacity, m /hr, Normal/Rated 3 10.5/10.5 Minimum flow, m /hr 1.11 Design Pressure, barg 12.3 Design Temperature, °C 85/0 Suction Pressure, bara, Rated 2 Operating Temperature, °C 43 Operating Pressure, bara 6 Driver Type Driver Power, kW Material of Construction, Casing/Elements Motor 5.5 SS316L Resin Trap Equipment Tag No. 6834-SP-11A/B/C/D Diameter, mm 60.3 Length, mm 300 Design Temperature, °C 85/0 Design Pressure, barg 12.3 Material of Construction, Casing/Elements SS316L Mesh Size, mm 0.202 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 136 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL DM Water Feed Pumps Equipment Tag No. 6834-P-24A/B Process Medium DM Water 3 Capacity, m /hr 12.0 Design Pressure, barg 5.1 Design Temperature, °C Suction Pressure, bara, Design/Rated 85/0 1.57/0.96 Operating Temperature, °C 43 Operating Pressure, bara 4.7 Material of Construction, Casing/Elements A743CF3M/SS316L DM Water Regeneration Pump Equipment Tag No. Process Medium 6834-P-36A/B DM Water 3 Capacity, m /hr 3.0 Suction Pressure, bara 1 Operating Temperature, °C 30 Operating Pressure, bara 5 Drive Type Motor Driver Power, kW 5.5 Material of Construction, Casing/Elements SS DM Water Neutralization Pumps Equipment Tag No. Process Medium 6834-P-38A/B DM Water 3 Capacity, m /hr, Normal/Rated 3 10.0/10.0 Minimum flow, m /hr 1.0 Design Pressure, barg 2.2 Design Temperature, °C Suction Pressure, kg/cm2(a), Design/Rated 85/0 0.8/0.78 Operating Temperature, °C 30 Operating Pressure, bara 2.6 Drive Type Drive Power, kW Material of Construction, Casing/Impeller Motor 4.0 PP/PP EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 137 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL HCl Dosing Pumps Equipment Tag No. Process Medium 6834-P-35A/B HCl Double Hydraulic Diaphragm Metering Pump Type Capacity, Lit/hr 180 Design Pressure, barg 3.7 Design Temperature, °C 85/0 Operating Temperature, °C 30 Operating Pressure, bara 3.0 Driver Type Motor Driver Power, kW 1.1 Material of Construction PP HCl Storage Tank Equipment Tag No. 6834-T-16 Process Medium HCl ID/Height, mm 1400/2730 3 Capacity, m 4 Design Pressure, barg ATM Design Temperature, °C 85/0 Material of Construction GRP HCl Unloading Pump Equipment Tag No. 6834-P-38 Process Medium HCl Capacity, L/hr 150 Design Pressure, barg 3.5 Design Temperature, °C 85/0 Material of Construction PTFE/PVDF EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 138 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL NaOH Dosing Pumps Equipment Tag No. 6834-P-34A/B/C Process Medium NaOH Double Hydraulic Diaphragm Metering Pump Type Capacity, Lit/hr 301 Design Pressure, barg 3.7 Design Temperature, °C 85/0 Suction Pressure, bara 1 Discharge Pressure, bara 3 Operating Temperature, °C 30 Driver Type Motor Driver Power, kW Material of Construction 2.2 SS316L/PTFE NaOH Storage Tank Equipment Tag No. 6834-T-15 Process Medium HCl ID/Height, mm 1400/2730 3 Capacity, m 4 Design Pressure, barg ATM Design Temperature, °C 85/0 Material of Construction SS NaOH Unloading Pump Equipment Tag No. Process Medium Capacity, L/hr Design Pressure, barg Design Temperature, °C Material of Construction 4.11.2 6834-P-39 NaOH 150 3.5 85/0 PTFE/PVDF Demineralised Water System Process Description Demineralised Water Package Unit 6834-A-07 (one operating, one standby/ regenerating), is designed to produce flow of 7 m3/h of demineralised water. The Demineralised water is supplied to the new heating system and connectivity to the existing DMW header is also provided to allow operation flexibility. Demineralised water unit will provide DMW to the following users: • Make up water to Steam Condensate Flash Drum (6834-V-05) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 139 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Amine Surge Tank (9103-T-11) • Make up water to Cooling Water Circulation Pump (9102-P-12A/B) • Start-up water to Stripped Overhead Circulation Pump (9102-P-11A/B) • Make up water to Amine Regenerator Reflux Drum (9103-V-12) • Existing DMW network system (for operational flexibility, normally no flow) 4.11.2.1 Demineralised Water Package The Demineralised Water Package is based on ion exchange technology (similar to the existing DMW package) and consists of two identical trains. The DMW package operates continuously and automatically and thus requires minimum intervention. The package includes the necessary control and safety devices. The Demineralised Water from the DMW package is routed to Demineralised Water Storage Tank (6834-T-08). Capacity of Demineralised Water Storage Tank is 83 m3. Fresh water is sent to the new users (DMW package & utility) continuously by means of the Drinking Water Feed Pumps (6834-P-23A/B, one operating, one standby) each having a design capacity of 10 m3/h. The duty/standby is selected via a selector switch in the DCS. The pumps are manually started and stopped through hand switches 68-HS1305/1306 and operated continuously. A minimum continuous flow recycle line with a restriction orifice (6834-RO-1303) ensures that there is always a minimum flow through the pump. Low low level alarms (68-LALL-006/007, via existing manual selector 68-HS-008) will shutdown the operating pump in the event of low-low level in Drinking Water Storage Tanks. The control ensures a safe and continuous operation and is summarized below: A. Flow Totaliser A flow totaliser placed in the main fresh inlet line to each ion exchange train sums the total water passing through the DMW unit. In normal operation, the end of a treatment cycle is determined on a volumetric basis by the totaliser which generates the order to switch from the online train to standby train. Following the switch over the regeneration sequence is commenced for the offline train. B. Conductivity Meter If high conductivity is reached before the end of the volumetric cycle, then the respective conductivity meter initiates the same automatic switch over order as generated by the volumetric cycle. If, in spite of this order, the conductivity continues to increase, then a separate high-high conductivity meter initiates a complete shutdown. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 140 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL C. Differential Pressure A differential pressure transmitter switch installed across the ion exchangers, also initiates the same switchover as the above volumetric cycle. D. Regeneration Demineralised water is used as service water for regeneration. From the storage tank (6834-T-08), regeneration DMW is delivered by means of the Regeneration Water Pumps 6834-P-36A/B. A solution of Caustic Soda is used to regenerate the anion resins. Concentrated Caustic Soda is stored in a storage tank. Before injection into the exchanger bed, the caustic soda is diluted by means of an in-line mixer. A solution of Hydrochloric Acid is used for cation resin regeneration. It is stored in the HCl storage Tank. The required dilution before injection into the exchanger bed is made by means of an in-line mixer. The regeneration effluents are collected in the concrete Neutralisation Pit where they are neutralised before being pumped out for disposal to effluent treatment plant. The pit is fitted with a pH-meter controller which controls acid dosing or caustic dosing to achieve neutralisation. Neutralisation Pit Pump re-circulates the effluent mixture for homogenisation. Plant air diffusion is also provided to enhance mixing. E. DMW Storage Tank (6834-T-08) The DMW package outlet line includes an automatic ON/OFF valve which is actuated by means of a signal coming from low/high level signal (68-LT-1305) on the DMW Storage Tank (6834-T-08). De-mineralized water from the DMW storage tank is directed, at a pressure and temperature of 3.7 barg and ambient temperature respectively by means of DMW Feed Pumps (6834-P-24A/B) to condensate flash drum (6834-V-05). The DMW storage tank is equipped with level alarms, High-High/Low-Low liquid level (LAHH-1306/LALL-1307). The former generates a High-High liquid level alarm in the control room, whilst the latter initiates Low low liquid level trip which shuts down the Regeneration Pumps 6834-P-36A/B in the DMW Package and DMW Feed Pumps. F. Demineralised Water Feed Pumps (6834-P-24A/B) Centrifugal type, DMW feed pumps (one running, one standby) are used to supply demineralised water at 3.7 barg pressure and ambient temperature, from DMW storage tank. Each pump is designed for a flow of 12 m3/hr based in heating system start-up (Filling inventory vessels such as condensates flash drum, De-aerator and Boilers in one shift). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 141 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL A minimum flow recycle line with a restriction orifice (6834-RO-1301) ensures that there is always a minimum flow through the pump. These pumps can be stopped automatically, by the low low alarm (68-LALL-1307) or manually, from the central control room using hand switch (68-HS-1307B/1308B) or local panel (68-HS-1307A/1308A). In the event of non ESD trip of operating pump, standby pumps will start automatically. 4.11.3 Demineralised Water System Control description 4.11.3.1 Demineralised Water Flow Control 68-FIC1828 Demineralised water outlet to the DM water storage tank (6834-T-08) is controlled by 68-FIC-1828. Fresh water flow to the Train-1 & 2 is measured by 68-FT-1825 and 68-FT-1827 respectively and final treated DM water to the DM water storage tank is measured by 68-FT-1828. Flow controller 68-FIC-1828 takes any of the above transmitter’s value as per the train selection, for calculating the output which directly commands the DM water storage tank control valve 68-LCV-1827. DM water storage tank MASTER level controller 68-LIC-1305 cascaded with SLAVE 68-FIC-1828 for allowing a maximum flow rate equal to the inlet flow rate available to DM package in order to guarantee a minimum recirculation flow rate. Alarm Controller Tag Control Description Unit Operating Set Point Low High 68-LIC-1305 DM Water Storage Tank level % XX XX XX 68-FIC-1828 DM Water package O/L flow m3/hr XX XX XX • DM Water Package flow low low alarm 68-FALL-1830 set at XXXX trips the Recirculation Pump 6834-P-37A/B • DM Water Storage Tank level control valve 68-LCV-1827 closes on instrument air failure. 4.11.3.2 Recirculation Water Flow Control 68-FIC-1826/68-FIC1829 Recycling fresh water flow controller 68-FIC-1826 (Train-A), 68-FIC-1829 (Train-B) determines the amount of recirculation flow passes through the control valve 68-FV1826 (Train-A), 68-FV-1829 (Train-B) to the cationic exchangers bed during phase no 1 (Service) and phase no 6 (Final rinse with recirculation). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 142 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Recycle water pumped from 6834-P-37A is measured by a vortex type flow meter 68-FT-1826 (Train-A) and 68-FT-1829 (Train-B). Set points for the above controllers are provided locally. Alarm Controller Tag Control Description Unit Operating Set Point Low High 68-FIC-1826 Train-A recirculation flow control m3/hr XX XX XX 68-FIC-1829 Train-B recirculation flow control m3/hr XX XX XX • Recirculation Pump 6834-P-37A discharge flow low low alarm 68-FALL-1837 trips the Recirculation Pump 6834-P-37A in MCC. • Recirculation Pump 6834-P-37B discharge flow low low alarm 68-FALL-1838 trips the Recirculation Pump 6834-P-37B in MCC. • Recirculation flow control valve 68-FV-1826 (Train-A) and 68-FV-1829 (Train-B) closes on instrument air failure. 4.11.3.3 Regeneration Water Flow Control Regeneration water from the DM Water Storage Tank (6834-T-08) to static mixers 6834-M-02A and 6834-M-02B is controlled by the flow controller 68-FIC-1835 and 68-FIC-1836 respectively. Regeneration water to static mixer 6834-M-02A and 6834-M-02B is measured by 68-FT1835 and 68-FT-1836. Set points for both the controllers are provided locally. Output of the controllers 68-FIC-1835 and 68-FIC-1836 directly commands the control valve 68-FV-1835 and 68-FV-1836, respectively. Alarm Controller Tag Control Description Unit Operating Set Point Low High 68-FIC-1835 Regeneration Pump discharge to Static Mixer 6834-M-02A m3/hr XX XX XX 68-FIC-1836 Regenerated Pump discharge to Static Mixer 6834-M-02B m3/hr XX XX XX • Regeneration Pump 6834-P-36A/B discharge flow low low alarm 68-FALL-1839 trips the Regeneration Pump 6834-P-36A/B, HCl Dosing Pumps 6834-P-35A/B and Caustic Dosing Pump 6834-P-34A/B. • Regeneration water flow control valves 68-FV-1835 and 68-FV-1836 closes on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 143 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.11.3.4 Pump ON/OFF Controls 1. Acid Dosing Pumps Tag/Alarm 68-PI-1825 68-PI-1826 68-PI-1827 68-LI-1825 68-FI-1839 68-LI-1307 68-AI-1831 68-LI-1830 Description Pump diaphragm failure Pump diaphragm failure Pump diaphragm failure HCL storage tank level low Regeneration Pump discharge flow low low DMW Storage Tank level low Neutralisation Pump discharge Neutralisation Pit low level Pump Tag No. 6834-P-35A 6834-P-35B 6834-P-35C Action Trips the pump and start the stand by pump Trips the pump and start the stand by pump Trips the pump and start the stand by pump 6834-P-35A, B & C Trips the running pumps 6834-P-35A, B & C Trips all the running pumps 6834-P-35A, B & C Trips all the running pumps 6834-P-35A, B & C Starts the duty pump 6834-P-35 B & C Trips the pump 2. Caustic Dosing Pumps Tag/Alarm 68-PI-1828 68-PI-1829 68-PI-1830 68-LI-1827 68-FI-1839 68-LI-1307 68-AI-1831 68-LI-1830 Description pump diaphragm failure pump diaphragm failure pump diaphragm failure NaOH Storage Tank level low low Regeneration Pump discharge DMW storage tank level low Neutralisation Pump discharge Neutralisation Pit low level Pump Tag No. 6834-P-34A 6834-P-34B 6834-P-34C 6834-P-34A, B & C 6834-P-34A, B & C 6834-P-34A, B & C Action Trips the pump and start the stand by pump Trips the pump and start the stand by pump Trips the pump and start the stand by pump Trips the running pumps Trips all the running pumps Trips all the running pumps 6834-P-34A, B & C Starts the duty pump 6834-P-34 B & C Trips the pump EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 144 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3. Regeneration Pumps Tag/Alarm Description Pump Tag No. Action 68-LI-1307 DMW storage tank level low-low 6834-P-36A & B Trips both the pump 68-FI-1839 Regeneration Pump flow low-low 6834-P-36A & B Trips both the pump 68-FI-1835 Static Mixer 6834-M02A inlet DM Water flow low 6834-P-36A & B Starts the stand-by pump 68-FI-1836 Static Mixer 6834-M02B inlet DM Water flow low 6834-P-36A & B Starts the stand-by pump 4. Recirculation Pumps Tag/Alarm Description Pump Tag No. Action 68-FI-1837 Recirculation pump flow low low 6834-P-37A Trips the pump 68-FI-1838 Recirculation pump flow low low 6834-P-37B Trips the pump 5. Neutralization Pumps Tag/Alarm 4.12 4.12.1 Description Pump Tag No. Action 68-LI-1831 Neutralisation tank level high 6834-P-38A/B Starts the duty pump 68-LI-1830 Neutralisation tank level low 6834-P-38A/B Trips both the pump BOILER FEED WATER DEAERATOR SYSTEM Equipment specification Steam Condensate Flash Drum Equipment Tag No. 6834-V-05 Size, (ID X T/T), mm 2600/7800 Design Pressure, barg 3.5/FV Design Temperature, °C, Min./Max. 0/150 Operating Pressure, barg 0.1 Operating Temperature, °C, 102 Material of Construction CS + 1.5mm CA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 145 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL De-aerator Feed Pumps Equipment Tag No. 6834-P-20A/B Type Horizontal Centrifugal 3 Design Capacity, m /hr 221 Design Pressure, barg 8.5 Design Temperature, °C, Min./Max. Suction Pressure, bara, Normal/Rated 0/150 1.82/5.54 Discharge Pressure, bara 4.51 Operating Temperature, °C 102 Driver Type Motor Driver Rating, kW 30 Material of Construction, Casing/Impeller CS/SS316 Steam Condensate Cooler Equipment Tag No. 6834-E-02 Type Forced Draft Design Duty, kW 5422 Design Pressure, barg Design Temperature, °C, Min./Max. Inlet Pressure, barg Operating Temperature, °C, In/Out No. of Fans 8.5 0/150 1.75 102/59 3 Fan Driver Type Motor Driver Rating, kW 15 Material of Construction, Casing/Impeller CS BFW De-aerator Package Equipment Tag No. 6834-A-08 3 Design Capacity, m /hr 110 Design Pressure, barg 3.5/FV Design Temperature, °C, Min./Max. 0/185 Operating Pressure, barg 0.2 Operating Temperature, °C 105 Material of Construction, Casing/Impeller CS + 3mm CA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 146 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Boiler Feed Water Pumps Equipment Tag No. Type Centrifugal 3 Flow Rate, m /hr 55 Design Pressure, barg 31 Design Temperature, °C, Min./Max. 0/185 Suction Pressure, barg, Max./Rated 5.55/1.92 Discharge Pressure, bara 21.8 Operating Temperature, °C 105 Driver Type Driver Rating, kW Material of Construction, Casing/Impeller 4.12.2 6834-P-22A/B/C Motor 110 CS/SS316 Boiler Feed Water De-aerator Description 4.12.2.1 Steam Condensate Flash Drum (6834-V-05) The LP steam condensates mixtures are collected in the Steam Condensate Flash Drum. The purpose of this vessel is to stabilise the steam condensate entering the drum and to cool down the inventory to 102°C to prevent cavitations in De-aerator Feed Pumps. The Flash Drum receives fluids from two phase steam condensates from condensate distribution header and DMW from DMW Feed Pumps 6834-P-24A/B. The operating pressure in the Flash Drum is 0.1 barg. During normal operation, minimum or no flow across 68-RO-1302 is expected and which is sized for steam condensate cooler failure case. Pressure relief valves (68-RV-1091A/B, one operating and one spare) protect the drum against overpressure. The RVs relieve to the atmosphere and are set at 3.5 barg. 4.12.2.2 Steam Condensate Cooler (6834-E-02) The relatively cool (43°C) DMW feed make-up entering the mixing compartment of the Steam Condensate Flash Drum picks up heat from the incoming hot condensate stream. To maintain its liquid state, the demineralised water/condensate mixture in the drum is continuously circulated through the Seam Condensate Cooler by the De-aerator Feed Pump 6834-P-20A/B. The temperature is controlled at 102°C by using temperature control valve (68-TV-1301) prior to forwarding the water to the Boiler Feed Water De-aerator unit for further treatment. 4.12.2.3 De aerator Feed Pumps (6834-P-20A/B) Centrifugal type, De-aerator Feed Pumps (6834-P-20A/B, one running, one standby) has a dual purpose: first to recycle approximately 49.8 % of the total normal discharge EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 147 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL flow back to the flash drum via the Steam Condensate Cooler. The second is to feed the balance of the pump discharge flow to the Boiler Feed De-aerator package (6834-A-08) for further treatment. These pumps will be stopped automatically, by the low-low alarm (68-LALL-1309) or manually, from the central control room using hand switch (68-HS-1309/1310) or local panel (68-HS-1309). In the event of a non ESD trip of the operating pump, the standby pump will start automatically. 4.12.2.4 Boiler Feed Water De-aerator Package (6834-A-08) The boiler feed water stream enters the BFW De-aerator Package (6834-A-08) at the top of the De-aerator column. It is contacted counter-currently with stripping steam, which heats and scrubs the incoming feed, forcing the water to give up its CO2 and most of its O2 content. Oxygen Scavenger is added to the water in the hold up section of the De-aerator to further reduce the O2 content. The De-aerator pressure is controlled at 0.2 barg by means of a pressure controller (68-PIC-1304) which acts on pressure control valve (68-PV-1304) located in the LP stripping steam line. The De-aerator is protected from over pressure by a set of pressure relief valves (68-PSV-1337A/B), set at 3.5 barg. The De-aerator package is designed for FV. The liquid level in the De-aerator drum is maintained by 68-LIC-1302 through 68-LV-1302 in the BFW feed inlet line. The Boiler Feed Water pumps (6834-P-22 A/B/C) take suction from a common manifold. The discharge pressure of Boiler Feed Water Pump is 20.8 barg. The minimum flow is controlled by 68-FIC-1305 using 68-FV-1305 and discharged liquid back to De-aerator drum. 4.12.2.5 Chemical Injection Package (6834-A-09) The BFW Chemical injection Package is used to inject Boiler Feed water with O2 Scavenger and a Complex Product. The Complex Product is administrated to increase pH value of the boiler feed water from 7 to between 9.0 and 10.5 to protect the internal walls of the steam drums against corrosion and scaling. The amount of complex product solution is proportional to the boiler feed water flow and is injected at the discharge of Boiler Feed Water pumps. The package includes for each chemical, a set of Chemical Storage Tank, Chemical Injections Pumps and Chemical Unloading Pump. Chemical Injection Pumps are of reciprocating, positive displacement, automatic metering type i.e. the amount of chemical injected is proportional to the boiler feed water flow as measured by the dedicated chemical pumps speed variation controllers. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 148 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL There are two sets of Chemical Injection Pumps (each comprising two electric motor driven gear pumps) provided for each chemical as follows; • Two Oxygen Scavenger Injection Pumps 6834-P-39A/B for De-aerator (6834-A08) treatment • Two Complex Product Injection Pumps 6834-P-41A/B for Steam Boiler (6834-A02A/B/C) Feed Water treatment 4.12.2.6 Boiler Feed Water Pumps (6834-P-22A/B/C) Centrifugal type Boiler Feed Water Pumps (two running, one standby) have dual purpose; the first is to supply Boiler Feed Water at 18.5 barg and 105°C to Steam Generation Package and the second is to supply BFW to the TGTU. A small stream is also connected to Sour Water Stripper Reboiler 6922-E-04 for desuperheating purpose. The pumps are designed to supply a normal continuous flow of oxygen free and pH controlled Boiler Feed Water to the Steam Boilers 6834-A-02 A/B/C and Reactor Effluent Cooler (9102-E-11). The minimum flow is controlled by flow controller 68-FIC-1305 by acting on flow control valve 68-FV-1305 which returns part of the pump discharge flow back to the Deaerator. In the event of a non ESD trip of the operating pump, the standby pump will start automatically. 4.12.3 Boiler Feed Water Deaerator Control Description 4.12.3.1 Steam Condensate Flash Drum Level Control Level in the Steam Condensate Flash Drum 6834-V-05 is maintained by 68-LIC-1301 by monitoring the level through the transmitter 68-LT-1301. Level is controlled by regulating the makeup DMW through the control valve 68-LV-1301. Controller Tag 68-LIC-1301 Alarm Control Description Unit Operating Set Point Low High Steam Condensate Flash Drum level % 50 18 79 • High high level alarm 68-LAHH-1308 in Steam Condensate Flash Drum trips the DM Water Feed Pumps 6834-P-24A/B. • Low low level alarm 68-LALL-1309 in Steam Condensate Flash Drum trips the Deaerator Feed Pumps 6834-P-20A/B. • Steam Condensate Flash Drum level control valve 68-LV-1301 closes on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 149 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.12.3.2 Steam Condensate Flash Drum Outlet Temperature Control Steam Condensate Flash Drum 6834-V-05 outlet temperature is monitored by 68-TT1301 and controlled by 68-TIC-1301 located in the suction of Deaerator Feed Pumps 6834/P-20A/B. Temperature control is achieved by regulating the steam condensate from the cooler 6834-E-02 through the control valve 68-TV-1301 located in the Steam Condensate Cooler outlet line entering in to the Steam Condensate Flash Drum. Controller Tag 68-TIC-1301 • Alarm Control Description Unit Operating Set Point Low High Steam Condensate Flash Drum temperature °C 102 97 107 Steam Condensate Flash Drum temperature control valve 68-TV-1301 opens on instrument air failure 4.12.3.3 Deaerator Feed Pumps Minimum Flow Control Deaerator feed pumps 6834-P-20A/B discharge one stream is routed to BFW Deaerator package and other stream is routed to Steam Condensate Cooler for maintaining temperature in the flash drum. Deaerator Feed Pumps 6834-P-20A/B minimum flow control is achieved by regulating the control valve 68-FV-1301 (located in the bypass of 68-TV-1301) which allows the minimum flow to pass even when the 68-TV-1301 is fully closed. Controller Tag Control Description 68-FIC-1301 Deaerator Feed Pumps flow control • Alarm Unit Operating Set Point Low High m3/hr 83 66.6 NA De-aerator feed pumps minimum flow control valve 68-FV-1301 opens on instrument air failure 4.12.3.4 Deaerator Level Control Level in the Deaerator is monitored by the level transmitter 68-LT-1302 and controlled by the level controller 68-LIC-1302. Level control is achieved by regulating the control valve 68-LV-1302 located in the Deaerator Feed Pumps flow to the Deaerator. Controller Tag Control Description 68-LIC-1302 Deaerator level control Alarm Unit Operating Set Point Low High % 50 16 86 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 150 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • High high Level alarm 68-LAHH-1312 in Deaerator closes the Deaerator inlet ON/OFF valve 68-XV-1301. • Low low level alarm 68-LALL-1310 in Deaerator executes the following actions: • • Boiler 6848-A-02A fuel gas inlet ON/OFF valve 68-XV-1302 close • Boiler 6848-A-02B fuel gas inlet ON/OFF valve 68-XV-1303 close • Boiler 6848-A-02C fuel gas inlet ON/OFF valve 68-XV-1304 close • BFW Pumps 6834-P-22A/B/C trip • De-aerator Feed Pumps 6834-P-20A/B trip • Steam Condensate Cooler Fans 6834-EM-2A1/2A2/2B1/2B2/2C1/2C2 trip • Boilers 6848-A-02A/B/C shutdown 68-LV-1302 closes on instrument air failure. 4.12.3.5 Boiler Feed Water Pumps Minimum Flow Control Boiler Feed Water Pumps 6834-P-22A/B/C discharge flow to the Steam Generation units is measured by 68-FT-1305 and minimum recirculation flow to Deaerator is controlled by 68-FIC-1305. The controller 68-FIC-1305 throttles the fail open control valve 68-FV-1305. Controller Tag 68-FIC-1305 Control Description BFW Pumps minimum flow Alarm Unit Operating Set Point Low High m3/hr 35 30 NA 4.12.3.6 Deaerator Pressure Control Deaerator 6834-A-08 pressure is monitored by 68-PT-1304 and controlled by the pressure controller 68-PIC-1304. The pressure is maintained through the pressure control valve 68-PV-1304 in the LP stripping steam inlet to the top of the Deaerator tank. 68-PIC-1304 opens the steam control valve 68-PV-1304 on falling pressure in the Deaerator. Controller Tag 68-PIC-1304 Control Description De-aerator top pressure control Alarm Unit Operating Set Point Low High barg 0.2 NA 0.3 Steam control valve 68-PV-1304 closes on instrument air failure. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 151 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.13 4.13.1 STEAM GENERATION PACKAGE Equipment Specifications Equipment Tag No. 6848-A-02A/B/C Water Tube Steam Generator Type Capacity, T/hr (Each Boiler) 45 Design Pressure, barg 22 Design Temperature, °C 220 Steam Outlet Temperature at LP Header, °C 163 Feed Water Temperature, °C, Min./Normal 43/105 Saturated Steam Outlet Pressure at LP Header, barg 5 Steam Pressure at Drum, barg 16.4 Feed Water Pressure, barg 18.5 Feed Water Flow, T/hr 45.409 Desuperheater Water Flow, kg/hr 541 Type of Fuel Natural Gas 3 Fuel Flow, Nm /hr 3296 Fuel Temperature, °C, (Operating/Design) Fuel Pressure, barg, (Operating/Design) Excess Air, % 25-50/100 6-7/9 10 3 Air Flow, Nm /hr 33860 Air Temperature at Air Heater Inlet, °C 25 Flue Gas Temperature at Furnace Outlet, °C 1037 Flue Gas Temperature at Economizer Inlet, °C 278 Flue Gas Temperature at Economizer Outlet, °C 157 Flue Gas Temperature at Stack, °C 157 Pressure Drop in Air Duct, mmWC 110 Air Pressure Drop in Burners, mmWC 160 Flue Gas Pressure Drop in Convection Coil, mmWC 67 Flue Gas Pressure Drop in Economizer, mmWC 42 Air Pressure at Fan Outlet, mmWC 364 Radiant Loss, %LHV 0.55 Unburned Loss, %LHV 0 Heat Loss in Flue Gas Stack, %LHV 4.72 Efficiency Calculated, (With Economizer), %LHV 93.49 Efficiency Calculated Without Drain, %LHV 93 Heat Introduced in Furnace, Kcal/h 27.2E6 2 269306 Heat Density in Furnace, Kcal/h.m EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 152 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Drums Drum Outside Diameter, mm Cylindrical Length, mm Thickness, mm Material Type of Head Upper 1326 9550 28 SA 515 Gr 70 Elliptical Lower 908 9550 22 SA 515 Gr 70 Elliptical Combustion Chamber Size, L X W X H, m Type of Screen Tubes Outer Diameter and Thickness, mm Tube Fixation Type Projected Surface, m2 Screen Header Numbers Header Outer Diameter x Thickness, mm 8.787 X 2.727 X 3.778 Membrane Water Tube Type 76.1 x 4 Expanded/Welded 98.74 4 219.1 x 12.7 Desuperheater Type Location Multi Nozzle Spray Steam Pressure Reducing and Desuperheating Station Convection Coil Surface, m2 Location Type Tubes Outer Diameter x Length, mm Pitch Trans. x Length, mm Material 729 Furnace Side/Parallel to Drums Expanded Tubes 51 x 3400 96 x 95 ASTM A 210 Gr A1 Economizer Surface, m2 Location Type 724 In the Flue Gas Duct Finned Tube Type Tubes Outer Diameter x Length, mm 48 x 2220 Pitch Trans. x Length, mm 114.3 x 90 Material SA210GrA1 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 153 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Casing Boiler Material/Thickness, mm Insulation CS Mineral Wool with Cladding Type Expanded Tubes Refractory, Combustion Chamber, Front Wall Refractory Cement Bricks Refractory, Combustion Chamber, Other Walls Refractory Cement Bricks Material ASTM A 210 Gr A1 Burners Number 1 Type Low NOx Location/Arrangement Front Wall Pilots or Igniters 1 Flame Failure Detector 2 Fan Number 1 Type Centrifugal 3 Air Flow Normal, Nm /hr Static Pressure, mmWC Driver 51000 500 Electric Motor Driver Power, kW 110 Speed, RPM 1550 Coupling Air Regulating Material Flexible Coupling Inlet Damper CS Air Duct Material CS Thickness, mm 4 Flue Gas Discharge Flow Rate, kg/hr 46112.4 Discharge Temperature, °C 155 Molecular Weight 27.59 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 154 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Flue Gas Duct Material Thickness, mm CS (Rated for High Temperature Service) 6 Stack Type Height/Top Dia/Bottom Dia, m Material Thickness, mm, (min.) Self Supporting 30/1/2 CS (Rated for High Temp. Service) 5 Boiler Blow Down Pit Tag No. Dimension Design Pressure, barg 6848-T-02 2200 x 1800 x 1000 0 Design Temperature, °C 220 Material of Construction Concrete 4.13.2 Steam Generation Package Process Description Auxiliary Steam Boiler Package is essentially constituted by: Three water tube – Clajtub type saturated steam boilers. 4.13.2.1 Steam Generation Package 6848-A-02A The main purpose of Steam Generation Package 6848-A-02A is to generate steam and supply steam to the Customer steam network grid at the required pressure and temperature. 4.13.2.1.1 Water/Steam Circuit The Water/Steam circuit of the Steam Generator is realised in the following way: • Boiler Feed Water enters into the external Economiser (6848-E-01A), which is a heat exchanger (water/flue gas) constituted by finned tubes. In this section, the feed water temperature is increased by absorption of the flue gas thermal heat. • When Sour fuel gas is used, the Boiler Feed Water is first sent to a preheating water circuit installed inside the water drum, before entering the Economiser (6848-E-01A). This preheating circuit prevents acid condensation inside the flue gas system (including the Economiser [6848-E-01A] outer surface) by keeping the temperature of the flue gas above the dew point of the acid gas. • From the Economiser (6848-E-01A) outlet, the feed water enters into steam drum 6848-V-02A. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 155 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Boiler functions on the basis of “steam/water natural circulation”, with evaporating rising circuits formed by the hottest tubes of boiler. Remaining tubes act as down comers, which feed the rising circuits. All the evaporating tubes are (except, where indicated in the boiler pressure parts drawings) expanded on both steam drum and water drum. • In the boiler evaporating tubes, a mixture of saturated water & steam is produced. Then the saturated steam is separated from the water droplets in the Steam Drum 6848-V-02A Separators. • The saturated steam from the steam drum is then sent to a temperature and pressure controlling section; • Pressure of the saturated steam is controlled by the Pressure Control Valve 68-PV1524 which gets the input from the Pressure Indicator Controller 68-PIC-1819. A pressure transmitter 68-PT-1819 senses the pressure in the steam header and provides the input to the 68-PIC-1819. • The temperature of the saturated steam is controlled by the Desuperheater (6848X-03A). Boiler Feed Water from the Boiler Feed Water Pumps 6834-P-22A/B/C discharge is injected into the Desuperheater 6848-X-03A. The flow of the Boiler Feed Water is controlled by a Temperature control valve 68-TV-1522. The temperature control valve gets the temperature input from 68-TIC-1522 which in turn gets the input from the Temperature Transmitter 68-TT-1522 which measures the temperature of the saturated steam. • The steam from the Desuperheater 6848-X-03A is then routed to the Main LP steam header. 4.13.2.1.2 Air/Flue Gas Circuit • The air/flue gas ducts of each of the three steam generator is arranged in the following way: • Combustion air is taken from the atmosphere by means of a Forced Draft Fan (6848-K02A), driven by an electric motor (6848-KM-02A). At the suction the combustion air passes through a Grid Filter 6848-S-03A, Sand Filter (6848-S-02A) and vertical air Silencer (6848-X-06A) and then a goose type vertical duct designed to have multiple stage inertial filtration of the entering combustion air. The inlet Sand Filter 6848-S-02A does not need any kind of maintenance or cleaning (self discharging type), goose neck type duct is advisable to be inspected through its lower manhole at least once in 6 months • Downstream of the Silencer 6848-X-06A, the air passes through the modulating inlet control damper (68-FV-1626) (pneumatically actuated); downstream of the Forced Draft Fan 6848-K-02A, the combustion air passes through a duct that delivers air to the wind-box EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 156 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Combustion air measuring device 68-FE-1526 (AIR-FOIL type) is installed downstream of the Forced Draft Fan 6848-K-02A • In the wind box the air is evenly distributed to the burner in order to optimise the combustion • Once the combustion takes place in the burner, the high temperature flue gases pass through the boiler furnace, enclosed by water cooled tubes. The water tubes assure a perfect tightness for the flue gases. At the end of combustion chamber, the flue gases turn to 180° entering through the evaporating convective section. The convective section is located on the right side of the furnace. At boiler outlet, the flue gases go through a connection duct and then pass through the external Economiser 6848-E-01A, where the flue gas temperature decreases by means of a heat transfer to Boiler Feed Water • Downstream of the Economiser 6848-E-01A, the flue gases pass through flue gas duct that connects the Economiser 6848-E-01A to the stack • Then the flue gases are discharged through the stack into the atmosphere • Air/flue gas circuit is provided also with a recirculation flue gas duct, that re circulates flue gas from Economiser outlet to AIR FOIL 68-FE-1526 and subsequently to burner wind-box inlet. The flue gas recirculation fan (FGRF) 6848-K-03A is installed in the Flue Gas Recirculation duct 4.13.2.1.3 Steam Generator Design & Process Main Data The Steam Generator data are summarised in the following table. These data are applicable to the Maximum operating Continuous Rate (MCR): Operating Data @ MCR Sl. # Data Unit Value Operating Data 1. Steam flow at boiler outlet t/h 44.96 2. Steam flow at battery limit (net to Customer) t/h 45 3. Steam temperature at battery limit °C 163 4. Steam pressure at battery limit barg 5 5. Feed water temperature °C 105 Design Data 1. Design pressure (boiler - economiser) barg 22 2. Hydraulic test pressure (boiler economiser) barg 33 3. Design Code ASME I EDITION 2007 ADDENDA 2009 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 157 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.13.2.1.4 Boiler Drums • The Water Drum 6848-V-03A and steam drum 6848-V-02A are symmetrically located on right side of the boiler when viewed from the burner side • The drums are manufactured with high quality steel according to ASME Code with submerged arc automatic welding • The drums are provided with manholes at both ends allowing a full inspection of the boiler and accessibility to all tubes for easy maintenance • From the upper part of water drum all water tubes converge into the lower part of the steam drum, ensuring the natural circulation • The Steam Drum 6848-V-02A is provided with internal Separators/Dryers, that ensure a very high steam purity, flanged nozzles for continuous blow down (CBD) outlet, Boiler Feed Water inlet, saturated steam outlet to common header, safety valves, level indicators and transmitters, pressure gauges and pressure transmitter, chemical injection inlet nozzle, nitrogen inlet and some spare connections (provided with blind flanges) • The water drum is provided with two nozzles to drain the boiler (to be opened only when the water inside the boiler is at ambient temperature) 4.13.2.1.5 Steam Drum Sl. # Data Unit Value Steam Drum 1. Internal diameter mm 1270 2. Shell thickness mm 28 3. Material SA516 Gr.70 Water Drum 1. Internal diameter mm 864 2. Shell thickness mm 28 3. Material SA516 Gr.70 Note: Before closing the steam drum manholes, Operator must verify that demisters are correctly installed inside the steam drum as shown in the following figure. That is with the perforated plate positioned above the wire mesh filters. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 158 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 23 - Steam Drum 4.13.2.1.6 Boiler Furnace • All the furnace walls are constituted by water-cooled membraned tubes. These tubes are seamless type • The tubes constituting the “D” shape are directly connected to the drums by mechanical expansion and seal welding. The front and rear wall tubes are welded to dedicated lower and upper headers • The front tubes are bent to create the burners throats, while the rear tubes are bent to allocate an inspection access door and two peep holes • The furnace dimensions are designed to assure an adequate cooling of the combustion gases • All tubes of the furnace are equally shaped and its membranes are welded each other to assure very high flue gas tightness and an equilibrated circulation of boiling water • Lower and upper headers of front and rear wall tubes are connected to both drums by external suppliers and risers tubes EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 159 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Data Unit Value Furnace Tubes 1. Outer diameter mm 76.1 2. Thickness mm 4 3. Material ASTM A210 Gr.A1 Furnace Headers 1. Outer diameter mm 219.1 2. Thickness mm 12.7 3. Material ASTM A106 Gr.B 4.13.2.1.7 Evaporating Tube Bank The evaporating tube bundle is located in the convective section, which is formed by adequately spaced tubes, heated by the cross flow of flue gas. The outer tubes, forming the external enveloping walls, are welded over the whole length thus providing a continuous tight gas enclosure membraned wall. A few tubes, in the enveloping external wall, have been bent in order to create the free area to locate two inspection doors (one in SH bank and the other in the middle of the convective section) for access and/or maintenance purposes. Sl. # Data Unit Value Convective Bank Tubes 1. Outer diameter mm 51 2. Thickness mm 3.2 3. Material ASTM A210 Gr.A1 Enclosure Tubes 1. Outer diameter mm 76.1 2. Thickness mm 4 3. Material ASTM A210 Gr.A1 4.13.2.1.8 Economiser • At the outlet of the flue gas from the steam generator, an external Economiser 6848-E-01A is located • This thermal heat exchanger consists of seamless tubes adequately finned and spaced so as to increase heat transfer coefficient • The flue gas heats the economizer tubes in cross flow • All the tubes are welded to the inlet and outlet horizontal headers. In order to separate the feed water circuitry, some baffles are installed inside the inlet and outlet headers EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 160 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL • A carbon steel casing, externally insulated, constitutes the enveloping economizer enclosure • The Economiser 6848-E-01A is provided with adequate drain and vent valves. The Economiser 6848-E-01A cannot be by-passed, so it is not necessary to provide a dedicated pressure safety valve. Sl. # Data Unit Value Economiser Tubes 1. Outer diameter mm 48.3 2. Thickness mm 3.2 3. Material ASTM A210 Gr.A1 Economiser Fins 1. Height mm 19 2. Thickness mm 1.5 3. Number of fins per meter 4. Material 200 Fe P04 UNI EN 10130 Economiser Headers 1. Outer diameter mm 114.3 2. Thickness mm 11.13 3. Material ASTM A106 Gr.B 4.13.2.1.9 Refractory • Refractory tiles are used to cover the furnace floor of the steam generator, both to reduce the absorbed thermal heat (increasing the natural circulation) and to allow future accessibility for any maintenance and/or inspection reasons • Refractory tiles are also used to protect the burner throats where combustion takes place • These refractory tiles are manufactured with high Alumina content and are suitable for high temperature operation. 4.13.2.1.10 External Insulation and Cladding The steam generator is insulated with high-density mineral wool panels of suitable thickness entirely applied to all external walls. Sl. # Data Unit Value Boiler Thermal Insulation 1. Material 2. Thickness 3. Density Mineral wool mm 140 (2 layers, 70 mm each) kg/m3 120 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 161 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The external insulation panels are enclosed in a cladding, made of painted aluminium, properly spaced and fixed through screws to allow an easy removal. 4.13.2.1.11 Air and Flue Gas Ducts • The steam generator is provided with combustion air ducts, located at the suction and at the delivery of the Forced Draft Fan 6848-K-02A that convey the combustion air from ambient to boiler wind-box • The steam generator is provided also with flue gas ducts that convey the flue gas from boiler outlet to Economiser 6848-E-01A inlet and from Economiser 6848-E01A outlet to steel stack • The steam generator is provided also with recirculation flue gas ducts, located at the suction and at the delivery of the Flue Gas Recirculation Fan 6848-6848-K-03A that re-circulates the required flow rate of flue gas from Economiser 6848-E-01A outlet to Boiler wind-box inlet through a dedicated entrance in Air-Foil 68-FE-1526 duct Sl. # Data Unit Value Combustion Air Ducts 1. Material S275 JR EN 10025 2. Thickness (all air ducts except intake air duct) mm 4 3. Thickness (intake air duct) mm 7 Flue Gas and Flue Gas Recirculation Ducts 1. Material 2. Thickness S275 JR EN 10025 mm 5 Boiler Base Frame The steam generator body is mounted on a steel base-frame, which supports it with a uniform load distribution. Ladders, Platforms and Stairways The Boiler, the Deaerator, the Stack and the air intake duct are provided with stairs, platforms and ladders in order to allow an easy access to the equipment and/or to the instruments installed on the equipments. Platforms area is completed with open grating, guards and handrails. Burners • One burner 6848-X-05A is installed in the Steam Generator, designed to burn both Sour type and Sweet type (FG2 and FG1) of fuel gas EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 162 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Burner is designed to have a turndown of 10:1 • Burner is provided with a pilot (Class 3 type) that can be fed by FG2 and FG1 • The pilot ignitor is of high energy type • During pilot operation, the combustion air to pilot is provided by the Forced Draft Fan 6848-K-02A, providing the minimum combustion air flow rate • In order to meet the specified low emissions target, at high boiler load, the burners can be operated in flue gas recirculation mode. The combustion air is mixed with a proper flue gas flow rate (about 15% of nominal flow rate), upstream of the boiler wind-box. The recirculation flue gas flow rate is provided by the Flue Gas Recirculation Fan 6848-K-03A The burner is mainly composed of the following equipment: • Air swirler adjustable manually by Operator from external burner front, by means of proper handle. The air register deliver the combustion air at the desired velocity and rotation into the burner throat • Burner front plate assembly complete with one viewing port and two openings for flame detectors (complete with ball swivels) • FG distribution system, complete with multiple gas lances and relevant nozzles • Central gas gun, complete with diffuser • One pilot complete with high energy ignitor, relevant transformer (installed in a dedicated junction box) and cable • Two flame detectors both to sense the burner main flame and the pilot flame • One observation peep hole • Burner refractory throat made of several pre formed bricks • Flexible hoses for FG both for pilot, distribution system to gas lances and central gas gun During boiler operation, in order to optimise the combustion, the FG flow rate is fed both to distribution system to multiple gas lances and to central gas gun. Forced Draft Air Fan (6848-K-02A) The Steam Generator is provided with one Forced Draft Air Fan (6848-K-02A) and its electric motor 6848-KM-02A. The combustion air flow rate is controlled by means of a modulating inlet control damper (pneumatically actuated) installed upstream of the Forced Draft Air Fan (6848-K-02A) suction. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 163 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The unit basically includes: • Grid Filter 6848-S-03A at inlet duct (installed at inlet section of the air intake duct) • Sand Filter 6848-S-02A at inlet duct (installed at inlet section of the air intake duct) • Combustion air Silencer 6848-X-06A (installed after Sand Filter 6848-S-02A) • Split housing (for rotor removal) provided with one inspection door and one plugged drain • Impeller (wheel and hub) statically and dynamically balanced in the manufacturer workshop to reduce vibration and noise • Shaft and relevant guard • Shaft seal • Flexible coupling and relevant guard • Anti-friction bearings • Electric motor 6848-KM-02A • Inlet vane control damper 6848-FV-1626 complete with pneumatic actuator • Thermal insulation on fan casing • flexible connections at suction and discharge sections • basement common for fan and electric motor Flue Gas Recirculation Fan The Steam Generator is provided with one Flue Gas Recirculation Fan (FGRF) 6848-K03A, coupled with its electric motor 6848-KM-03A. The flue gas recirculation flow rate is controlled by means of a modulating inlet control damper 6848-FV-1524 (pneumatically actuated), installed upstream of the Flue Gas Recirculation Fan 6848-K-03A suction connection. The unit basically includes: • Housing, provided with one inspection door and one drain • Impeller (wheel and hub), statically and dynamically balanced in the manufacturer workshop to reduce vibration and noise • Shaft and relevant guard • Shaft seal • Transmission belts and pulley and relevant guard EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 164 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Anti-friction bearings • Electric motor 6848-KM-03A • Inlet vane control damper 6848-FV-1524, complete with pneumatic actuator • Outlet non return damper • Flexible connections, at suction and discharge sections • Thermal insulation on fan casing • Basement, common for fan and electric motor Chemical Dosing Units Each Steam Generator is provided with one Phosphate chemical dosing unit, whose purpose is to inject Phosphate into boiler Steam Drum 6848-V-02A. Each unit basically includes: • One Phosphate Storage Tank 6848-T-03A • Two Phosphate Dosing Pumps 6848-P-01A/02A, one working and the other stand-by and respective electric motors 6848-PM-01A/02A, piping, valves and instruments • One tank mixer 6848-M-01A and its electric motor 6848-MM-01A • One steel catch basin Sampling System • Each Steam Generator is provided with one sampling system for two samples: one for boiler feed water at Economiser 6848-E-01A inlet, one for saturated steam • The sampling system consists of sample conditioning bench, relevant piping, measurement and safety instruments, all mounted on a common panel • All samplings are manual type sample • All the samples of the sampling system are cooled by Demineralised Water. The required cooling water flow rate is taken from raw water line supply. Stack • Each Steam Generator is provided with a double dedicated steel stack 6848-X-01A, that discharges the flue gas from boiler to the atmosphere • The stack is cylindrical self-supporting type, manufactured into three sections for shipping reasons • Each section is connected to the other by means of coupling flanges EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 165 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The stack has the following characteristics: Sl. # Data Unit Value Steel Stack 6848-X-01A 1. Material S275 JR 2. Internal Diameter Mm 1240 3. Outer Diameter Mm 1700 till 11.45m 1500 up to top 4. Thickness (Inner Duct) Mm 8 5. Thickness (Outer Duct) Mm 8 6. Total Height M 30 • The Stack 6848-X-01A is provided with proper insulation between the two jackets • Platform is provided at 6 m and 12 m elevation and ladders are provided for approaching the platforms • A manhole is provided at the bottom of the Stack for internal inspection • The Stack 6848-X-01A is also provided with nozzles necessary for instruments installation including CEMS installation • A drain is provided at the bottom of the Stack • An internal plate conveys the possible condensate (from flue gas condensation or external atmospheric events) to the drain system • This drain must be periodically opened to empty the stack of any condensate accumulation Steam Silencer Each Steam Generator is provided with one Steam Silencer 6848-X-02A for start-up vent in order to respect the required noise limit. 4.13.3 Control Description The Steam Generator is provided with a Boiler Control Panel containing the Burner Management System (BMS) and the Boiler Control System (BCS). The Steam Generator is provided with its own Local Panel (LP) connected to the Boiler Control Panel. Boiler control system (BCS) is responsible for the continuous control of the boilers and all the below mentioned controls are implemented in BCS (PLC). 4.13.3.1 Boiler Level Control The boiler level control is performed with single or three elements philosophy. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 166 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL If the steam flow (68-FT-1524) is greater than the settable threshold then the boiler level control is allowed to work in three element controls. If the steam flow (68-FT-1524) is less than the settable threshold then the boiler level control is allowed to work in single element behaviour. But there is also a provision to select three element controls at any time. Single Element Control When the single element philosophy is active the Inverse acting level controller 68-LIC1522 regulates the feed water flow control valve 68-LV-1522 to maintain the boiler level. The boiler drum level is measured by 68-LIT-1522 and controlled by 68-LIC-1522; set point is set locally and 0-100% output of 68-LIC-1522 directly controls the level control valve 68-LV-1522. Three Element Control Three elements used in this controls are Feed water flow (68-FT-1522), boiler level (68-LT-1522) and steam flow (68-FT-1524). When the three element philosophy is active the Inverse acting feed water flow controller 68-FIC-1522 regulates the feed water flow control valve 68-LV-1522 to maintain the boiler drum level. The main compensated steam flow 68-FT-1524 is applied to the output of the level controller 68-LIC-1522 to adjust the set point to the feed water control 68-FIC-1522 proportional to varying steam demands. 0-100% output of 68-FIC-1522 directly commands the level control valve 68-LV-1522. Controller 68-LIC-1522 68-FIC-1522 Alarm Unit Operating Set point Low High Boiler drum level % 50 34 62 Boiler Feed Water flow 3 XX NA NA Control Loop m /hr High high level alarm (68-LAHH-1523A/B/C) set at 72% and low low level alarm (68-LALL-1523A/B/C) set at 23% in boiler drum. 1. Closes the following valves: 2. • Main fuel gas shutoff valves 68-XV-1528 & 68-XV-1529 • Pilot gas shut off valves 68-XV-1531 & 68-XV-1532 Opens the following valves: • Main fuel gas vent valve 68-XV-1530 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 167 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • 3. Pilot gas venting valve 68-XV-1533 Trips the following: • FD fan 6848-K-01A • Re-circulation Glue Gas Fan 6848-K-02A • Boiler feed water level control valve 68-LV-1522 closes on instrument air failure. Schematic diagram of level control is shown below. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 168 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 24 – Schematic of Boiler 1 Element/3 Element Drum Level EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 169 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.13.3.2 SH Steam Temperature Control Super heated steam temperature control is achieved by direct acting temperature controller 68-TIC-1552 which regulates the water flow to the Desuperheater. SH steam temperature is controlled by 68-TIC-1522. Set point of 68-TIC-1522 set by operator on the HMI and is corrected by output of LP steam header direct acting temperature controller 68-TIC-1820 and commands the Desuperheater control valve 68-TV-1522. Controller Tag. Control Loop Alarm Unit Operating Set Point Low High 68-TIC-1522 SH steam temperature °C 163 158 168 68-TIC-1820 Steam header °C XX 158 168 • Desuperheater control valve 68-TV-1522 closes on instrument air failure 4.13.3.3 Boiler Steam Pressure Control The Steam Drum 6848-V-02A pressure is maintained by inverse acting pressure controller 68-PIC-1523A which determines the burner load to maintain the drum pressure. Boiler drum steam pressure is measured by 68-PT-1523 which is fed as a Process variable to 68-PIC-1523A and the set point is set by operator on the HMI. 0-100% CV of the controller 68-PIC-1523A is the power that burner should produce to maintain the steam pressure to the set point value. The required power is expressed as MWreq=CV*Pmax [MW] Where Pmax–maximum power that can be produced with the burner lighted at the maximum load (set by the supplier). Controller 68-PIC-1523A • Alarm Control Loop Unit Operating Set Point Low High Boiler drum pressure bar 16.4 19 20 High high steam pressure alarm (68-PAHH-1522A/B/C) in Boiler Drum 1. Closes the following valves: • Main fuel gas shutoff valves 68-XV-1528 & 68-XV-1529 • Pilot gas shut off valves 68-XV-1531 & 68-XV-1532 2. Opens the following valves: • Main fuel gas vent valve 68-XV-1530 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 170 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Pilot gas venting valve 68-XV-1533 3. Trips the following: • FD Fan 6848-K-01A • Re-circulation Flue Gas Fan 6848-K-02A 4.13.3.4 Fuel Gas Flow Control Fuel gas flow to produce the required power MWreq is determined by the Inverse acting flow controller 68-FIC-1525. Fuel gas flow is measured by the transmitter 68-FT-1525A and controlled by 68-FIC1525. Set point is the required FG flow, which is calculated from the formula QNG REQ =min {3.6 *106 * MWREQ/HVFG, QFG STOICH} [kg/h], Where HVFG [kJ/kg] - Fuel gas heat value QFG STOICH - stoichiometric fuel gas flow required for actual combustion air flow. MWREQ- Required power for the burner is calculated from steam pressure controller 68-PIC-1523A. Output (0-100%) of 68-FIC-1525 directly commands the fuel gas control valve 68-FV-1525. 68-FIC-1525 is turned on to manual mode after 5 seconds the 68-FIC-1526 (combustion air flow controller) has been turned on manual mode. Controller 68-FIC-1525 Control Loop Fuel gas flow to boiler Alarm Unit Operating Set Point High 1 High 2 kg/hr XX 2800 2900 High high-1 flow alarm (68-FAHH-1525B/C/D) set at 2900 Kg/hr and high high-2 flow alarm (68-FAHH-1525 B/C/D) set at 3020 Kg/hr in boiler 1. 2. Closes the following valves: • Main fuel gas shutoff valves 68-XV-1528 & 68-XV-1529. • Pilot gas shut off valves 68-XV-1531 & 68-XV-1532. Opens the following valves: • Main fuel gas vent valve 68-XV-1530. • Pilot gas venting valve 68-XV-1533. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 171 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3. Trips the following: • FD fan 6848-K-01A. • Re-circulation Flue Gas Fan 6848-K-02A Fuel gas flow control valve 68-FV-1525 to boiler closes on instrument air failure. 4.13.3.5 Combustion Air Flow Control Combustion air flow required to burn the amount of fuel gas is determined by the Inverse acting air flow controller 68-FIC-1526. Combustion air flow is measured from the transmitter 68-FT-1526A and controlled by 68-FIC-1526; the set point is determined by the formula QAIR REQ = (QFG * STOICH) [kg/h], Where QFG =max {QFG req, QFG meas} [kg/h], STOICH [KG/KG]-Air/FG stoichiometric ratio. QFG req is calculated from the fuel gas controller set point 68-FIC-1525 and QFG mean value is taken from the fuel gas flow transmitter 68-FIT-1525. O2 correction calculated from 68-AIC-1522 is also applied for adjusting airflow set point. Output (0-100%) of 68-FIC-1526B directly commands the air control damper 68-FV-1526. 68-FIC-1526 is turned on to manual mode after 5 seconds the 68-FIC-1525A (fuel gas flow controller) has been turned on manual mode. Controller 68-FIC-1526 Control Loop Combustion air flow to boiler Alarm Unit Operating Set Point Low High kg/hr XX NA NA • Low low combustion air flow alarm (68-FALL-1525 B/C/D) set at 38,500 Kg/hr in boiler 1. Closes the following valves: 2. • Main fuel gas shutoff valves 68-XV-1528 & 68-XV-1529. • Pilot gas shut off valves 68-XV-1531 & 68-XV-1532. Opens the following valves: • Main fuel gas vent valve 68-XV-1530. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 172 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • 3. • Pilot gas venting valve 68-XV-1533. Trips the following: • FD Fan 6848-K-01A • Re-circulation Flue Gas Fan 6848-K-02A combustion air flow control valve 68-FV-1525 to boiler locks at the position on instrument air failure 4.13.3.6 Oxygen Control Oxygen concentration in the stack flue gas is maintained by the Inverse acting oxygen controller 68-AIC-1522 which determines the increase/decrease factor of the excess air which is used in the set point determination of 68- FIC-1526B (combustion air flow). Set point is determined by the expected oxygen for the required load MW REQ and is obtained by linear interpolation on the oxygen curve (provided by BONO). Output (0-100%) of 68-AIC-1522 is scaled to the range 1.3 – 0.7 which is the correction factor applied to the air excess in the calculation of the combustion air flow set point (68-FIC-1526B). Above control can be disabled/enabled from the HMI as required. Controller 68-AIC-1522 Alarm Control Loop Unit Operating Set Point Low High Oxygen analyzer controller % XX 2.2 6.7 4.13.3.7 Flue Gas Recirculation Control The position of the flue gas recirculation damper 68-FV-1524 is measured by 68-FZT1524 and controlled by controller 68-ZIC-1524. Set point is the desired position of the flue gas damper for the required load and is obtained by linear interpolation on the flue gas recirculation curve (provided by BONO). Output (0-100%) of 68-ZIC-1524 directly commands the flue gas recirculation damper 68-FV-1524. Flue gas control can be enabled/disabled by operator by means of software selector on local HMI and on remote DCS. Controller 68-ZIC-1524 Control Loop Flue gas damper position controller Alarm Unit Operating Set Point Low High % XX NA NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 173 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Flue gas flow control valve 68-FV-1524 to boiler locks at the position on instrument air failure. 4.13.3.8 Boiler Steam Pressure (VENT) Control Saturated steam flow through the vent valve to maintain the boiler steam pressure is controlled by a direct acting pressure controller 68-PIC-1523B. Steam drum pressure transmitter 68-PIT-1523; Set point is provided by the operator on the HMI and output (0-100%) directly commands the vent control valve 68-PV-1523. If the boiler steam pressure increases then the controller 68-PIC-1523B increases the output to open the vent control valve 68-PV-1523, which maintains the steam pressure nearer to the set value. 68-PIC-1523B Alarm Control Loop Unit Operating Set Point Low High Steam pressure vent bar 17.4 NA NA Controller • High high steam pressure alarm (68-PAHH-1522A/B/C) set at 20barg in boiler drum 1. Closes the following valves: 2. 3. • Main fuel gas shutoff valves 68-XV-1528 & 68-XV-1529. • Pilot gas shut off valves 68-XV-1531 & 68-XV-1532. Opens the following valves: • Main fuel gas vent valve 68-XV-1530. • Pilot gas venting valve 68-XV-1533. Trips the following: • FD Fan 6848-K-01A • Re-circulation Flue Gases Fan 6848-K-02A • Steam pressure vent control valve 68-PV-1523 closes on instrument air failure. 4.13.3.9 Header Steam Pressure Control The three boilers supplied by BONO are connected via an Ethernet link and exchange the data themselves to co-operate on MASTER/SLAVE logic to maintain the desired pressure in the steam header. As per design only two boilers can feed the steam to the header continuously. Each boiler generates a signal named “consent to modulation for header PIC” and this signal is set when the following conditions are verified: • Burner is lighted EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 174 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • 68-MOV-1522 located in super heated steam to LP steam header is not closed • The boiler pressure has reached the opening threshold for the 68-MOV-1522 • At least one of the other two boiler control systems has not set the signal “consent to modulation for header PIC”. Header steam pressure direct acting controller 68-PIC-1819 purpose is to maintain the steam header pressure and management is performed by the control system of the “MASTER” boiler (first boiler which starts to feed the header through its 68-MOV-1522). Steam header pressure is measured by 68-PIT-1819 and controlled by 68-PIC-1819, set point is provided by the operator on the HMI of the “MASTER” boiler. Output of the controller (0-100%) pass through the split range function 68-PY-1819, where the two outputs of the split range function commands directly the header pressure control valve 68-PV-1524 of the “MASTER”, “SLAVE” boilers (second boiler which starts to feed the header through its 68-MOV-1522 is known as slave boiler) and the commands of 68-PV-1523 to the third boiler is forced to 0%. 4.13.3.10 Fan Controls Forced Draft Fan (6848-K-02A) The FD Fan motor can be started only if all the following conditions are verified: • Presence of motor available signal (68-ZL-1548) • Absence of motor fault signal (68-ZA-1548) • Presence of close limit switch of combustion air damper 68-FV-1526 (68-ZSC-1526) Fan motor can be started and stopped manually from the HMI. Flue Gas Recirculation Fan (6848-K-03A) The flue gas recirculation fan motor can be started only if all the following conditions are verified: • Presence of motor available signal (68-ZL-1549) • Absence of motor fault signal (68-ZA-1549) • Presence of close limit switch of the flue air damper 68-FV-1524 (68-ZSC-1524) Fan motor can be started and stopped manually from the HMI. Start/stop tag details for Forced draft and recirculation fans are as follows: Sl. # Tag No. Description 1. 68-HSOA-1548 Forced draft fan start 2. 68-HSCA-1548 Forced draft fan stop 3. 68-HSOA-1549 Recirculation air fan start 4. 68-HSCA-1549 Recirculation air fan stop EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 175 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.13.3.11 Valve Management ON/OFF MOV1522 Each boiler contains a MOV which feeds the steam to the header Valve can be operated in Local/Remote by changing the selecting switch (68-HSR1522C) located in the local panel. If the valve fault status signal (68-XA-1522) is active then the valve cannot be controlled from BCS. Automatic Mode Automatic mode of the MOV can be selected from the HMI and if the valve is not in fault mode then the valve will open automatically on the following conditions: • Burner is ON • Steam Drum pressure 68-PT-1523 is higher than threshold (68-PSH-1523C) • other two boilers have not yet set the consent to modulation for header PIC signal If any of the above condition is not satisfied then the valve will close automatically. Manual Mode When the manual mode of MOV is selected from HMI then the valve can only be operated from the HMI open/close commands (68-HSO-1522A/68-HSC-1522B). On/Off Valve Controls Boiler Blow Down Valve (68-XV-1525) The valve is opened automatically if at least any one of the following conditions is satisfied: • The burner is ON • Hot standby mode is active (enabled manually) and the boiler level is higher than a opening threshold value The valve is closed automatically if at least any one of the following conditions is satisfied: • The burner is off • Hot standby mode is not active • Hot standby mode is active and the boiler level is lower than a closure threshold value EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 176 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Hot Stand-by Boiler Pressure Valve (68-XV-1523) The valve is opened automatically when all the following conditions are satisfied: • Hot standby mode is active • The Steam Drum pressure 68-PT-1523 is lower than an opening threshold (PSL-1523) The valve is closed automatically if at least any one of the following conditions is satisfied: • Hot standby mode is not active • Hot standby mode is active and the upper drum boiler pressure 68-PT-1523 is higher than a closure threshold (PSH-1523) Pre heating Feed Water Valves (68-XV-1523, 68- XV-1524) For commanding the above valves to permit feed water to boiler lower drum, following conditions needs to be satisfied: • Burner is OFF • Operator has selected FG2 (H2S) from the HMI 4.13.3.12 LP Steam Header Pressure Control Saturated steam from all the three boiler packages are connected in to the LP steam header and the pressure in the header is measured by 68-PT-1306 and controlled by the pressure controller 68-PIC-1306. Pressure in the header is maintained by the control valve 68-PV-1306 located in the steam vent line to atmosphere. Increase of pressure above the operating range will route the steam to the vent through the control valve 68-PV-1306. • Alarm Controller Tag Control Description Unit Operating Set Point Low High 68-PIC-1306 LP steam header pressure barg 5 4.5 5.5 LP steam header pressure low low pressure 2oo3 (68-PALL-1303A/B/C) alarm set at 4 barg initiates the following: • Fuel gas on/off valve 68-XV-1302 to the boiler 6848-A-02A close • Fuel gas on/off valve 68-XV-1303 to the boiler 6848-A-02B close • Fuel gas on/off valve 68-XV-1304 to the boiler 6848-A-02C close • Deaerator Feed Pumps 6834-P-20A/B trip • BFW Pumps 6834-22A/B/C trip • Steam Condensate Cooler Fans trip EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 177 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • • 4.14 4.14.1 Boiler Packages 6848-A-02A/B/C shutdown Steam to vent valve 68-PV-1306 opens on instrument air failure CHEMICAL INJECTION SYSTEMS Antifoam Injection Package 9103-A-11 4.14.1.1 Equipment Specification Antifoam Storage Tank Equipment Tag No. 9103-T-12 Size, ID/Height, mm 1550/1600 Chemical Antifoam Design Pressure bar(a) 1.01 Design Temperature °C 85/0 Operating Pressure bar(g) ATM. Operating Temperature, °C Material of Construction 52 AISI 316L Antifoam Injection Pumps Equipment Tag No. Pump Type Chemical 9103-P-16A/B Double Diaphragm Antifoam Capacity, L/hr 55 Design Pressure, bar(g) 12 Discharge Pressure, bar(g) 8.5 Design Temperature, °C 120/0 Driver Type Motor Rated Power, kW Material of Construction 0.37 SS316TI/PTFE Antifoam Unloading Pump Equipment Tag No. Pump Type Chemical Capacity, L/hr 9103-P-19 Air Operated Pump Antifoam 2000 Design Pressure, bar(g) 8.7 Discharge Pressure, bar(g) 1.2 Design Temperature, °C 85/0 Material of Construction AISI 316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 178 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Antifoam Tank Agitator Equipment Tag No. 9103-M-12 Speed, RPM 155 Driver Rating, kW 0.37 Material of Construction AISI 316L6 4.14.1.2 Antifoam Package 9103-A-11 Description Antifoam Package consists of an Antifoam Storage Tank 9103-T-12 and two numbers of Antifoam Injection Pumps 9103-P-16A/B. The Antifoam Storage Tank 9103-T-12 is having an agitator 9103-M-12. Antifoam from drums are transferred to the tank through an unloading pump 9103-P-19. The Antifoam Injection Pumps 9103-P-16A/B are having discharge pulsation dampner and calibration pots at the suction line. 4.14.1.3 Antifoam Injection Package Control Description The Antifoam Storage Tank (9103-T-12) level is monitored by 91-LI-1521 and antifoam from the storage tanks is injected to the following areas via the injection pumps (9103-P-16A/B): • Acid Gas Amine Absorber 9103-C-11 • Lean/Rich Amine Exchangers 9103-E-11A/B • Amine Regenerator 9103-C-12 • Tail Gas Amine Absorber 9102-C-12 Following parameters are to be monitored: Tag No. Description Unit 91-FI-1533 9103-P-16A/B common discharge flow 91-PI-1559 Alarm High Low LPH 40 70 9103-P-16A discharge pressure barg NA 9.5 91-PI-1560 9103-P-16B discharge pressure barg NA 9.5 91-LI-1521 antifoam storage tank level (9103-T12) % 6 NA Following are the details of the switches & alarm related to motor controls: Tag No. Description 91-HSOA-1582 Remote “ START” for the Pump 9103-P-16A 91-HSOA-1583 Remote “ START” for the Pump 9103-P-16B 91-HSCA-1582 Remote “ STOP” for the Pump 9103-P-16A 91-HSCA-1583 Remote “ STOP” for the Pump 9103-P-16B EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 179 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Tag No. 4.14.2 Description 91-ZL-1582 9103-P-16A Pump Available signal 91-ZL-1583 9103-P-16B Pump Available signal 91-XS-1582 9103-P-16A Pump ESD trip signal 91-XS-1583 9103-P-16B Pump ESD trip signal 91-ZI-1582 9103-P-16A Pump running indication 91-ZI-1583 9103-P-16B Pump running indication • Low low level alarm (91-LALL-1520) set at 3% in Antifoam Storage Tank 9103-T-12 trips the Antifoam Injection Pumps (9103-P-16A/B) • High high diaphragm pressure alarm (91-PAHH-1565) set at 8.5 barg in Antifoam Injection Pump 9103-P-16A initiates the pump changeover • High high diaphragm pressure alarm (91-PAHH-1566) set at 8.5 barg in Antifoam Injection Pump 9103-P-16B initiates the pump changeover • ESD-0, ESD-1, ESD-2 shutdown signals activates the tripping of both the Antifoam Injection Pumps (9103-P-16A/B). Caustic Injection Package 9103-A-13 4.14.2.1 Equipment Specification Caustic Storage Tank Equipment Tag No. Size, ID/Height, mm Chemical Design Pressure bar(a) Design Temperature °C Operating Pressure bar(g) Operating Temperature, °C Material of Construction 9103-T-14 1550/1600 Caustic 1.01 85/0 ATM. 52/0 AISI 316L Caustic Injection Pumps Equipment Tag No. Pump Type Chemical Capacity, L/hr Design Pressure, bar(g) Discharge Pressure, bar(g) Design Temperature, °C Driver Type Rated Power, kW Material of Construction 9103-P-103A/B Double Diaphragm Caustic 55 11.5 5 120/0 Motor 0.37 SS316TI/PTFE EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 180 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Caustic Unloading Pump Equipment Tag No. 9103-P-104 Pump Type Air Operated Pump Chemical Caustic Capacity, L/hr 2000 Design Pressure, bar(g) 8.7 Discharge Pressure, bar(g) 1.2 Design Temperature, °C 85/0 Material of Construction AISI 316L Caustic Tank Agitator Equipment Tag No. 9103-M-14 Chemical Caustic Speed, RPM 155 Material of Construction AISI 316L 4.14.2.2 Caustic Package 9103-A-13 Description Caustic is injected to the suction of Desuperheater Circulation Pumps 9102-P-11. Caustic Package consists of a Caustic Storage Tank 9103-T-14 and two numbers of Caustic Injection Pumps 9103-P-103A/B. The Caustic Storage Tank 9103-T-14 is having an agitator 9103-M-14. Caustic from drums are transferred to the tank through an unloading pump 9103-P-104. The Caustic Pumps 9103-P-103A/B are having discharge pulsation dampner and calibration pots at the suction line. 4.14.2.3 Caustic Injection Package Control Description Following parameters are to be monitored: Tag No. Description Unit 91-FI-1535 9103-P-103A/B common discharge flow 91-PI-1563 Alarm Low High LPH 40 70 9103-P-103A discharge pressure barg NA 7.5 91-PI-1564 9103-P-103B discharge pressure barg NA 7.5 91-LI-1525 caustic storage tank level (9103-T14) % 6 NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date:03/09/2012 Page: 181 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Following are the details of the switches & alarm related to motor controls: Tag No. 4.14.3 Description 91-HSOA-1586 Remote “ START” for the Pump 9103-P-103A 91-HSOA-1587 Remote “ START” for the Pump 9103-P-103B 91-HSCA-1586 Remote “ STOP” for the Pump 9103-P-103A 91-HSCA-1587 Remote “ STOP” for the Pump 9103-P-103B 91-ZL-1586 9103-P-103A Pump Available signal 91-ZL-1587 9103-P-103B Pump Available signal 91-XS-1586 9103-P-103A Pump ESD trip signal 91-XS-1587 9103-P-103B Pump ESD trip signal 91-ZI-1586 9103-P-103A Pump running indication 91-ZI-1587 9103-P-103B Pump running indication • Low low level alarm (91-LALL-1524) Set at 3% in caustic storage tank 9103-T-14 trips the Caustic Injection Pumps (9103-P-103A/B) • High high diaphragm pressure alarm (91-PAHH-1569) set at 5 barg in Caustic Injection Pump 9103-P-103A initiates the pump changeover • High high diaphragm pressure alarm (91-PAHH-1570) set at 5 barg in Caustic Injection Pump 9103-P-103B initiates the pump changeover • ESD-0, ESD-1, ESD-2 shutdown signals activates the tripping of both the Caustic Injection Pumps (9103-P-103A/B) Corrosion Inhibitor Injection Package 9103-A-12 4.14.3.1 Equipment Specification Corrosion Inhibitor Storage Tank Equipment Tag No. 9103-T-13 Size, ID/Height, mm 3 Storage Capacity m Chemical 1550/1600 3 Corrosion Inhibitor Design Pressure bar(a) 1.2 Design Temperature °C 85/0 Operating Pressure bar(g) ATM. Operating Temperature, °C 52/0 Material of Construction SS 316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 182 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Corrosion Inhibitor Injection Pumps Equipment Tag No. 9103-P-101A/B Pump Type Double Diaphragm Chemical Corrosion Inhibitor Capacity, L/hr 55 Design Pressure, bar(g) 12 Discharge Pressure, bar(g) 8.5 Design Temperature, °C 85/0 Driver Type Motor Rated Power, kW Material of Construction 0.37 SS 316TI/PTFE Corrosion Inhibitor Unloading Pump Equipment Tag No. 9103-P-102 Pump Type Air Operated Pump Chemical Corrosion Inhibitor Capacity, L/hr 2000 Design Pressure, bar(g) 8.7 Discharge Pressure, bar(g) 1.2 Design Temperature, °C 85/0 Material of Construction AISI 316L Corrosion Inhibitor Tank Agitator Equipment Tag No. 9103-M-13 Speed, RPM 155 Rated Power, kW 0.37 Material of Construction AISI 316L 4.14.3.2 Corrosion Inhibitor Package 9103-A-12 Description Corrosion Inhibitor Package consists of a Corrosion Inhibitor Storage Tank 9103-T-13 and two numbers of Corrosion Inhibitor Injection Pumps 9103-P-101A/B. The Corrosion Inhibitor Storage Tank 9103-T-13 is having an agitator 9103-M-13. Corrosion Inhibitor from drums is transferred to the tank through an unloading pump 9103-P-102. The Corrosion Inhibitor Pumps 9103-P-101A/B are having discharge pulsation dampner and calibration pots at the suction line. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 183 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.14.3.3 Corrosion Inhibitor Injection Package Control Description Following parameters are to be monitored: Tag No. Description Unit Alarm Low High 91-FI-1534 9103-P-101A/B common discharge flow LPH 40 70 91-PI-1561 9103-P-101A discharge pressure barg NA 9.5 91-PI-1562 9103-P-101B discharge pressure barg NA 9.5 91-LT-1523 corrosion inhibitor storage tank % 6 NA Following are the details of the switches & alarm related to motor controls: Tag No. Description 91-HSOA-1584 Remote “ START” for the Pump 9103-P-101A 91-HSOA-1585 Remote “ START” for the Pump 9103-P-101B 91-HSCA-1584 Remote “ STOP” for the Pump 9103-P-101A 91-HSCA-1585 Remote “ STOP” for the Pump 9103-P-101B 91-ZL-1584 9103-P-101A Pump Available signal 91-ZL-1585 9103-P-101B Pump Available signal 91-XS-1584 9103-P-101A Pump ESD trip signal 91-XS-1585 9103-P-101B Pump ESD trip signal 91-ZI-1584 9103-P-101A Pump running indication 91-ZI-1585 9103-P-101B Pump running indication • Low low level alarm 91-LALL-1523 set at 3 % in Corrosion Inhibitor Storage Tank 9103-T-13 trips the Corrosion Inhibitor Injection Pumps (9103-P-101A/B) • High high diaphragm pressure alarm 91-PAHH-1567 set at 8.5 barg in Corrosion Inhibitor Injection Pump 9103-P-101A initiates the pump changeover • High high diaphragm pressure alarm 91-PAHH-1568 set at 8.5 barg in Corrosion Inhibitor Injection Pump 9103-P-101B initiates the pump changeover • ESD-0, ESD-1, ESD-2 shutdown signals activates the tripping of both the Corrosion Inhibitor Injection Pumps 9103-P-101A/B. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 184 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.14.4 Complex Product Injection Package 6834-A-09 4.14.4.1 Equipment Specification Complex Product Storage Tank Equipment Tag No. 6834-T-18 Size, ID/Height, mm 3 Storage Capacity m Chemical 950/1500 1 Complex Product Design Pressure bar(a) 1.01 Design Temperature °C 85/0 Operating Pressure bar(g) ATM. Operating Temperature, °C 52/0 Material of Construction AISI 316L Complex Product Injection Pumps Equipment Tag No. 6834-P-41A/B Pump Type Double Diaphragm Chemical Complex Product Capacity, L/hr 1.87 Design Pressure, bar(g) 31 Discharge Pressure, bar(g) 25 Design Temperature, °C 120/0 Driver Type Motor Rated Power, kW Material of Construction 0.18 SS 316TI/PTFE Complex Product Unloading Pump Equipment Tag No. Pump Type Chemical Capacity, L/hr 6834-P-42 Air Operated Pump Complex Product 2000 Design Pressure, bar(g) 8.7 Discharge Pressure, bar(g) 1.2 Design Temperature, °C 85/0 Material of Construction AISI 316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 185 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Complex Product Tank Agitator Equipment Tag No. 6834-M-04 Speed, RPM 243 Rated Power, kW 0.25 Material of Construction AISI 316L 4.14.4.2 Complex Product Injection Package Description Complex Product Injection Package consists of a Complex Product Storage Tank 6834-T-18 and two numbers of Complex Product Injection Pumps 6834-P-41A/B. The Complex Product Storage Tank 6834-T-18 is having an agitator 6834-M-04. Complex Product from drums is transferred to the tank through an unloading pump 6834-P-42. The Complex Product Injection Pumps 6834-P-41A/B are having discharge pulsation dampner and calibration pots at the suction line. 4.14.4.3 Complex Product Injection Process control Description The complex product is injected to the boiler feed water going to the steam generation package and to the boiler feed water going to TGTU. The control is achieved by maintaining the ratio between the total Boiler Feed Water flow and Complex Product flow. The Boiler Feed Water flow rate to Steam Generation Boiler A/B/C is measured by 68FT 1522, 68-FT-1622, 68-FT-1722 respectively and 68-FT-1304 measures the boiler feed water flow rate to TGTU. The Complex Product Pumps (6834-P-41A/B) common discharge flow rate is measured by 68-FT-1311. Total summation of all the above BFW flow is summated in the calculation block 68-FY-1304 and multiplied with the fixed ratio X (X=complex product/total BFW) in the multiplication block 68-FFY-1311. The output from 68-FFY-1311 is fed as a set point to the MASTER complex product flow controller 68-FIC-1311. The complex product pumps 6834-P-41A/B stroke length (0-15 mm) is measured by the stroke indicators 68-ZI-1303/1304 and the strokes are controlled by the position controllers 68-ZIC-1303, 68-ZIC-1304. Complex product flow controller 68-FIC-1311 is cascaded with the position controllers 68-ZIC-1303 and 68-ZIC-1304 and provides set point to the position controllers. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 186 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Controller Tag Control Description Alarm Unit Operating Set Point Low High L/hr 1.78 0.2 1.78 68-FIC-1311 Complex product flow control 68-ZIC-1303 6834-P-41A position control % 100 NA NA 68-ZIC-1304 6834-P-41B position control % 100 NA NA The complex product injection pumps can be operated from the DCS when the Pumps are selected to “Remote” at its local panel. Following are the details of the switches & alarm related to motor controls: Tag No. Description 68-HSOA-1324 Remote “ START” for the Pump 6834-P-41A 68-HSOA-1332 Remote “ START” for the Pump 6834-P-41B 68-HSCA-1324 Remote “ STOP” for the Pump 6834-P-41A 68-HSCA-1332 Remote “ STOP” for the Pump 6834-P-41B 68-ZL-1324 6834-P-41A Pump Available signal 68-ZL-1332 6834-P-41B Pump Available signal 68-XS-1324 6834-P-41A Pump ESD trip signal 68-XS-1332 6834-P-41B Pump ESD trip signal 68-ZI-1324 6834-P-41A Pump running indication 68-ZI-1332 6834-P-41B Pump running indication Following parameters are to be monitored Tag No. Description Unit Alarm Low High 68-PI-1318 6834-P-41A Pump discharge pressure barg NA 26.5 68-PI-1316 6834-P-41B Pump discharge pressure barg NA 26.5 68-LI-1317 Complex product storage tank 6834-T18 level % 6 NA • Low low level alarm 68-LALL-1316 set at 3% in Complex Product Storage Tank trips the Complex Product Injection Pumps 6834-P-41A/B • High high diaphragm pressure alarm 68-PAHH-1326 set at 25.0 barg in Complex Product Injection Pump 6834-P-41A initiates the pump changeover • High high diaphragm pressure alarm 68-PAHH-1327 set at 25.0 barg in Complex Product Injection Pump 6834-P-41B initiates the pump changeover • ESD-0, ESD-1, ESD-2 shutdown signals activates the tripping of both the Complex Product Injection Pumps 6834-P-41A/B. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 187 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.14.5 Oxygen Scavenger Injection Package 6834-A-09 4.14.5.1 Equipment Specification Oxygen Scavenger Storage Tank Equipment Tag No. 6834-T-17 Size, ID/Height, mm 3 Storage Capacity m Chemical 950/1500 1 Oxygen Scavenger Design Pressure bar(a) 1.01 Design Temperature °C 85/0 Operating Pressure bar(g) ATM. Operating Temperature, °C 52/0 Material of Construction AISI 316L Oxygen Scavenging Injection Pumps Equipment Tag No. 6834-P-39A/B Pump Type Double Diaphragm Chemical Oxygen Scavenger Capacity, L/H 0.55 Design Pressure, bar(g) 10.5 Discharge Pressure, bar(g) 6.5 Design Temperature, °C 120/0 Driver Type Motor Rated Power, kW Material of Construction 0.18 SS 316TI Oxygen Scavenger Unloading Pump Equipment Tag No. 6834-P-40 Pump Type Air Operated Pump Chemical Oxygen Scavenger Capacity, L/h 2000 Design Pressure, bar(g) 8.7 Discharge Pressure, bar(g) 1.2 Design Temperature, °C 85/0 Material of Construction AISI 316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 188 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Oxygen Scavenger Tank Agitator Equipment Tag No. 6834-M-03 Speed, RPM 243 Rated Power, kW 0.25 Material of Construction AISI 316L 4.14.5.2 Oxygen Scavenger Injection Package Description Oxygen Scavenger Injection Package consists of a Oxygen Scavenger Storage Tank 6834-T-17 and two numbers of Oxygen Scavenger Injection Pumps 6834-P-39A/B. The Oxygen Scavenger Storage Tank 6834-T-17 is having an agitator 6834-M-03. Oxygen Scavenger from drums is transferred to the tank through an unloading pump 6834-P-40 The Oxygen Scavenger Injection Pumps 6834-P-39A/B is provided with discharge pulsation dampener and calibration pots at the suction line. 4.14.5.3 Oxygen Scavenging Injection Process control Description The oxygen scavenger is injected directly in to the De-aerator package (6834-A-08) and the flow rate of Oxygen Scavenger is measured by 68-FT-1310. Oxygen Scavenger Injection Pumps 6834-P-39A, 6834-P-39B stroke length is measured by 68-ZT-1301 and 68-ZT-1302 respectively. Stroke length of 6834-P-39A, 6834-P-39B is manually adjusted by the controllers 68-HIC-1301 and 68-HIC-1302, respectively. The Oxygen Scavenger Injection Pumps can be operated from the DCS when the Pumps are selected to “Remote” at its local panel Following are the details of the switches & alarm related to motor controls: Tag No. Description 68-HSOA-1323 Remote “ START” for the Pump 6834-P-39A 68-HSOA-1331 Remote “ START” for the Pump 6834-P-39B 68-HSCA-1323 Remote “ STOP” for the Pump 6834-P-39A 68-HSCA-1331 Remote “ STOP” for the Pump 6834-P-39B 68-ZL-1322 6834-P-39A Pump Available signal 68-ZL-1331 6834-P-39B Pump Available signal 68-XS-1322 6834-P-39A Pump ESD trip signal 68-XS-1331 6834-P-39B Pump ESD trip signal 68-ZI-1322 6834-P-39A Pump running indication 68-ZI-1331 6834-P-39B Pump running indication EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 189 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Following parameters are to be monitored: Tag No. 4.14.6 Description Alarm Unit Low High 68-PI-1317 6834-P-39A Pump discharge pressure barg NA 8 68-PI-1315 6834-P-39B Pump discharge pressure barg NA 8 68-LI-1315 Oxygen Scavenger Storage Tank 6834-T-17 level % 6 80 68-FI-1310 Oxygen Scavenger Injection flow rate LPH 0.2 0.7 • Low low level alarm 68-LALL-1314 set at 3 % in oxygen scavenger tank 6834-T-17 trips the Oxygen Scavenger Injection Pumps 6834-P-39A/B • High high diaphragm pressure alarm 68-PAHH-1324 set at 6.5 barg in Oxygen Scavenger Injection Pump 6834-P-39A initiates the pump changeover • High high diaphragm pressure alarm 68-PAHH-1325 set at 6.5 barg in oxygen scavenger Injection Pump 6834-P-39B initiates the pump changeover • ESD-0, ESD-1, ESD-2 shutdown signals activates the tripping of both the Oxygen Scavenger Pumps 6834-P-39A/B. Biocide Injection Package 6932-A-06 4.14.6.1 Equipment Specification Biocide Storage Tank Equipment Tag No. 6932-T-04 Size, ID/Height, mm 3 Storage Capacity m Chemical 1300/2300 3 Biocide Design Pressure bar(a) 1.01 Design Temperature °C 85/0 Operating Pressure bar(g) ATM. Operating Temperature, °C 52/0 Material of Construction AISI 316L EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 190 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Biocide Injection Pumps Equipment Tag No. Pump Type Chemical Capacity, L/H 6932-P-07A/B Double Diaphragm Biocide 12/65/110 Design Pressure, bar(g) 10 Discharge Pressure, bar(g) 5.5 Design Temperature, °C 120/0 Driver Type Motor Rated Power, kW Material of Construction 0.75 SS 316TI/PTFE Biocide Unloading Pump Equipment Tag No. Pump Type Chemical Capacity, L/h 6932-P-08 Air Operated Pump Biocide 2000 Design Pressure, bar(g) 8.7 Discharge Pressure, bar(g) 1.2 Design Temperature, °C 85/0 Material of Construction AISI 316L 4.14.6.2 Biocide Injection Package Description Biocide Injection Package consists of a Biocide Storage Tank 6932-T-04 and two numbers of Biocide Injection Pumps 6932-P-07A/B. Biocide from drums is transferred to the tank through an unloading pump 6932-P-08. The Biocide Injection Pumps 6932-P-07A/B is provided with discharge pulsation dampener and calibration pots at the suction line. 4.14.6.3 Biocide Injection Process control Description The biocide storage tank 6932-T-04 level is measured by 69-LI-1328. Biocide from the storage tank is injected to Sea Cooling Water through remote stroke adjusting pumps (6932-P-07A/6932-P-07B). Stroke lengths of 3 stage 6932-P-07A are measured by 69-ZT-1301, 69-ZT-1326 and 69-ZT-1328. Manual adjustment of stroke is done via the controllers 69-HIC-1301, 69-HIC-1326 and 69-HIC-1328. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 191 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Stroke lengths of 3 stage 6932-P-07B are measured by 69-ZT-1302, 69-ZT-1327 and 69-ZT-1329. Manual adjustment of stroke is done via the controllers 69-HIC-1302, 69-HIC-1327 and 69-HIC-1329. Following parameters are to be monitored: Tag No. Description Unit Alarm Low High st 69-FI-1319 6932-P-07A/B 1 stage common discharge flow LPH 80 130 69-FI-1323 6932-P-07A/B 2nd stage common discharge flow LPH 80 130 69-FI-1324 6932-P-07A/B 3rd stage common discharge flow LPH 80 130 69-PI-1330 6932-P-07A 1st stage discharge pressure barg NA 6.5 69-PI-1340 stage discharge pressure barg NA 6.5 rd 6932-P-07A 3 stage discharge pressure barg NA 6.5 st barg NA 6.5 stage discharge pressure barg NA 6.5 69-PI-1343 6932-P-07B 3 stage discharge pressure barg NA 6.5 69-LI-1328 Biocide Storage Tank (6932-T-04) level % 6 NA 69-PI-1342 69-PI-1331 69-PI-1341 6932-P-07A 2 nd 6932-P-07B 1 stage discharge pressure 6932-P-07B 2 nd rd The Biocide injection pumps can be operated from the DCS when the Pumps are selected to “Remote” at its local panel. Following are the details of the switches & alarm related to motor controls: Tag No. Description 69-HSOA-1352 Remote “ START” for the Pump 6932-P-07A 69-HSOA-1353 Remote “ START” for the Pump 6932-P-07B 69-HSCA-1352 Remote “ STOP” for the Pump 6932-P-07A 69-HSCA-1353 Remote “ STOP” for the Pump 6932-P-07B 69-ZL-1352 6932-P-39A Pump Available signal 69-ZL-1353 6932-P-39B Pump Available signal 69-XS-1352 6932-P-07A Pump ESD trip signal 69-XS-1353 6932-P-07B Pump ESD trip signal 69-ZI-1352 6932-P-07A Pump running indication 69-ZI-1353 6932-P-07B Pump running indication • Low low level alarm 69-LALL-1329 set at 10 % in biocide storage tank 6932-T-04 trips the Biocide Injection Pumps 6932-P-07A/B • High high diaphragm pressure alarm 69-PAHH-1344 set at 5.5 barg in 1st stage Biocide Injection Pump 6932-P-07A initiates the pump changeover EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 192 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.14.7 • High high diaphragm pressure alarm 69-PAHH-1346 set at 5.5 barg in 2nd stage Biocide Injection Pump 6932-P-07A initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1328 set at 5.5 barg in 3rd stage Biocide Injection Pump 6932-P-07A initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1345 set at 5.5 barg in 1st stage Biocide Injection Pump 6932-P-07B initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1347 set at 5.5 barg in 2nd stage Biocide Injection Pump 6932-P-07B initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1329 set at 5.5 barg in 3rd stage Biocide Injection Pump 6932-P-07B initiates the pump changeover • ESD-0, ESD-1, ESD-2 shutdown signals activates the tripping of both the Biocide Injection Pumps 6932-P-07A/B. Scale Inhibitor Injection Package 6932-A-07 4.14.7.1 Equipment Specification Scale Inhibitor Storage Tank Equipment Tag No. 6932-T-05 Size, ID/Height, mm 3 Storage Capacity m Chemical 2480/4900 24 Scale Inhibitor Design Pressure bar(a) 1.2 Design Temperature °C 85/0 Operating Pressure bar(g) ATM Operating Temperature, °C 52/0 Material of Construction AISI 316L Scale Inhibitor Injection Pumps Equipment Tag No. Pump Type Chemical Capacity, L/H 6932-P-09A/B Double Diaphragm Scale Inhibitor 26/41/4 Design Pressure, bar(g) 10 Discharge Pressure, bar(g) 5.5 Design Temperature, °C 120/0 Driver Type Motor Rated Power, kW Material of Construction 0.37 SS 316TI/PTFE EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 193 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Scale Inhibitor Unloading Pump Equipment Tag No. 6932-P-10 Pump Type Air Operated Pump Chemical Scale Inhibitor Capacity, L/h 5000 Design Pressure, bar(g) 8.7 Discharge Pressure, bar(g) 1.2 Design Temperature, °C 85/0 Material of Construction SS 316TI 4.14.7.2 Scale Inhibitor Injection Package Description Scale Inhibitor Injection Package consists of a Scale Inhibitor Storage Tank 6932-T-05 and two numbers of Scale Inhibitor Injection Pumps 6932-P-09A/B. Scale Inhibitor from drums is transferred to the tank through an unloading pump 6932-P-10. The Scale Inhibitor Injection Pumps 6932-P-09A/B are having discharge pulsation dampner and calibration pots at the suction line. 4.14.7.3 Scale Inhibitor Injection Process control Description The Scale Inhibitor Storage Tank 6932-T-05 level is measured by 69-LI-1330. Scale Inhibitor from the storage tank is injected to sea cooling water through Injection Pumps 6932-P-09A/6932-P-09B. Following parameters are to be monitored: Tag No. 69-FI-1322 69-FI-1321 69-FI-1320 69-PI-1332 69-PI-1333 69-PI-1334 69-PI-1335 69-PI-1336 69-PI-1337 69-LI-1330 Description 6932-P-09A/B 1st stage common discharge flow 6932-P-09A/B 2nd stage common discharge flow 6932-P-09A/B 3rd stage common discharge flow 6932-P-09A 1st stage discharge pressure 6932-P-09A 2nd stage discharge pressure 6932-P-09A 3rd stage discharge pressure 6932-P-09B 1st stage discharge pressure 6932-P-09B 2nd stage discharge pressure 6932-P-09B 3rd stage discharge pressure Scale Inhibitor Storage Tank (6932-T05) level Unit Alarm Low High LPH 2 8 LPH 35 45 LPH 20 30 barg barg barg barg barg barg NA NA NA NA NA NA 6.5 6.5 6.5 6.5 6.5 6.5 % 6 80 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 194 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The scale inhibitor injection pumps can be operated from the DCS when the Pumps are selected to “Remote” at its local panel. Following are the details of the switches & alarm related to motor controls: Tag No. Description 69-HSOA-1354 Remote “ START” for the Pump 6932-P-09A 69-HSOA-1355 Remote “ START” for the Pump 6932-P-09B 69-HSCA-1354 Remote “ STOP” for the Pump 6932-P-09A 69-HSCA-1355 Remote “ STOP” for the Pump 6932-P-09B 69-ZL-1354 6932-P-09A Pump Available signal 69-ZL-1355 6932-P-09B Pump Available signal 69-XS-1354 6932-P-09A Pump ESD trip signal 69-XS-1355 6932-P-09B Pump ESD trip signal 69-ZI-1354 6932-P-09A Pump running indication 69-ZI-1355 6932-P-09B Pump running indication • Low low level alarm 69-LALL-1331 set at 3% in Scale Inhibitor Storage Tank 6932-T05 trips the Scale Inhibitor Injection Pumps (6932-P-09A/B) • High high diaphragm pressure alarm 69-PAHH-1338 set at 5.5 barg in 1st stage Scale Inhibitor Injection Pump 6932-P-09A initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1348 set at 5.5 barg in 2nd stage Scale Inhibitor Injection Pump 6932-P-09A initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1350 set at 5.5 barg in 3rd stage Scale Inhibitor Injection Pump 6932-P-09A initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1339 set at 5.5 barg in 1st stage Scale Inhibitor Injection Pump 6932-P-09B initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1349 set at 5.5 barg in 2nd stage Scale Inhibitor Injection Pump 6932-P-09B initiates the pump changeover • High high diaphragm pressure alarm 69-PAHH-1351 in 3rd stage Scale Inhibitor Injection Pump 6932-P-09B initiates the pump changeover • ESD-0, ESD-1, ESD-2 shutdown signals activates the tripping of both the Scale Inhibitor Injection Pumps 6934-P-09A/B. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 195 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.14.8 Catalyst Injection Package 9101-A-01 4.14.8.1 Equipment Specification Catalyst Storage Tank Equipment Tag No. 9101-T-01 Size, ID/Height, mm 3 Storage Capacity m Chemical 950/1500 1 Catalyst Design Pressure bar(a) 1.01 Design Temperature °C 85/0 Operating Pressure bar(g) ATM Operating Temperature, °C 52/0 Material of Construction AISI 316L Catalyst Injection Pumps Equipment Tag No. Pump Type Chemical Capacity, L/H 9101-P-11A/B Double Diaphragm Catalyst 0.55 Design Pressure, bar(g) 8 Discharge Pressure, bar(g) 5 Design Temperature, °C 85/0 Driver Type Motor Rated Power, kW Material of Construction 0.37 SS 316TI/PTFE Catalyst Unloading Pumps Equipment Tag No. Pump Type Chemical Capacity, L/h 9101-P-12 Air Operated Pump Catalyst 2000 Design Pressure, bar(g) 8.7 Discharge Pressure, bar(g) 1.2 Design Temperature, °C 85/0 Material of Construction SS 316TI EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 196 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4.14.8.2 Catalyst Injection Package Description Catalyst Injection Package consists of a Catalyst Storage Tank 9101-T-01 and two numbers of Catalyst Injection Pumps 9101-P-11A/B. Catalyst from drums is transferred to the tank through an unloading pump 9101-P-12. The Catalyst Injection Pumps 9101-P-11A/B are having calibration pots at the suction line. 4.14.8.3 Catalyst Injection Process control Description The Catalyst Storage Tank level 9101-T-01 is monitored by 91-LI-1127 and Catalyst Injection Pumps 9101-P-11A/B common discharge flow is measured by 91-FI-1128. Following parameters are to be monitored: Tag No. Description Unit Alarm Low High 91-FI-1128 9101-P-11A/B common discharge flow LPH 0.2 0.7 91-PI-1127 9101-P-11A discharge pressure barg NA 6 91-PI-1129 9101-P-11B discharge pressure barg NA 6 91-LI-1127 catalyst storage tank 9101-T01 level % 6 NA Following are the details of the switches & Alarm related to motor controls: Tag No. Description 91-HSOA-1129 Remote “ START” for the Pump 9101-P-11A 91-HSOA-1130 Remote “ START” for the Pump 9101-P-11B 91-HSCA-1129 Remote “ STOP” for the Pump 9101-P-11A 91-HSCA-1130 Remote “ STOP” for the Pump 9101-P-11B 91-ZL-1129 9101-P-11A Pump Available signal 91-ZL-1130 9101-P-11B Pump Available signal 91-XS-1129 9101-P-11A Pump ESD trip signal 91-XS-1130 9101-P-11B Pump ESD trip signal 91-ZI-1129 9101-P-11A Pump running indication 91-ZI-1130 9101-P-11B Pump running indication • Low low level alarm 91-LALL-1128 set at 3% in Catalyst Storage Tank 9101-T-01 trips the Catalyst Injection Pumps 9101-P-11A/B • High high diaphragm pressure alarm 91-PAHH-1128 set at 5 barg in Catalyst Injection Pump 9101-P-11A initiates the pump changeover EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 197 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • High high diaphragm pressure alarm 91-PAHH-1130 set at 5 barg in Catalyst Injection Pump 9101-P-11B initiates the pump changeover • ESD-0, ESD-1, ESD-2 shutdown signals activates the tripping of both the Catalyst Injection Pumps 9101-P-11A/B. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date:03/09/2012 Page: 198 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION V PRE-REQUISITE FOR START-UP EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 199 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.1 GENERAL For Start-up of the SRU Upgrade Facilities the pre-requisites are given below: • All vent and drain valves position are as per P&ID • All spectacle spacers and spectacle blinds are as per P&ID • Acid gas from AGRU 1 & 2 to the Acid Gas Enrichment Unit isolation valve 91-BV1881 is in closed condition • Electrical power is available • Fire & gas system of process unit is tested and in normal operation • Ensure that DCS, F&G and ESD systems are available • Acid gas flare system is in operation • LP Flare is in operation • All process line isolating valves are in closed condition • Ensure all ‘Lock Open’ and ‘Lock Closed’ valves are in their normal operating positions as per P&ID • Ensure that all safety devices have been set to the appropriate set-point as per P&ID • Ensure all mechanical equipment have been installed properly • All instrument root valves are open • All instrument vent/drain valves are closed • Ensure that no shutdown conditions are present (ESD) • Confirm availability of all tools, consumables, and spare parts that are required for start-up • Confirm that the required valid “Permit to Work” has been issued prior to the commencement of start-up activities • Ensure that fire protection system is ready for operation • Ensure that the AGRU 1 & 2 are running and ready to provide acid gas to the AGEU Prior to the starting up of the plant there are several operations that must be conducted to prepare the plant for the actual start-up. This section covers the work required in preparing the unit for initial start-up. The jobs can be categorized as follows: • Plant inspection • Final inspection of vessels and equipments EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 200 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Line and Equipment leak test It is important that these above procedures to be carried out thoroughly and at earliest possible to achieve a smooth, trouble free and steady normal operation. 5.2 INTERFACE ACTIVITIES The following tie-ins between the NGL 1, 2, 3 & 4 and the SRU Upgrade Facilities are to be completed before the start-up of the new facilities. Process • Acid Gas from NGL-3 AGRU 1 & 2 • Acid Gas from NGL 1 & 2 Blowers • Acid Gas from NGL-4 K-8201A/B • Acid Gas from AGEU Regenerator Reflux Drum 9103-V-12 to SRU • Sour Water from Acid Gas KO Drum Return Pump 9103-P-14A/B to SRU • Acid Water from SRU to Amine Sump 9103-V-10 Utilities • Sea Cooling Water from new Sea Cooling Water system to the existing Sea Cooling Water system • Sea Cooling Water Return from AGEU/TGTU to existing Sea Water Observation Sump 6932-X-01 • 20” LP Flare header interconnection from new units to the existing units • NGL-4 Sea Cooling Water system new Sea Water Filters S-8840A/B • Line from existing Drinking Water Storage Tank 6834-T-01A/B to the new Drinking Water Pumps 6834-P-23A/B • Interconnection between existing Drinking Water Pumps 6834-P-01A/B and new Drinking Water Pumps 6834-P-23A/B • Interconnection between new DM Water network to the existing DM Water network • Interconnection between the new plant air header to the old plant air header • Interconnection between the existing 6”-GI-82-0357-C01A nitrogen header to the new nitrogen header • Interconnection between the existing Lean Gas from Booster Compressor suction to the LP Fuel Gas KO Drum 6236-V-05 • Interconnection between the lean gas from 6103-K-01A/B and the LP Fuel Gas KO Drum 6236-V-05 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 201 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Interconnection between the existing fuel gas line upstream of 65-XV-001 and the LP Fuel Gas KO Drum 6236-V-05 • Interconnection from existing fuel gas header 6”-6536-FG-101-C12P to Incinerator 9101-F-14 and Reducing Gas Generator 9102-F-11 • Interconnection of the following new flare lines to the existing LP Flare Header 10”-6922-FL-013-C14P: • From LP Fuel Gas KO Drum 6236-V-05 drain line • LP Fuel Gas KO Drum 6236-V-05 PSVs 62-PSV-176/176S outlet lines • Fuel gas from steam generation package 6848-A-02A/B/C • From LP Fuel Gas KO Drum 6236-V-05 vent 62-PV-1303 • From LP Fuel Gas KO Drum 6236-V-05 inlet pressure control valves 62-PV1301A/62-PV-1301B/62-PV-1302 • Interconnection from existing fuel gas line 2”-6536-FG-011-C12P to LP Acid Gas flare header as purge gas • Interconnection from the existing Service Water Pump P-3103 discharge to the Electro Chlorination Package 6932-A-05 • Interconnection between the existing Instrument Air supply to the new Sea Cooling Water Filters 6932-S-02A/B • Interconnection between the existing Plant Air supply to the Sea Cooling Water Filters 6932-S-02A/B • Interconnection between the existing nitrogen supply system to the new Electro Chlorination system • Interconnection between the existing Spent Caustic system and the new Spent Caustic form Desuperheater Circulation Pumps 9102-P-11A/B • Oily Waste Water from SRU Upgrade new Utilities/Process area to the existing Oily Waste Water Sump 6922-X-01 • From new Stripped Water Cooler 6922-E-02/Cooling water return from AGEU/TGTU to Sea Water Observation Sump 6932-X-01 analyzer 69-AT-1301 outlet to the existing Observation & Buffer Sump 6922-X-04 • Interconnection between the existing instrument air header and the new instrument air header • Interconnection between the new Biocide Injection Package 6932-A-06 and the existing Sea Cooling Water Pumps P-1618 AR/BR/CR suction • Interconnection between the new Scale Inhibitor Injection Package 6932-A-07 and the existing Sea Cooling Water Pumps P-1618 AR/BR/CR discharge. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 202 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.3 START-UP OF UTILITIES 5.3.1 Start-up Sequence Utilities are started in the following sequence: 5.4 5.4.1 1. Instrument Air/Plant Air System 2. Nitrogen System 3. Drinking Water System 4. Oily Water Drain System 5. Effluent and Waste Water Treatment System 6. Flare System 7. Fuel Gas System 8. Sea Cooling Water System 9. Chemical Injection System 10. DM Water System 11. Boiler Feed Water Deaerator System 12. Steam Generation System INSTRUMENT AIR/PLANT AIR SYSTEM Pre Start-up Checks Ensure the following pre start-up checks are completed before the start-up: 1. Ensure the Readiness of Instrument Air Compressor, Instrument Air Dryer and all its auxiliary equipments. 2. Ensure all the instruments are lined up. 3. Ensure that the Air Compressor Discharge Drum 6837-V-10 & Instrument Air Receiver 6837-V-11 are clean. Ensure the following PSVs are calibrated, reinstated and lined-up as shown in P&ID: PSV Tag No. Description 68-PSV-1401 PSV after intercooler 68-PSV-1402 PSV after intercooler 68-PSV-1106/1106S Air compressor Discharge drum PSV 68-PSV-1107/1107S Instrument air receiver PSV 68-PSV-1408 Adsorber 6837-V-14A 68-PSV-1409 Adsorber 6837-V-14A EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 203 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL PSV Tag No. 5.4.2 Description 68-PSV-1458 Adsorber 6837-V-15A 68-PSV-1459 Adsorber 6837-V-15B Instrument Air compressor Start-up There are two Instrument Air Compressors (2 x 100% capacity). The compressors operate on Duty/Standby configuration. Each compressor is monitored and controlled by the package controller (UCP) which contains Siemens S7-400H series PLC and provides information to the DCS through redundant modbus TCP/IP communication link. Air Compressors LCP details are tabulated below: Sl. # Tag No. 6837-K-02A Service 6837-K-02B 1. 68-HS-1403 68-HS-1453 Local/Remote Selector Switch 2. 68-HS-1402 68-HS-1452 Load/Unload Selector switch 3. 68-HSOA-1414 68-HSOA-1464 Start Push Button 4. 68-HSCA-1415 68-HSOA-1465 Stop Push Button 5. 68-HS-1404 68-HS-1454 Lamp Test Push Button 6. 68-HS-1401 68-HS-1451 Emergency Stop Push Button 7. 68-HS-1405 68-HS-1455 Reset Push Button 8. 68-XL-1408 68-XL-1458 Voltage ON lamp (white) 9. 68-XL-1409 68-XL-1459 Compressor loaded lamp 10. 68-XL-1410 68-XL-1460 Automatic operation lamp 11. 68-XL-1411 68-XL-1461 General warning lamp 12. 68-XL-1412 68-XL-1462 General shutdown lamp Details of DCS tags for Air Compressors are tabulated below: Sl. # Tag No. 6837-K-02A 6837-K-02B Service 1. 68-HSOA-1428 68-HSOA-1478 Remote Start Button 2. 68-HSCA-1428 68-HSOC-1478 Remote Stop Button 3. 68-UA-1401 68-UA-1451 Compressor common alarm Note: Press lamp test push button in local control panel and ensure all the lamps are in working normal. The procedure for start-up of one unit (6837-K-02A) of IA Compressor is covered in this section. The same procedure is applicable for other unit (6837-K-02B). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 204 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Instrument air compressor can be started in two modes. I. Local Mode In local mode, the start/stop of the compressor is done from the local control station (LCS). For operating the Compressor in local mode, the selectors switch 68-HS-1403 in Local Control Station to be selected to local position. The loading/unloading is done by the operator using the loading/unloading switch 68-HS-1402 in the LCS. During Local mode loading and unloading of the compressor is based on the compressor outlet pressure transmitter signal 68-PT-1406. Local mode is used for service or maintenance purposes. II. Remote Mode Remote-Auto and Remote-Manual modes are possible under remote mode of operation. In Remote mode, start and stop of the individual compressors are initiated from UCP/DCS operating stations. In Remote-Auto mode, the UCP sequence control has total control over selection, start & stop and pressure control of both the compressors. All local controls are disabled in this mode except emergency stop from field. In Remote mode, the loading/unloading of compressors is based on the air receiver pressure transmitter signal 68-PT-1311. 5.4.3 Start-up permissive conditions: • Availability of instruments and in healthy condition • Motor available signal (68-XU-1428) from MCC • Ensure the below mentioned interlocks in UCP of I/A Compressor are normal: Tag No. Description 68-PAHH-1406 Compressor outlet pressure high-high 68-PDALL-1401 Compressor air inlet pressure low-low 68-PALL-1402 Compressor oil pressure low-low 68-PDAHH-1403 Compressor oil filter DP high-high 68-TAHH-1401 LP stage outlet temperature high-high 68-TAHH-1402 Compressor oil temperature high-high 68-TAHH-1403 LP stage inlet temperature high-high 68-TAHH-1405 Compressor outlet temperature high-high 68-TAHH-1406 Main motor (U1) winding temperature high-high 68-TAHH-1407 Main motor (V1) winding temperature high-high 68-TAHH-1408 Main motor (W1) winding temperature high-high 68-TAHH-1412 Main motor(U2) winding temperature high-high 68-TAHH-1413 Main motor (V2) winding temperature high-high 68-TAHH-1414 Main motor (W2) winding temperature high-high EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 205 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Tag No. Description 68-TAHH-1410 Main motor bearing (DE) temperature high-high 68-TAHH-1411 Main motor bearing (NDE) temperature high-high 68-HS-1401 Emergency stop button at LCP 68-XS-1424 ESD signal to UCP Following interlocks are bypassed automatically during start-up of compressor: • 68-PT-1402 (Lube oil pressure) low low alarm • Compressor trip (68-XZA-1428) and stop (68-XI-1428) feedback Both the above interlocks are bypassed for 20 seconds. The local start-up procedure for 6837-K-02A is given below: 1. Select both the compressors to “Local” from the Local Control panel through selector switch 2. Open 6837-K-02A discharge isolation valve 3. Close the Plant air header pressure control valve 68-PV-1310 and the upstream block valve 4. Close the Air Dryer Package pre-filter upstream isolation valves 5. Confirm ‘Motor available’ signal (68-XU-1428) exists 6. Before starting the Compressor main motor, Set loading & unloading Pressure set point at XX barg in UCP HMI 7. Start Compressor 6837-K-02A through Local Start Push Button and ensure that compressor is started and running 8. Ensure that the Cooling Air Fans (6837-EFM-03AA/AB) and External After Cooler Fan Motor (6837-EFM-04A) is running and its running indication in DCS/HMI 9. Ensure that oil pump is running and the oil pressure is 2.3 barg 10. Ensure compressor runs in unloaded condition for 20 seconds 11. Load the Air Compressor by Pressing Push button 68-HS-1402 in the local panel 12. Ensure that the compressor is loaded by checking the pressure 68-PT-1406 located in the HP Stage compressor outlet 13. Confirm ‘Loaded’ indication (68-XL-1409) in local control station 14. Confirm the Compressor loads up to XX barg, based on the value taken from 68PT-1406 located on the compressor outlet EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 206 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 15. Check the performance of the Compressor by monitoring the following parameters: • Discharge Pressure (68-PI-1406) • Discharge Temperature (68-TI-1405) • Motor Amperage • Oil Temperature (68-TI-1402) • Oil Pressure (68-PI-1402) • Motor Winding Temperatures • Compressor vibration • Motor vibration • Compressor and motor bearing temperatures Note: Instrument air compressors can also be started from DCS by selecting the “Remote” in LCP and Auto/manual button to “Auto” in UCP-HMI. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 207 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 25 - IA Compressor Start-up D Instrument Air Compressor Start Sequence Y 20 sec load delay, oil pressure trip (68-PT-1402) needs to be bypassed up to this time Manual Unload N Take corrective action N Interlocks & start-up permissive healthy Ready to load/unload Note-A Set pressure <Actual Pressure (68-PT-1311) Y Check load, unload selector switch 68-HS-1402 Local/remote selection Loading SOV 68-XY-1401 energizes Load Local/remote Selector switch in LCP 68-HS-1403 N Unloading SOV 68-XY-1403 energizes Y Loading SOV 68-XY-1401 energizes and unloading SOV 68-XY-1403 deenergizes After 20 minutes Compressor stops Local Loading hour counter starts Remote Auto/ Manual selection in HMI Auto DCS A B Set pressure <Actual Pressure (68-PT-1406) PLC HMI (Manual) c Loading SOV 68-XY-1401 energizes N Unloading SOV 68-XY-1403 energizes Y After 20 minutes Compressor stops Loading hour>Set value Y Service change over-Running compressor stop, reset the loading hour counter and start the standby C B Note A Motor available signal (68-XU-1428) from MCC No emergency stop (68-HS-1401) active No ESD signal (68-XS-1424) active Compressor O/L pressure high-high (68-PT-1406) Running hour counter starts Disable control from UCP and DCS Start signal activated Compressor air I/L pressure low-low (68-PDT-1401) Compressor oil pressure low-low (68-PT-1402) Compressor oil filters DP high-high (68-PDT-1403) LP stage O/L temperature high-high (68-TT-1401) Start from LCP-68HSOA-1414 Main motor, cooling fan motor and after cooler fan motor starts Running hour >24H Y Main motor, cooling fan motor and after cooler fan motor starts 20 sec load delay, Oil pressure trip (68-PT-1402) needs to be bypassed up to this time Auto change over-Running compressor stop & reset the loading hour counter and start the standby Compressor oil temperature high-high (68-TT-1402) LP stage I/L temperature high-high (68-TT-1403) Compressor O/L temperature high-high (68-TT1405) Overload relays of main motor, inter external after cooler motors Main motor winding temperatures high-high EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 208 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.4.4 Instrument Air Dryer start-up The dryer package consists of two trains of dryers (6837-A-03 & 6837-A-04) which are to be operated (2 X 50%) together and this repetitive operation is controlled from UCP panel. ON/OFF valve details in the dryer package are tabulated below: Sl. # Tag No. 6837-A-03 Service 6837-A-04 1. 68-XV-1416 68-XV-1466 Purge on/off valve 2. 68-XV-1417 68-XV-1467 Purge on/off valve 3. 68-XV-1418 68-XV-1468 Air inlet on/off valve 4. 68-XV-1419 68-XV-1469 Air inlet on/off valve Details of tags for Air dryers are tabulated below: Sl. # 5.4.5 5.4.6 Tag No. Service 6837-A-03 6837-A-04 1. 68-HSOA-1408 68-HSOA-1458 Remote start Button 2. 68-HSCA-1409 68-HSOC-1459 Remote stop Button 3. 68-UA-1402 68-UA-1452 Dryer common alarm 4. 68-UA-1403 68-UA-1453 Dryer changeover failure alarm Instrument Air Dryer Start-up Checks 1. Ensure the UCP for air dryers is powered up and ensure that all controls are in place. 2. Close air supply towards the dew point analyzer AI-1401 & AI-1451 and by-pass its alarm on both units 6837-A-03 & 6837-A-04. 3. Start the air compressor and wait for pressure to develop in the compressor discharge drum. 4. Slowly open the pre-filters inlet manual isolation valve. 5. Check the connections of the air dryer for air leaks and repair if necessary. Dryer Start There are two Nos. Instrument Air Dryer Package (6837-A-03/04) consisting of heaterless desiccant dryers of 2 X 50% capacity. Each Dryer Package consists of two vessels (one drying, one regenerating), a set of duplex pre-filter and after-filter. Unit start/stop of the package can be done either from UCP or from DCS. No local mode of operation available for dryer package. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 209 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL At the initial start for the availability of the dryer, the position of valves is as follows: • 68-XV-1418/68-XV-1468-open (tower - A in drying) • 68-XV-1419/68-XV-1469-closed • 68-XV-1416/68-XV-1466-Closed • 68-XV-1417/68-XV-1467-open (tower - B in regeneration mode) Also after opening the manual valves following are required to be checked to start the dryer • Tower pressures 68-PT-1408/68-PT-1409 • Tower pressures 68-PT-1458/68-PT-1459 • Dryer available status has to be selected by the operator from HMI • All the alarm conditions for healthy status to be checked before start-up Start the dryer by activating the following commands: • 68-HSOA-1408 for Dryer-6837-A-03 • 68-HSOA-1458 for Dryer-6837-A-04 When drying is started, as a first step (step-0), ensure Adsorber-A (6837-V-14A) is initialised into drying and Adsorber-B (6837-V-14B) is initialised into depressurizing for 5 seconds. Ensure the following valves’ condition: • 68-XV-1418 & 68-XV-1417 are in OPEN condition • 68-XV-1419 & 68-XV-1416 are in CLOSE condition In step-1, ensure that Adsorber-A (6837-V-14A) is in the drying mode and Adsorber-B (6837-V-14B) is being pressurised for 55 seconds. Ensure the following valves’ condition: • 68-XV-1418 & 68-XV-1419 are in OPEN Condition • 68-XV-1417 & 68-XV-1416 are in CLOSE condition Tower B will pressurize up to the running pressure (7.8 bar), after pressure is reached both the towers will be operational for a brief period (5 seconds) together. In step-2, ensure that Adsorber-A (6837-V-14A) is in the drying mode and Adsorber-B (6837-V-14B) is in purge saving mode (this mode manually selected, when dew point is more than -30°C) until the dryer outlet dew point value is greater than the set point for the dew point or for a maximum duration of 24 hours. Ensure the following valves condition: • 68-XV-1418 & 68-XV-1419 are in OPEN Condition • 68-XV-1417 & 68-XV-1416 are in CLOSE condition EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 210 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL In step-3, ensure that Adsorber-A (6837-V-14A) is in the regenerating mode and Adsorber-B (6837-V-14B) is in drying mode for 195 seconds. Ensure the following valves’ condition: • 68-XV-1419 & 68-XV-1416 are in OPEN condition • 68-XV-1418 & 68-XV-1417 are in CLOSE Condition In step-4, ensure that Adsorber-A (6837-V-14A) is in the pressurizing mode and Adsorber-B (6837-V-14B) is in drying mode for 55 seconds. Ensure the following Valves’ condition: • 68-XV-1419 & 68-XV-1418 are in OPEN condition • 68-XV-1417 & 68-XV-1416 are in CLOSE Condition In step-5, ensure that Adsorber-A (6837-V-14A) is in the purge saving mode (this mode Manually Selected, when dew point is more than -30°C) and Adsorber-B (6837-V-14B) is in drying mode until the dryer outlet dew point value is greater than the set point for the dew point or for a maximum duration of 24 hours. Ensure the following Valves’ condition: • 68-XV-1419 is in OPEN condition • 68-XV-1418,68-XV-1417 & 68-XV-1416 are in CLOSE Condition In step-6, ensure that Adsorber-A (6837-V-14A) is in the drying mode and Adsorber-B (6837-V-14B) is in regenerating mode for 195 seconds. Ensure the following valves’ condition: • 68-XV-1418 & 68-XV-1417 are in OPEN condition • 68-XV-1419 & 68-XV-1416 are in CLOSE condition Repeat the above test for TRAIN B (6837-V-15A & 6837-V-15B) dryers. Steps 2 and 5 will be valid only when the purge saving is requested from UCP. Following table shows the valve positions of Tower A, B with respect to the above mentioned phase sequence. Valve Status Sl. # Operational Phase Period 1. A: Drying B:Depressurising 5 sec XV-1418 XV-1417 XV-1416 XV-1419 2. A: Drying B: pressurising 55 sec XV-1418 XV-1419 XV-1416 XV-1417 3. A: Drying B:Purge saving DEW>set Max-24 hrs XV-1418 XV-1419 XV-1416 XV-1417 Open Close EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 211 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Operational Phase Valve Status Period Open Close 4. A: Regenerating B: Drying 195 sec XV-1419 XV-1416 XV-1417 XV-1418 5. A: Pressurising B: Drying 55 sec XV-1419 XV-1418 XV-1416 XV-1417 6. A: Purge saving B: Drying DEW>set Max-24 hrs XV-1419 XV-1418 XV-1416 XV-1417 7. A:Drying B:Regenerating 195 sec XV-1418 XV-1417 XV-1416 XV-1419 Note: In the above table only train-A dryer is considered. 5.5 NITROGEN SYSTEM 5.5.1 Lining up of Nitrogen from existing system to the New Distribution Header Ensure that the following end user isolation valves are closed: • Nitrogen line to the Reaction Furnace 9101-F-01 • Nitrogen line to the Antifoam Storage Tank 9103-T-12 • Nitrogen line to the Reducing Gas Generator 9102-F-11 • Nitrogen line to the Incinerator Package 9101-F-14 • Utility stations in AGEU area • Nitrogen line to the Amine Sump 9103-V-10 • Nitrogen line to the Amine Regenerator 9103-C-12 • Nitrogen line to the Waste Water Degasser 6922-V-07 • Nitrogen line to the Amine Surge Tank 9103-T-11 • Nitrogen line to the Utility Station in Effluent & Waste Water Treatment area • Nitrogen line to Utility Station in TGTU area • Nitrogen line to the Steam Generation Package 6848-A-02A/B/C • Nitrogen line to the Utility station in Heating Medium system area • Nitrogen line to the Utility station in Fuel Gas area Lining up of Nitrogen • Ensure that the vent and drain valves are closed in the header. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 212 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.6 5.6.1 • Open the 3” isolation valve 68-GV-1953 from the existing 6”-GI-88-0357-C01A Nitrogen header to the new distribution header slowly and pressurise the header with Nitrogen. • Verify from the pressure gauge 68-PT-1309 that the pressure in the Nitrogen header is increasing slowly. • After pressurising the main header, slowly open the isolation valves for the sub headers 3”-9138-IG-312-C12M, 3”-6838-IG-126-C12M & 3”-6838-IG-123-C12M to process/utility area at battery limit and pressurise the lines. • Check that the headers are pressurised by checking the pressure gauges 68-PG1329/1331/1351. • Open the 2” isolation valves from the header for the utility stations of heating medium system and the fuel gas system. • Open the end user isolation valves and purge the lines to remove oxygen content. • Check for any leak in the system. DRINKING WATER SYSTEM Lining up of Drinking Water to existing network 1. Ensure that the Drinking Water Storage Tank 6834-T-01A/B level is more than 50%. 3. Ensure that the isolation valve at the tie-in point (T-002) of the new and old drinking water network is closed. 4. Ensure that the vent and drain valves near the tie-in point is closed. 5. Ensure that the new drinking water line to existing network is cleaned by flushing and the leak test has been completed. 6. Open the Drinking Water isolation valves from the Tanks 6834-T-01A/B and slowly fill up the new drinking water lines. 7. Prime the Drinking Water Pumps 6834-P-23A/B. 8. Start the Drinking Water Pump 6834-P-23A on minimum circulation. 9. Ensure that the line connecting the existing network is filled by opening the vent and bleeding air near the tie-in point. 10. Check for any leaks in the line. 5.6.2 Lining up of Drinking Water to DMW Package 1. Ensure that the isolation valve at the inlet of the DMW Unit is closed. 2. Ensure that the drain valve upstream of the DMW Unit is closed. 3. Ensure that the new drinking water line to DMW Unit is cleaned by flushing and the leak test has been completed. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 213 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4. Start the Drinking water pump 6834-P-23A and slowly open the discharge isolation valve and fill the line connecting the DMW Unit by opening the drain line upstream of the isolation valve. 5. Check for any leaks in the line. 6. After filling the line up to DMW Unit with Drinking water, it can be lined up to DMW Unit whenever required. 5.7 EFFLUENT & WASTE WATER TREATMENT SYSTEM 5.7.1 Lining up of Waste Water Degasser 6922-V-07 1. Ensure that the Degasser and pipelines are flushed and cleaned and ready for lining up. 2. Confirm that the drain and vent valves are closed. 3. Ensure that waste water from Tail Gas Treatment Unit is available and Cooling Water Circulation Pumps 9102-P-12A/B are running. 4. Ensure that high high level alarm 69-LAHH-1311 and high high pressure 69-PAHH1311 of the Degasser is not active in the ICSS. 5. Reset ESD. Ensure that the waste water from Cooling Water Circulation Pumps 9102-P-12A/B inlet ON-OFF valve 69-XV-1312 is opened. 6. Ensure water level starts rising in the Degasser by monitoring 69-LT-1311 & 1301 and cross checked through 69-LG-1302. 7. Ensure that the low low level trip 69-LALL-1311 is cancelled after the level reaches 300 mm and also ensure that the Waste Water Degasser Pumps 6922-P08A/B suction ON-OFF valve 69-XV-1316 is open. 8. Ensure that low level alarm 69-LAL-1301 is cancelled after the level reaches 450 mm. 9. Open the suction isolation valves of the Waste Water Degasser Pumps 6922-P08A/B. 10. Prime the Waste Water Degasser Pumps 6922-P-08A/B by opening the casing vents. 11. Energize Waste Water Degasser Pumps 6922-P-08A/B from MCC. 12. Put Waste Water Degasser Pumps 6922-P-08A/B LOR switch to ‘Remote’ at Local Control Station. 13. Select Waste Water Degasser Pump 6922-P-08A as “DUTY” and 6922-P-08B as “STANDBY” from the ICSS. 14. Ensure the minimum flow recycle line 2″ isolation valve is opened for the pump 6922-P-08A. 15. Start the “DUTY” pump 6922-P-08A from the ICSS. 16. Ensure that the pump is running without any abnormal noise and vibration. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 214 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.7.2 Lining up of Sour Water Stripper 6922-C-01 1. Slowly open the 2″ discharge valve of the pump 6922-P-08A and line up sour water to the Sour Water Filter 6922-S-06. 2. Ensure that the sour water from 6922-P-08A discharge to the observation sump 2″ isolation valve is closed. 3. Slowly open the sour water filter 2″ inlet isolation valve and fill the filter with the sour water. 4. Open the 2″ vent valve of the sour water filter and release air. Close the vent isolation valve after filling the filter. 5. Slowly open the filter outlet 2″ isolation valve and the Sour/Stripped Water Exchanger 6922-E-01 tube side inlet 2″ isolation valve. 6. Open the Sour/Stripped Water Exchanger 6922-E-01 tube side outlet 2″ isolation valve and the 69-FV-1314 upstream and downstream isolation valves. 7. Put 69-FV-1314 in manual and open the control valve slowly and allow the waste water to flow through to the Sour Water Stripper. 8. Now put 69-LIC-1301 in auto mode with a set point of 50% and 69-FV-1314 in remote mode. 9. Ensure that the level starts to build at the bottom of the Sour Water Stripper by checking the level gauge 69-LG-1306. 10. Ensure low low level 69-LALL-1316 is cancelled in the Sour Water Stripper when the level rises. 11. Ensure that the low level alarm 69-LAL-1306 is also cancelled as the level goes up. 12. Now open the 3″ suction isolation valve of the Stripped Water Pumps 6922-P-10A/B and prime the pumps. 13. Energize Stripped Water Pumps 6922-P-10A/B from MCC. 14. Put Stripped Water Pumps 6922-P-10A/B LOR switch to ‘Remote’ at field control panel. 15. Select Stripped Water Pumps 6922-P-10A as “DUTY” and 6922-P-10B as “STANDBY” from the ICSS. 16. Ensure the minimum flow recycle line 2″ isolation valve is opened for the pump 6922-P-10A. 17. Start the “DUTY” pump 6922-P-10A from the ICSS. 18. Ensure that the pump rated discharge pressure 8.6 bara is reached by checking the discharge pressure gauge 69-PG-1322. 19. Open the Sour/Stripped Water Exchanger 6922-E-01 shell inlet and outlet 2″ isolation valves. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 215 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 20. Open the Stripped Water Cooler 6922-E-02 inlet and outlet 2″ isolation valves. 21. Start the Stripped Water Cooler fan motors 6922-EM-02 AA/6922-EM-02 AB. 22. Line up 69-FV-1317 upstream and downstream isolation valves. 23. Slowly open 69-FV-1317 manually and line up the stripped water to the Observation & Buffer Sump 6922-X-04. 24. Line up the analyser 69-AT-1302 in the stripped water line. 5.7.3 Lining up of Stripper Overhead Circulation Pump 6922-P-11A/B 1. Line up start-up water through 69-LV-1325. 2. Prime the Stripper Overhead Circulation Pump 6922-P-11A/B. 3. Select the Pump 6922-P-11A as ‘DUTY’ and 6922-P-11B as ‘STANDBY’ from ICSS. 4. Start the Stripper Overhead Circulation Pump 6922-P-11A. 5. Take level controller 69-LIC-1325 in ‘AUTO’ with a set point of 50% and ensure the control valve 69-LV-1325 is controlling the level at 50%. 6. Take flow control valve 69-FV-1316 in ‘AUTO’ with a set point 13.2 m3/hr. 7. Open the inlet and outlet isolation valves of the Stripper Overheads Cooler 6922-E-03. 8. Start Stripper Overheads Cooler 6922-E-03AA/6922-E-03AB fans. 9. Take 69-TIC-1315 in AUTO with a set point of 55°C. 5.7.4 Lining up of Sour Water Stripper overhead Sour Gas 1. Ensure that 69-PV-1315A upstream and downstream isolation valves are closed. 2. Reset ESD and ensure that the ON-OFF valve 69-XV-1313 is open. 3. Ensure that the upstream and downstream isolation valves of 69-PSV-1303A are lock open and the bypass valve is closed. 4. Ensure that the upstream isolation valves of 69-PSV-1303B are lock closed and the downstream isolation valves are open. 5. Take 69-PIC-1315 in manual and close 69-PV-1315A fully. 6. Ensure that 69-PV-1315B upstream and downstream isolation valves are open and close 69-PV-1615 fully. 7. Now put 69-PIC-1315 in Auto with a set point of 1.0 barg and take 69-PV-1315A/B in Remote. 5.7.5 Pressurising Waste Water Degasser 6922-V-07 with Nitrogen 1. Ensure that the Nitrogen inlet shut down valve 69-XV-1315 is opened after resetting the ESD. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 216 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 2. Close 69-PV-1307 fully on manual. Open the 69-PV-1307 upstream and downstream isolation valves. 3. Slowly open 69-PV-1307 in manual till the pressure in the Degasser and Stripper reaches 1.0 barg and indicated by 69-PT-1307/1311/1315. Now put the controller 69-PIC-1307 in auto with a set point of 1.0 barg. 4. Take 69-PIC-1315 in AUTO. Since the isolation valves of 69-PV-1315A are closed, ensure that 69-PV-1315B opens when the pressure goes above 1.0 barg. Line up 69-PV-1315A upstream and downstream isolation valves and line up sour gas to TGTU. 5.7.6 Lining up of Sour Water Stripper Reboiler 1. Ensure that Sour Water Stripper Reboiler 6922-E-04 shell side is filled with sour water by checking 69-LT-1317/69-LG-1307. 2. Ensure that the 2” isolation valves of the Steam line from the Reboiler Steam inlet to the Reboiler vapour outlet line 2”-6848-LS-138-C12W-HC are closed. 3. Put steam inlet control valve 69-FV-1315 in manual and close it fully. 4. Ensure that after resetting ESD, steam inlet line ON/OFF valve 69-XV-1314 is open. 5. Open the 2″ vent valve in the steam inlet line to the reboiler and the condensate outlet line from the reboiler. 6. Open the vents and drains in the Reboiler Condensate Drum 6922-V-09. 7. Open the 69-LV-1327 upstream drain and close the bypass valve. 8. Ensure that the steam inlet line is warmed up upstream of the 8” isolation valve 68-GV-1928 and steam is charged. 9. Open the 2” bypass valves of the flow control valve 69-FV-1315. 10. Open the steam inlet 2″ warm up valve upstream of 68-XV-1314 slowly and admit steam into the Reboiler. 11. The Reboiler and the Reboiler Condensate Drum are warmed up by the steam and the condensed steam starts to come out of the drains and vents. 12. When full flow of steam comes out of the drains and vents, close all the vents and drains. 13. Close the 2″ steam inlet warm up bypass valve and open the steam inlet 8″ main isolation valve slowly. 14. Open 69-FV-1315 manually by 10%. 15. Close the bypass valves of the 69-FV-1315. 16. Ensure the temperature of the vapour line from the Reboiler increases as the steam flow is increased. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 217 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 17. When the temperature of the vapour line measured by 69-TT-1314 is increased to 120°C, put the steam flow controller 69-FIC-1315 in ratio control with the sour water flow 69-FIC-1314. 18. Line up Boiler Feed Water to the Desuperheater 6922-X-01. Take the temperature controller 69-TIC-1327 in AUTO with a set point of 148°C. 19. Ensure that the condensate level starts to increase in the Reboiler Condensate Drum 6922-V-09 through 69-LG-1308/69-LT-1327. 20. Ensure that the low level alarm 69-LAL-1327 (set at 400 mm) is cancelled when the level is rising in the Reboiler Condensate Drum 6922-V-09. 21. When the level in the drum reaches 50%, line up the level control valve 69-LV1327, put it on AUTO with a set point of 50%. 5.8 FLARE SYSTEM Reference: P&ID No. 2970-6-51-0033 5.8.1 Start-up of LP Flare System 1. Ensure that the isolation valve 62-BV-2211 is closed near the tie-in point T-18. 2. Ensure that the following new LP Flare lines are purged with Nitrogen and are under Nitrogen pressure: • 10”-6236-FL-033-D14M from 62-PSV-176/176S • 8”-6848-FL-036-C12P from Steam Generation Package 6848-A-02A/B/C • 2”-6236-FL-053-D14M from 62-PV-1301A/B vents • 6”-6236-FL-052-D14M from 62-PV-1303 • 2”-6236-BD-005-C14P-HI from LP Fuel Gas KO Drum 6236-V-05 3. Ensure that the vent and drain valves in the new flare header is closed. 4. Ensure that the spectacle blind in the new LP Flare header 10”-6236-FL-033-D14M connecting with the existing header at tie-in point T-18 is in open position. 5. Slowly open the 10” isolation valve in the new LP Flare header 10”-6236-FL-033D14M connecting with the existing header at tie-in point T-18. 6. Line up 62-PV-1303 upstream and downstream isolation valves to LP Flare as shown in P&ID. 7. Line up 62-PSV-176/176S upstream and downstream isolation valves from LP Fuel Gas KO Drum 6236-V-05 to LP Flare header as per requirement. 8. Line up Steam Generation Package 6848-A-02A/B/C relief header 8”-6848-FL-036C12P to LP Flare header as per requirement. 9. Line up the vent lines 2”-6236-FL-053-D14M from 62-PV-1301A/B to the new LP flare header as per requirement. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 218 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10. Line up the drain line 2”-6236-BD-005-C14P from new LP Fuel Gas KOD 6236-V-05 to the new LP flare header as per requirement. 11. Line up the drains and vents from the fuel gas system to LP Flare whenever required by reversing the spectacle blind to open position and opening the drain/ vent valve as per requirement. 5.8.2 LP ACID GAS FLARE SYSTEM Reference: P&ID No. 2970-6-50-0039 Start-up of LP Acid Gas Flare System 1. Ensure that the LP Flare header isolation valve is closed near the tie-in point T-69. 2. Ensure that the following new LP Acid Gas Flare lines are purged with Nitrogen and are under Nitrogen pressure: a. 2”-6236-FG-131-C12P purge fuel gas line to the Acid Gas Flare header b. 20”-9103-AG-104-C14P from AGRU 1 & 2 c. 6”-6922-AL-064-C14P from 69-PSV-1303A/1303B d. 2”-6922-AL-065-C14P from Sour Water Stripper 6922-C-01 e. 16”-9103-AL-117-C14P from Regenerator Reflux Drum 9103-V-12 f. 2”-9102-AG-116-A1C1 from sulphiding line of Hydrogenation Reactor 9102-V-11 g. 6”-9103-AL-110-C14P from Regenerator Reflux Drum 9103-V-12 PSV-1505/1506 h. 6”-9103-AL-101-C14P from Lean Acid Gas KO Drum 9103-V-14 i. 6”-9103-AL-104-C14P from Acid Gas Amine Absorber 9103-C-11 PSV-1503/1504 j. 14”-9101-AL-565-C14P from Acid Gas Pre-heater 9101-E-06 PSV-1071A/B k. 2”-9136-FG-056-C12P from Incinerator Fuel Gas Skid 9101-E-06 l. 12”-9103-AL-107-C14P from Regenerator 9103-C-12 PSV-1508/1509 m. 6”-9102-AL-102-C14P PSV-1303/1304. from Desuperheater/Contact Condenser 9102-C-11 n. 8”-9102-AL-110-C14P from Tail Gas Amine Absorber 9102-C-12 PSV-1334/1346 o. 2”-9136-FG-202-C12P from Fuel Gas distribution p. 20”-9103-AL-113-C14P Acid Gas flare header 3. Slowly open the 20” isolation valve in the new LP Flare header 20”-9103-AL-113C14P connecting with the existing header at tie-in point T-069. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 219 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4. Reverse the 2”-6236-FG-131-C12P purge fuel gas line spectacle blind to open position. Line up purge fuel gas to the Acid Gas Flare header as per requirement. 5. Line up AGRU 1 & 2, 20”-9103-AG-104-C14P to Acid Gas flare as per requirement. 6. Line up 69-PSV-1303A/1303B from the Sour Water Stripper 6922-C-01 to the new LP Acid Gas flare header as per requirement. 7. Line up 2”-6922-AL-065-C14P from Sour Water Stripper 6922-C-01 69-PV-1315B to the new LP Acid Gas flare header as per requirement. 8. Line up 16”-9103-AL-117-C14P from Regenerator Reflux Drum 9103-V-12 to the new LP Acid Gas flare header as per requirement. 9. Line up PSV-1505/1506 from Regenerator Reflux Drum 9103-V-12 to the new LP Acid Gas flare header as per requirement. 10. Line up 6”-9103-AL-101-C14P from Lean Acid Gas KO Drum 9103-V-14 to the new LP Acid Gas flare header as per requirement. 11. Line up 91-PSV-1503/1504 from Acid Gas Amine Absorber 9103-C-11 to the new LP Acid Gas flare header as per requirement. 12. Line up 91-PSV-1071A/B from Acid Gas Pre-heater 9101-E-06 to the new LP Acid Gas flare header as per requirement. 13. Line up 2”-9136-FG-056-C12P from Incinerator Fuel Gas skid 9101-E-06 to the new LP Acid Gas flare header as per requirement. 14. Line up 91-PSV-1508/1509 from Regenerator 9103-C-12 to the new LP Acid Gas flare header as per requirement. 15. Line up 91-PSV-1303/1304 from Desuperheater/Contact Condenser 9102-C-11 to the new LP Acid Gas flare header as per requirement. 16. Line up 91-PSV-1334/1346 from Tail Gas Amine Absorber 9102-C-12 to the new LP Acid Gas flare header as per requirement. 17. Line up 2”-9136-FG-202-C12P from fuel gas distribution to the new LP Acid Gas flare header as per requirement. 18. Line up 20”-9103-AL-113-C14P Acid Gas flare header to the new LP Acid Gas flare header as per requirement. 5.9 FUEL GAS SYSTEM Line-up Fuel Gas from the Existing 1st Stage Booster Compressor 6701-K-10/ 20/30 in NGL-3 5.9.1 1. Ensure that the fuel gas inlet isolation valves to the new Steam Boiler Package 6848-A-02A/B/C are in closed position and the lines are under Nitrogen pressure of 0.5 barg. 2. Ensure LP Fuel Gas KO Drum 6236-V-05 drain line isolation valve is closed. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 220 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3. Ensure Booster Compressor 6701-K-10/20/30 in NGL-3 is running. 4. Ensure 62-PV-1301A/B & 62-PV-1302 control valves are closed manually and the upstream and downstream isolation valves are closed. 5. Ensure 62-XV-1301 in the fuel gas supply line from Booster Compressor 6701-K-10/ 20/30 is open and the upstream isolation valve is closed. 6. Ensure 62-XV-1302 in the back-up supply fuel gas from 6103-K-01 A/B is open and the upstream isolation valve is closed. 7. Ensure 62-XV-1303 in the back-up supply fuel gas from 30” existing line is open and the upstream isolation valve is closed. 8. Ensure 62-PV-1303 is closed in auto with a set point of 7.8 barg and its upstream and downstream isolation valves are open. 9. Ensure 62-PSV-176 inlet and outlet isolation valves are open and the bypass is closed. 10. Ensure 62-PSV-176S inlet isolation valve is closed and outlet isolation valve is open. 11. Ensure that the spectacle blind on fuel gas supply line from Booster Compressor 6701-K-10/20/30 is in open position. 12. Open the 6” isolation valve slowly from the Booster Compressor 6701-K-10/20/30 and pressurise the line up to 62-XV-1301 upstream isolation valve. 13. Open 62-XV-1301 upstream isolation valve slowly and gradually pressurise the line up to 62-PV-1301A upstream isolation valve. 14. Open 62-PV-1301A bypass 3” isolation valves slowly and pressurise the fuel gas KO Drum 6236-V-05 gradually up to 7.0 barg. 15. Close the 62-PV-1301A bypass 3” isolation valves. 16. Open the 62-PV-1301A downstream isolation valve. 17. Put 62-PIC-1301 in auto with a set point of 7.0 barg. 18. Open 62-PV-1303 upstream and downstream isolation valves. 19. Open the upstream and downstream isolation valves of 62-PV-1301B/1302. 5.10 SEA COOLING WATER SYSTEM The start-up procedure for the Sea Cooling Water Pumps 6932-P-04A/B is given below: 5.10.1 Pre-start up checks Before starting the pump the following checks should be made 1. Rotate the pump shaft by hand to make sure that the pump rotates freely and the impellers are correctly positioned EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 221 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 2. The electric motor is properly lubricated 3. Direction of Rotation of the motor is checked and marked 4. Ensure all the piping connections are tight 5. Check for foundation bolts tightness 6. Check all bolting connections for tightness (coupling bolts, mechanical seal gland bolts, driver bolts) 7. Ensure the coupling guard is in place 5.10.2 5.11 Initial Starting and Lining Up of Sea Cooling Water 1. Open the Sea Cooling Water Pump 6932-P-04A discharge MOV 69-MOV-1301 by 10% 2. Start pre-lubrication liquid flow for the pump 3. Start the pump and open the discharge MOV 69-MOV-1301 immediately within 30 seconds 4. Observe the operation of the pump for any abnormal noise and vibration. 5. Measure the pump shaft vibration and lube oil temperature at regular intervals. 6. Line up sea cooling water to the header. 7. Start Biocide Injection and Scale Inhibitor Injection as per section 5.12.3 and 5.12.4 and start injection of the chemicals. 8. Line up sea cooling water to the following heat exchangers one by one by opening the high point vents and releasing air. • Lean Amine Trim Cooler 9103-E-15 • Regenerator Condenser Trim Cooler 9103-E-16 • Contact Condenser Trim Cooler 9102-E-13A/B • Acid Gas Cooler 9103-E-101A/B ELECTRO CHLORINATION PACKAGE START-UP Control of the package is via Allen Bradley compact logix PLC located in the control panel which also contains an HMI which provides facility for the operator to input selections of duty and stand-by equipments and adjustments of system parameters in addition to providing system of status, indications and alarms. Both automatic and manual operation of the package is possible, but manual operation is recommended only for maintenance purpose. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 222 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Electro chlorination package switch details are listed below: Sl. # Tag No. Service 1. 69-HSR-1480L Local selector switch 2. 69-HSR-1480R Remote selector switch 3. 69-HSOA-1451 Package start command from DCS 4. 69-HSCA-1451 Package stop command from DCS 5. 69-HS-1451 Package trip from UCP 6. 69-HS-1452 Package trip from field 7. 69-HS-1453 Package trip from field 8. 69-HSR-1470 Manual selected at transformer rectifier 9. 69-HSOA-1470 Transformer unit start 10. 69-HSCA-1470 Transformer unit stop Control valve and ON-OFF valve details are tabulated below: Sl. # 5.11.1 Tag No. Description 1. 69-XV-1451 Auto back wash filter 69-S-03A valve 2. 69-XV-1454 Auto back wash filter 69-S-03B valve 3. 69-XV-1452 Auto back wash filter drain valve 4. 69-XV-1455 Auto back wash filter drain valve 5. 69-XV-1456 Auto back wash filter 69-S-03A discharge valve 6. 69-XV-1456 Auto back wash filter 69-S-03B discharge valve 7. 69-XV-1457 Electrolyser – A inlet valve 8. 69-XV-1458 Electrolyser – B inlet valve Normal start-up of Electro Chlorination Plant: Before starting the package, ensure the following emergency shutdown causes are normal/healthy: Sl. # Tag No. Description 1 69-HS-1451 Emergency stop in UCP 2 69-HS-1452 Emergency stop in ECP skid 3 69-HS-1453 Emergency stop in ECP skid 4 69-XS-1336 Sea cooling water pump (6932-P-04A/B) trip 5 66-GF-02-1801 Hydrogen gas high-high alarm 6 66-GF-02-1801 Hydrogen gas high-high alarm EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 223 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 1. Open the Electro chlorination I/L PCV 69-PCV-1463 upstream and downstream isolation valves. 2. Open Auto Backwash Filters 6932-S-03A/B inlet and outlet isolation valves. 3. Open Electrolyser 6932-G-01A/B inlet and outlet isolation valves. 4. Open Hydrogen Dilution Blowers 6932-K-01A/B discharge isolation valves. 5. Ensure that Sea Cooling Water Pumps 6932-P-04A/B is started and running. 6. Open Auto Backwash Filter inlet PCV 69-PCV-1463, manually and slowly fill up the Sea Water Filter 6932-S-03A. Put 69-PCV-1463 in auto with a set point of 3.5 barg. 7. Select ‘LOCAL’ for the unit start-up from UCP. 8. Select Auto Backwash Filter 6932-S-03A as duty Filter from UCP. 9. Select Electrolyser Stream 6932-G-01A as duty form UCP. 10. Select Dilution Blower 6932-K-01A as duty blower from UCP. 11. Select Dosing Pump 6932-P-05A as duty pump from UCP. 12. Press ‘start’ from UCP. 13. Ensure that system status indication changes to ‘starting’. Ensure that Start lamp is flashing. 14. Ensure Auto Backwash Filter outlet XV, XV-1453 opens and sea water flow is established through the filters. 15. Ensure that the duty dilution blower 6932-K-01A is started. 16. After a 30 second delay, Ensure that the Electrolyser inlet XV, XV-1457 is opened and sea water flows through the Electrolyser. 17. Ensure that the Transformer/Rectifier 6932-TA-08A is energised after confirming the flow through the Electrolyser with the help of Magnetic flow meter 69-FT-1451. 18. Ensure that the ‘system running’ indication is illuminated. 19. Ensure that the Sodium Hypochlorite generated is sent to the Degassing Tank 6932-T-02. 20. Ensure that the level in Degassing Tank 6932-T-02 starts rising. 21. Fill the Dosing Pump 6932-P-05A by opening the suction isolation valve and releasing air through the casing vent valve. 22. Ensure that the Dosing Pump 6932-P-05A starts after the level reaches the low alarm level of 924 mm measured by 69-LT-1452. 23. Ensure that Sodium Hypochlorite is continuously dosed at a rate of 7 m3/hr and 1.25 ppm concentration to the Sea Cooling Water by dosing pumps (6932-P05A/05B). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 224 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 24. Ensure that Sodium Hypochlorite is shock dosed at a rate of 11 m3/hr and 6 ppm concentration for 15 minutes in every 6 hours by dosing pumps (6932-P-05A/05B). 25. Ensure that the following indications are healthy a. Autoback wash Filter Outlet Pressure Status Healthy b. Autoback wash Filter 6932-S-03A/B Status Healthy c. Electrolyser 6932-G-01A/B inlet flow healthy d. Electrolyser Inlet Temperature Healthy e. Hydrogen Blower Outlet Pressure Status Healthy f. Transformer/Rectifier 6932-RC-101A/B Healthy. 26. Ensure that the time for START-UP is 5 minutes. Manual start-up of electro chlorination package: 1. Manual operation is provided for maintenance and commissioning purposes only. 2. Select the Auto/Manual switch to manual mode in UCP HMI for manual start of ECP. 3. Following manual controls are available: 5.12 5.12.1 • Manual operation of each actuated on/off valve (69-XV-1457/69-XV-1458), (69XV-1453/69-XV-1456), (69-XV-1452/69-XV-1455) via a manual override facility, mounted on the valve • Flow control valve (69-FV-1453) which regulates the flow of sodium hypochlorite dosing to sea water can be operated by flow controller in UCP manually • Dilution blowers, dosing pumps and transformer rectifiers can be operated manually by selecting local mode at RCU in the field • Manual operation of each Transformer/Rectifier (6932-RC-101A/6932-RC-101B) can be done via local start/stop push buttons (69-HSOA-1470/69-HSCA-1470), by selecting manual button (69-HSR-1470) mounted on the front panel of each T/R. CHEMICAL INJECTION SYSTEM Complex Product Injection Package (6834-A-09) Fill the Complex Product Tank, 68-T-18 with Complex Product Chemical. WARNING: REVIEW THE COMPLEX PRODUCT MSDS AND ENSURE THAT APPROPRIATE SAFETY MEASURES ARE TAKEN BEFORE HANDLING THE CHEMICAL. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 225 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 1. Ensure that the Complex Product Inhibitor Tank, 68-T-18 is clean and dry for charging chemicals. 2. Line up the Complex Product Unloading Pump (6834-P-42) (Pneumatic driven) with chemical Tote Tank through the pump suction line and open isolation valve on the suction line. 3. Check plant air pressure and line up air to the unloading pump. 4. Open the isolation valve on the tank fill line and start Complex Product Unloading Pump (6834-P-42) and start filling the tank. Check all connections and confirm that there is no leakage. 5. Vent the instruments and line up for operation. 6. Monitor the level from the ICSS as the level increases. Ensure that the low low level, 68-LALL-1316 and the low-level alarm, 68-LAL-1317 are reset at their respective set point. 7. Fill the tank up to its maximum operating level, stop the chemical unloading pump (6834-P-42) by closing the plant air isolation valve and close the isolation valve on the fill line. Close the isolation valve on the pump suction line. 8. Open the Complex Product Injection Pump, 68-P-41A/B manual suction valve and fill the pumps. 9. Open pump discharge valve and close valve at injection point and upstream drain valve. 10. Set the stroke adjuster of the Complex Product Injection Pump, 68-P-41A/B to 10%. 11. Start the pump and check for flow at the injection point drain valve. Then stop the pump. 12. The system is now ready for start-up. The manual stroke is later adjusted to the desired injection rate based on the actual chemical requirement at the injection points. 5.12.2 Oxygen Scavenger Injection Package (6834-A-09) Fill the Oxygen Scavenger Storage Tank, 6834-T-17 with Oxygen Scavenger Chemical. WARNING: REVIEW THE OXYGEN SCAVENGER MSDS AND ENSURE THAT APPROPRIATE SAFETY MEASURES ARE TAKEN BEFORE HANDLING THE CHEMICAL. 1. Ensure that the Oxygen Scavenger Storage Tank, 6834-T-17 is clean and dry for charging chemicals. 2. Line up the Oxygen Scavenger Unloading Pump (6834-P-40) (Pneumatic driven) with chemical Tote Tank through the pump suction line and open isolation valve on the suction line. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 226 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3. Check plant air pressure and line up air to the unloading pump. 4. Open the isolation valve on the tank fill line and start Oxygen Scavenger Transfer Pump (6834-P-40) and start filling the tank. Check all connections and confirm that there is no leakage. 5. Vent the instruments and line up for operation. 6. Monitor the level from the ICSS as the level increases. Ensure that the low low level trip, 68-LALL-1314 and the low-level alarm, 68-LAL-1315 are reset at their respective set point. 7. Fill the tank up to its maximum operating level, stop the chemical unloading pump (6834-P-42) by closing the plant air isolation valve and close the isolation valve on the fill line. Close the isolation valve on the pump suction line. 8. Open the Oxygen Scavenger Injection Pump, 68-P-39A/B manual suction valve and fill the pumps. 9. Open pump discharge valve and close valve at injection point and upstream drain valve. 10. Set the stroke adjuster of the Oxygen Scavenger Injection Pump, 68-P-39A/B to 10%. 11. Start the pump and check for flow at the injection point drain valve. Then stop the pump. 12. The system is now ready for start-up. The manual stroke is later adjusted to the desired injection rate based on the actual chemical requirement at the injection points. 5.12.3 Biocide Injection Package (6932-A-06) Filling the Biocide Tank, 6932-T-04 with Biocide Chemical WARNING: REVIEW THE BIOCIDE MSDS AND ENSURE THAT APPROPRIATE SAFETY MEASURES ARE TAKEN BEFORE HANDLING ANY CHEMICAL. 1. Ensure that the Biocide Tank, 6932-T-04 is clean and dry for charging chemicals. 2. Line up the Biocide Unloading Pump (6932-P-08) (Pneumatic driven) with chemical Tote Tank through the pump suction line and open isolation valve on the suction line. 3. Check plant air pressure and line up air to the unloading pump. 4. Open the isolation valve on the tank fill line and start Biocide Unloading Pump (6932-P-08) by opening the plant air isolation valve to the pump and start filling the tank. Check all connections and confirm that there is no leakage. 5. Line up instruments for operation. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 227 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6. Monitor the level from the ICSS as the level increases. Ensure that the low low level trip, 69-LALL-1329 and the low-level alarm, 69-LAL-1328 are reset at their respective set point. 7. Fill the tank up to its maximum operating level, stop the Biocide Unloading Pump (6932-P-08) by closing the plant air isolation valve and close the isolation valve on the fill line. Close the isolation valve on the pump suction line. 8. Open the Biocide Injection Pump, 6932-P-07A/B manual suction valves and fill the pumps. 9. Open pump discharge valve and close valve at injection point and upstream drain valve. 10. Set the stroke adjuster of the Biocide Injection Pump, 6932-P-07A/B to 10%. 11. Start the pump and check for flow at the injection point drain valve. Then stop the pump. 12. The system is now ready for start-up. The manual stroke is later adjusted to the desired injection rate based on the actual chemical requirement at the injection points. 5.12.4 Scale Inhibitor Injection Package (6932-A-07) Filling the Scale Inhibitor Tank 6932-T-05 with Scale Inhibitor Chemical WARNING: REVIEW THE SCALE INHIBITOR MSDS AND ENSURE THAT APPROPRIATE SAFETY MEASURES ARE TAKEN BEFORE HANDLING ANY CHEMICAL. 1. Ensure that the Scale Inhibitor Tank, 6932-T-05 is clean and dry for charging chemicals. 2. Line up the Scale Inhibitor Unloading Pump (6932-P-10) (Pneumatic driven) with chemical Tote Tank through the pump suction line and open isolation valve on the suction line. 3. Check plant air pressure and line up air to the unloading pump. 4. Open the isolation valve on the tank fill line and start Scale Inhibitor Transfer Pump (6932-P-10) by opening the plant air isolation valve to the pump and start filling the tank. Check all connections and confirm that there is no leakage. 5. Vent the instruments and line up for operation. 6. Monitor the level from the ICSS as the level increases. Ensure that the low low level trip, 69-LALL-1331 and the low-level alarm, 69-LAL-1330 are reset at their respective set points. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 228 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7. Fill the tank up to its maximum operating level, stop the Scale Inhibitor Unloading Pump (6932-P-10) by closing the plant air isolation valve and close the isolation valve on the fill line. Close the isolation valve on the pump suction line. 8. Open the Scale Inhibitor Injection Pump, 6932-P-09A/B manual suction valves and fill the pumps. 9. Open pump discharge valve and close valve at injection point and upstream drain valve. 10. Set the stroke adjuster of the Scale Inhibitor Injection Pump, 6932-P-09A/B to 10%. 11. Start the pump and check for flow at the injection point drain valve. Then stop the pump. 12. The system is now ready for start-up. The manual stroke is later adjusted to the desired injection rate based on the actual chemical requirement at the injection points. 5.12.5 Catalyst Injection Package (9101-A-01) Filling the Catalyst Tank 9101-T-09 with Aquisulf Catalyst Chemical WARNING: REVIEW THE CATALYST MSDS AND ENSURE THAT APPROPRIATE SAFETY MEASURES ARE TAKEN BEFORE HANDLING ANY CHEMICAL. 1. Ensure that the Catalyst Tank, 9101-T-01 is clean and dry for charging chemicals. 2. Line up the Catalyst Unloading Pump (9101-P-12) (Pneumatic driven) with chemical Tote Tank through the pump suction line and open isolation valve on the suction line. 3. Check plant air pressure and line up air to the unloading pump. 4. Open the isolation valve on the tank fill line and start Catalyst Unloading Pump (9101-P-12) by opening the plant air isolation valve to the pump and start filling the tank. Check all connections and confirm that there is no leakage. 5. Vent the instruments and line up for operation. 6. Monitor the level from the ICSS as the level increases. Ensure that the low low level trip, 91-LALL-1128 and the low-level alarm, 91-LAL-1127 are reset at their respective set points. 7. Fill the tank up to its maximum operating level, stop the chemical transfer pump (9101-P-12) by closing the plant air isolation valve and close the isolation valve on the fill line. Close the isolation valve on the pump suction line. 8. Open the Catalyst Injection Pump, 9101-P-11A/B suction isolation valves and fill the pumps. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 229 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 9. Open pump discharge valve and close valve at injection point and upstream drain valve. 10. Set the stroke adjuster of the Catalyst Injection Pump, 9101-P-11A/B to 10%. 11. Start the pump and check for flow at the injection point drain valve. Then stop the pump. 12. The system is now ready for start-up. The manual stroke is later adjusted to the desired injection rate based on the actual chemical requirement at the injection points. 5.12.6 Antifoam Injection Package (9103-A-11) Fill the Antifoam Tank, 9103-T-12 with Antifoam Chemical WARNING: REVIEW THE ANTIFOAM MSDS AND ENSURE THAT APPROPRIATE SAFETY MEASURES ARE TAKEN BEFORE HANDLING ANY CHEMICAL. 1. Ensure that the Antifoam Tank, 9103-T-12 is clean and dry for charging chemicals. 2. Line up the Antifoam Unloading Pump (9103-P-19) (Pneumatic driven) with chemical Tote Tank through the pump suction line and open isolation valve on the suction line. 3. Check plant air pressure and line up air to the unloading pump. 4. Open the isolation valve on the tank fill line and start Antifoam Unloading Pump (9103-P-19) by opening the plant air isolation valve to the pump and start filling the tank. Check all connections and confirm that there is no leakage. 5. Vent the instruments and line up for operation. 6. Monitor the level from the ICSS as the level increases. Ensure that the low low level trip, 91-LALL-1520 and the low-level alarm, 91-LAL-1521 are reset at their respective set points. 7. Fill the tank up to its maximum operating level, stop the Antifoam Unloading Pump (9103-P-19) by closing the plant air isolation valve and close the isolation valve on the fill line. Close the isolation valve on the pump suction line. 8. Open the Antifoam Injection Pump, 9103-P-16A/B suction valves and fill the pumps. 9. Open pump discharge valve and close valve at injection point and upstream drain valve. 10. Set the stroke adjuster of the Antifoam Injection Pump, 9103-P-16A/B to 10%. 11. Start the pump and check for flow at the injection point drain valve. Then stop the pump. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 230 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 12. The system is now ready for start-up. The manual stroke is later adjusted to the desired injection rate based on the actual chemical requirement at the injection points. 5.12.7 Corrosion Inhibitor Injection Package (9103-A-12) Filling the Corrosion Inhibitor Tank, 9103-T-13 with Corrosion Inhibitor Chemical. WARNING: REVIEW THE CORROSION INHIBITOR MSDS AND ENSURE THAT APPROPRIATE SAFETY MEASURES ARE TAKEN BEFORE HANDLING ANY CHEMICAL. 1. Ensure that the Corrosion Inhibitor Tank, 9103-T-13 is clean and dry for charging chemicals. 2. Line up the Corrosion Inhibitor Unloading Pump (9103-P-102) (Pneumatic driven) with chemical Tote Tank through the pump suction line and open isolation valve on the suction line. 3. Check plant air pressure and line up air to the unloading pump. 4. Open the isolation valve on the tank fill line and start Corrosion Inhibitor Unloading Pump (9103-P-102) by opening the plant air isolation valve to the pump and start filling the tank. Check all connections and confirm that there is no leakage. 5. Vent the instruments and line up for operation. 6. Monitor the level from the ICSS as the level increases. Ensure that the low low level trip, 91-LALL-1522 and the low-level alarm, 91-LAL-1523 are reset at their respective set points. 7. Fill the tank up to its maximum operating level, stop the Corrosion Inhibitor Unloading Pump (9103-P-102) by closing the plant air isolation valve and close the isolation valve on the fill line. Close the isolation valve on the pump suction line. 8. Open the Corrosion Inhibitor Injection Pump, 9103-P-101A/B suction valves and fill the pumps. 9. Open pump discharge valve and close valve at injection point and upstream drain valve. 10. Set the stroke adjuster of the Corrosion Inhibitor Injection Pump, 9103-P-101A/B to 10%. 11. Start the pump and check for flow at the injection point drain valve. Then stop the pump. 12. The system is now ready for start-up. The manual stroke is later adjusted to the desired injection rate based on the actual chemical requirement at the injection points. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 231 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.12.8 Caustic Injection Package (9103-A-13) Filling the Caustic Storage Tank, 9103-T-14 with Caustic WARNING: REVIEW THE CAUSTIC MSDS AND ENSURE THAT APPROPRIATE SAFETY MEASURES ARE TAKEN BEFORE HANDLING ANY CHEMICAL. 1. Ensure that the Caustic Storage Tank, 9103-T-14 is clean and dry for charging chemicals. 2. Line up the Caustic Unloading Pump (9103-P-104) (Pneumatic driven) with chemical Tote Tank through the pump suction line and open isolation valve on the suction line. 3. Check plant air pressure and line up air to the unloading pump. 4. Open the isolation valve on the tank fill line and start Caustic Unloading Pump (9103-P-104) by opening the plant air isolation valve to the pump and start filling the tank. Check all connections and confirm that there is no leakage. 5. Vent the instruments and line up for operation. 6. Monitor the level from the ICSS as the level increases. Ensure that the low low level trip, 91-LALL-1524 and the low-level alarm, 91-LAL-1525 are reset at their respective set points. 7. Fill the tank up to its maximum operating level, stop the Caustic Unloading Pump (9103-P-104) by closing the plant air isolation valve and close the isolation valve on the fill line. Close the isolation valve on the pump suction line. 8. Open the Caustic Injection Pump, 9103-P-103A/B manual suction valves and fill the pumps. 9. Open pump discharge valve and close valve at injection point and upstream drain valve. 10. Set the stroke adjuster of the Caustic Injection Pump, 9103-P-103A/B to 10%. 11. Start the pump and check for flow at the injection point drain valve. Then stop the pump. 12. The system is now ready for start-up. The manual stroke is later adjusted to the desired injection rate based on the actual chemical requirement at the injection points. 5.13 5.13.1 DEMINERALIZED WATER SYSTEM Demineralized Water Unit Start-up Demineralized Water Unit (2 trains) is designed for automatic operation via unit control panel which contains Siemens S7-400 PLC. All the alarms, indications and EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 232 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL status signals generated within the package are transmitted from package UCP to DCS through serial link (modbus through TCP/IP). The list of switches used in the operation of DM water package is tabulated below: Sl. # Tag No. Train-A Train-B Service 1. 68-HS-1840 A 68-HS-1840 B Auto/Man/Off selector-Auto 2. 68-HS-1841 A 68-HS-1841 B Auto/Man/Off selector-Manual 3. 68-HS-1843 A 68-HS-1843 B Auto/Man/Off selector-off 4. 68-HS-1842 A 68-HS-1842 B Step advance push button 5. 68-HSOA-1845 A 68-HSOA-1845B Remote start from DCS 6. 68-HSCA-1845 A 68-HSCA-1845B Remote stop from DCS The list of ON/OFF valves is tabulated below: Sl. # Tag No. Train-A Train-B Service 1. 68-XV-1825 68-XV-1840 Cation Exchanger Inlet 2. 68- XV-1831 68-XV-1846 Cation Exchanger outlet 3. 68-XV-1833 68-XV-1848 Anion Exchanger inlet 4. 68-XV-1838 68-XV-1852 Anion Exchanger outlet 5. 68- XV-1856 68-XV-1855 DM Water common header inlet 6. 68-XV-1832 68-XV-1847 AE-1825 pH Analyzer inlet 7. 68-XV-1839 68-XV-1853 AE-1826 Conductivity Analyzer inlet 8. 68-XV-1830 68-XV-1844 HCL drain to pit 9. 68-XV-1837 68-XV-1851 NaOH drain to pit 10. 68-XV-1828 68-XV-1843 DM+HCL inlet to cationic exchanger 11. 68-XV-1835 68-XV-1854 DM+ NaOH inlet to anionic exchanger 12. 68-XV-1829 68-XV-1845 Regeneration inlet to cationic exchanger 13. 68-XV-1836 68-XV-1850 Regeneration inlet to anionic exchanger 14. 68-XV-1826 68-XV-1841 Recycle water to cation exchanger 15. 68-XV-1827 68-XV-1842 Cation exchanger to neutralization pit 16. 68-XV-1834 68-XV-1849 Anion exchanger to neutralization pit 17. 68-XV-1857 Neutralization pump discharge 18. 68-XV-1858 Neutralization pump recycle EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 233 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The list of Pumps is tabulated below: Sl. # 1. Tag No. Train-A 6834-P-37A Service Train-B 6834-P-37B Recycling pump 2. 6834-P-34A/B/C NaOH dosing pump 3. 6834-P-35A/B/C HCL dosing pump 4. 6834-P-36A/B Regeneration pump 5. 6834-P-38A/B Neutralization pump The operational status of the package is indicated by the following signals: Sl. # Tag No. Train-A Service Train-B 1. 68-XL-1840A 68-XL-1840B Package working in auto mode 2. 68-XL-1841A 68-XL-1841B Package working in manual mode 3. 68-XL-1843A 68-XL-1843B Package is in offline 4. 68-XL-1850A 68-XL-1850B service phase 5. 68-XL-1851A 68-XL-1851B waiting regeneration phase 6. 68-XL-1852A 68-XL-1852B Acid regeneration/caustic regeneration 7. 68-XL-1853A 68-XL-1853B Acid slow rinse/caustic slow rinse 8. 68-XL-1854A 68-XL-1854B caustic slow rinse 9. 68-XL-1855A 68-XL-1855B Final rinse with recirculation 10. 68-XL-1856A 68-XL-1856B Waiting ready phase 11. 68-XL-1857A 68-XL-1857B Pre-service phase 12. 68-UA-1844 Irregular valves/pumps position 13. 68-XL-1858 Neutralization 14. 68-XL-1859 Effluent discharge 15. 68-XL-1860 Neutralization recirculation 16. 68-XL-1861 Neutralization standby Startup of the Demineralized Water System 1. Put the AUTO/MANUAL/OFF selector in UCP in MANUAL position for Train-A (68-HS-1841A). 2. Put the AUTO/MANUAL/OFF selector in UCP in MANUAL position for Train-B (68-HS-1841B). 3. Put the LOR selector of all the pumps in ‘Remote’ and select the duty and standby pumps in UCP and put them in auto. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 234 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4. Put the Train-A in ‘SERVICE’ mode (Phase No. 1) by pressing the Step Advance push button 68-HS-1842A in the UCP once. 5. Ensure that the following valves are open in Train–A: a. 68-XV-1825 b. 68-XV-1831 c. 68-XV-1833 d. 68-XV-1854 e. 68-XV-1830 f. 68-XV-1837 g. 68-XV-1832 6. Now Train A is on line. 7. Put Train B in ‘WAITING READY’ mode (Phase No. 7) by pressing the Step Advance push button 68-HS-1842B in the UCP. 8. Ensure that the following valves in Train-B are open: a. 68-XV-1844 b. 68-XV-1851 9. Ensure that drinking water is available in the existing Drinking Water Storage Tanks 6834-T-01A/B. 10. Open the isolation valve from the existing Drinking water storage tank 6834-T-01A to the new Drinking Water Pumps 6834-P-23A/B slowly and fill up the suction lines of the pumps. 11. Prime the Drinking Water Pumps 6834-P-23A/B by opening the casing vents and releasing air. 12. Put the LOR switch of the Drinking Water Pump 6834-P-23A in ‘LOCAL’ position. 13. Start the Drinking Water Pump 6834-P-23A on recirculation, gradually open the discharge valve and slowly pressurize the Demineralized Water Unit Train A. 14. Ensure 68-LCV-1827 is lined up and it is fully open on manual. 15. Ensure the Demineralized Water Storage Tank 6834-T-08 water level is raising. 16. When the level is 30% in the storage tank, take 68-LCV-1827 in auto with a set point of 70%. 17. After stabilising the unit, put the AUTO/MANUAL/OFF selector in UCP in AUTO for both A & B trains. 18. Prime the Recycling and Regeneration pumps. 19. Prepare HCl (33%) and Caustic solutions (50%). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 235 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.13.2 Demineralized Water Unit Sequence A. Phase No. 1: Service 1. Ensure that when put in service the following XVs of Train-A are open: a. 68-XV-1825: Cation Exchanger I/L b. 68-XV-1831: Cation Exchanger O/L c. 68-XV-1833: Anion Exchanger I/L d. 68-XV-1838: Anion Exchanger O/L e. 68-XV-1856: Demin. Water common header I/L f. 68-XV-1832: AE-1825 pH Analyzer I/L g. 68-XV-1839: AE-1826 Conductivity Analyzer I/L h. 68-XV-1830: HCl drain line i. 68-XV-1837: NaOH drain line 2. Ensure that 68-FIC-1825 is on line and the flow rate through the train is 7 m3/hr. 3. Ensure that Train A is in line for a through put of 168 m3 (=24 hours @ 7 m3/hr) measured by the flow totaliser 68-FQI-1825 or until the high conductivity 68-AAH1829 measured by the Analyzer 68-AI-1829. 4. Ensure that Train A is transferred to Phase No. 2 ‘Waiting Regeneration’ mode after step 3. 5. Ensure that the high conductivity alarm is ON if 68-AAH-1829 is ON for 5 minutes. 6. Ensure that this service phase is terminated if 68-AAH-1829 is ON for additional 30 minutes. B. 1. Phase No. 2: Waiting Regeneration Ensure that the following XVs are open in this phase: a. 68-XV-1830 b. 68-XV-1837 2. Ensure that the following conditions do not exist: a. Acid Level Low (68-LAL-1825) b. Caustic Level Low (68-LAL-1827) 3. Ensure that the following alarms are not present: a. Irregular valve position alarm 68-UA-1844 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 236 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL b. Both Regeneration Pumps unavailable c. Dosing Pumps unavailable 4. Ensure that this phase duration is 2 minutes. C. 1. Phase No. 3: Acid Regeneration/Caustic Regeneration Ensure that the following XVs are open: a. 68-XV-1829 b. 68-XV-1828 c. 68-XV-1827 d. 68-XV-1836 e. 68-XV-1835 f. 68-XV-1834 2. Ensure that Acid Dosing Pump 6834-P-35A/B/C is started and dosing 174 litres/ hour of acid for regeneration. 3. Ensure that Caustic Dosing Pump 6834-P-34A/B/C is started and dosing 126 litres/ hour of caustic for regeneration. 4. Ensure that Regeneration Pump 6834-P-36 A/B is started and supplies 1173 litres/ hour of dilution water for acid regeneration and 2300 litres/hour of dilution water for caustic regeneration. 5. Ensure that the following control valves are in line to control the dilution water to the acid and caustic dosing systems: a. 68-FIC-1835 in auto with a set point of 2175 litres/hour b. 68-FIC-1836 in auto with a set point of 1000 litres/hour 6. Ensure that the Neutralisation Pit Pump 6834-P-38 A/B starts when the level in the Neutralisation Pit rises to high level 68-LAH-1831. 7. Ensure that the duration of this regeneration phase is 25 minutes. D. 1. Phase No. 4: Acid Slow Rinse/Caustic Slow Rinse Ensure that the following XVs are open: a. 68-XV-1830 b. 68-XV-1837 c. 68-XV-1827 d. 68-XV-1836 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 237 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. 68-XV-1835 f. 68-XV-1834 g. 68-XV-1828 h. 68-XV-1829 2. Ensure that the Regeneration Pump 6834-P-36 A/B is started and supplies 1000 litres/hour to the Cationic Exchanger 6834-S-21A and 2175 litres/hour to the Anionic Exchanger 6834-S-22A for rinsing. 3. Ensure that the controllers 68-FIC-1835 and 68-FIC-1836 are inline. 4. Ensure that the rinsing duration is 54 minutes. E. 1. Phase No. 5: Caustic Slow Rinse Ensure that the following XVs are open: a. 68-XV-1837 b. 68-XV-1836 c. 68-XV-1835 d. 68-XV-1834 2. Ensure that the Regeneration Pump 6834-P-36 A/B is started and supplies 2175 litres/hour to the Anionic Exchanger 6834-S-22A for rinsing. 3. Ensure that the controller 68-FIC-1835 is online. 4. Ensure that the rinsing duration is 29 minutes. F. 1. Phase No. 6: Final Rinse with Recirculation Ensure that the following XVs are open: a. 68-XV-1831 b. 68-XV-1833 c. 68-XV-1826 d. 68-XV-1839 2. Ensure that the Recirculation Pump 6834-P-37 A is started and recirculates 10 m3/hour water through the cationic and anionic exchangers 3. Ensure that the rinsing duration is 30 minutes. 4. Ensure that after 30 minutes of rinsing, 68-AAH-826 alarm is OFF. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 238 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5. Ensure that if the alarm 68-AAH-826 is ON after 30 minutes of recirculation, the Regeneration Failure alarm starts and the final rinse with recirculation phase continues until 68-AAH-826 is OFF. G. Phase No. 7: Waiting Ready Ensure that the following XVs are open: a. 68-XV-1830 b. 68-XV-1837 H. 1. Phase No. 8: Pre-service Recirculation Ensure that the following XVs are open: a. 68-XV-1831 b. 68-XV-1833 c. 68-XV-1826 d. 68-XV-1839 e. 68-XV-1838 f. 68-XV-1830 g. 68-XV-1837 2. Ensure that the Recirculation Pump 6834-P-37 A is started and circulates 10 m3/hr water through the system. 3. Ensure that the duration of this phase is 10 minutes. 4. Ensure that the high conductivity 68-AAH-1826 alarm is not present at the end of the duration of this phase. 5. Ensure that if the alarm 68-AAH-1826 is present, then the Pre-service circulation continues till the alarm is cancelled. 5.13.3 Neutralization Pit The waste water generated during regeneration of the Demineralized Plant is collected in the Neutralization Pit (6834-T-014). Once the level reaches the required level, ensure the following 4 Phases to pump out the effluent. A. Phase No. P1: Waiting Ready 1. Check of conditions for recirculation. 2. Check the level 68-LT-1831/68-LT-1830 in Neutralization Pit 6834-A-01. 3. Ensure duration of this phase is 1 minute. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 239 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4. Activation of level alarm 68-LAH-1831 in pit leads to phase No. P2. Recirculation B. Phase No. P2: Recirculation 1. Ensure that the Neutralization Pit Pump 6834-P-38 A/B starts at 68-LAH-1831. 2. Ensure that 68-XV-1858 is open. 3. Ensure that 68-XV-1857 is closed. 4. Ensure the duration of this phase is 15 minutes. 5. At the end of re-circulation time if pH is within range, then discharge phase 4 starts. C. Phase No. P3: Neutralization 1. Ensure that the Neutralization Pit Pump 6834-P-38 A/B starts at LAH-1831. 2. Ensure that 68-XV-1858 is open. 3. Ensure that 68-AAH-1831 (pH is more than 9) starts Acid Dosing Pumps 6834-P-35C. 4. Ensure that 68-AAL-1831 (pH is less than 6) starts Caustic Dosing Pumps 6834-P34C. 5. Activation of low low alarm 68-LALL-1830 in neutralization pit trips the neutralization, acid and caustic dosing pumps. D. Phase No. P4: Effluents Discharge 1. Ensure that the Neutralization Pit Pump 6834-P-38 A/B starts discharging effluents when pH analyzer 68-AI-1831 is in the range (pH: 6-9) for more than 5 minutes. 2. Ensure that 68-XV-1857 is open. 3. Ensure that the Neutralization Pit Pump 6834-P-38 A/B stops at low level alarm level of the pit 68-LAL-1831. 4. By simulating 68-LALL-1830 check the trip signal of Neutralization Pit Pump 6834P-38 A/B in MCC. Operator can abort Manual Step-by-Step mode and continue operating in Automatic Mode by simply putting the AUTO/MAN/OFF selectors in AUTO position. The sequence will continue operating from last selected phase during Step-by-Step mode. Details of ON/OFF valve positions against the respective phase are tabulated below: Tag No. Demineralization - Phase Number Neutralization Phase Number 1 Train “A” Train “B” 1 2 3 4 5 6 7 8 68-XV-1825 68-XV-1840 O C C C C C C C 68- XV-1831 68-XV-1846 O C C C C O C O 68-XV-1833 O C C C C O C O 68-XV-1848 2 3 4 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 240 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Tag No. Demineralization - Phase Number Neutralization Phase Number 1 2 3 4 Train “A” Train “B” 1 2 3 4 5 6 7 8 68-XV-1838 68-XV-1852 O C C C C O C O 68- XV-1856 68-XV-1855 O C C C C C C C 68-XV-1832 68-XV-1847 O C C C C C C C 68-XV-1839 68-XV-1853 O C C C C O C O 68-XV-1830 68-XV-1844 O O C O O O O O 68-XV-1837 68-XV-1851 O O C O O O O O 68-XV-1828 68-XV-1843 C C O O C C C C 68-XV-1835 68-XV-1854 C C O O O C C C 68-XV-1829 68-XV-1845 C C O O C C C C 68-XV-1836 68-XV-1850 C C O O O C C C 68-XV-1826 68-XV-1841 C C C C C O C O 68-XV-1827 68-XV-1842 C C O O O C C C 68-XV-1834 68-XV-1849 C C O O O C C C 68-XV-1857 C C C C C C C C C C C O 68-XV-1858 C C C C C C C C C O O C Details of pump status against the respective phase are tabulated below: Pump Tag No. Train “A” 6834-P-37A Train “B” Demineralization - Phase Number 1 2 3 4 5 6834-P-37B ON 6834-P-34A 6834-P-34B ON 6834-P-35B 6834-P-36B 6834-P-38A 6834-P-38B 8 1 2 3 4 ON ON ON ON 6834-P-35C 6834-P-36A 7 ON 6834-P-34C 6834-P-35A 6 Neutralization Phase Number ON ON ON ON ON ON EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 241 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.14 BOILER FEED WATER DEAERATOR SYSTEM 5.14.1 Lining up of Steam Condensate Flash Drum 6834-V-05 1. Open the 2” drum vent isolation valve to atmosphere. 2. Open the 2” drain valve from the Steam Condensate Flash Drum 6834-V-05. 3. Open the 12” Condensate Distribution Header isolation valves at battery limit and near the Steam Condensate Flash Drum 6834-V-05 slowly and introduce condensate from condensate distribution header and warm up the Steam Condensate Flash Drum 6834-V-05. 4. Ensure enough time is given for the warming up of the drum and then open the condensate header isolation valves fully. 5. Close the 2” drain valve from the Steam Condensate Flash Drum 6834-V-05. 6. Ensure that low low level trip 68-LALL-1309 is cancelled when the water level is rising. 7. Ensure that low level alarm 68-LAL-1301 is cancelled when the level is rising in the drum. 8. Ensure that the level in the drum is rising by checking the level transmitter 68-LT1301/1308/68-LG-1303. 9. When the level is around 50%, close the condensate inlet isolation valve near the drum. 10. Open the Deaerator Feed Pumps 6834-P-20A/B suction isolation valves and the common suction line isolation valve and warm up the pumps by opening the casing vent isolation valves. 11. Prime the pumps by opening the casing vent isolation valves and releasing air. 12. Ensure that the Deaerator Package 6834-A-08 inlet isolation valves from the Deaerator Feed Pumps 6834-P-20A/B discharge is closed. 13. Open the Steam Condensate Coolers fans 6834-E-02A/B/C inlet and outlet isolation valves. 14. Line up condensate from Steam Condensate Cooler 6834-E-02 to Steam Condensate Flash Drum 6834-V-05 isolation valve. 15. Open the discharge valve of Deaerator Feed Pump 6834-P-20A. 16. Open the minimum flow control valve 68-FV-1301 in manual by 50% and the upstream and downstream isolation valves. 17. Ensure that the temperature control valve 68-TV-1301 is manually closed. 18. Start Deaerator Feed Pump 6834-P-20A from the local panel. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 242 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 19. Now the Deaerator Feed Pump 6834-P-20A is circulating water back to the Steam Condensate Flash Drum 6834-V-05 through the Steam Condensate Cooler 6834-E-02. 20. Line up temperature control valve 68-TV-1301 upstream and downstream isolation valves and take 68-TV-1301 in AUTO with a set point of 102°C. 21. Line up Demineralised Water from Demineralised Water Feed Pumps 6834-P-24A/B by opening the upstream and downstream isolation valves of 68-LV-1301. 22. Take 68-LV-1301 in AUTO with a set point of 50%. 5.14.2 Lining up of BFW Deaerator Package 6834-A-08 1. Open the 2” Deaerator Column vent isolation valve to atmosphere. 2. Open the 3” drain valve from the Deaerator Storage Vessel 6834-A-08. 3. Reset ESD and ensure the Deaerator inlet ON-OFF valve 68-XV-1301 opens. 4. Line up 68-LV-1302 upstream and downstream isolation valve. 5. Open 68-LV-1302 manually by 10%. 6. Warm up the Deaerator Storage Vessel and the Deaerator Column with the condensate from Deaerator Feed Pumps. 7. After allowing sufficient time for the warming up of Deaerator, close the 3” drain valve from the drum. 8. Now the level in the drum starts to rise. 9. Ensure that the low low level trip 68-LALL-1310 in the drum is cancelled when the level rises. 10. Ensure that the low level alarm 68-LAL-1310 is cancelled when the level rises. 11. When the level reaches 50%, put 68-LIC-1302 in AUTO with a set point of 50%. 12. Line up LP saturated steam by opening the upstream and downstream isolation valves of 68-PV-1304. 13. Put 68-PV-1304 in AUTO with a set point of 1.21 bara. 14. Drain condensate from the Deaerator if required to maintain the level at 50%. 15. Start Boiler Feed Water Pump 6834-P-22A and recirculate the condensate to the Deaerator through the minimum flow line. 16. Start O2 Scavenging Injection from the Chemical Injection Package 6834-A-09 as per section 5.12.2 and line up to the Deaerator at a rate of 0.55 l/hr. 17. Take a sample from the Sample cooler 68-SC-1004 at the suction of the Boiler Feed Water Pump 6834-P-22A and analyse for dissolved Oxygen. 18. If O2 and CO2 in the sample are less than 5 parts per billion then the Boiler Feed Water is ready for lining up to the steam generation units. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 243 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.15 STEAM GENERATION PACKAGE START-UP 5.15.1 Checks for Start-up • First of all it is necessary to be sure that all lines up to boiler package battery limit (including water, steam, compressed air, fuel gas etc.) have been completely and properly cleaned to eliminate from internal side of lines, any possible presence of impurities/oxides, debris, rust and scales. This is very important for the first time start-up of the Boiler subsequent to a long shutdown and there is a reasonable doubt about possible accumulation of deposits on line internal parts • In the case boiler start-up is subsequent to a long boiler shutdown (for instance: for maintenance, inspection or repair purposes), the Operator visual inspection should be extended to internal and external parts and it should cover at least the following essential points: • Check of cleaning of all involved piping by means of appropriate fluids so that piping is internally free from scale and impurities. Operator must always take care to achieve an ideal clean tube condition, in order to avoid any obstruction to the instruments, valves and fittings that could seriously jeopardize the boiler/plant functionality and operation. This visual inspection should be extended till to check the drains and to see if the fluid is discharged without any obstruction and free from scales or other impurities; • Water gauge passages and other boiler mounting openings are clear • Manhole doors are in position with good gaskets and satisfactorily tightened • All Boiler and Economizer valves and fittings are operated and checked • Combustion chamber and flue gas circuits are checked for cleanliness with refractory brickwork in good condition and expansion allowances are clear • All valves and fittings installed on remaining lines (such as instrument air, cooling water, fuel lines and so on) are proven clear and in working order • All installed instrumentation are in good and working conditions • Before start-up of the steam generator, it should be verified that all the auxiliary equipments are in proper working condition and all the control devices have been positively tested Critical checks for start-up of Boiler: • Verify the proper functioning of the level gauge (Boiler). If necessary level gauge drains are to be operated and the level gauge is checked. Ensure that water comes out of the level gauge drains and that upstream piping is not blocked by impurities. In case of doubt and if necessary remove the drain valves and clear the upstream piping of blockages • Verify that all the Boiler and Economizer drains are closed EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 244 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 5.15.2 • Verify that main steam stop valve and relevant by-pass valves are completely closed • Verify the proper operation of all the control and block valves • Verify that all equipment inspection doors are properly closed • Verify that feed water is available with proper quality Water Filling • Before the Boiler start-up operation, boiler has to be filled with water up to the operating level • Feed water must always be introduced slowly into the boiler. The filling water flow rate depends on the water temperature. • In general 20°C is the minimum recommended value of the feed water temperature. If this value is higher than 40°C, the steam generator should be filled very slowly in order to prevent stress on the boiler components (particularly on drums) • Before starting boiler filling, all vent valves (both manual and actuated) shall be fully opened • Ensure that the manual start-up vent valves GV-5045 & GV-5046 are fully open • Boiler and Economizer drains shall be opened (in order to check their proper operation). Boiler and Economizer drain valves shall be closed after few minutes • All the vent valves are to be kept open. This is to vent out air pockets inside steam generator tubes to atmosphere • When water exits from the Economizer vent, the relevant Economizer vent manual valve has to be closed. • Keep 68-PIC-1819 in Manual Mode and Open 68-PV-1524 fully (MV=100%). • Open the start-up vent 68-PV-1523 fully in Manual Mode. • Confirm that the LP Steam Outlet 68-MOV-1522 is in closed position. • Ensure that the BFW Pumps 6834-P-22 A/B/C are running. • Ensure that the BFW inlet 68-XV-1522 & 68-XV-1524 are open. • Ensure that complex product Injection package is started as per section 5.12.1 and complex product is dosed at a rate of 1.87 l/hr to the BFW. • Gradually open the 68-LV-1522 in Manual Mode and fill the downstream line. • Gradually open the valve GV-5013 and fill the Boiler Steam Drum 6848-V-02A with DM water. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 245 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Fill the Boiler gradually and open the drain lines one by one for flushing. • Close all the drain valves after ensuring sediment free water from Boiler. • Monitor the level in the Steam Drum. • Check for water leakages if any. • Raise the Steam Drum Water level up to normal level. • Confirm that the all drain valves are closed properly. • Water filling is completed when drum level is at about 50 mm below the normal water level (NWL) so that there is enough volume for expansion during subsequent water heating when burner is lighted. Note: Achieving of drum level is a necessary and mandatory pre-condition for boiler start-up operation. Normal Water Level is located +50 mm above Steam Drum centre line. 5.15.3 Fuel Gas Line-up 1. Ensure that the main fuel gas line and the pilot fuel gas line are purged with nitrogen and are under nitrogen pressure. 2. Ensure that the fuel gas lines are leak tested. 3. Ensure that the vent and drain valves in the fuel gas lines are closed. 4. Ensure that fuel gas inlet filter 6848-S-01A elements are available and boxed up. 5. Ensure that the fuel gas inlet 68-XV-1302 is open. 6. Slowly open the isolation valve upstream of 68-XV-1302 and pressurise the line. Check the pressure increase through 68-PG-1314. 7. Open the isolation valve BV-5167 and slowly pressurise the downstream lines. 8. Open 68-PCV-1522 in Manual Mode slowly and pressurise the Main Fuel Gas Line. 9. Open the Block valve BV-5190 and slowly pressurise the Pilot Fuel Gas line. 10. Check for any gas leakages. 5.15.4 FD Fan Start-up 1. Confirm that necessary lubricants/grease is filled as per specifications. 2. Confirm that the Cooling water is lined-up and the water flows through the Sight Flow Glass (SFG). 3. Ensure that the Inlet damper is fully open. 4. Keep the “LOR” selector Switch in ‘Local’ mode. 5. Rotate the shaft, half turn, by hand to ensure free rotation of the Fan. 6. Confirm that the FD Fan 6848-K-02A is ready to start. 7. Inform to the substation. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 246 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 8. Start the FD Fan by pressing START push button. 9. Ensure that there is no abnormal noise and vibration 5.15.5 Burner Start-up Burner management system (BMS): The burner operation is performed in fully automatic through Burner management system (BMS). The BMS performs the following basic functions: 1. Continuous check of all valves and dampers of combustion systems 2. Pre-firing cycle. 3. Light-off cycle of burner. 4. Boiler Stop cycle. 5. ESD-Master fuel trip. 6. Post firing purge. Steam generation unit-Burner start-up: Note: Tags considered in this document are all related to BOILER A. Steam generation unit Local panel details (6848A02A-LP-003) are tabulated below: Sl. # Tag No. Description 1. 68-HSO-1526 Burner start 2. 68-HSC-1527 Burner stop 3. 68-HS-1528 Reset button 4. 68-HS-1524 Emergency shutdown 5. 68-HSR-1529 Local/Remote selector 6. 68-HS-1530 Lamp test button 7. 68-XL-1541 Burner firing lamp 8. 68-XL-1542 Burner shutdown lamp Control valve/ON-OFF valve details are tabulated below: Sl. # Tag No. Description 1. 68-XV-1528 Main gas shut off valve-1 2. 68-XV-1529 Main gas shut off valve-2 3. 68-XV-1530 Main gas vent valve 4. 68-XV-1531 Pilot gas shut off valve-1 5. 68-XV-1532 Pilot gas shut off valve-2 6. 68-XV-1533 Pilot gas vent valve EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 247 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Tag No. Description 7. 68-FV-1525 Fuel gas control valve 8. 68-FV-1524 Flue gas recirculation damper 9. 68-FV-1526 Combustion air damper Burner start can be done from HMI, Local panel and DCS. DCS start is active only in remote mode and start on HMI or local panel is active in local mode. Burner Consent to Start: The start of the burner is allowed only if all the following consents are set: • Burner is OFF • Combustion Air fan (6848-K-02A) is running • Flue gas recirculation fan (6848-K-03A) is running (If enabled) • Below mentioned burner Shutdowns are not present Sl. # 1. Tag No./Alarm Description 1. 68-PAHH-1528A/B/C Combustion chamber pressure high-high 2. 68-LALL-1523A/B/C Boiler level low-low 3. 68-LAHH-1523A/B/C Boiler level high-high 4. 68-PAHH-1522A/B/C Saturated steam pressure high-high 5. 68-PALL-1525A/B/C Upstream burner gas pressure low-low 6. 68-PAHH-1526A/B/C Downstream burner gas pressure high-high 7. 68-FALL-1526B/C/D Combustion air flow low-low 8. 68-FAHH-1525B/C/D Natural gas flow High-High 9. 68-PALL-1527A/B/C Instrument air pressure low-low 10. 68-HS-1523 ESD from boiler control panel 11. 68-HS-1524 ESD from boiler local control panel 12. 68-HS-1525 Emergency shutdown 13. 68-ZI-1548 Forced draft fan not running 14. 68-XS-1327 Emergency shutdown from ESD 15. NA Burner main, pilot shutoff and vent valves discrepancies The burner can be started only manually by the operator from LCP or DCS. The following permissives for burner start-up are to be satisfied. a. The burner is off. The burner is not already “STARTING” or “ON”. b. Burner shutdown alarms are not present. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 248 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL c. Combustion Air Fan 6848-K-02A is running. d. Flue Gas Recirculation Fan 6848-K-03A is running. (If flue gas recirculation control is enabled). 2. Select “LOCAL” in the Local Burner Panel. 3. Press the “START” push button HSO-1526 from the Local Burner Panel. 4. Set the minimum opening for the air flow control damper 68-FV-1526 from the LBP for purge. 5. Ensure that the air purge is done for 5 minutes. 6. After air purge is done ensure that the damper FV-1526 opening is decreased to the burner light off threshold. 7. If flue gas recirculation controller is enabled, set the opening for the flue gas recirculation damper FV-1524. 8. Ensure that the flue gas recirculation damper 68-FV-1524 is open. 9. Ensure that the flue gas recirculation purge is done for 1 minute. 10. After flue gas purge is done ensure that the damper 68-FV-1524 is decreased to the burner light off threshold. 11. After 2 seconds of the PURGE VALID signal given by BMS, ensure that the burner ignition transformer is powered. 12. After 2 seconds of powering of the transformer, ensure the burner igniter vent valve 68-XV-1533 is closed and opens the burner igniter shut-off valves 68-XV-1531 and 68-XV-1532. 13. Ensure that after 5 seconds, the burner ignition transformer is powered off. 14. Ensure that the flame is detected by the flame scanner 68-BE-1523. 15. If flame is detected, ensure ‘Pilot On’ indication is available in LBP. 16. If the flame scanner 68-BE-1523 does not detect the flame, ensure that the burner restart is attempted automatically after 1 minute without purging the combustion chamber again. Note: The system can try the restart for 3 times. If flame is not detected again, the shutdown of the burner is started and purge valid signal is reset. 17. When the pilot ignition is successful, ensure that the main burner vent valve 68-XV1530 is closed and the main shut-off valves 68-XV-1528 and 68-XV-1529 are opened. 18. After 5 seconds for flame stabilization, the pilot vent valve 68-XV-1533 is opened and the pilot shut off valves 68-XV-1531 and 68-XV-1532 are closed. 19. Ensure that the flame scanners 68-BE-1522A & 68-BE-1522B detect flame. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 26 - Burner Management Sequence for Steam Generation Package Rev.: 0 Date: 03/09/212 Page: 249 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 250 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL /212 5.15.6 Boiler Normal Start-up 1. Raise the furnace Temperature gradually as per the Vendor IOM. 2. Operate the Boiler as per the Vendor IOM. 3. When the Drum Pressure reaches 1.5 barg (Hot) tighten the Drums bolts/nuts. 4. Steam Trap line-up: • Ensure that the steam flow through the trap bypass line. • Open the steam trap down steam valve. • Open the steam trap upstream valve. • Close the bypass valve. 5. Observe and monitor the parameters: • Fuel Gas Flow/Pressure • Combustion Air flow • Furnace Pressure • FD Fan Discharge Pressure • Drum Level/Pressure • Main Steam line Pressure 6. Check for Boilers expansions, if any. 7. Ensure that the Main Steam line distribution headers, all vents and drains are opened. 8. Check the furnace for flue gas leakages, if any. 9. Gradually increase the Drum pressure by throttling the start-up vent valve 68-PV-1523. 10. Ensure that the Drum level is maintained. 11. Gradually raise the air flow and fuel gas flow to increase the Drum pressure. 12. Check and confirm that the expansion of the Boiler at various locations is as per the design values. 13. Collect the Boiler water sample periodically and analyse the sample in lab for oil traces. 14. When the Drum Pressure reaches 5 barg, gradually open the Main Steam line MOV-1522 and crack open the downstream isolation valve to warm up the main steam line Header. 15. Line up all the steam traps along the main header and open the drain valves fully in the steam traps and drain all the condensate from the header. / EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 251 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL /212 16. Keep open the traps drain valves till superheated steam comes out of the drain lines. 17. When the superheated steam is noticed close the steam trap drain valves one by one and line up the steam traps to the condensate header. 18. Ensure that the condensate header is already warmed up. 19. When the steam header is warmed up, close all the drains and vents and open the MOV-1522 downstream isolation valve fully and charge the header. 20. Gradually increase the header pressure to the normal operating pressure. 21. Take all the controls in auto. 22. Open the continuous blow down valve and give blow down as necessary. 23. Line up Complex Product Injection pump 6834-P-41A/B and start dosing the chemical as per requirement. 5.15.7 Start-up from Cold Condition (Manual Mode) “Start-up from cold condition” refers to the boiler that is being started at atmospheric pressure and ambient temperature. While starting the Boiler on Cold conditions, the following also has to be verified: • Economizer manual vent valves are closed • Boiler and Economizer manual drain valves are closed • Desuperheater 6848-X-03A Boiler Feed water control valve 68-TV-1522 is closed as it is not necessary to use the Desuperheater 6848-X-03A during initial start-up as the first steam produced is still “cold” • Motorized main steam stop valve and relevant motorized by-pass valve are completely closed. Before lighting any burner the Forced Draft Fan 6848-K-02A and the Flue Gas Recirculation Fan 6848-K-03A are to be started in order to allow the system to be ready to initiate the boiler purging and also the fuel gas lines leakage test. Provided that all detailed sequences and controls as described in BMS Controls are satisfied, it is necessary to wait for a sufficient time to completely purge all boiler flue gas passages. Light up the first burner according to the operating sequence described on BMS controls. The boiler thermal heat input introduced through the burner must be maintained at boiler minimum load. / EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 252 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL /212 When saturated steam starts to exit from vents installed on the saturated steam line (this means that boiler pressure is slightly higher than atmospheric pressure) the vent valve installed on the saturated steam line to be closed to increase the Boiler pressure. During start-up, the boiler pressurisation curve (that is, saturated pressure and saturated temperature vs. time) shown in the following figure “Boiler start-up curve” to be followed for pressurisation. To follow the burner should be operated at minimum allowable firing rate and if necessary the burner should be shut down and subsequently (after purging time) started up. Note: Faster start-up can cause serious damages to boiler. In order to comply with boiler pressurisation limit curve shown on following figure the burner can be lighted off/lighted on, as long as necessary. During boiler pressurisation, do not exceed the following limitations: • 30°C/h: from ambient temperature up to about 130°C (2 barg steam pressure) • 55°C/h: from 2 barg steam pressure till to MCR operating pressure During the boiler heating ramp, when adequate steam pressure is reached the burner load/fuel heat input can be increased from its minimum, but in any case the boiler pressurisation curve shall be correctly followed. When adequate steam flow rate is reached, the Boiler Feed Water to Desuperheater 6848-X-03A is lined up. / EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 253 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL /212 Fig. 27 - Burner Management Sequence for Steam Generation Package / EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 254 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL /212 5.15.8 Start-up from Hot Condition If the steam generator is in “hot" condition (that is, the boiler is close to the value of operating pressure/temperature, condition that practically occurs immediately after or a few hours after a boiler trip) the following conditions often exist: • Main steam stop valve 68-MOV-1522 and its by-pass valve are closed • Actuated start-up vent valve 68-PV-1523 is closed Before starting the boiler again, Operator shall check the existing differential pressure between Steam Drum 6848-V-02A pressure and steam header downstream of main steam stop valve pressure. When the two pressures are equalised then steam from Steam Drum can be lined up to the header. After opening the actuated start-up steam vent valve the burner is started at minimum firing conditions. The Boiler pressure slowly increases. When the pressure increases above the header pressure, the produced steam from Steam Drum can be lined up to the steam network through the motorised main steam shut off valve 68-MOV-1522. If the steam network grid pressure is higher than the boiler pressure, the motorised steam shut off valve 68-MOV-1522 should remain closed. In case steam network grid pressure is lower than the Boiler pressure and main stop valve is closed, then the bypass valve is crack opened to pressurise the network grid. At the end of this pressurisation activity, when the network grid pressure is equal or a little bit lower than boiler pressure (approx 0,5 bar), the motorised main steam stop valve shall be fully opened by Operator. After that, the actuated start-up vent valve shall be gradually closed. During this transfer, the firing rate shall be maintained constant. Then the firing ramp can be started. It is strongly recommended during boiler ramping, do not exceed the following limitations: • 5.15.9 / 55°C/h: from 2 barg steam pressure to MCR operating pressure Going On Line • Once the Boiler has reached the operating pressure, the main shut off steam valve can be opened completely (provided that downstream steam network grid is warmed up and ready to take the boiler steam). The start-up vent valve can now be closed. • When this transfer is completed and the alignment between Steam Generator and steam network grid line has been stabilised, the Boiler load can be increased from minimum load. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 255 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL /212 5.16 • When the Boiler is stabilized, the Steam Pressure Controller 68-PIC-1819 can be put in AUTO. • The Steam Pressure Controller 68-PIC-1819 varies the firing rate of the fuel gas according to the pressure set point. • The entire system should be kept under close surveillance until full load operating conditions are achieved. There is always the possibility of a defect in the safety cut outs. • The operation of burner and the flame pattern shall be closely monitored during start-up phase. • Two scanners are installed on each burner so to reveal the flame presence. The flame pattern must be checked directly on field by Operator through the peepholes installed on each burner and in the rear furnace wall. • The flame pattern shall be set in order to have a good flame, without furnace tube impingement and achieving minimum unburned emissions (basically CO content on flue gases). • Operator shall verify that the combustion takes place correctly, monitoring the flame pattern. LEAK CHECKING OF SYSTEMS Leak checking of process systems to be done after maintenance of equipment or break open of piping flanges for repair/maintenance works. Preparation: Ensure that the following activities are completed: • Relevant Work Permit have been filled up and signed • The system is reinstated as per P&IDs • Pressurising manifold with suitable PSV and pressure gauge will be used. Leak Check: Leak check shall be done as below: / • Isolate the process system, using the available block valves • Close all vent and drains • Prepare a list of flanges and other critical locations to be checked. • Connect an air hose preferably from the plant air header or otherwise from a temporary compressor discharge manifold through temporary hoses. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 256 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL /212 5.17 • Pressurise the system step by step and hold the pressure at 25%, 50%, 75% and operating pressure and carry out a thorough leak check of all the listed flanges and other systems using tape and soap solution. Attend to leaks, if any after depressurisation. • Repeat the above procedure till there is no leak identified • Hold the pressure for 30 minutes and record the pressure loss. If the pressure loss is less than 0.05 bar/hr, the system will be considered to be leak free. PURGING Purging of process lines and equipments with Nitrogen is to be carried out prior to introduction of acid gases into the process system. Process System and piping which contains acid gases are Nitrogen purged using an approved inerting procedure. A. Pre-requisite for Nitrogen Purging 1. Verify portable radios are available for communication. 2. Verify that all-loose materials and tools have been cleaned up prior to nitrogen purging. 3. Obtain Oxygen monitors for testing Oxygen concentration during purging. 4. Verify that all personnel are appropriately equipped with required PPEs including hard hats, goggles, earplugs and gas monitoring equipment. 5. Prior to initiating purge, a toolbox talk shall be held for the personnel regarding the purging and the hazards of Nitrogen gas. B. Preparation 1. Risk assessment shall be done prior to purging of each system. 2. System shall be marked and identified in the P&ID. Also the point used for purging will be marked in P&ID. 3. The PI and PGs in the system will be used for monitoring the system pressure. 4. Pressure test with nitrogen is carried along with the nitrogen purging. 5. Depressurisation points shall be chosen such that the whole system is depressurised and no pressure is trapped downstream of check valves. C. Purging Procedure for Vessels & Equipment 1. Purging of Process Systems is critical for a safe start-up of the facility. / 2. Purging is accomplished by using Nitrogen. 3. While carrying out the vessels and equipment purging ensure vents and pressure taps such as gauge glass, level control bridles, spare pumps, etc., are properly purged. Purging and testing should be continued until Oxygen content is less than 2%. A sample is taken in each case from the system being purged at the purge EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 257 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL /212 pressure and passed through an Oxygen monitor, which reads directly in percent Oxygen. / 4. Consider each line and piece of equipment to assure complete purging of air. Purge interconnecting piping systematically to avoid leaving air pockets in these systems. Ensure that all appropriate valves are open or closed as required. Particular attention should be given to block the valves located at the upstream of relief valves. 5. If proper tapings are not available, arrange necessary flanged nipples to fix Nitrogen hose or to make purge outlet. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 258 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION VI START-UP OF PLANT EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 259 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.1 GENERAL The start-up procedure of the SRU depends on the exact situation of the unit at any particular point of time. The various cases are: • Start-up after a major turnaround shutdown • Start-up after an emergency shutdown, where the unit is ready to be taken on stream immediately When starting the unit after a shutdown, only the relevant procedures are followed depending on the status of the various sections of the unit and nature of jobs carried out. All safety precautions as per the safety rules and regulations are followed while taking over and starting up of any equipment or section of the unit. There are standard procedures to be followed as per the QP safety manuals for inspection, followed by accepting/deblinding any equipment before taking in line. Smooth start-up will depend to a larger degree on how well the unit is checked prior to start-up. In a major turnaround shutdown, all vessel internals are inspected, and if there are any modifications to be carried out, it is completed and the vessels boxed up. All safety items should be checked before, during and after start-up to ensure safe and stable operation. During start-up, the operating conditions of each unit must be adjusted to bring the product specifications in line with the design values. During the period of off-spec product it should be vented to flare system as far as possible to meet the required specification. Prior planning of various start-up activities can eliminate delay and improve the safety of personnel and equipment. 6.2 START-UP SEQUENCE It will be necessary to start-up all or section of the plant after shutting down plant for various reasons viz.; mechanical repair, repair of critical equipments/pipeline leaks, utilities failure or any operating problem. The process plants are to be started in the following sequence: 1. Incinerator 2. Acid Gas Enrichment Unit 3. Sulphur Recovery Unit 4. Tail Gas Treatment Unit EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 260 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3 START-UP OF PROCESS 6.3.1 Start-up of Incinerator 9101-F-14 Start-up of the Incinerator involves the following activities: 1. Purging of the system and pilot ignition 2. Main burner ignition, heat-up and introduction of Tail gases. 6.3.1.1 Purging Of the System and Pilot Ignition a. Pre-requisites 1. Air inlets, burner and incinerator/stack passages are in good condition and free of foreign material. 2. All personnel have been evacuated from the Incinerator, duct work, associated equipment and all access and inspection doors closed and sealed. 3. Blower VFD’s are operated through full range to check the blower response. 4. All safety shut off valves in fuel gas lines are closed. 5. Fuel system vents are open and venting properly to atmosphere. Lines are properly drained and cleared of condensate. 6. A complete functional check of the safety interlocks has been made after any overhaul or other significant maintenance. 7. The area is clear of obvious safety hazards and flammable gases are not present in the area. 8. All lines have been blown down with plant air to ensure they are free of debris that might plug metering orifices and burner tips. 9. Utilities (fuel gas, instrument air and plant air) are established and initial operational checks performed on the elements in each line. 10. Burner elements and pilot are in their proper position in accordance with specifications shown in the burner assembly and pilot drawings. 11. Power has been supplied to control systems and to safety interlocks. 12. Meters or gauges indicating fuel header pressure to the unit are functional. 13. Ensure that the following Pressure self regulating valves are set according to the instrument data sheets. • Pilot gas supply PCV-1155 set at 0.7 barg • Pilot air supply PCV-1164 set at 0.7 barg 14. Isolation valves for all pressure gauges and pressure transmitters are open and their respective bleed valves are closed. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 261 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 15. Purge air has been established for the sight ports and flame scanners. Flame scanners have clear lenses and the scanner isolation ball valves are open. b. Local Control Panel Incinerator is equipped with a Local Control Panel 9101-F-14-LP-001. This panel is used for the start-up of the Incinerator System. The LCP is supplied with the following indications: Tag No. Description Colour 91-XL-1173 System Ready for Purge Green 91-XL-1174 Purge in Progress Green 91-XL-1175 Purge Complete Green 91-XL-1176 Pilot Flame On Green 91-XL-1177 Main Burner On Green 91-XA-1178 Common Alarm Red 91-XL-1180 BE-1155A Flame Detected Green 91-XL-1181 BE-1155B Flame Detected Green 91-XL-1182 BE-1155C Flame Detected Green 91-HS-1162 Reset Black 91-HS-1163 Start Purge Black 91-HS-1164 Start Pilot Black 91-HS-1165 Start Burner Black 91-HS-1166 Normal Stop Black 91-HS-1167 Emergency Shutdown Red – Mushroom Head 91-HS-1168 Lamp Test Black Control valve and ON-OFF valve details are tabulated below: Sl. # Tag No. Description 1. 91-XV-1155 Fuel gas upstream block valve 2. 91-XV-1156 Fuel gas vent valve 3. 91-XV-1157 Fuel gas downstream block valve 4. 91-XV-1158 Pilot gas upstream block valve 5. 91-XV-1159 Pilot gas vent valve 6. 91-XV-1160 Pilot gas downstream block valve 7. 91-XV-1161 Instrument air block valve 8. 91-XV-1162 Pilot air block valve 9. 91-FV-1155 Fuel gas control valve EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 262 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Prior to the start-up of the Incinerator ensure the following: • BMS (PLC-UCP) is powered up • Signal 91-XS-1170 to force fuel gas flow rate controller 91-FIC-1155 to 0% output is present. • Signal 91-XS-1171 to force combustion air flow rate controller 91-FIC-1156 to 100% output is absent. • Fuel gas control valve 91-FV-1155 at minimum stop position. • Fuel gas upstream (91-XV-1155) and downstream (91-XV-1157) is closed. • Fuel gas vent valve (91-XV-1156) is opened. • Pilot gas upstream (91-XV-1158) and downstream (91-XV-1160) is closed. • Pilot gas vent valve (91-XV-1159) is opened. • Instrument air block valve (91-XV-1161) is closed. • Pilot air block valve (91-XV-1162) is closed. Note: Press lamp test switch 91-HS-1168 on the local panel and ensure all the lamps are working. c. Purge Cycle Prior to the ignition of any burner it is important to purge the Incinerator with fresh air which will sweep away any combustible that may have accumulated in the system. Start-up of Blowers: • Select Local on the local/remote selector switch 9101-RCU-KM-12A/B • Force VFD (9101-K-12A/B) to minimum speed from the DCS • Press motor start switch in 9101-RCU-KM-12A/B • Open the O/L damper 1. Ensure the following BMS Shutdown alarm conditions in Incinerator are normal: Tag No. Description 91-XS-1185 Remote ESD signal 91-HS-1167 Local ESD (PB on LCP) 91-FALL-1156B Combustion Air flow low low alarm 91-PALL-1155 Fuel gas pressure low low alarm 91-PALL-1156 Fuel gas pressure low low alarm 91-PAHH-1156 Fuel gas pressure high high alarm 91-BSLL-1155 Flame fail (2oo3) alarm 91-TAHH-1160 Incinerator Temperature high high alarm EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 263 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Note: During start-up, the discrepancy alarms of BMS ON/OFF valves trips the Incinerator. 2. Ensure that the following permissives to start the purge are available: Tag No. Description Position/Status 91-BSL-1155A Flame Scanner Switch Not energized (No flame) 91-BSL-1155B Flame Scanner Switch Not energized (No flame) 91-BSL-1155C Flame Scanner Switch Not energized (No flame) 91-BSL-1156 Flame Rod Switch Not energized (No flame) 91-ZSL-1155 Fuel Gas Control valve Valve at low-fire position 91-ZSC-1155 Fuel Gas upstream block valve Valve closed 91-ZSO-1156 Fuel Gas vent valve Valve open 91-ZSC-1157 Fuel Gas downstream block valve Valve closed 91-ZSC-1158 Pilot Fuel Gas upstream block valve Valve closed 91-ZSO-1159 Pilot Fuel Gas vent valve Valve open 91-ZSC-1160 Pilot Fuel Gas downstream block valve Valve closed 3. If purge permissives are met, ensure that the System Ready for Purge lamp 91-XL1173 on LCP is lit. 4. Press ‘START PURGE’ pushbutton 91-HS-1163 from LCP 9101-F14-LP-001. 5. Ensure that the force signal (91-XS-1171) to FIC-1156 is energized and forces the flow controller FIC-1156 to manual mode with 100% output. 6. Ensure that the shut off valves 91-XV-1161 & 91-XV-1162 are opened and air is supplied to the pilot and purge air to the flame scanners. 7. Ensure that the combustion air flow measured by 91-FT-1156C indicates a flow of >45500 Sm3/hr. 8. Ensure that the ‘PURGE IN PROGRESS’ lamp 91-XL-1174 on LCP is lit. 9. Ensure purging is completed in 5 minutes. 10. Ensure that ‘PURGE COMPLETE’ lamp 91-XL-1175 on the LCP is lit. 11. At the end of 5 minutes, the forcing signal 91-XS-1171 is de-energised allowing FIC-1156 to return to automatic mode, since no fuel gas is flowing to the burner at this point the output to the VFD is at its minimum, 11106 Sm3/hr. 12. Ensure that this condition exists for another 5 minutes. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 264 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL d. Pilot Ignition 1. Ensure that there are no alarms present in the UCP (BMS). 2. Ensure that the above listed permissives are met. 3. Press ‘START PILOT’ push button 91-HS-1164 from LCP. 4. Ensure that ‘PURGE COMPLETE’ indication is no more present. 5. Ensure that the pilot vent valve 91-XV-1159 is closed. 6. Ensure that the pilot block valves 91-XV-1158 & 91-XV-1160 are opened after receiving the CLOSE feedback 91-ZSC-1159 of the vent valve 91-XV-1159. 7. Ensure that the ignition transformer 91-XS-1183 is energised. 8. Ensure that after 10 seconds, ignition transformer 91-XS-1183 is de-energised. 9. Ensure that after 10 seconds, if pilot is ON, the flame is detected by the Pilot Flame Rod 91-BE-1156. 10. Ensure that the ‘PILOT FLAME ON’ lamp 91-XL-1176 on the LCP is lit. 11. Ensure that pilot stabilisation timer of 60 seconds is completed from UCP HMI. 12. If no pilot flame is detected by the flame rod, ensure that after 10 seconds, SRU tail gas Incinerator is tripped. 13. Ensure that the COMMON ALARM lamp 91-XA-1178 is lit. 14. Check the DCS/UCP for the first out alarm condition. 15. Clear the alarm condition. 16. RESET the system by pressing the RESET push button 91-HS-1162 from LCP. 17. Restart the system from the beginning. 18. If a flame is detected by 91-BE-1156 at the end of the 10 second trial period, then the second pilot flame stabilization timer will be started. 6.3.1.2 Main Burner Ignition, Heat-up and Introduction of Tail Gases 1. After pilot stabilisation timer of 60 seconds is completed, press ‘START BURNER’ pushbutton 91-HS-1165 on LCP 9101-F14-LP-001. 2. Ensure that fuel gas vent valve 91-XV-1156 is closed. 3. Ensure that the vent valve closing feedback is received from the limit switch 91-ZSC-1156. 4. Ensure that the fuel gas block valves 91-XV-1155 & 91-XV-1157 are opened. 5. Ensure that the burner fuel gas control valve 91-FV-1155 is at its minimum stop position. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 265 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6. Ensure that in a 10 second trial for ignition period, the burner main flame is detected by 2oo3 voting of flame scanners 91-BE-1155A, 91-BE-1155B & 91-BE1155C. 7. Ensure that the ‘MAIN BURNER ON’ lamp 91-XA-1178 is lit in LCP. 8. If no pilot flame is detected by the flame scanners, ensure that after 10 seconds, SRU tail gas Incinerator is tripped. 9. Ensure that the COMMON ALARM lamp 91-XA-1178 is lit. 10. Check the DCS/UCP for the first out alarm condition. 11. Clear the alarm condition. 12. RESET the system by pressing the RESET push button 91-HS-1162 from LCP. 13. Restart the system from the beginning. 14. Ensure that if the main flame is confirmed at the end of the main burner trial-forignition period, then a 60 second low fire timer in the BMS is automatically started. 15. Ensure at the end of the 60 second low fire period, the BMS stops sending the forcing signal 91-XS-1170 to the DCS. 16. Increase slowly the set point of 91-TIC-1155 so that the temperature of the incinerator does not rise faster than 50°C per hour, until the normal operating temperature of 817°C is reached. 17. Ensure that at 817°C the pilot is turned off. 18. Ensure that 91-XV-1158 & 91-XV-1160 are closed. 19. Ensure that 91-XV-1159 is opened. 20. Ensure that 91-XV-1162 is closed. 21. Ensure that there is a flow of 4.6 Sm3/hr. of purge cooling air through a restriction orifice RO-1155 to the pilot around 91-XV-1162. 22. To introduce tail gases ensure that the system is in operation with no alarm condition. 23. Ensure that the Incinerator temperature at 91-TE-1156 is greater than or equal to 817°C. 24. Now the system is ready for introduction of tail gases. 25. The flow of waste gases can be started and stopped in any order. However the waste gases should be introduced one at a time to the Incinerator. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 266 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 28 - Incinerator Burner Start-up Flow Chart EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 267 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.2 Start-Up of Acid Gas Enrichment Unit Pre-requisites • Preparation of Antifoam • Preparation of Corrosion Inhibitor • Preparation of Amine Solution 6.3.2.1 Preparation of Antifoam 1. Ensure that the Antifoam Injection Pumps 9103-P-16A/B and the Agitator 9103-M12 are energised in MCC. 2. Ensure that the Antifoam Storage Tank 9103-T-12 is cleaned internally. 3. Ensure that all the drain and vent valves in the package are closed. 4. Introduce minimum flow of Nitrogen to the Antifoam Storage Tank and read the flow through the flow indicator 91-FI-1537. 5. Procure the Antifoam drums to the site and place it near the unloading pumps 9103-P-19A/B. 6. Connect the drums to the unloading pumps through flexible hose. 7. Start the unloading pumps and transfer antifoam to the tank. 8. Ensure that the low low level trip 91-LALL-1520 & low level alarm 91-LAL-1521 are cancelled while making up the solution. 9. Ensure the level in the tank from 91-LG-1510 and 91-LT-1521 and ensure the tank does not overflow. 10. Start agitator 9103-M-12 from the local panel to mix the solution thoroughly. 6.3.2.2 Lining up of Antifoam Injection Pumps 9103-P-16A/B 1. Ensure that the Antifoam Injection pumps 9103-P-16A/B suction strainer elements are fixed and boxed up. 2. Ensure that the Antifoam Injection Pumps 9103-P-16A/B discharge PSVs 91-PSV1602/1603 are lined up. 3. Open the Antifoam Storage Tank outlet isolation valve to the injection pumps and fill the lines with the antifoam solution. 4. Open the discharge isolation valve of the Antifoam Injection Pump 9103-P-16A. 5. Open the common discharge isolation valve of the Antifoam Injection Pumps 9103P-16A/B. 6. Select the LOR switch of the Antifoam Injection Pump 9103-P-16A in Local. 7. Start the Antifoam Injection Pump 9103-P-16A from local control station. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 268 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 8. Ensure that the Antifoam Injection Pump 9103-P-16A is developing pressure by checking the discharge pressure transmitter 91-PT-1559. 9. Stop the pump and keep the Antifoam Injection Pump 9103-P-16A ready for dosing. 10. Repeat the above procedure for Antifoam Injection Pump 9103-P-16B and keep it ready. 11. Line up Antifoam to the Acid Gas Amine Absorber 9103-C-11 or Amine Regenerator 9103-C-12 as required. 6.3.2.3 Preparation of Corrosion Inhibitor 1. Ensure that the Corrosion Inhibitor Injection Pumps 9103-P-101A/B and the Agitator 9103-M-13 are energised in MCC. 2. Ensure that the Corrosion Inhibitor Storage Tank 9103-T-13 is cleaned internally. 3. Ensure that all the drain and vent valves in the package are closed. 4. Transport the Corrosion Inhibitor drums to the site and place it near the unloading pumps 9103-P-102. 5. Connect the drums to the unloading pumps through unloading hose. 6. Start the unloading pumps and transfer Corrosion Inhibitor to the tank. 7. Ensure that the low low level trip 91-LALL-1522 is cancelled while making up the solution. 8. Ensure the level in the tank from 91-LG-1511 and 91-LT-1523 and ensure the tank does not overflow. 9. Start agitator 9103-M-13 from the local panel to mix the solution thoroughly. 10. Keep the Corrosion Inhibitor Injection Pumps 9103-P-101A/B ready for dosing. 6.3.2.4 Lining up of Corrosion Inhibitor Injection Pumps 9103-P-101A/B 1. Ensure that the Corrosion Inhibitor Injection pumps 9103-P-101A/B suction strainer elements are fixed and boxed up. 2. Ensure that the Corrosion Inhibitor Injection Pumps 9103-P-101A/B discharge PSVs PSV-1504/1505 are lined up. 3. Open the Corrosion Inhibitor Storage Tank outlet isolation valve to the injection pumps and fill the lines with the Corrosion Inhibitor solution. 4. Open the discharge isolation valve of the Corrosion Inhibitor Injection Pump 9103P-101A. 5. Open the common discharge isolation valve of the Corrosion Inhibitor Injection Pumps 9103-P-101A/B. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 269 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6. Put the stroke length of the Corrosion Inhibitor Injection Pump 9103-P-101A at minimum position. 7. Keep the LOR switch of the Corrosion Inhibitor Injection Pump 9103-P-101A in ‘Local’. 8. Start the Corrosion Inhibitor Injection Pump 9103-P-101A from local control station. 9. Ensure that the Corrosion Inhibitor Injection Pump 9103-P-101A is developing pressure by checking the discharge pressure transmitter 91-PT-1561. 10. Stop the pump and keep the Corrosion Inhibitor Injection Pump 9103-P-101A ready for dosing. 11. Repeat the above procedure for Corrosion Inhibitor Injection Pump 9103-P-101B and keep it ready. 12. Line up Corrosion Inhibitor to the Acid Gas Amine Absorber 9103-C-11 or Amine Regenerator 9103-C-12 as required. 6.3.2.5 Filling Amine Surge Tank 9103-T-11 with Dow Ucarsol HS-103 (Amine Solution) 1. Ensure that the Amine Surge Tank 9103-T-11 internals are clean and the man ways are boxed up. 2. Ensure that the following valves are closed. a. Lean Amine from Lean Amine Trim Cooler 9103-E-15 to the Tank 9103-T-11. b. Amine from Amine Filters 9103-S-11/12/13 to the Tank 9103-T-11. c. DM Water line to the Tank 9103-T-11. d. Lean Amine Pump 9103-P-13A/B minimum flow line isolation valves to the Tank 9103-T-11. e. Lean Amine from Tank 9103-T-11 to Lean Amine Pump 9103-P-13A/B isolation valve. f. Hydrocarbon skimming facility isolation valves. g. PSV-1513/1517/1518 outlet header isolation valve to the Tank 9103-T-11. 3. Ensure that the drain and vent valves of the Tank 9103-T-11 are isolated. 4. Ensure that the Tank PVRV-1521/PVRV-1522 upstream isolation valves are lined up. 5. Ensure that the Amine Surge Tank 9103-T-11 is purged with Nitrogen. 6. Line up tank vent valve 91-PV-1526B upstream isolation valve and take the control valve in Remote. 7. Take the pressure controller 91-PIC-1526 in Auto with a set point of 0.02 barg. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 270 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 8. Line up the Nitrogen supply line to the tank isolation valves and take the control valve 91-PV-1526A in Remote. 9. Ensure that all the instruments in the Amine Surge Tank 9103-T-11 are lined up. 10. Receive the road tanker containing amine solution and place it near the Amine Surge Tank 9103-T-11 filling station. 11. Connect a 2” flexible metallic hose to the road tanker unloading line. 12. Connect the other end of the flexible metallic hose to the suction of the Amine Unloading Pump 9103-P-18. 13. Ensure that the amine unloading pump suction strainer element is in place. 14. Connect the discharge of the amine unloading pump 9103-P-18 to the loading line 2”-9103-M-141-A189 of the Amine Surge Tank 9103-T-11 with a flexible metallic hose. 15. Connect plant air to the pneumatic amine unloading pump 9103-P-18. 16. Ensure that the air vent valve (if any) of the pneumatic pump is open. 17. Open the amine loading line isolation valves of the Amine Surge Tank 9103-T-11. 18. Open the road tanker unloading line isolation valve slowly and fill the metallic hose. 19. Start the Amine Unloading Pump 9103-P-18 by supplying plant air, and start to load the amine into the Amine Surge Tank 9103-T-11. 20. Ensure that low low level trip 91-LT-1511 (1000 mm) is cancelled in ICSS. 21. Ensure that the low level alarm 91-LAL-1512 (1150 mm) is cancelled as the level rises. 22. Monitor 91-LT-1512 and build the level up to 40% in the Amine Surge Tank 9103-T-11. 23. Stop pumping amine into the Amine Surge Tank 9103-T-11. 24. Close the tanker outlet valve and the Amine Surge Tank 9103-T-11 amine make up line isolation valves. 25. Drain amine from all the transfer lines and the metallic hoses and remove the metallic hoses. 26. Find the quantity of amine pumped into the Amine Surge Tank 9103-T-11. 27. If the added amine is 100% in concentration then DM water is to be added to dilute the solution to 50%. 28. Open DM water make up to the Tank and fill DM water by observing the flow through the flow gauge 91-FI-1529 in the DM water line equivalent to the Amine quantity. 29. The concentration of the solution in the Tank now is 50%. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 271 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 30. Collect a sample of the Amine solution and send it to laboratory for analysing the concentration. 31. When the sample concentration is given by the lab, necessary correction may be carried out to make the concentration of 50% amine. 32. Now the amine solution at 50% concentration is ready to be transferred to the AGEU and TGTU. 33. Ensure that the tank is blanketed by Nitrogen by checking through the pressure transmitter 91-PT-1526. 6.3.2.6 Transfer of Amine from Amine Surge Tank 9103-T-11 to Acid Gas Amine Absorber 9103-C-11 1. Ensure that the Amine absorption section is under nitrogen pressure. 2. Ensure that the drain and vent isolation valves are closed in the Lean Amine Pumps 9103-P-13A/B suction and discharge lines. 3. Ensure that the H2S Analyzer 91-AI-1506 from Lean Amine Cooler 9103-E-14 outlet line joining the suction of the Lean Amine Pump 9103-P-13A/B isolation valve is closed. 4. Open the Amine Surge Tank 9103-T-11 outlet line to Lean Amine Pump 9103-P13A/B isolation valve and fill up the line with amine. 5. Open the suction isolation valves of the Lean Amine Pumps 9103-P-13A/B and fill the pumps by opening the casing vent valves. 6. Ensure that the Lean Amine from the Lean Amine Pumps 9103-P-13A/B discharge to the Tail Gas Amine Absorber 9103-C-12 is closed. 7. Ensure that the Lean Amine from the Lean Amine Pumps 9103-P-13A/B discharge to the Lean Amine Filter 9103-S-11/12/13 isolation valve is closed. 8. Put the LOR switch position to “Local” position. 9. Ensure that the Lean Amine Pumps 9103-P-13A/B are energized. 10. Reset PSD (Process Shut Down) from ICSS. 11. Ensure that Lean amine to Acid Gas Amine Absorber 9103-C-11 inlet ON-OFF valve 91-XV-1504 is opened. 12. Line up Lean Amine to Acid Gas Amine Absorber 9103-C-11 flow controller 91-FV-1501 isolation valves and close the bypass valve. Close the control valve 91-FV-1501 fully in manual. 13. Ensure that all the drain valves in the lean amine line to the Acid Gas Amine Absorber 9103-C-11 are closed. 14. Start the Lean Amine Pump 9103-P-13A on minimum flow from local control station. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 272 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 15. Ensure that the minimum flow line isolation valves are opened and the control valve 91-FV-1511 is lined up and the controller 91-FIC-1511 is in AUTO with a set point of 300 m3/hr. 16. Check the discharge pressure is normal at 6.50 barg from the pressure gauge 91-PG-1522. 17. Slowly open the discharge valve of the pump and fill the discharge line. 18. Open the Lean amine to Acid Gas Amine Absorber 9103-C-11 isolation valve and fill the downstream lines. 19. Open the flow control valve 91-FV-1501 slowly and start filling up the Acid Gas Amine Absorber 9103-C-11 with the amine. 20. Ensure that the Acid Gas Rich Amine Pumps 9103-P-12 A/B suction isolation valves are closed. 21. Ensure that the level is increasing in the Acid Gas Amine Absorber 9103-C-11 by checking the level transmitter 91-LT-1505 & level gauge 91-LG-1505A/B/C/D. 22. Ensure that the low low level alarm 91-LALL-1516 is cancelled as the level rises. 23. Ensure that the low level alarm 91-LAL-1506 is cancelled is cancelled as the level rises. 24. When the level reaches 100%, close the flow control valve 91-FV-1501 fully and close the isolation valve at pump discharge which is going to the Acid Gas Amine Absorber 9103-C-11. 6.3.2.7 Filling Lean Amine Filters 9103-S-11/12/13 with Lean Amine Solution 1. Ensure that the Lean Amine Pump 9103-P-13A is running on minimum flow. 2. Ensure that the drain and vent valves in the Lean Amine Filters 9103-S-11/12/13 are closed. 3. Ensure that Lean Amine Filter 9103-S-11 and Fines Filter 9103-S-13 elements are fixed in the respective filter elements. 4. Ensure that the Activated carbon Filter 9103-S-12 is loaded with the media and boxed up. 5. Ensure that the amine from Amine Sump Pump isolation valve is isolated near the filters. 6. Ensure that the upstream and downstream isolation valves of the 91-PSV-1512 are opened, the upstream isolation valve is closed for 91-PSV-1513 and the bypass valve is closed for Lean Amine Filter 9103-S-11. 7. Ensure that the upstream and downstream isolation valves of the 91-PSV-1515 are opened, the upstream isolation valve is closed for 91-PSV-1514 and the bypass valve is closed for Activated Carbon Filter 9103-S-12. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 273 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 8. Ensure that the upstream and downstream isolation valves of the 91-PSV-1517 are opened, the upstream isolation valve is closed for 91-PSV-1516 and the bypass valve is closed for Fines Filter 9103-S-13. 9. Ensure all the instruments in the Lean Amine Filters are lined up. 10. Ensure that the bypass for the Activated Carbon Filter and Fines Filter is closed. 11. Open slowly the Lean Amine Pump 9103-P-13A/B discharge isolation valve to the filters and fill up the lines. 12. Crack open the Lean Amine Filter 9103-S-11 vent valve at the top. 13. Line up the flow control valve 91-FV-1507 and slowly open 91-FV-1507 on manual. 14. Slowly fill up the Lean Amine Filter 9103-S-11 until all the nitrogen is displaced through the vent and the amine just starts to overflow through the vent. 15. Close the vent valve at the top of the Lean Amine Filter 9103-S-11. 16. Crack open the vent valve at the top of the Activated Carbon Filter 9103-S-12. 17. Crack open the inlet isolation valve for the Activated Carbon Filter 9103-S-12 from the Lean Amine Filter 9103-S-11. 18. Fill the vessel with amine by displacing nitrogen through the vent valve at the top. 19. When the amine just starts to overflow through the vent valve, close the valve immediately. 20. Crack open the vent valve of the Fines Filter 9103-S-13 at the top. 21. Crack open the inlet isolation valve for the Fines Filter 9103-S-13 and start filling the vessel with amine. 22. The nitrogen inside the vessel is displaced through the vent and when the amine just starts to overflow through the vent immediately close the vent valve. 23. Open the outlet valve of the Fines Filter 9103-S-13 and fill the line up to the Amine Surge Tank 9103-T-11. 6.3.2.8 Lining up of Lean Amine Filters 9103-S-11/12/13 1. Ensure that the Lean Amine Filter 9103-S-11, Activated Carbon Filter 9103-S-12 and Fines Filter 9103-S-13 are filled with the amine. 2. Open the Lean amine Filters outlet isolation valves and line up the amine to the Amine Surge Tank 9103-T-11. 3. Take Lean Amine Filters inlet control valve 91-FV-1507 in manual and slowly open the control valve so that the amine starts to flow through the amine filters. 4. Slowly open the control valve till the flow measured by 91-FT-1507 reaches 155.6 m3/hr. 5. Put the flow control valve 91-FV-1507 in auto with a set point of 155.6 m3/hr. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 274 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6. Check the pressure drop across the Lean Amine Filter 9103-S-11 and ensure that it is less than 0.7 barg from 91-PDT-1517. 7. Check the pressure drop across the Activated Carbon Filter 9103-S-12 and ensure that it is less than 0.7 barg from 91-PDT-1518. 8. Check the pressure drop across the Fines Filter 9103-S-13 and ensure that it is less than 0.7 barg from 91-PDT-1519. 6.3.2.9 Transfer of Amine from Acid Gas Amine Absorber 9103-C-11 to the Amine Regenerator 9103-C-12 1. Ensure that all the drain valves in the Rich amine line to the Lean/Rich Amine Exchanger 9103-E-11A/B and to the Regenerator 9103-C-12 are closed. 2. Open the suction isolation valves of Acid Gas Rich Amine Pumps 9103-P-12A/B and fill the suction lines. 3. Prime the pumps by opening the casing vent valves of the pumps and releasing Nitrogen. 4. Put the switch position of the Acid Gas Rich Amine Pumps 9103-P-12A/B to ‘LOCAL’ position. 5. Ensure that the Acid Gas Rich Amine Pumps 9103-P-12A/B are energized. 6. Line up the Rich Amine Pump 9103-P-12A minimum flow control valve 91-FV-1508 and open it manually by 50%. 7. Start the Acid Gas Rich Amine Pump 9103-P-12A from local control station on minimum flow. 8. Check the discharge pressure is normal at 7.50 barg from the pressure gauge 91-PG-1536. 9. Ensure that the pump is running without any abnormal noise and vibration. 10. Open the discharge valves of the pump slowly and fill the discharge line and circulate the Rich Amine back to the Acid Gas Amine Absorber 9103-C-11 through the minimum flow line control valve 91-FV-1508. 11. Open the Rich amine to Lean/Rich Exchanger inlet isolation valves 9103-E-11A/B and fill the downstream lines and the exchanger. 12. Open the Lean Rich Exchanger outlet isolation valve and fill the downstream lines up to 91-FV-1520. 13. Take the flow control valve 91-FV-1520 in manual and open the control valve slowly and start taking level in Amine Regenerator 9103-C-12. 14. Ensure that the level is increasing in the Amine Regenerator 9103-C-12 by checking the level transmitter 91-LT-1510 and level gauge 91-1506A/B. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 275 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 15. Ensure that the Amine Regenerator 9103-C-12 low low level alarm 91-LALL-1517 is cancelled as the level rises. 16. Ensure that the Amine Regenerator 9103-C-12 low level alarm 91-LAL-1510 is cancelled as level increases. 17. When the level reaches 50%, close the flow control valve 91-FV-1520 fully and stop the Rich Amine Pump 9103-P-12A from the local control station. 18. Check the level in the Acid Gas Amine Absorber 9103-C-11 and ensure that it does not drop below 50%. 19. If the level drops below 50% in the Acid Gas Amine Absorber 9103-C-11, stop the Acid Gas Rich Amine Pump 9103-P-12A immediately. 20. Start the Lean Amine Pump 9103-P-13A and fill the Acid Gas Amine Absorber 9103-C-11 as mentioned previously. 6.3.2.10 Filling up of Lean Amine Section with Amine 1. Ensure that the drain and vent valves of the Hot Lean Amine Pumps 9103-P-17A/B, lean amine side of the Lean/Rich Exchanger 9103-E-11A/B, Lean Amine Cooler 9103-E-14 and Lean Amine Trim Cooler 9103-E-15 are closed. 2. Ensure that the Amine Regenerator 9103-C-12 is filled with amine upto 50% level. Check the level in 91-LT-1510 and also cross check with 91-LG-1506A/B. 3. Open the Hot Lean Amine Pumps 9103-P-17A/B suction isolation valves slowly and fill the lines and the pumps with amine by opening the casing vent valves of the pumps and by releasing Nitrogen. 4. Ensure that the Hot Lean Amine Pumps 9103-P-17A/B are energized in MCC. 5. Put the LOR switch of the Hot Lean Amine Pumps 9103-P-17A/B to “LOCAL” at local control station. 6. Ensure that the minimum flow line of the Hot Lean Amine Pumps 9103-P-17A/B is lined up and the flow control valve 91-FV-1512 is opened by 20% on manual. 7. Start the Hot Lean Amine Pump 9103-P-17A from local control station. 8. Ensure that the Hot Lean Amine Pump 9103-P-17A discharge pressure is normal at 6.80 barg. 9. Ensure that the Hot Lean Amine Pump 9103-P-17A is pumping amine back to the Amine Regenerator 9103-C-12 through the minimum flow control valve 91-FV-1512. 10. Put the minimum flow control valve 91-FV-1512 in ‘Auto’ with a set point of 250 m3/hr. 11. Ensure that the Hot Lean Amine Pumps 9103-P-17A/B discharge ON-OFF valve 91-XV-1507 is opened. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 276 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 12. Open the Hot Lean Amine Pump 9103-P-17A discharge isolation valve slowly and fill the Lean/Rich Exchanger 9103-E-11A/B inlet strainer and the lean amine side of the Lean/Rich Exchanger 9103-E-11A/B. 13. Open the Lean/Rich Amine Exchanger 9103-E-11A/B outlet isolation valve and fill the outlet lines. 14. Open the Lean Amine Cooler 9103-E-14 inlet isolation valves and start filling the Exchanger. 15. Open the high point vent in the Lean Amine Cooler 9103-E-14 and release Nitrogen. 16. Close the vent valve when the amine just starts to come out of the vent valve. 17. Open the outlet isolation valve of the Lean Amine Cooler 9103-E-14 and fill the outlet lines. 18. Ensure that the Amine line from the Lean Amine Cooler 9103-E-14 outlet to the Analyzer AT-1506 isolation valve is closed. 19. Open the Lean Amine Trim Cooler 9103-E-15 inlet isolation valve and fill the Cooler with amine. 20. Ensure that the Lean Amine Trim Cooler 9103-E-15 bypass control valve 91-TV1509 is closed. 21. Open the high point vent in the Lean Amine Trim Cooler 9103-E-15 and release Nitrogen. 22. Close the high point vent isolation valve when the amine just starts to overflow. 23. Open the outlet isolation valve of the Lean Amine Trim Cooler 9103-E-15 and fill the outlet lines. 24. Check the level in the Amine Regenerator 9103-C-12 through the 91-LT-1510. If the level is less than 30%, make up the level as previously mentioned to 50%. 25. Put 91-FV-1530 in ‘Manual’ and open the control valve by 10% and line up the amine to Amine Surge Tank 9103-T-11. 26. Open the Amine Surge Tank inlet isolation valve and line up lean amine to Amine Surge Tank 9103-T-11. 27. Stop the Hot Lean Amine Pump 9103-P-17A from the local control station. 6.3.2.11 Establishing Amine Circulation in the System 1. Ensure that Amine Surge Tank 9103-T-11 is having more than 50% level. If not then make up the tank from road tankers as mentioned previously. 2. Ensure that the Lean Amine Pump 9103-P-13A/B suction, discharge and minimum flow lines are lined up. 3. Put the LOR switch of the Lean Amine Pump in ‘Remote’. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 277 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4. Start the Lean Amine Pump 9103-P-13A from ICSS and put 9103-P-13B in AUTO. 5. Open the minimum flow control valve 91-FV-1511 in manual and adjust the valve opening to ensure a minimum flow of 375 m3/Hr. 6. Now put the minimum flow control valve in auto with a set point of 375 m3/hr. 7. Reset Process Shutdown and ensure that the Acid Gas Amine Absorber 9103-C-11 inlet ON-OFF valve 91-XV-1504 is opened. 8. Open the Lean Amine Pump 9103-P-13A/B discharge valve to the Acid Gas Amine Absorber 9103-C-11. 9. Open the Acid Gas Amine Absorber 9103-C-11 inlet flow control valve 91-FV-1501 in manual by 10%. 10. Ensure that the level in Acid Gas Amine Absorber 9103-C-11 is rising by checking the level transmitter 91-LT-1505. 11. Ensure that the Acid Gas Rich Amine Pumps 9103-P-12A/B suction, discharge and minimum flow isolation valves are lined up and the pumps are primed. 12. Put the Acid Gas Rich Amine Pumps 9103-P-12A/B LOR switch in ‘Remote’ and start the pump 9103-P-12A from ICSS and put the pump 9103-P-12B in AUTO. 13. Open the minimum flow control valve 91-FV-1508 in manual and adjust the valve opening to get a flow of 375 m3/hr. 14. Take the minimum flow control valve 91-FV-1508 in Auto with a set point of 375 m3/hr. 15. Ensure that the Rich Amine to the Amine Regenerator 9103-C-12 isolation valves are lined up. 16. Open the Amine Regenerator inlet control valve 91-FV-1520 to 10% in manual. 17. Ensure that the level in the Amine Regenerator started to rise through 91-LT-1510. 18. Ensure that the suction, discharge and the minimum flow lines are lined up. 19. Put the LOR switch of the Hot Lean Amine Pumps 9103-P-17A/B in ‘Remote’ and start the pump 9103-P-17A from ICSS and put the pump 9103-P-17B in AUTO. 20. Open the minimum flow control valve 91-FV-1512 in manual and adjust the control valve opening to get a minimum flow of 250 m3/hr. 21. Put the control valve 91-FV-1512 in auto with a set point of 250 m3/hr. 22. Ensure that the Hot Lean Amine Pumps 9103-P-17A/B discharge ON-OFF valve 91-XV-1507 is open. 23. Line up the Hot Lean Amine Pumps discharge to the Lean/Rich Amine Exchanger 9103-E-11, Lean Amine Cooler 9103-E-14, Lean Amine Trim Cooler 9103-E-15 and the Amine Surge Tank 9103-T-11. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 278 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 24. Slowly increase the flow rate from the Lean Amine Surge Tank 9103-T-11 to the Acid Gas Amine Absorber 9103-C-11 by opening the control valve 91-FV-1501 to 487 m3/hr. 25. Ensure that the minimum flow control valve of the Lean Amine Pumps 9103-P13A/B is closed. 26. Correspondingly to maintain level in the Acid Gas Amine Absorber, open the flow Control valve 91-FV-1520 manually till the level is maintaining. Now put the flow control valve in auto with a set point of 487 m3/hr. 27. Ensure that the minimum flow control valve 91-FV-1508 of the Acid Gas Rich Amine Pumps 9103-P-12A/B is closed. 28. To maintain the level in the Amine Regenerator 9103-C-12, open the flow control valve 91-FV-1530 slowly till the level in the Regenerator is maintaining. 29. Put flow control valve 91-FV-1530 in auto with a set point of 487 m3/hr. 30. Ensure that the minimum flow control valve 91-FV-1512 of the Hot Lean Amine Pumps 9103-P-17A/B is closed. 31. Open the Sea Cooling water inlet isolation valve of the Lean Amine Trim Cooler 9103-E-15 and fill the cooler. 32. Open the Sea Cooling water outlet isolation valve and establish the cooling water flow. 33. Ensure that the temperature control valve 91-TV-1509 of the lean amine in the Lean Amine Trim Cooler 9103-E-15 is closed. 34. Ensure that the temperature control valve 91-TV-1513 of the lean amine in the Lean/Rich Exchanger 9103-E-11A/B is closed. 6.3.2.12 Lining up of Regenerator Overhead System 1. Ensure that the drain and vent isolation valves in the Regenerator overhead system are closed. 2. Ensure that the Regenerator overhead 91-PSV-1508 isolation valves are lined up, 91-PSV-1509 upstream isolation valve is closed and the bypass valves are closed. 3. Ensure that the Regenerator Condenser Cooler 9103-E-12 inlet and outlet isolation valves are lined up and the vent and drain valves are closed. 4. Ensure that the Regenerator Condenser Trim Cooler 9103-E-16 inlet and outlet isolation valves are lined up and the vent and drain valves are closed. 5. Ensure that the Regenerator Reflux Drum 9103-V-12 drain and vent valves are closed. 6. Ensure that the Regenerator Reflux Drum 9103-V-12 pressure control valves 91-PV1503A/B are lined up and they are in closed condition. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 279 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7. Ensure that the Regenerator Reflux Drum 9103-V-12 acid gas to Acid Gas KO Drum 9101-V-04 line ON-OFF valve XV-1516 is open. 8. Put the Regenerator Reflux Drum 9103-V-12 pressure controller 91-PIC-1503 in Auto with a set point of 1.0 barg and the pressure control valves 91-PV-1503A/B in Remote. 9. Line up DM water to the Regenerator Reflux Drum 9103-V-12 by opening the flow control valve 91-FV-1521 manually. 10. Check that the level in the Regenerator Reflux Drum 9103-V-12 is increasing by checking the level gauge 91-LG-1502 and 91-LT-1506. 11. When the level in the Regenerator Reflux Drum 9103-V-12 is around 40% close the DM water make up and the flow control valve 91-FV-1521. 12. Start the Regenerator Condenser Cooler fans 9103-EM-12AA/AB/AC/BA/BB/BC/ CA/CB/CC/DA/DB/DC. 13. Line up sea cooling water to the Regenerator Condenser Trim Cooler 9103-E-16 by opening the inlet and outlet isolation valves. 14. Line up the Regenerator Condenser Trim Cooler 9103-E-16 temperature control valve 91-TV-1509 and put it on Auto with a set point of 49°C. 6.3.2.13 Lining up of Regenerator Reboiler 9103-E-13 System 1. Ensure that the Regenerator Reboiler 9103-E-13 is filled with amine solution by checking the level gauge 91-LG-1503. 2. Open the drain valve upstream of Reboiler steam inlet ON-OFF valve 91-XV-1505 and drain all the condensate. 3. Warm up the steam line upstream of Reboiler steam inlet ON-OFF valve 91-XV1505 till there is full fledged steam coming out from the drain valve. 4. Close the drain valve. Open the drain valve downstream of the Reboiler steam inlet ON-OFF valve 91-XV-1505 and drain all the condensate. 5. Reset Process shutdown and ensure that Reboiler steam inlet ON-OFF valve 91-XV1505 is open. 6. Open the bypass valves of the Reboiler Steam inlet flow control valve 91-FV-1503 and start warming up the steam lines and Reboiler tubes. 7. Ensure that Regenerator Reboiler Condensate Pot 9103-V-13 is also being warmed up through the equalisation line. 8. Open the drain valve in the condensate outlet line of the Regenerator Reboiler Condensate Pot 9103-V-13. 9. When all the condensate is drained and steam is coming out of the drain, close the drain valve. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 280 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10. Open the Reboiler condensate outlet line drain valve and drain all the condensate. 11. Warm up the Reboiler tubes till hot condensate comes out of the drain line. 12. Open the Reboiler steam inlet flow control valve 91-FV-1503 by 5% and heat the Reboiler amine solution. 13. Close the drain line valve and allow the condensate level to be built up in the Regenerator Reboiler Condensate Pot 9103-V-13. 14. Ensure that the level is building up in the Regenerator Reboiler Condensate Pot 9103-V-13 by checking the level gauge 91-LG-1504A/B. 15. Ensure that low level alarm 91-LAL-1508 is cancelled in the Pot. 16. Line up Regenerator Reboiler Condensate Pot 9103-V-13 condensate outlet line level control valve 91-LV-1508 and put the controller in auto with a set point of 50%. 17. Ensure that the level in Regenerator Reboiler Condensate Pot 9103-V-13 is maintained at 50%. 18. Gradually increase the opening of the steam inlet control valve 91-FV-1503 and heat the amine solution at a rate of 25°C/hr till the Regenerator bottom temperature reaches 130°C. 19. Put the Reboiler steam inlet flow controller 91-FIC-1503 in “Remote” and enter the ratio of steam to rich amine at 118.5 in the ratio controller 91-HIC-1503 and take the ratio controller in Auto. 20. Put the Regenerator top temperature controller 91-TIC-1510 in Auto with a set point of 118°C. 21. Line up the Regenerator Reflux Drum Pumps 9103-P-11A/B by opening the suction and discharge valves and priming the pumps by opening the casing vent and releasing Nitrogen. 22. Ensure that the Regenerator Reflux Drum Pumps 9103-P-11A/B discharge to the Waste Water Degasser is isolated. 23. Ensure that the Regenerator Reflux Drum Pumps 9103-P-11A/B minimum flow line control valve FV-1505 is lined up. 24. Put the minimum flow controller 91-FIC-1505 in Auto with a set point of 20 m3/hr. 25. Put the LOR switch of the Regenerator Reflux Drum Pumps 9103-P-11A/B in ‘Remote’ position. 26. Start the Regenerator Reflux Drum Pumps 9103-P-11A from the ICSS and put 9103-P-11B in AUTO. 27. Line up the reflux from the Regenerator Reflux Drum Pumps 9103-P-11A to the Regenerator 9103-C-12 by lining up the control valve 91-FV-1531. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 281 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 28. Put the level controller 91-LIC-1506 of the Regenerator Reflux Drum 9103-V-12 in Auto with a set point of 50%. 29. Put the reflux flow control valve 91-FV-1531 in remote mode. 30. Ensure that the top temperature of the Regenerator is being maintained at around 118°C. 6.3.2.14 Lining up of Acid Gas to the Acid Gas Amine Absorber 1. Ensure that the vent and drain valves in the Acid Gas Coolers 9103-E-101A/B, Lean Acid Gas KO Drum 9103-V-14, Acid Gas KO Drum Return Pumps 9103-P-14A/B are closed. 2. Ensure that the sea cooling water to Acid Gas Coolers 9103-E-101A/B inlet filter elements are fixed and boxed up. 3. Open the Sea Cooling water inlet and outlet isolation valves and line up sea cooling water to Acid Gas Coolers 9103-E-101A/B. 4. Ensure that the 91-VRV-1577 upstream isolation valve is lined up in the sea cooling water inlet of Acid Gas Coolers 9103-E-101A/B. 5. Ensure that the 91-VRV-1578 upstream isolation valve is lined up in the sea cooling water outlet of Acid Gas Coolers 9103-E-101A/B. 6. Ensure that the 91-TSV-1501 upstream isolation valve is opened & 91-TSV-1502 upstream isolation valve is closed in the sea cooling water outlet of Acid Gas Coolers 9103-E-101A/B. 7. Ensure that the 91-PSV-1501 in Lean Acid Gas KO Drum 9103-V-14 isolation valves is opened, 91-PSV-1502 upstream isolation valves are closed and the bypass valves are closed. 8. Reset Process shutdown from ICSS. 9. Ensure that Acid Gas inlet ON-OFF valve 91-XV-1501 is opened to the Acid Gas Cooler 9103-E-101A/B and the ON-OFF valve 91-XV-1502 to the Acid Gas Flare Header is closed. 10. Open the isolation valves downstream of ON-OFF valve 91-XV-1502 and lock the valves in open position. 11. Open the isolation valve upstream of ON-OFF valve 91-XV-1501 and lock the valve in open position. 12. Line up pressure control valve 91-PV-1502 of the Acid Gas Amine Absorber 9103-C11 and take the pressure controller 91-PIC-1502 in Auto with a set point of 0.2 barg. 13. Ensure that the 91-PSV-1503 in Acid Gas Amine Absorber 9103-C-11 isolation valves are lined up and the PSV-1504 upstream isolation valves are closed and the bypass valves are closed. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 282 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 14. Inform AGRU 1 & 2 (Existing units) to line up Acid Gas to AGEU. 15. Open the isolation valves of the Acid Gas line to AGEU in the battery limit slowly and admit acid gas into the Acid Gas Coolers 9103-E-101A/B. 16. Ensure that the temperature of the acid gas at the outlet of the acid gas coolers is 53°C by checking the temperature indicator 91-TI-1501. 17. When there is an increase in the level of the Lean Acid Gas KO Drum which is read from the LG-1501A/B & LT-1501, Line up Acid Gas KO Drum Return Pumps 9103-P14A/B. 18. Open the suction isolation valves of the Acid Gas KO Drum Return Pumps 9103-P14A/B and prime the pumps by opening the casing vents and releasing Nitrogen. 19. Reset process shutdown and ensure that the ON-OFF valve 91-XV-1503 in the pump discharge is open. 20. Ensure that the pumps 9103-P-14A/B discharge to the Sour Water Stripper 6922-C01 is isolated. 21. Put the LOR switch of the pumps in ‘Remote’ and start the pump 9103-P-14A from ICSS and put pump 9103-P-14B in AUTO. 22. Open the pump discharge valves and then open LV-1501 gradually. 23. Put the Lean Acid Gas KO Drum level controller 91-LIC-1501in auto with a set point of 50%. 24. Put the lean amine flow control valve 91-FV-1501 to the Acid Gas Amine Absorber 9103-C-11 in ratio control with the acid gas feed. 25. Check the Incinerator 9101-F-14 performance as acid gas is routed to it from the Acid Gas Amine Absorber. 26. Open 91-PV-1503A in manual and route acid gases from Regenerator Reflux Drum 9103-V-12 to flare. Keep 91-PV-1503B closed in manual. 27. When the acid gases produced from Regenerator is stabilized, put the pressure controller 91-PIC-1503 in Auto with a set point of 1.0 barg. 28. Check the differential pressure 91-PDT-1522 in the Acid Gas Amine Absorber and 91-PDT-1523 in the Amine Regenerator 9103-C-12. If the differential pressures shows increasing trend then antifoam has to be dosed to amine feed to that tower. 29. After stabilising the plant, inform NGL-1/2/4 to line up acid gases one by one. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 283 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.3 Start-Up of Sulphur Recovery Unit The first start-up of the SRU following a major overhaul may be carried out independent of the TGTU BSR Section. In this case the SRU tail gases will be routed to the Incinerator and closed to the TGTU. The start-up of sulphur recovery unit involves the following activities: 1. Confirm LP heating steam is in service to all sulphur lines, Sulphur Degassing Pit 9101-T-01/01B heating coils and trace heating lines. 2. Confirm acid gas shutdown valve 9103-XV-1516 from the upstream amine Regenerator Reflux Drum 9103-V-12 to the Acid Gas KO Drum 9101-V-04 is closed. 3. Confirm that the SRU tail gas ON/OFF valve 91-XV-1097 from the Final Separator 9101-V-05 to the Incinerator 9101-F-14 is open. 4. Confirm that the SRU tail gas ON/OFF valve 9101-XV-1098 from Final Separator 9101-V-05 to the Tail Gas Treatment Unit is closed. 5. Introduce BFW to the SRU Reaction Furnace Boiler 9101-E-07 Steam Drum 9101-V07 and establish a normal operating water level in the vessel. 6. Introduce BFW through the BFW Preheater and establish normal operating levels in the Last Condenser, Reaction Furnace Condenser 9101-E-01 and 1st Stage Condenser 9101-E-02. 7. Now Reaction Furnace burner to be started to heat up the system. 6.3.3.1 Start-up of Reaction Furnace (9101-F-01) Burner Reaction Furnace-BMS sequence The burner management system of Reaction Furnace is incorporated in ESD system. Reaction furnace LCP 9101-F-01–LP-005 hand switches detail is tabulated below: Sl. # Tag No. Description 1. 91-HS-1211 Start purge 2. 91-HS-1212 Start ignition 3. 91-HS-1213 Emergency shutdown 4. 91-HS-1214 Lamp test Reaction Furnace 9101-F-01 hardwired auxiliary console hand switches detail is tabulated below: Sl. # Tag No. Description 1. 91-HS-1217 Acid gas ON/OFF 2. 91-HS-1218 Fuel gas ON/OFF EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 284 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Reaction furnace LCP 9101-F-01–LP-005 lamp indication detail is tabulated below: Sl. # Tag No. Description 1. 91-XA-1211 Reaction furnace burner shutdown 2. 91-XL-1212 Ready for purge 3. 91-XL-1213 Purge ON 4. 91-XL-1214 Ready for ignition 5. 91-XL-1215 Ignition ON 6. 91-XL-1216 Fuel gas ON 7. 91-XL-1217 Acid gas ON 8. 91-BAL-1055A Flame-1 ON 9. 91-BAL-1055B Flame-2 ON Reaction Furnace 9101-F-01 soft pushbutton details in DCS is tabulated below: Sl. # Tag No. Description 1. 91-HS-1216 Quench steam valve 91-XV-1078 ON/OFF 2. 91-HS-1040 Quench steam valve 91-XV-1079 ON/OFF 3. 91-HS-1219 Nitrogen valve ON/OFF switch 4. 91-HS-1220 System reset 5. 91-HS-1017 Start-up bypass for 91-PALL-1025 Control valve/ON-OFF valve details are tabulated below: Sl. # Tag No. Description 1. 91-XV-1048 Fuel gas shut-off valve-1 2. 91-XV-1099 Fuel gas shut-off valve-2 3. 91-XV-1100 Fuel gas vent valve 4. 91-FV-1009 Fuel gas flow control valve 5. 91-XV-1001 Acid gas shut-off valve 6. 91-XV-1102 Acid gas shut-off valve 7. 91-XV-1110 Nitrogen shut-off valve 8. 91-XV-1127 Nitrogen shut-off valve 9. 91-XV-1101 Main combustion air shut-off valve 10. 91-FV-1002 Combustion air control valve 11. 91-FV-1002B Secondary air control valve 12. 91-FV-1003 Make-up air control valve 13. 91-XV-1078 Quench steam ON/OFF valve 14. 91-XV-1079 Quench steam ON/OFF valve EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 285 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The burner light-on is carried out in three steps: i. System reset ii. Pre-ignition purge iii. Fuel gas burner light-on i. System Reset 1. Check the following shutdown interlocks are absent in the ICSS: Sl. # Tag No. Description 1. 91-HS-1012A Reaction furnace ESD pushbutton (CCR) 2. 91-HS-1213 Reaction furnace ESD pushbutton (LCP) 3. 65-XS-1008 AGR shutdown 4. 91-BSL-1055A/B Flame failure of reaction furnace (2oo2) 5. 65-HS-001 General plant shutdown activation (existing) 6. 65-XA-1001 Existing SRU shutdown 7. 91-TT-1050 Rupture pin failure 8. 65-XS-1024 Total power Shutdown 9. 65-PT-1003A/B/C Instrument air pressure low-low 10. 65-XS-1015 Steam pressure failure (low low pressure) 11. 91-HS-1011 Unit-91 general shutdown button 12. 91-XS-1901 Confirmed gas detection 13. 65-XS-1020 Fuel gas low-low pressure 14. 91-LT-1003 Acid gas KOD (9101-V-04) high-high level 15. 91-LT-1006 Steam drum (9101-V-07) low-low level 16. 91-LT-1009 RF condenser (9101-E-01) low-low level 17. 91-LT-1012 1st condenser (9101-E-02) low-low level 18. 91-PT-1025 Acid gas inlet low-low pressure 19. 91-XS-1063/1064 Blowers (9101-K-01A/B) are not running 20. 91-PT-1054A/B/C Air for acid gas burner high-high pressure 21. 91-FT-1140 Acid gas to reaction furnace low-low flow 22. 91-FT-1129 Process air to acid gas burner flow low-low 23. 91-FT-1130 Fuel gas to reaction furnace flow low-low If the above conditions do not exist, the Reaction furnace BMS system can be reset. When the BMS reset is pressed, following shutdown causes are automatically bypassed during start-up: a. 91-FT-1129 (Combustion Air low-low flow) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 286 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL b. 91-FT-1130 (Fuel gas to reaction furnace low-low) c. 91-FT-1140 (Acid gas to reaction furnace low-low) d. 91-BSL-1055A/B (Flame detector signal) e. 91-PT-1025 (Acid gas I/L pressure low-low) 2. Start any one of Process Air Blower 9101-K-01A & 9101-K-01B. 3. The following conditions are to be satisfied for the pre-ignition purge: a. No flame present – 91-BSL-1055A/91-BSL-1055B. b. Fuel Gas cut-in valve XV-1048 is in close position – 91-ZSC-1048. c. Fuel Gas cut in valve XV-1099 is in close position - 91-ZSC-1099. d. Fuel Gas vent valve XV-1100 is in open position - 91-ZSO-1100. e. Ensure “READY FOR RESET” (91-XL-1218) is lit in ICSS. 4. RESET the system by pressing the Soft switch 91-HS-1220 from DCS and ensure the following: a. Energizing of combustion air control valve SOV 91-FY-1002B and 91-FY-1002. b. Process air flow controller 91-FIC-1002, 91-FIC-1002B to manual mode and output at start position. c. Fuel gas flow controller 91-FRC-1009 to manual mode and output at start position. d. “READY FOR PURGE” lamp (91-XL-1212) is lit on the local panel and also in ICSS. e. “SYSTEM IN SHUTDOWN” lamp 91-XA-1211 will extinguish on the LCP and ICSS. ii. Pre-ignition Purge 1. Ensure the control valves for combustion air 91-FV-1002, fuel gas control valve 91-FV-1009 and steam valves are in start position at the ICSS and in field. 2. Press the start purge button 91-HS-1211 at the local control panel. 3. Ensure the “SYSTEM READY FOR PURGE” is unlit. 4. Ensure that the Nitrogen shutdown valve 91-XV-1127 for furnace purging and 91XV-1110 for flame scanner, sight glass purging are opened. 5. Ensure that main Process air shutdown valve 91-XV-1101 is closed. 6. Verify whether the ‘PURGE ON’ lamp 91-XL-1213 is lit for 20 minutes (purge timer) in the Local Control Panel. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 287 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7. After the purge time is over, ensure that the ‘PURGE ON’ lamp 91-XL-1213 is unlit in the Local Control Panel. 8. Ensure that ‘PURGE COMPLETE’ lamp 91-XL-1219 is lit on the ICSS. 9. Ensure the “READY FOR IGNITION” lamp 91-XL-1214 is lit on local panel. 10. Ensure that the Nitrogen cut-in valve 91-XV-1127 is closed. iii. Fuel Gas Burner Light On 1. Ensure that the air inlets, burner and outlet passages are boxed up and free of foreign material. 2. Ensure that all personnel have been evacuated from the reaction furnace area, ductwork and associated equipment and all access and inspecting doors closed and sealed. 3. Ensure that the Process Air Blower 9101-K-01A/B is running. 4. Ensure that all safety shut off valves are closed. 5. Ensure that the Fuel System vents are open and venting to atmosphere. Lines are properly drained and cleared of condensate. 6. Ensure that a complete functional check of the safety interlocks has been made. 7. Ensure that the area is clear of obvious safety hazards and flammable gases are not present in the area. 8. Ensure that all lines have been blown down with plant air to insure they are free of debris that might plug metering orifices and burner tips. 9. Ensure that utilities like fuel gas, instrument air, nitrogen and plant air are available and initial operational checks performed on the elements in each line. 10. Ensure that the burner elements are in their proper position. 11. Ensure that power has been supplied to control systems and to safety interlocks. 12. Ensure that the gauges indicating fuel header pressure to the unit are functional. 13. Ensure that the pressure self regulating valves are set according to the instrument data sheets. 14. Ensure that the isolation valves for all the pressure gauges and pressure transmitters are open and their respective bleed valves are closed. Valves are sealed in position as indicated on P&IDs. 15. Ensure that the minimum purge period is satisfactorily completed. 16. Ensure that the control valves of the fuel gas 91-FV-1009, quench steam 91-XV1078, 91-XV-1079 and Combustion Air 91-FV-1002 are closed. 17. Ensure that the igniter is in the correct position and that the fuel gas gun is ready for operation with fuel gas. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 288 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 18. Open the fuel gas control valve 91-FV-1009 and combustion air control valve 91-FV-1002B to the pre-determined position. 19. Press the ‘START IGNITION’ push button 91-HS-1212 from the local control panel. 20. Ensure that ‘READY FOR IGNITION’ lamp 91-XL-1214 is unlit. 21. Ensure that the igniters insert SOV 91-XY-1103 is energised. 22. Ensure that the igniter insertion is proved by limit switch 91-ZSC-1103. 23. Ensure the Process air shutdown valve 91-XV-1101 is opened. 24. Ensure fuel gas bleed valve 91-XV-1100 is closed and fuel gas shutdown valves 91-XV-1048 and 91-XV-1099 are opened. 25. Ensure that the igniter transformer is energised for 10 seconds and sparking begins. 26. Ensure that the igniter transformer is de-energised and igniter retracts automatically (91-ZSO-1103) after 10 seconds of ignition timer. 27. If flame is detected then ensure that the ‘FLAME ON’ lamps (91-BAL-1055A, 91-BAL-1055B) are lit on the local control panel. 28. Permit is provided to open the steam quench shutdown valve 91-XV-1078 and 91-XV-1079 from ICSS soft switches. 29. Permit is provided to open the acid gas shutdown valve 91-XV-1102. 30. Ensure that the ‘FUEL GAS ON’ lamp 91-XL-1216, 91-XL-1216A is lit in the Local Control Panel and ICSS respectively. 31. Open the instrument air purge valve to sight glasses, flame scanners and nozzles. 32. Ensure that the Nitrogen purge valve to sight glasses, flame scanners and nozzles is closed. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 289 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 29 – Reaction Furnace Start-up Start A & Note A B Note B Ready for Reset XL-1218 ON Y Purge completed Acid gas cut-off valves XV-1102, XV1001 and XV-1516 opens Purge complete XL-1219 System Reset HS-1220 Acid gas XL-1217 ON Nitrogen SDV-XV-1127 close Automatic bypass of combustion air flow (FT-1129), fuel gas flow (FT-1130), acid gas flow (FT-1128) low low alarm and acid gas inlet pressure (PT-1025) low low alarm Ready for ignition XL-1214 Start Ignition-HS1212 Furnace is fully operational Burner light on timer 10 min starts Force combustion air FIC1002 and fuel gas FIC-1009 controllers to manual mode and output to minimum 10% System ready for purge XL1401 Purge start-HS1211 Common alarm XL1405 Nitrogen SDV-XV-1127, XV-1110 open · Igniter insert SOV XY-1103 energized · combustion air XV-1101 opens · Fuel gas vent valve XV-1100 closes · Fuel gas block valves XV-1048 and XBV-1099 opens · Igniter transformer energized for 10 seconds Purge timer 20min starts Purge ON XL-1213 Nitrogen flow alarm FAL-1131 Should be healthy within 15 sec Flame detected on 1oo2 logic N N Y BAL-1055A, BAL-1055B ON Fuel Gas XL-1216 ON Quench Steam StartHS-1216, HS-1040 Y XV-1078, XV-1079 open Purge interlocks are healthy till purge timer completes N Following causes should be healthy: · ESD push button in CCR-HS-1012A · ESD push button HS-1213 in LCP · General plant shutdown activation 65-HS-001 · Existing SRU shutdown 65-XA-1001 · Total power shutdown 65-XS-1024 · Instrument air LL pressure 65-PT-1003A/B/C · BFW/steam failure 65-XS-1015 · Unit 91 General shutdown 91-HS-1011 · Confirmed gas detection 91-XS-1901 · Fuel gas LL pressure 65-XS-1020 · Acid gas KOD HH level 91-LT-1003 · Steam drum level low low 91-LT-1006 · Furnace condenser level low low 91-LT-1009 · 1st Condenser level low low 91-LT-1012 · Both blowers (9101-K-01A/B) are not running (91-XS-1063/1064) · Air pressure Hi Hi 91-PT-1054A/B/C · Process air flow low low 91-FT-1129 · Acid gas inlet pressure low low 91-PT-1025 · Fuel gas flow low low 91-FT-1130 · Acid gas flow low low 91-FT-1128 · AGR Shutdown 65-XS-1008 Acid Gas Start-HS1217 Light ON timer out XL-1406 Y B A Gradually open acid gas control valve 91-FV-1503B and close fuel gas control valve 91-FV-1009 close Following are the permissives for purging: · No flame detection by BSL-1055A/B · FG Block valve XV-1048 in close position · FG Block valve XV-1099 in close position · FG Vent valve XV-1100 in open position EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 290 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.3.2 Heating Up the System 1. Take fuel gas controller 91-FIC-1009 in manual and slowly increase the fuel gas to Reaction Furnace. 2. Take the combustion air controller 91-FIC-1002/91-FIC-1002B in manual and increase the combustion air to the Reaction Furnace. 3. Proceed to heat up the Reaction Furnace at 50°C/hr Note 1) If the converters have been filled with catalyst following the unit’s precommissioning refractory dry out phase, then for the first start-up of the unit, the rate of temperature increase of the process air must be initially controlled to slowly heat up the converters at 10-15°C/hr to 90°C to ensure any free water and moisture is removed in the converters catalyst beds. In this case the introduction of BFW to the steam generators will be delayed until the converters catalyst beds are first heated through to 90°C. 2) As the SRU process gas system and the SRU converters does not contain sulphur compounds at this time, firing of fuel gas in the Reaction Furnace burner may be carried out in excess air conditions. 4. Open LP steam shutdown valve 91-XV-1079 to the Reaction Furnace. 5. To suppress the formation of carbon and soot at stoichiometric firing conditions, introduce LP steam to the SRU Reaction Furnace burner fuel gas line when a temperature of >300°C is seen in the Reaction Furnace and the SRU converters are heated through to >120°C. Set the steam flow in the ratio of 1:1 (by wt.) of fuel gas. Note that the furnace temperature will dictate the amount of steam used. Too much steam could result in interference of the burners flame detectors resulting in a burner trip. Before opening steam valves ensure steam lines are fully drained of condensate. 6. Continue to heat up the Reaction Furnace at 50°C/hr 7. When steam blows from the SRU Reaction Furnace Boiler 9101-E-07 atmospheric vent, set Reaction Furnace Boiler pressure controller 91-PV-1003 in automatic mode at 24.0 barg and route excess steam to the LP steam system. 8. Using the MS steam produced in the SRU Reaction Furnace Boiler, heat the Process Air Pre-heater 9101-E-05 outlet process air temperature at 50°C/hr to 210°C 9. When steam emits from each LP Steam Generator 9101-E-01/9101-E-02 atmospheric vents, close vents and route excess steam to the LP steam system. 10. Open LP steam to 9101-E-08 and start heating the BFW to 120°C. 11. Now the 1st Stage Auxiliary Burner 9101-F-02 and the 2nd Stage Auxiliary Burner 9101-F-03 to be started to heat up the converters up to their normal operating temperatures. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 291 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.3.3 1st Stage Auxiliary Burner 9101-F-02 Start-up 1st Stage Auxiliary Burner - BMS Sequence The burner management system of 1st Stage Auxiliary Burner is incorporated in ESD system. 1st stage auxiliary burner LCP 9101-F-102 –LP-006 hand switches detail is tabulated below: Sl. # Tag No. Description 1. 91-HS-1226 Start burner 2. 91-HS-1227 Stop burner 3. 91-HS-1228 Lamp test 1st stage auxiliary burner 9101-F-02 hardwired aux console hand switches detail is tabulated below: Sl. # Tag No. Description 1. 91-HS-1223 Acid gas ON/OFF 2. 91-HS-1224 Fuel gas ON/OFF 1st stage auxiliary burner LCP 9101-F-102–LP-006 lamp indication detail is tabulated below: Sl. # Tag No. Description st 1. 91-XA-1226 1 stage burner shutdown 2. 91-XL-1227 Ready for ignition 3. 91-XL-1228 Ignition ON 4. 91-XL-1229 Fuel gas ON 5. 91-XL-1230 Acid gas ON 6. 91-BAL-1003A Flame-1 ON 7. 91-BAL-1003B Flame-2 ON System Reset to be done by activating the soft push button 91-HS-1225 in DCS. Control valve/ON-OFF valve details are tabulated below: Tag No. Sl. # Description 1. 91-XV-1028 Fuel gas block valve-1 2. 91-XV-1131 Fuel gas block valve-2 3. 91-XV-1132 Fuel gas vent valve 4. 91-FV-1018 Process air control valve 5. 91-FV-1019 Acid gas control valve 6. 91-FV-1020 Fuel gas control valve EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 292 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The burner light-on is carried out in below steps: i. System Reset ii. Fuel Gas Burner Light-On iii. Acid Gas Introduction i. System Reset 1. Check the following shutdown interlocks are absent in the ICSS: • Reaction furnace shutdown • 1st stage auxiliary burner flame failure (91-BALL-1003A/B) • Acid gas flow low-low (91-FT-1134) • Fuel gas flow low-low (91-FT-1135) • Combustion air flow low-low (91-FT-1133) If the above conditions do not exist, the 1st stage auxiliary burner BMS system can be reset. 2. When the BMS reset is pressed, following shutdown causes are automatically bypassed during start-up (start-up override) a. 91-FT-1133 (Combustion Air low-low flow) b. 91-FT-1135 (Fuel gas flow low-low) c. 91-FT-1134 (Acid gas flow low-low) 3. Ensure that any one of Process Air Blower 9101-K-01A & 9101-K-01B is started and running. 4. If the above conditions are satisfied then ensure “1st STAGE BURNER READY FOR RESET” (91-XL-1232) is lit in ICSS. 5. RESET the system by pressing the Soft switch 91-HS-1225 from ICSS and ensure the following: a. Energizing of fuel gas control valve SOV 91-FY-1020. b. Combustion air flow controller 91-FIC-1018 to manual mode and output at start position. c. Fuel gas flow controller 91-FIC-1020 to manual mode and output at start position. d. “READY FOR IGNITION” lamp 91-XL-1227 and 91-XL-1227A is lit on the local panel and also in ICSS respectively. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 293 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. “SYSTEM IN SHUTDOWN” lamp 91-XA-1226 and 91-XA-1226A will extinguish on the LCP and ICSS, respectively. ii. Fuel Gas Burner Light On 1. Ensure that the air inlets, burner and outlet passages are boxed up and free of foreign material. 2. Ensure that all safety shut off valves are closed. 3. Ensure that the Fuel System vents are open and venting to atmosphere. Lines are properly drained and cleared of condensate. 4. Ensure that a complete functional check of the safety interlocks has been made. 5. Ensure that the area is clear of obvious safety hazards and flammable gases are not present in the area. 6. Ensure that all lines have been blown down with plant air to insure they are free of debris that might plug metering orifices and burner tips. 7. Ensure that utilities like fuel gas, instrument air, plant air and nitrogen are available and initial operational checks performed on the elements in each line. 8. Ensure that the burner elements are in their proper position. 9. Ensure that power has been supplied to control systems and to safety interlocks. 10. Ensure that the gauges indicating fuel header pressure to the unit are functional. 11. Ensure that the pressure self regulating valves are set according to the instrument data sheets. 12. Ensure that the isolation valves for all the pressure gauges and pressure transmitters are open and their respective bleed valves are closed. Valves are sealed in position as indicated on P&IDs. 13. Ensure that the minimum purge period is satisfactorily completed. 14. Ensure that the control valves of the fuel gas 91-FV-1020, quench steam and Combustion Air 91-FV-1018 are closed. 15. Ensure that the igniter is in the correct position and that the fuel gas gun is ready for operation with fuel gas. 16. Open the fuel gas control valve 91-FV-1020 and Process air control valve 91-FV1018 to the pre-determined position. 17. Press the ‘START IGNITION’ push button 91-HS-1226 from the local control panel. 18. Ensure that ‘READY FOR IGNITION’ lamp 91-XL-1227 is unlit on the local control panel and 91-XL-1227A is unlit on the ICSS. 19. Ensure “IGNITION ON” 91-XL-1288A lamp lit in ICSS and 91-XL-1228 lamp in Local panel. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 294 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 20. Ensure “Ist STAGE BURNER IN SHUTDOWN” 91-XA-1126 lamp extinguished in Local panel and 91-XA-1126A lamp extinguished in ICSS. 21. Ensure combustion air control valve SOV 91-FY-1018 energized. 22. Ensure Combustion air flow controller 91-FIC-1018 and fuel gas controller 91-FIC1020 to manual mode and output forced to start position at 10% 23. Ensure that the igniters insert SOV 91-XY-1234 is energised. 24. Ensure that the igniter insertion is proved by limit switch 91-ZSC-1234. 25. Ensure fuel gas bleed valve 91-XV-1132 is closed and fuel gas shutdown valves 91-XV-1028 and 91-XV-1131 are opened. 26. Ensure that the igniter transformer is energised for 10 seconds and sparking begins. 27. Ensure that the igniter transformer is de-energised and Igniter retracts automatically (91-ZSO-1234) after 10 seconds ignition timer. 28. If flame is detected then ensure that the ‘FLAME ON’ lamp 91-BAL-1003A, 91-BAL1003B) are lit on the local control panel. 29. Permit is provided to open the steam quench valve. 30. Permit is provided to open the acid gas control valve 91-FV-1019. 31. Ensure that the ‘FUEL GAS ON’ lamp 91-XL-1229 is lit in the Local Control Panel. 32. Ensure combustion air controller 91-FIC-1018 and fuel gas controller 91-FIC-1020 force signal removed. 33. Ensure that the ‘FUEL GAS ON’ lamp 91-XL-1229A is lit in ICSS. 34. Open the instrument air purge valve to sight glasses, flame scanners and nozzles is opened. 35. Ensure that the Nitrogen purge valve to sight glasses, flame scanners and nozzles is closed. 36. Take the fuel gas controller 91-FIC-1020 in manual and slowly increase the fuel gas to the burner. 37. Take the combustion air controller 91-FIC-1018 in manual and increase the air to the burner. 38. Slowly open the fuel gas and combustion air and increase the 1st Stage Converter inlet temperature to 230°C. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 295 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 30 - 1st Stage Auxiliary Burner Management Sequence EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 296 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.3.4 2nd Stage Auxiliary Burner 9101-F-03 Start-up 2nd Stage Auxiliary Burner-BMS Sequence The burner management system of 2nd Stage Auxiliary Burner is incorporated in ESD system. 2nd Stage Auxiliary Burner LCP 9101-F103–LP-007 hand switches detail is tabulated below: Sl. #. Tag No. Description 1. 91-HS-1195 Start burner 2. 91-HS-1196 Stop burner 3. 91-HS-1197 Lamp test 2nd Stage Auxiliary Burner hardwired aux console hand switches detail is tabulated below: Sl. # Tag No. Description 1. 91-HS-1192 Acid gas ON/OFF 2. 91-HS-1193 Fuel gas ON/OFF 2nd Stage Auxiliary Burner LCP 9101 F103–LP-007 lamp indication detail is tabulated below: Sl. # Tag No. Description 1. 91-XA-1191 2nd stage burner shutdown 2. 91-XL-1192 Ready for ignition 3. 91-XL-1193 Ignition ON 4. 91-XL-1194 Fuel gas ON 5. 91-XL-1195 Acid gas ON 6. 91-BAL-1003A Flame -1 ON 7. 91-BAL-1003B Flame-2 ON System Reset to be done by activating 91-HS-1194 in DCS. Control valve/ON-OFF valve details are tabulated below: Sl. # Tag No. Description 1. 91-XV-1031 Fuel gas block valve-1 2. 91-XV-1133 Fuel gas block valve-2 3. 91-XV-1134 Fuel gas vent valve 4. 91-FV-1025 Process air control valve 5. 91-FV-1026 Acid gas control valve 6. 91-FV-1027 Fuel gas control valve EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 297 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL The burner light-on is carried out in below steps: i. System reset ii. Fuel gas burner light-on iii. Acid gas introduction i. System Reset 1. Check the following shutdown interlocks are absent in the ICSS: • Reaction Furnace shutdown • 2nd Stage Auxiliary Burner flame failure (91-BALL-1004A/B). • Acid gas flow low-low (91-FT-1137) • Fuel gas flow low-low (91-FT-1138) • Combustion air flow low-low (91-FT-1136) If the above conditions do not do not exist “2nd Stage Auxiliary Burner” BMS system can be reset. 2. When the BMS reset is pressed, following shutdown causes are automatically bypassed during start-up (start-up override) a. 91-FT-1136 (Combustion Air low-low flow) b. 91-FT-1138 (Fuel gas flow low-low) c. 91-FT-1137 (Acid gas flow low-low) 3. Ensure that any one of Process Air Blower 9101-K-01A & 9101-K-01B is running. 4. If the above conditions are satisfied then Ensure “2nd STAGE BURNER READY FOR RESET” (91-XL-1197) is lit in ICSS. 5. “RESET” the system by pressing the Soft switch 91-HS-1194 from ICSS and ensure the following: a. Energizing of fuel gas control valve SOV 91-FY-1027. b. Combustion air flow controller 91-FIC-1025 to manual mode and output at start position. c. Fuel gas flow controller 91-FIC-1027 to manual mode and output at start position. d. “READY FOR IGNITION” lamp 91-XL-1192 and 91-XL-1192A is lit on the local panel and ICSS respectively. e. “SYSTEM IN SHUTDOWN” lamp 91-XA-1191 and 91-XA-1191A will extinguish on the LCP and ICSS, respectively. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 298 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL ii. Fuel Gas Burner Light On 1. Ensure that the air inlets, burner and outlet passages are boxed up and free of foreign material. 2. Ensure that all safety shut off valves are closed. 3. Ensure that the Fuel System vents are open and venting to atmosphere. Lines are properly drained and cleared of condensate. 4. Ensure that a complete functional check of the safety interlocks has been made. 5. Ensure that the area is clear of obvious safety hazards and flammable gases are not present in the area. 6. Ensure that all lines have been blown down with plant air to insure they are free of debris that might plug metering orifices and burner tips. 7. Ensure that utilities like fuel gas, instrument air, nitrogen and plant air are available and initial operational checks performed on the elements in each line. 8. Ensure that the burner elements are in their proper position. 9. Ensure that power has been supplied to control systems and to safety interlocks. 10. Ensure that the gauges indicating fuel header pressure to the unit are functional. 11. Ensure that the pressure self regulating valves are set according to the instrument data sheets. 12. Ensure that the isolation valves for all the pressure gauges and pressure transmitters are open and their respective bleed valves are closed. Valves are sealed in position as indicated on P&IDs. 13. Ensure that the control valves of the fuel gas 91-FV-1027, quench steam and Combustion air 91-FV-1025 are closed. 14. Ensure that the igniter is in the correct position and that the fuel gas gun is ready for operation with fuel gas. 15. Open the fuel gas control valve 91-FV-1027 and combustion air control valve 91FV-1025 to the pre-determined position. 16. Press the ‘START IGNITION’ push button 91-HS-1195 from the local control panel. 17. Ensure that ‘READY FOR IGNITION’ lamp 91-XL-1192, 91-XL-1192A is unlit on the local control panel and ICSS respectively. 18. Ensure “IGNITION ON” lamp 91-XL-1193A, 91-XL-1193 lamp lit in ICSS and Local panel respectively. 19. Ensure “2nd STAGE BURNER IN SHUTDOWN” lamp 91-XA-1191 and 91-XA-1191A extinguished in Local panel and ICSS respectively. 20. Ensure combustion air control valve SOV 91-FY-1025 energized. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 299 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 21. Ensure Combustion air flow controller 91-FIC-1025 and fuel gas controller 91-FIC1027 forced to manual mode and output forced to start position at 10%. 22. Ensure that the igniters insert SOV 91-XY-1199 is energised. 23. Ensure that the igniter insertion is proved by limit switch 91-ZSC-1199. 24. Ensure fuel gas bleed valve 91-XV-1134 is closed and fuel gas shutdown valves 91XV-1031 and 91-XV-1133 are opened. 25. Ensure that the igniter transformer is energised for 10 seconds and sparking begins. 26. Ensure that the igniter transformer is de-energised and Igniter retracts automatically (91-ZSO-1199) after 10 seconds ignition timer. 27. If flame is detected then ensure that the ‘FLAME ON’ lamps (91-BAL-1004A, 91BAL-1004B) are lit on the LCP and ICSS. 28. Permit is provided to open the steam quench valve. 29. Permit is provided to open the acid gas control valve 91-FV-1026. 30. Ensure that the ‘FUEL GAS ON’ lamp 91-XL-1194 is lit in the Local Control Panel. 31. Ensure that the ‘FUEL GAS ON’ lamp 91-XL-1194A is lit in ICSS. 32. Ensure combustion air controller 91-FIC1025 and fuel gas controller 91-FIC-1027 force signals removed. 33. Open the instrument air purge valve to sight glasses, flame scanners and nozzles. 34. Ensure that the Nitrogen purge valve to sight glasses, flame scanners and nozzles is closed. 35. Slowly increase the fuel gas to the burner by keeping the Fuel gas flow controller 91-FIC-1027 in manual. 36. Slowly increase the combustion air to the burner by keeping the Combustion air flow controller 91-FIC-1025 in manual. 37. Slowly open the fuel gas and combustion air and increase the 2nd Stage Converter inlet temperature to 230°C. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 31 - 2nd Stage Auxiliary Burner Management Sequence Rev.: 0 Date: 03/09/2012 Page: 300 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 301 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.3.5 Lining up Of Acid Gas to Reaction Furnace 1. When the Reaction Furnace temperature is >1250°C set the Reaction Furnace burner control system to slightly sub-stoichiometric firing conditions with steam being injected as noted above to prevent the formation of carbon. 2. Acid gas may now be introduced to the SRU Reaction Furnace burner provided the following points are first confirmed: • The SRU converters catalyst beds are at their normal operating temperatures of 230 and 210°C, respectively • The SRU Reaction Furnace burner is operating on fuel gas in slightly substoichiometric firing conditions with steam injection to fuel gas and process air lines • There is sufficient acid gas available from the upstream Amine Regenerator, at a stable flow rate of and at/or above the minimum design flow required for the SRU to operate satisfactorily. 3. Confirm that the acid gas system has been purged with nitrogen. 4. Using a utility water hose connected to the Acid Gas KO Drum utility connection, introduce water to establish a low level of water in the Acid Gas KO Drum 9101-V-04. 5. Using MS steam from the SRU Reaction Furnace Boiler 9101-E-07, continue increasing the Acid Gas Pre-heater 9101-E-06 outlet temperature at 50°C/hr to 210°C. 6. Confirm available acid gas flow is at or above the minimum turndown required of 5935 kg/hr, (2349 m3/hr) for the SRU to operate. 6.3.3.6 Reaction Furnace Acid Gas Burner Light-On 1. Ensure the acid gas control valves 91-PV-1503A/91-PV-1503B from AGEU Regenerator Reflux Drum 9103-V-12 is closed. 2. Ensure the 1st Stage and 2nd Stage Auxiliary Burner “FLAME ON” indication is available. 3. Ensure Acid Gas KOD 9101-V-04 level 91-LAHH-1003 and acid gas feed pressure 91-PALL-1025 is healthy. 4. Activate the “ACID GAS ON SWITCH” 91-HS-1217 on hardwired console. 5. Ensure acid gas cut-off valve 91-XV-1102, 91-XV-1001 and 91-XV-1516 is open. 6. After 30 seconds “ACID GAS ON” lamp 91-XL-1217, 91-XL-1217A is lit on the local panel and ICSS respectively. 7. Gradually open the acid gas valve 91-PV-1503B and close the fuel gas control valve 91-FV-1009 and combustion air controller 91-FIC-1018 to be adjusted accordingly to provide the process air requirement for the acid gas. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 302 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 8. Ensure the minimum air flow rate while switching between fuel gas and acid gas. 9. As soon as a flow of acid gas is introduced to the Reaction Furnace burner, commence reducing fuel gas flow to the burner. 10. When fuel gas flow has stopped, isolate fuel gas line by closing fuel gas shutdown valves. 11. Stop steam injection to the fuel gas and process air lines to the Reaction Furnace burner. 12. Set all controllers in automatic mode. 13. Remove the override from the acid gas low flow trip. 14. Acid Gas is now to be introduced to the 1st and 2nd Stage Auxiliary Burners 6.3.3.7 1st Stage Auxiliary Burner Acid Gas Burner Light-On 1. Ensure the acid gas control valve 91-FV-1019 is closed. 2. Activate the acid gas on switch 91-HS-1223 on hardwired console. 3. Ensure acid gas control valve SOV 91-FY-1019 energized. 4. Acid gas controller is forced at the start-up position to ensure acid gas flow is above low-low flow trip setting 5. “1ST STAGE ACID GAS ON” lamp 91-XL-1230, 91-XL-1230A is lit on the local panel and ICSS respectively. 6. Gradually open the acid gas valve 91-FV-1019 and close the fuel gas control valve 91-FV-1020 and combustion air controller 91-FIC-1018 to be adjusted accordingly to provide the process air requirement for the acid gas. 7. Ensure the minimum air flow rate while switching between fuel gas and acid gas. 6.3.3.8 2nd State Auxiliary Burner Acid Gas Burner Light-On 1. Ensure the acid gas control valve 91-FV-1026 is closed. 2. Activate the acid gas on switch 91-HS-1192 on hardwired console. 3. Ensure acid gas control valve SOV 91-FY-1026 energized. 4. Acid gas controller is forced at the start-up position to ensure acid gas flow is above low-low flow trip setting. 5. Ensure “2nd STAGE ACID GAS ON” lamp 91-XL-1195, 91-XL-1195A is lit on the local panel and ICSS respectively. 6. Gradually open the acid gas valve 91-FV-1026 and close the fuel gas control valve 91-FV-1027, Combustion air controller 91-FIC-1025 to be adjusted accordingly to provide the process air requirement for the acid gas. 7. Ensure the minimum air flow rate while switching between fuel gas and acid gas. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 303 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.3.9 Sulphur Production 1. When the SRU operation has stabilised, commission the tail gas analyser and set in automatic with the trim air control valve to maintain a H2S:SO2 of 2.0:1.0. 2. Following a period of approximately 30-60 minutes after the introduction of acid gases to the SRU Reaction Furnace Burner, commence checking of the SRU condensers, sultraps for liquid sulphur. 3. If the sultraps have not been pre-filled with flake or powdered sulphur then the following procedure should be adopted to fill the sultraps with liquid sulphur. Note: It is necessary to use a respirator or fresh air breathing apparatus to ensure complete operator safety during this operation. • Slowly open each of the condensers sulphur outlet drain valves and observe through the open sultrap inspection door • When opening a sultrap if acid gas vapour appears, usually as a white smoky gas, this will indicate that no liquid sulphur has collected behind the isolation valve. The sultrap should be closed immediately in this case and only opened again after about 10 minutes. If only a bluish haze with little pressure behind it shows from the sultrap, this indicates that the sultrap is filling with liquid sulphur and the condensers sulphur outlet valve can be left open. • Check the sultrap inspection door at regular intervals until sulphur is seen to flow from each seal • When sulphur is seen at the condensers sulphur outlet valve may now be left open to allow the sulphur to flow freely • Repeat this exercise until sulphur is seen to flow from all three seals Note: It may take a considerable period of time, possibly several hours before sulphur is seen to flow from the third condenser. • Check the Sulphur Degassing Pit 9101-T-01/01B is showing an increase in level • When there is sufficient level in Sulphur Degassing Pit 9101-T-01/01B, start Sulphur Degassing Pumps 9103-P-03A/B/09A/B recirculating the liquid sulphur back to the pit • Start steam ejector and line up the vent gases to Incinerator • Ensure that the air flow 91-FI-1056 from safe location shows the normal value. • Start AQUISULF catalyst injection to the Degassing pit • Start Sulphur Product Pumps 9101-P-04A/B/10A/B and line up liquid sulphur to the Sulphur Storage Tank 9101-T-02 via the level control valve 91-LV-1014/1051. • When sufficient level is there in the Sulphur Storage Tank 9101-T-02 start the Sulphur Tank Pumps 9101-P-15A/B and transfer liquid sulphur to QAPCO. The start-up of the SRU is now complete. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 304 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.4 Start-up of Tail Gas Treatment Unit 6.3.4.1 Pre-requisites I. Preparation of Caustic Solution 1. Ensure that the Caustic Storage Tank 9103-T-14 is cleaned internally. 2. Ensure that the Caustic Injection Pumps 9103-P-103A/B and the Agitator 9103-M-14 are energised in MCC. 3. Ensure that all the drain and vent valves in the package are closed. 4. Procure the Caustic Solution drums/tanks to the site and place it near the unloading pump 9103-P-104. 5. Connect the drums/tanks to the unloading pump. 6. Start the unloading pump and transfer the required amount of Caustic Solution to the tank. 7. Make up the required concentration of the Caustic Solution by adding DM water to the tank. 8. Ensure that the low low level trip 91-LALL-1524 is cancelled while making up the solution. 9. Ensure the level in the tank from 91-LG-1512 and 91-LT-1525 and ensure the tank is filled upto the required level. 10. Start agitator 9103-M-14 from the local panel to mix the solution thoroughly. II. Establishing Desuperheater/Contact Condenser 9102-C-11 circulation 1. Ensure that the suction and discharge isolation valves of the Cooling Water Circulation Pumps 9102-P-12A/B are closed. 2. Ensure that the Cooling Water Circulation Pumps 9102-P-12A/B suction to the Waste Water Degasser 6922-V-07 isolation valves are closed. 3. Open the DM water make up to the suction of the Cooling Water Circulation Pumps 9102-P-12A/B and increase level in the top section of the Desuperheater/Contact Condenser 9102-C-11. 4. When the level in the Desuperheater/Contact Condenser 9102-C-11 top section reaches 50% which is noted through the 91-LG-1302/91-LT-1305, close the DM water make up to the pumps suction. 5. Take the flow control valve 91-FV-1307 in auto with a set point of 197 m3/hr. 6. Ensure that the flow control valve 91-FV-1305 is closed fully on manual and the upstream and downstream isolation valves are closed. 7. Start Cooling Water Circulation Pump 9102-P-12A from ICSS and circulate the water in the Desuperheater/Contact Condenser 9102-C-11 top chimney tray. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 305 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 8. Select Cooling Water Circulation Pump 9102-P-12B in AUTO from ICSS and open the suction and discharge isolation valves and prime the pump. 9. Line up 91-LV-1307 to top up Desuperheater/Contact Condenser 9102-C-11 bottom section. 10. Open 91-LV-1307 manually and top up Desuperheater/Contact Condenser 9102-C-11 bottom section. 11. Open the DM water make up to the suction of the Cooling Water Circulation Pumps 9102-P-12A/B to maintain the level at 50% at top section. 12. Check the level in the Desuperheater/Contact Condenser 9102-C-11 bottom by checking 91-LG-1303A/B & 91-LT-1307. 13. When the level in the Desuperheater/Contact Condenser 9102-C-11 bottom reaches 50%, close the DM water make up to the pump suction and put the level control valve 91-LV-1307 in auto with a set point of 50%. 14. Take the flow control valve FV-1314 in auto with a set point of 199 m3/hr. 15. Start Desuperheater Circulation Pump 9102-P-11A from ICSS and start circulating the water. 16. Ensure that the Desuperheater Circulation Pump 9102-P-11B is taken in AUTO from ICSS and the suction and discharge isolation valves are opened and primed. 17. Line up pH analyzer 91-AT-1302 in the suction of the Desuperheater Circulation Pumps 9102-P-11A/B. III. Lining up of Caustic Solution Injection Pumps 9103-P-103A/B 1. Ensure that the Caustic Solution Injection pumps 9103-P-103A/B suction strainer elements are fixed and boxed up. 2. Ensure that the Caustic Solution Injection Pumps 9103-P-103A/B discharge PSVs PSV-1606/1607 are lined up. 3. Open the Caustic Storage Tank outlet isolation valve to the injection pumps and fill the lines with the Caustic Solution. 4. Open the suction isolation valves of the injection pumps. 5. Open the discharge isolation valve of the Caustic Injection Pump 9103-P-103A. 6. Put the LOR switch of the Caustic Injection Pump 9103-P-103A in ‘Local’. 7. Start the Caustic Solution Injection Pump 9103-P-103A from LCP. 8. Put the stroke length of the Caustic Solution Injection Pump 9103-P-103A at 10%. 9. Ensure that the Caustic Solution Injection Pump 9103-P-103A is developing pressure by checking the discharge pressure transmitter 91-PT-1563. 10. Open the drain valve near the dosing point and ensure that the line is clear. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 306 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11. Line up Caustic Solution to the Desuperheater Circulation Pump suction till a pH of 9.0 to 10.0 is achieved in the circulating solution. IV. Calibration of Caustic Injection Pumps 1. Stop the Caustic Injection Pumps 9103-P-103A/B from ICSS. 2. Slowly open the calibration pot inlet isolation valves and fill up the pot up to the full level. 3. Close the suction isolation valves of the Pumps upstream of the calibration pot. 4. Open the Caustic Injection Pump 9103-P-103A discharge isolation valve. 5. Set the Caustic Injection Pump 9103-P-103A stroke to 10%. 6. Start the Caustic Injection Pump 9103-P-103A from ICSS. 7. Note down the time taken to pump out the liquid from the calibration pot. 8. Calculate the pumping rate from the volume of the calibration pot and time taken to pump the liquid from the pot. 9. Repeat the above procedures for stroke length of 20%, 30%, 40%, 50%, 60%, 70%, 80%, 90% and 100%. 10. List all the values and find out the pumping rate at different stroke lengths. 6.3.4.2 Preparation for Start-up 1. Ensure that the instrument air from instrument air header to the Reducing Gas Generator 9102-F-11 isolation valve is closed. 2. Ensure that the spectacle blind is in open position downstream of the isolation valve of the instrument air from instrument air header to the Reducing Gas Generator 9102-F-11. 3. Ensure that the fuel gas from fuel gas distribution to Reducing Gas Generator 9102-F-11 isolation valve is closed. 4. Ensure that the spectacle blind is in open position downstream of the isolation valve of the fuel gas from fuel gas distribution to Reducing Gas Generator 9102-F-11. 5. Ensure that the steam from steam distribution to Reducing Gas Generator 9102-F-11 isolation valve is closed. 6. Ensure that the spectacle blind is in open position downstream of the isolation valve of the steam from steam distribution to Reducing Gas Generator 9102-F-11. 7. Ensure that the combustion air from combustion air blower 9102-K-11A/B to Reducing Gas Generator 9102-F-11 isolation valve is closed. 8. Ensure that the spectacle blind is in open position downstream of the isolation valve of the combustion air from combustion air blower 9102-K-11A/B to Reducing Gas Generator 9102-F-11. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 307 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 9. Ensure that the Nitrogen from Nitrogen distribution header to Reducing Gas Generator 9102-F-11 isolation valve is closed. 10. Ensure that the spectacle blind is in open position downstream of the isolation valve of the Nitrogen from Nitrogen distribution header to Reducing Gas Generator 9102-F-11. 11. Ensure that the drain and vent valves in the Reducing Gas Generator 9102-F-11 section is closed. 12. Ensure that all the instruments in Reducing Gas Generator 9102-F-11, Hydrogenation Reactor 9102-V-11, Reactor Effluent Cooler 9102-E-11 are lined up. 13. Ensure that the Reactor Effluent Cooler 9102-E-11 atmospheric steam vent isolation valves are open. 14. Ensure that the Reactor Effluent Cooler 9102-E-11 vents and drains isolation valves are closed. 15. Ensure that the SRU tail gas valve to the TGTU 91-XV-1098 is closed at SRU. 6.3.4.3 Lining up of Reactor Effluent Cooler 9102-E-11 1. Open Reactor Effluent Cooler 9102-E-11 tail gas outlet to Desuperheater/Contact Condenser 9102-C-11 ON-OFF valve 91-XV-1332 from ICSS by selecting open position in HS-1303A. 2. Close the Reactor Effluent Cooler 9102-E-11 tail gas outlet to Incinerator 9101-F-14 bypass ON-OFF valve 91-XV-1331 from ICSS by selecting close position in HS-1303A. 3. Ensure that the steam outlet isolation valve from Reactor Effluent Cooler 9102-E-11 is closed. 4. Ensure that the Boiler Feed Water from distribution header to the Reactor Effluent Cooler isolation valves are closed and the level control valve 91-LV-1302 is closed fully on manual. 5. Ensure that the Boiler Feed Water is available from utility plant. 6. Ensure that the process gas from the Desuperheater/Contact Condenser 9102-C-11 to the Tail Gas Amine Absorber 9102-C-12 isolation valve is closed. 7. Open the process gas recycle isolation valve from the Desuperheater/Contact Condenser 9102-C-11 top to the Reducing Gas Generator 9102-F-11. 8. Ensure that the process gas start-up bypass from the Desuperheater/Contact Condenser 9102-C-11 to the Incinerator 9101-F-14 is lined up and take the pressure controller 91-PIC-1308 in Auto with a set point of 0.25 barg. 9. Connect a Nitrogen hose to the vent line of the start-up bypass line from the Desuperheater/Contact Condenser 9102-C-11 to the Reducing Gas Generator 9102-F-11. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 308 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10. Open the isolation valve of the start-up bypass line near the Reducing Gas Generator 9102-F-11. 11. Introduce Nitrogen through the hose to the Reducing Gas Generator via the process gas inlet line. 12. Ensure that the start-up pressure control valve PIC-1308 opening to control the excess Nitrogen gases to the Incinerator from Desuperheater/Contact Condenser 9102-C-11. Close the nitrogen valve. 13. Open the Start-up Gas Steam Ejector 9102-X-11 process gas inlet and outlet isolation valves. 14. Open the Boiler Feed Water to Reactor Effluent Cooler 9102-E-11 isolation valves. 15. Open the level control valve 91-LV-1302 in manual and introduce Boiler Feed Water to the Reactor Effluent Cooler 9102-E-11. 16. Slowly increase the level in the Reactor Effluent Cooler 9102-E-11. 17. When the level in the Reactor Effluent Cooler 9102-E-11 is around 85%, take the level control valve LV-1302 in Auto with a set point of 80%. 6.3.4.4 Circulating Nitrogen through TGTU 1. Ensure that RGG, Hydrogenation Reactor, Reactor Effluent Desuperheater/Contact Condenser is pressurised with nitrogen. Cooler and 2. Open LP Steam drain valve and slowly open the upstream isolation valve to the Start-Up Gas Steam Ejector 9102-X-11. 3. Drain the condensate from the LP steam line and slowly warm up the line. 4. Open the steam ejector outlet isolation valve and then open the steam inlet isolation valve to the steam ejector 9102-X-11. 5. Open the process gas inlet line to the steam ejector and start circulating Nitrogen around the TGTU BSR Section. Nitrogen gases will flow through and around the RGG, Hydrogenation Reactor, Reactor Effluent Cooler and DCC Desuperheater/Contact Condenser 9102-C-11 with excess gases being vented to the Incinerator through 91-PV-1308. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Rev.: 0 Date: 03/09/2012 Page: 309 of 517 Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 32 - Burner Management Sequence for RGG Start A Note A Note B & Y Fuel gas vent valve XV-1308 close, Fuel gas XV-1303, XV-1304 and air shutdown valve XV-1306 open, igniter insertion, activation of 10 sec timer for ignition transformer System Reset HS-1400 Automatic bypass of combustion air (FT-1309), fuel gas (PT-1305) low low alarm Confirm FG, combustion air, quench steam control valve closed System ready for purge-XL-1401 Burner ignition timer completed N Flame Detected on 2oo3 logic Purge start HS-1401 Nitrogen SDV-XV-1307, XV-1301 open Y BAL-1301, BAL-1302, BAL-1303 ON Fuel Gas ON-XL-1404 Nitrogen flow alarm FAL-1308 Y Quench steam start-HS-1406 N XV-1305 open, XL-1407 ON Common Alarm XL-1405 Purge timer – 7.5 minutes completed N Tail gas Start-HS-1052A from DCS Light ON timer out XL-1406 Y Purge Complete XL-1403 Nitrogen SDV-XV-1307 close, 10 min light on cycle initiated XV-1098 open Instrument air purge valve XV-1032 open and close nitrogen purge valve XV-1301 Furnace is fully operational Burner start HS-1402 A Note A Following causes should be healthy for system reset: 1. RGG DCS soft push button HS-1336 2. RGG ESD push button HS-1337 in LCP 3. ESD total plant shutdown XS-1101 4. ESD level-1 shutdown XS-1102 5. ESD level-2 shutdown XS-1103 6. FG to RGG burner HI HI pressure PAHH-1303 7. Combustion air high high pressure PT-1341 8. Reactor effluent cooler low low level LT-1309 9. RGG process gas Outlet temperature high high TT1305 Note B Following are the interlocks for purging: 1. No flame detection by BSL-1301/1302/1303 2. Nitrogen flow low should be absent 3. FG control valve at low fire position 4. FG Block valve XV-1303 in close position 5. FG Block valve XV01304 in close position 6. FG vent valve XV-1308 in open position EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 310 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.3.4.5 Lighting up of Burner in Reducing Gas Generator 9102-F-11 Burner Light On The burner light-on is carried out in three steps. i. System reset ii. Pre-ignition purge iii. Direct fuel gas light-on i. System Reset 1. Check the following shutdown interlocks are absent in the ICSS: a. RGG Shutdown soft push button from DCS – 91-HS-1336 b. RGG ESD push button (Local Panel) – 91-HS-1337 c. ESD Level 0 Total Plant Shutdown – 65-XS-1101 d. ESD Level 1 Shutdown – 65-XS-1102 e. ESD Level 2 Shutdown – 65-XS-1103 f. Fuel Gas to RGG burner high high pressure – 91-PT-1303 g. Combustion air high high pressure – 91-PT-1341 h. Reactor Effluent Cooler low low level – 91-LT-1309 i. RGC Process gas outlet high high temperature – 91-TT-1305 If the above conditions are not exists, then the RGG BMS system can be reset. 2. The following shutdown causes are automatically bypassed during start-up a. 91-PT-1305 (Fuel Gas low low pressure) b. 91-FT-1309 (Combustion Air low low flow) 3. Start Combustion Air Blower 9102-K-11A To start the Blower 9102-K-11A, the following permissives are to be satisfied: a. Instrument air must be available and the seal air low low pressure 91-PALL1460 is reset. b. The lube oil tank level 91-LT-1451 is more than 30%. c. Lube oil temperature in the tank 91-TT-1473 is greater than 15°C. d. The auxiliary lube oil pump 91-P-13A is started and running and the low low lube oil pressure 91-PI-1459 is reset. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 311 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. All trip functions must be healthy. f. Three minute restart timer is completed. g. The Blower is not running h. IGV valve 91-PCV-1453 is closed i. Blow off valve 91-FV-1451 is open j. Blower ready to start indication is ON k. Blower running indication is OFF. l. Blower common trip alarm is OFF. Blower Start-up a. Ensure that blower ready to start indication is available in the Local Control Panel. b. Switch ON the electrical heater for the Lube Oil tank 91-E-15AA. c. Ensure that the temperature of the Lube oil is increasing by checking 91-TI-1463. d. When the temperature reaches 45°C ensure that the heater is cut off automatically. e. Ensure that when the temperature reaches 40°C, the heater is cut in automatically. f. Start the Auxiliary Oil Pump 91-P-13A. g. Ensure that the Auxiliary Oil Pump 91-P-13A develops a discharge pressure of 5.50 barg. h. Line up the instrument air to the seal system of the blower and ensure that the low low seal air pressure 91-PALL-1460 is reset by 91-HS-1471. i. Select “Local” from the Local Control Panel 9102K11A-LP-003 selector switch 91-HS-1452. j. Start the Blower by pushing the start push button 91-HS-1454. k. Ensure that the Blower is started and running. l. Ensure that the Lube Oil Cooler duty fan is started and running. m. Ensure that the air filter inlet inertial fan is started and running. n. Ensure that the IGV valve opens in unloaded condition. o. Ensure that the blow off valve 91-FV-1451 is open. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 312 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL p. After 17 minutes ensure that the Auxiliary Oil Pump 91-P-13A is stopped and the Blower load function is enabled. q. Load the Blower from the Local Control Panel selector switch 91-HS-1455. r. Ensure the discharge pressure of the blower is 1.57 bara. s. The following conditions are to be satisfied for the pre-ignition purge: i. No flame present – 91-BSL-1301/1302/1303 ii. Sufficient purge Nitrogen flow rate – 91-FAL-1308 iii. FG Control valve at low fire position – 91-FZSL-1311 iv. Fuel Gas cut-in valve XV-1303 is in close position – 91-ZSC-1303 v. Fuel Gas cut in valve XV-1304 is in close position - 91-ZSC-1304 vi. Fuel Gas vent valve XV-1308 is in open position - 91-ZSO-1308 Ensure the above conditions are satisfied. t. Ensure that the combustion air flow control valve 91-FV-1304, Fuel Gas flow control valve FV-1311 and quench steam flow control valve FV-1310 are closed. u. RESET the system by pressing the pushbutton 91-HS-1400 from the local control panel. ii. Pre-ignition Purge 1. Verify whether the ‘System ready for purge’ lamp 91-XL-1401 is lit after RESET at Local Control Panel. 2. Ensure that the Nitrogen shutdown valve 91-XV-1307 for furnace purging and 91-XV-1301 for flame scanner, sight glass purging are opened. 3. Ensure that main combustion air shutdown valve 91-XV-1306 & instrument air valve 91-XV-1302 (for flame scanner, sight glass purging) are closed. 4. Open the Nitrogen line isolation valve slowly and set a flow rate of 125 m3/hr read by 91-FT-1308. 5. Press ‘Purge Start’ Pushbutton 91-HS-1401 from the Local Control Panel. 6. Ensure that the ‘Purge On’ lamp 91-XL-1402 is lit in the Local Control Panel. 7. Set the purge timer at 7.5 minutes. 8. Verify whether the ‘Purge On’ lamp 91-XL-1402 is lit for 7.5 minutes in the Local Control Panel. 9. After the purge time is over, ensure that the ‘Purge On’ lamp 91-XL-1402 is unlit in the Local Control Panel. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 313 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10. Ensure that ‘Purge Complete’ lamp 91-XL-1403 is lit on the Local Control Panel. 11. Ensure that the Nitrogen cut-in valve 91-XV-1307 is closed. iii. Fuel Gas Burner Light On 1. Ensure that the air inlets, burner and outlet passages are boxed up and free of foreign material. 2. Ensure that all personnel have been evacuated from the RGG area, ductwork and associated equipment and all access and inspecting doors closed and sealed. 3. Ensure that the Combustion Air Blower 9102-K-11A/B is running. 4. Ensure that all safety shut off valves are closed. 5. Ensure that the Fuel System vents are open and venting to atmosphere. Lines are properly drained and cleared of condensate. 6. Ensure that a complete functional check of the safety interlocks has been made. 7. Ensure that the area is clear of obvious safety hazards and flammable gases are not present in the area. 8. Ensure that all lines have been blown down with plant air to insure they are free of debris that might plug metering orifices and burner tips. 9. Ensure that utilities like fuel gas, instrument air, Nitrogen and plant air are available and initial operational checks performed on the elements in each line. 10. Ensure that the burner elements are in their proper position. 11. Ensure that power has been supplied to control systems and to safety interlocks. 12. Ensure that the gauges indicating fuel header pressure to the unit are functional. 13. Ensure that the pressure self regulating valves are set according to the instrument data sheets. 14. Ensure that the isolation valves for all the pressure gauges and pressure transmitters are open and their respective bleed valves are closed. Valves are sealed in position as indicated on P&IDs. 15. Ensure that the 2” steam drum vent isolation valves of the reactor effluent cooler are open. 16. Ensure that the Reactor Effluent Cooler is filled with boiler feed water and the level is being maintained at 80%. 17. Ensure that the minimum purge period is satisfactorily completed. 18. Ensure that the control valves of the fuel gas - 91-FV-1311, quench steam – 91-FV1310 and Combustion Air – 91-FV-1304 are closed. 19. Ensure that the igniter is in the correct position and that the fuel gas gun is ready for operation with fuel gas. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 314 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 20. Ensure that the ‘Purge Complete’ lamp 91-XL-1403 is lit in the local control panel. 21. Open the fuel gas control valve 91-FV-1311 from ICSS to the pre-determined position signalled by the lamp 91-FZAL-1311 at the local control panel. 22. Open the combustion air control valve 91-FV-1304. 23. Press the ‘Burner Start’ push button 91-HS-1402 from the local control panel. 24. Ensure that ‘Purge Complete’ lamp 91-XL-1403 is unlit. 25. Ensure that the igniter insert SOV is energised. 26. Ensure that the igniter insertion is proved by limit switch 91-ZSC-1400. 27. Ensure that the igniter transformer is energised for 10 seconds and sparking begins. 28. Ensure that the combustion air shutdown valve 91-XV-1306 is opened. 29. Ensure that the fuel gas bleed valve 91-XV-1308 is closed. 30. Ensure that the fuel gas shutdown valves 91-XV-1303 and 1304 are opened. 31. Ensure that the igniter transformer is de-energised and Igniter retracts automatically (91-ZSO-1400) after 10 seconds ignition timer. 32. If flame is detected then ensure that the ‘FLAME ON’ lamps (91-BAL-1301, 91-BAL1302, 91-BAL-1303) are lit. 33. Ensure that the fuel gas control valve correct start-up position lamp 91-FZSL-1311 is unlit. Note: Permit is provided to open the steam quench shutdown valve 91-XV-1305 from ICSS soft switch 91-HS-1406 34. Permit is provided to open the tail gas shutdown valve 91-XV-1098 from ICSS soft switch 91-HS-1052A. 35. Ensure that the ‘FUEL GAS ON’ lamp 91-XL-1404 is lit in the Local Control Panel. 36. Ensure that the ‘FUEL GAS ON’ lamp 91-XL-1410 is lit in ICSS. 37. Ensure that the instrument air purge valve 91-XV-1302 to sight glasses, flame scanners and nozzles is opened. 38. Ensure that the Nitrogen purge valve 91-XV-1301 to sight glasses, flame scanners and nozzles is closed. 6.3.4.6 Hydrogenation Reactor Catalyst Sulphiding 1. Warm up the Hydrogenation Reactor 9102-V-11 at 50°C/hr by opening the combustion air and the fuel gas to the RGG. 2. Open the LP steam shutdown valve 91-XV-1305 to the RGG by manual reset of the soft push button 91-HS-1406 from ICSS. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 315 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 3. When RGG outlet and Hydrogenation Reactor inlet temperature is 200°C and the Hydrogenation Reactor is heated through to >120°C, introduce LP steam to the RGG by opening the steam inlet control valve 91-FV-1310. 4. Set the steam flow in a ratio of 2:1 by weight to fuel gas in 91-HIC-1311. 5. Boiler feed water in the Reactor Effluent Cooler 9102-E-11 are heated by the effluent gases from the Hydrogenation Reactor 9102-V-11 and steam will start coming out of the drum vent. 6. Slowly close the drum vent and increase the pressure in the drum to the LP steam header pressure of 5.0 barg which is read by the drum pressure gauge 91-PT-1309. 7. When the drum pressure reaches 5.0 barg, open the steam outlet isolation valve connecting to the header and close the drum vent fully at the same time. 8. When the Hydrogenation Reactor has heated through to 200°C the sulphiding of the catalyst should be started. 9. Check the temperature transmitters in the catalyst bed 91-TT-1303/1306/1308/ 1309/1318/1319/1320/1321/1322 from ICSS. 10. All the temperature points should be around 200°C. 11. Line up the isolation valves of the Acid Gas sulphiding line from Regenerator Reflux Drum 9103-V-12 to the Hydrogenation Reactor 9102-V-11. 12. Open the Acid Gas sulphiding line control valve 91-HV-1301 slowly and introduce acid gases to the Hydrogenation Reactor 9102-V-11. 13. Introduce acid gases for 1% - 2% volume of H2S initially in the process gases. Note: The reaction of H2S in the Hydrogenation Reactor catalyst is exothermic. For every 1% volume of H2S entering the reactor a catalyst temperature increase of approximately 15°C can be expected. 14. Slowly increase Hydrogenation Reactor inlet temperature at a rate of approximately 15°C/hr to 315°C whilst keeping the catalyst bed delta temperature <25°C. 15. If the exothermic reactions produce a catalyst bed delta temperature >25°C then reduce the flow of H2S acid gas into the Hydrogenation Reactor. Note: Under no circumstances should catalyst temperature be allowed to exceed 425°C as damage to the catalyst and equipment will occur. 16. As soon as amine acid gas is introduced into the Hydrogenation Reactor inlet line start sampling the reactors inlet and outlet process gas. 17. A hand held Drager tube type sampling system is suggested where an immediate read out of H2S in % or ppm can be seen. 18. Continue sampling reactor outlet gas at one hour intervals. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 316 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 19. When the Hydrogenation Reactor has been fully sulphided, the reactor outlet gas H2S concentration will equal the inlet gas H2S concentration. 20. Maintain the reactor catalyst bed temperature at 390°C with the H2S rich amine acid gas flow to the reactor for a minimum of 4 hours to ensure the catalyst is fully sulphided. 21. Stop the flow of the H2S rich amine acid gas to the inlet of the Hydrogenation Reactor by closing the isolation valves near the Hydrogenation Reactor inlet line and the Regenerator Reflux Drum. 22. Depressurise the line through the drain line given upstream of the check valve. 23. Connect a Nitrogen hose to the acid gas line and purge the line through the drain line to acid gas flare. 24. Close the control valve 91-HV-1301 in the acid gas line. 25. Reverse the spectacle blinds to close position at both the ends of the acid gas line. 26. Reduce the reactor inlet temperature to 290°C by slowly reducing the firing. 27. Sulphiding of the reactor catalyst is now complete and the TGTU is now ready to receive and process SRU tail gases. 6.3.4.7 Lining up of Tail Gases to the TGTU 1. Confirm that the SRU is operating at near to its minimum design acid gas feed rate. 2. When the SRU operation has stabilised commission the tail gas analyzer 91-AT-1001. 3. Set a H2S:SO2 ratio of 4.0:1.0 in the controller 91-ARC-1001. 4. Open the Reactor Effluent Cooler 9102-E-11 outlet ON-OFF valve 91-XV-1331 to the Incinerator 9101-F-14. 5. Close the Reactor Effluent Cooler 9102-E-11 outlet ON-OFF valve 91-XV-1332 to the Desuperheater/Contact Condenser 9102-C-11. 6. Open the manual isolation valve in the Desuperheater/Contact Condenser 9102-C-11 gas outlet to the Tail Gas Amine Absorber 9102-C-12. 7. Simultaneously open the SRU tail gas ON-OFF valve 91-XV-1098 to the TGTU and close the ON-OFF valve 91-XV-1097 to the Incinerator 9101-F-14. 8. Slowly open the downstream isolation valve of the ON-OFF valve 91-XV-1098 and start the tail gas flow to the Reducing Gas Generator. 9. Close the LP steam supply isolation valve to the Start-up Gas Steam Ejector 9102-X-11. 10. Close the process gas inlet isolation valve to the Start-up Gas Steam Ejector 9102-X-11 and outlet valve from the Start-up Gas Steam Ejector 9102-X-11. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 317 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11. Close BSR section start-up vent gas pressure control valve 91-PV-1308 and manual isolation valves. 12. Close Nitrogen supply to the RGG process gas inlet line. 13. Observe Hydrogenation Reactor operation, catalyst temperature will increase as exothermic reactions take place in the reactors catalyst. 6.3.4.8 Lining up of TGTU Wet Section 1. Ensure that the DCC 9102-C-11 process outlet gas isolation valve to the Tail Gas Amine Absorber 9102-C-11 is open. 2. Ensure that DCC top chimney tray level is made up and the Cooling Water Circulation Pump 9102-P-12A/B is running circulating water back to the DCC top section. 3. Ensure that sea cooling water is lined up to the Contact Condenser Trim Cooler 9102-E-13A/B. 4. Ensure that the Contact Condenser Cooler 9102-E-12 fans are started and running. 5. Ensure that the DCC bottom Desuperheater section water level is made up and the Desuperheater Circulation Pump 9102-P-11A/B is started and circulating water to the Desuperheater bottom 9102-C-11. 6. Ensure that the desuperheater circulating water pH is maintained in the range of 9.0-10.0. 7. Line up lean amine to the Tail Gas Amine Absorber 9102-C-12 by opening all the isolation valves from the Lean Amine Pumps 9103-P-13A/B discharge. 8. Reset process shutdown and ensure that lean amine to Tail Gas Amine Absorber 9102-C-12 inlet ON-OFF valve 91-XV-1310 is opened. 9. Open the lean amine flow control valve 91-FV-1301 slowly and establish a flow of lean amine to the Tail Gas Amine Absorber 9102-C-12. Put the control valve 91-FV1301 in auto with a set point of 110 m3/hr. 10. Ensure that the low low level alarm 91-LALL-1301 in the Tail Gas Amine Absorber 9102-C-12 is cancelled. 11. Check the level transmitter 91-LT-1308 and ensure that the level is increasing in the Tail Gas Amine Absorber 9102-C-12. 12. When the level reaches to about 50% in the Tail Gas Amine Absorber 9102-C-12, line up the Tail Gas Rich Amine Pumps 9102-P-16A/B by opening the suction and discharge isolation valves. 13. Keep the Tail Gas Rich Amine Pumps 9102-P-16A/B discharge control valves 91-FV1325 & 91-FV-1303 in closed condition. 14. Fill up the Tail Gas Rich Amine Pumps 9102-P-16A/B casing, by opening the casing vent valve and releasing Nitrogen. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 318 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 15. Put the LOR switch of the Tail Gas Rich Amine Pumps 9102-P-16A/B in ‘Remote’. 16. Reset the process shutdown and ensure that the Tail Gas Rich Amine Pumps 9102-P-16A/B discharge ON-OFF valve 91-XV-1309 is opened. 17. Start the Tail Gas Rich Amine Pump 9102-P-16A from ICSS. Put the Tail Gas Rich Amine Pump 9102-P-16B in AUTO from ICSS. 18. Open the minimum flow control valve 91-FV-1303 in manual and establish a flow rate of 31.25 m3/hr. Put the controller 91-FIC-1303 in AUTO with a set point of 31.25 m3/hr. 19. Take the level controller 91-LIC-1308 in AUTO with a set point of 50%. 20. Take the flow controller 91-FIC-1325 in REMOTE and ensure the level of the Tail Gas Amine Absorber is maintained at 50%. 21. Ensure that the level in the Acid Gas Amine Absorber 9103-C-11 is maintained due to the lining up of the rich amine from Tail Gas Amine Absorber 9102-C-12. 22. Ensure that the SRU is in stable operation and the acid gas feed to the SRU at or above the minimum design flow rate. 23. Ensure that the TGTU Hydrogenation Reactor is in a stable operation. 24. Open the Reactor Effluent Cooler process gas outlet valve 91-XV-1322 to the DCC and the close the process gas outlet valve 91-XV-1331 to the Incinerator 9101-F-14 through the hand switch 91-HS-1303A from the ICSS. 25. Check the Tail Gas Amine Absorber 9102-C-12 outlet vent gas line H2 and H2S analysers 91-AI-1301 in ICSS. The H2 analyser should show a minimum of 1.5% excess H2 in the vent gases. 26. Closely observe the Incinerator’s operation as the unit stops incineration of the H2S rich process gases from the Reactor Effluent Cooler and commences incineration of the very dilute in H2S rich vent gases from the Tail Gas Amine Absorber. 27. Ensure that the DCC cooling water circulation level control valve 91-LV-1305 is taken in auto with a set point of 50%. 28. Ensure that the DCC Desuperheater top up water control valve 91-LV-1307 is taken in auto with a set point of 50%. 29. Ensure that the level in the Contact Condenser is always maintained at 50% by making up with DM water if needed. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 319 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 6.4 RAMP UP OF PLANT LOAD 1. Check the flow of acid gases from Regenerator Reflux Drum 9103-V-12 to Acid Gas KO Drum 9101-V-04 of SRU is above the minimum turndown required of 5935 kg/hr, for the SRU to operate. 2. Gradually increase the flow from Regenerator Reflux Drum 9103-V-12 to Acid Gas KO Drum 9101-V-04 of SRU. 3. Ensure the Acid Gas Pre-heater 9101-E-06 outlet temperature is maintained at 200°C. 4. Adjust the process air flow to the Reaction furnace accordingly. 5. Ensure that the Process Air pre-heater 9101-E-05 outlet temperature is maintained at 200°C. 6. Ensure that steam drum 9101-V-07 level is maintained. 7. Ensure that 1st Stage Converter 9101-V-01 inlet temperature is maintained at 230°C. 8. Ensure that 2nd Stage Converter 9101-V-02 inlet temperature is maintained at 210°C. 9. Ensure that the level in the Sulphur Degassing Pit 9101-T-01 is maintained. 10. Ensure that the tail gases from the SRU to the TGTU have gradually increased due to the load increase in the SRU. 11. Ensure that the combustion air flow to the Reducing gas Generator has increased accordingly. 12. Ensure that the Hydrogenation Reactor 9102-V-11 inlet temperature and outlet temperature are maintained at 290°C and 320°C. 13. Ensure that the BFW level is maintained in the Reactor Effluent Cooler 9102-E-11. 14. Ensure that the Tail Gas Amine Absorber level, pressure and temperature parameters are maintained. 15. Ensure that the Incinerator is at its normal operating temperature of 817°C. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 320 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION VII OPERATION & MONITORING EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 321 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7.1 PROCESS PLANT OPERATION AND MONITORING 7.1.1 Acid Gas Enrichment Unit The absorption of H2S by the Methyl Di Ethanol Amine (MDEA) in the Acid Gas Amine Absorber 9103-C-11 is a function of the following: • The flow and distribution of MDEA falling down the Acid Gas Amine Absorber tower through the upward flow of process gases • The temperature of the lean MDEA entering the Acid Gas Amine Absorber 9103-C-11. • The concentration and condition of the lean MDEA entering the Acid Gas Amine Absorber 9103-C-11 Monitoring of the amine unit will include the following: • Regularly check the following vessels and towers level gauges and compare with DCS indicated levels: Sl. # 1. • Vessel Lean Acid Gas KO Drum Vessel Tag No. Level Gauge Tag No. 9103-V-14 9103-LG-1501A 9103-LG-1501B 2. Acid Gas Amine Absorber 9103-C-11 9103-LG-1505A 9103-LG-1505B 9103-LG-1505C 9103-LG-1505D 3. Amine Regenerator 9103-C-12 9103-LG-1506A 9103-LG-1506B 4. Regenerator Reflux Drum 9103-V-12 9103-LG-1502 5. Regenerator Reboiler Condensate Pot 9103-V-13 9103-LG-1504A 9103-LG-1504B 6. Regenerator Reboiler 9103-E-13 9103-LG-1503 Regularly check the function of the following level transmitters and alarms to confirm correct operation: Sl. # 1. 2. Vessel Lean Acid Gas KO Drum Acid Gas Amine Absorber Vessel Tag No. Level Transmitter Tag No. 9103-V-14 9103-LT-1501 9103-LT-1502 9103-LT-1503 9103-C-11 9103-LT-1505 9103-LT-1504 9103-LT-1516 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 322 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # • Vessel Tag No. Level Transmitter Tag No. 3. Amine Regenerator 9103-C-12 9103-LT-1509 9103-LT-1510 9103-LT-1517 4. Regenerator Reflux Drum 9103-V-12 9103-LT-1506 9103-LT-1518 5. Regenerator Reboiler Condensate Pot 9103-V-13 9103-LT-1508 Confirm that the following pumps are operating satisfactorily. Periodically run each spare pump and check the operation: Sl. # • Vessel Pump Pump Tag No. 1. Acid Gas KO Drum Return Pump 9103-P-14A/B 2. Acid Gas Rich Amine Pumps 9103-P-12A/B 3. Hot Lean Amine Pumps 9103-P-17A/B 4. Regenerator Reflux Drum Pumps 9103-P-11A/B 5. Lean Amine Pumps 9103-P-13A/B 6. Amine Sump Pump 9103-P-15 Confirm that the following air cooler fans are operating satisfactorily. Periodically run each spare fan and check the operation: Sl. # 1. 2. Fan Fan Tag No Regenerator Condenser Cooler 9103-E-12AA 9103-E-12AB 9103-E-12AC 9103-E-12BA 9103-E-12BB 9103-E-12BC 9103-E-12CA 9103-E-12CB 9103-E-12CC 9103-E-12DA 9103-E-12DB 9103-E-12DC Lean Amine Cooler 9103-E-14AA 9103-E-14AB 9103-E-14AC 9103-E-14BA 9103-E-14BB 9103-E-14BC EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 323 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Fan Fan Tag No 9103-E-14CA 9103-E-14CB 9103-E-14CC 9103-E-14DA 9103-E-14DB 9103-E-14DC 9103-E-14EA 9103-E-14EB 9103-E-14EC 9103-E-14FA 9103-E-14FB 9103-E-14FC 9103-E-14GA 9103-E-14GB 9103-E-14GC 9103-E-14HA 9103-E-14HB 9103-E-14HC 9103-E-14IA 9103-E-14IB 9103-E-14IC 9103-E-14JA 9103-E-14JB 9103-E-14JC • Maintain lean amine flows to the amine absorbers at the correct flows for efficient absorption of H2S in the towers. • Maintain amine and gas temperatures as given below: Flow • Pressure, bar(a) Temp. °C Amine flow to Acid Gas Amine Absorber 9103-C-11 4.69 45 Process gas flow to Acid Gas Amine Absorber 9103-C-11 1.38 49 Regularly test the concentration of the lean amine. Add fresh amine if the strength is <50%. A low strength or weak solution will result in the inefficient absorption of H2S in the absorber with the possibility of slippage of off specification treated gas. This will be detected by the treated gas analyser 91-AI-1501 showing a higher than normal concentration of H2S and other sulphur species in the absorber effluent vent gases to the Incinerator 9101-F-14 resulting in an increase of SO2 emissions to atmosphere from the Incinerator Stack 9101-X01. Increasing the amine solution strength should correct this problem. An initial EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 324 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL correction may be possible by increasing the circulating flow of the amine solution above its normal design flow rate until the strength of the solution can be corrected. • Regularly check the H2S/H2 analyzer 91-AT-1501 for normal operation. • Regularly check that the nitrogen blanketing systems to the Amine Surge Tank 9103-T-11 and to the Amine Sump 9103-V-10 are operating; failure of a blanketing gas system and the ingress of air will result in the degradation of the amine and the production of sludge in the system. • Maintain the Amine Surge Tank 9103-T-11 at minimum level, 20-30%, so that space is available in the tank to store amine from the system at times when the unit is shutdown for inspection. • Replace water losses by adding condensate to the Amine Surge Tank 9103-T-11. • Maintain a steam (Kg/hr) to the Regenerator Re-boiler 9103-E-13 to rich amine (m3/hr) to the Amine Regenerator 9103-C-12 ratio of 118.5:1.0 to ensure efficient stripping of H2S from the amine in the Amine Regenerator 9103-C-12. Insufficient LP steam flow to the Regenerator Re-boiler 9103-E-13 or fouling of the Re-boiler tubes will result in incomplete regeneration of the rich amine solution. Increasing the LP steam flow should correct the problem, however severely fouled Re-boiler tubes will require a unit shutdown to allow the Re-boiler to be cleaned. • Monitor the Acid Gas Amine Absorber 9103-C-11 differential pressure indicator and Amine Regenerator 9103-C-13 differential pressure indicator as given below. A gradual increase in pressure differential in a tower over a period of time will indicate fouling, whilst an increase in pressure differential over a short period will indicate foaming or flooding of the tower. In this case antifoam should be injected into an injection point before the problem tower and the amine circulation flow should be temporarily reduced to reduce the liquid/vapour loadings across the towers packed sections. Tower • Tag No. High alarm Acid Gas Amine Absorber 9103-C-11 9103-PDI-1522 0.15 bar Amine Regenerator 9103-C-13 9103-PDI-1523 0.2 bar Monitor the amine filters beds differential pressure indicators as given below. When a filter pressure differential pressure reaches an advised number (high alarm), remove the filter from service to replace its filtration medium/cleaning. Tower Tag No. High alarm Lean Amine Filter 9103-S-11 9103-PDI-1517 0.5 bar Activated Carbon Filter 9103-S-12 9103-PDI-1518 0.5 bar Fines Filter 9103-S-13 9103-PDI-1519 0.5 bar EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 325 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • If corrosion is detected in the amine system then inject Corrosion Inhibitor into one or more of the injection points to protect the system. • Normal Operating Parameters - AGEU Tag. No Description Value Unit 91-TI-1501 Acid gas feed to Acid Gas Amine Absorber temperature 48 °C 91-FI-1501 Lean amine flow to Acid Gas Amine Absorber 487 m3/hr 91-TI-1511 Lean amine temperature to Acid Gas Amine Absorber 45 °C 91-TI-1504 Treated gas from Acid Gas Amine Absorber temperature 46 °C 91-AI-1501 Treated gas H2S analyser 560 ppmv 91-PIC-1502 Treated gas pressure 1.20 bara 91-FIC-1520A Rich amine flow from Rich Amine Pump 635 m3/hr 91-TIC-1513 Rich amine to Amine Regenerator temperature 104 °C 91-PDI-1522 Differential Pressure across Acid Gas Amine Absorber trays 0.1 barg 91-LIC-1505 Acid Gas Amine Absorber bottom level 50 % 91-TI-1506 Reboiler outlet Vapour temperature 131 °C 91-FIC-1503 LP steam flow to Reboiler 23789 m3/hr 91-TG-1515 LP steam inlet to Reboiler temperature 159 °C 91-LIC-1508 Regenerator Reboiler Condensate Pot level 50 % 91-PIC-1503 Regenerator Reflux Drum top pressure 1.0 barg 91-FIC-1530 Hot lean amine flow to Lean/Rich Amine Exchanger flow 669 m3/hr 91-TI-1519/ 1520 Hot lean amine from Lean/Rich Amine Exchanger temperature 84 °C 91-TIC-1509 Lean amine to Amine Surge Tank temperature 45 °C 91-PIC-1526 Amine Surge Tank pressure 0.02 barg 91-FIC-1507 Lean amine flow to Lean Amine Filters 155.6 m3/hr 91-PDI-1517 Differential pressure across Lean Amine Filter 0.5 barg 91-PDI-1518 Differential pressure across Activated Carbon Filter 0.5 barg 91-PDI-1519 Differential pressure across Fines Filter 0.5 barg 91-PDI-1523 Differential pressure across Regenerator trays 0.16 barg EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 326 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7.1.2 Sulphur Recovery Unit The operation and monitoring of the SRU includes the following activities: a. Acid Feed Gas System • Regularly check Acid Gas KO Drum 9101-V-04 level gauge 91-LG-1001 and compare with DCS indicated level 91-LI-1001 • Check for excessive liquid carryover from the upstream AGEU Amine Regenerator 9103-C-12 • Do not drain sour water to the open sewer from low point drains due to the toxic nature of the H2S saturated water and gas in the KO drums. b. H2S:SO2 Ratio Control The most important control variable in the operation of a SRU is the H2S:SO2 ratio in the tail gas at the outlet of the SRU Final Separator 9101-V-05. The following points should be noted: • If the Tail Gas Analyser 91-ARC-1001 should be temporarily out of service, sample the tail gas and analyse for H2S:SO2. Analysis of the tail gas may be carried out crudely by Drager tube or by chemical lab analysis. • Maintain the Tail Gas Analyser 91-ARC-1001 in good working order to ensure the SRU is operating at its maximum efficiency for conversion of H2S to liquid sulphur in the SRU converters (9101-V-01 & 9101-V-02) and have the correct ratio of H2S and SO2 gases for the TGTU. • The main air to acid gas ratio controller 91-HIC-1001 point is adjusted as necessary to change the main process air flow control valve position. The Tail Gas Analyser 91-ARC-1001 will control the trim air to fine tune the air required by the process to achieve the desired H2S:SO2 ratio in tail gases. When the TGTU is in service with the SRU then the SRU tail gases H2S:SO2 ratio should be 4.0:1.0. If the SRU is in service without the TGTU then the tail gases H2S:SO2 ratio should be 2.0:1.0. If the composition of the acid gas should change then the analyser may drive the trim air control valve 91-FV-1003 fully open or fully closed; in this case a small adjustment will have to be made to the main air to acid gas ratio controller to increase or decrease the total air to allow the Tail Gas Analyser to bring the trim air control valve 91-FV-1003 back onto control. • The control room operator responsible for the amine unit must inform the SRU control room operator of impending changes in acid gas flow rates and/or upset operating conditions in these units that will affect the operation of the SRU and TGTU. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 327 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL c. Controllers Operation To ensure good control of the processes at all times the following should be noted: • When the acid gas flow is steady, and the SRU is on automatic, set all controllers for maximum speed and accuracy of response with control stability. A sudden reduction in acid gas feed without the accompanied change in air rate could result in high temperatures in the SRU converters (9101-V-01 & 9101-V-02) catalyst beds; whilst a sudden increase in acid gas feed without the corresponding increase in air rate will result in an increase in the amount of acid gas in the SRU tail gas and increased load on the TGTU Desuperheater/Contact Condenser 9102-C-11 and possibly the Incinerator 9101-F-14. • An increase in H2S concentration and decrease of SO2 in the SRU tail gas to the TGTU will cause a decrease in temperature rise across the Hydrogenation Reactor 9102-V-11, whilst an increase in SO2 and decrease of H2S concentration in the SRU tail gas to the TGTU will cause an increase in temperature rise across the Hydrogenation Reactor 9102-V-11. • The SRU Tail Gas Analyser 91-ARC-1001 should be set to a maximum possible speed and response in order not to cause the SRU tail gas compositions of H2S and SO2 to vary too widely. • Steam Generators BFW level controllers should be set to maintain the water levels at their recommended levels. A swinging water level may cause water to be carried over into the steam system which will cause downstream problems with process units operations. d. Reaction Furnace Monitoring: The following points should be noted to ensure good reaction furnace operation: • Control of the SRU Reaction Furnace 9101-F-01 temperature is most important to ensure the correct reactions are occurring with the acid gas in the furnace. The Reaction Furnace 9101-F-01 temperature should ideally be maintained >1250°C to maximise thermal sulphur production in the Reaction Furnace 9101-F-01. • If Reaction Furnace 9101-F-01 temperatures appear excessive, check air and acid gas or fuel gas meters, and the Tail Gas Analyser 91-ARC-1001, to be sure the air to acid gas ratio is correct. • Be alert for hot spots on the outside of the shell of the Reaction Furnace 9101-F01 that would indicate refractory trouble. • Observe Reaction Furnace 9101-F-01 inlet pressure, an increase above normal will indicate a possible partial blockage in downstream converters and condensers and/or in the TGTU Hydrogenation Reactor and wet section towers. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 328 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. SRU Converters (9101-V-01 & 9101-V-02) The following points will help ensure efficient converter operation: • Keep close surveillance of the temperatures at the inlet of SRU 1st Stage Converter 9101-V-01 and 2nd Stage Converter 9101-V-02. Keep these temperatures at 230/210ºC to avoid liquid sulphur deposition on the catalyst. • Sulphur deposition in a SRU 1st Stage Converter 9101-V-01 and 2nd Stage Converter 9101-V-02 catalysts is indicated by a progressive catalyst bed temperature drop starting at the top and continuing downward. If this is noted, increase the corresponding converter inlet temperature by adjusting the upstream auxiliary burner outlet temperature to carry out a rejuvenation of the converters catalyst. • Over long periods of operation a decrease in the activity of a SRU 1st Stage Converter 9101-V-01 and 2nd Stage Converter 9101-V-02 catalysts will be seen. The reaction of the H2S and SO2 in the process gas combining to form sulphur vapour is seen by the exothermic reaction in the converters. As the converters catalysts age this exothermic temperature rise reaction will be seen to move further down the converters catalyst bed. The temperature rise across the first converter will decrease whilst the temperature increase across the second converter will increase. • An increased pressure drop across the SRU, seen by an increased pressure on the Reaction Furnace 9101-F-01 process air inlet line pressure indicator 91-PI-1054 A/B/C, could indicate the deposition of soot/carbon deposits on the converters catalysts. Soot and carbon deposits are the result of operating the SRU at start-up or during a hot inert gas sweep with insufficient process air or steam injection to the fuel gas in the Reaction Furnace 9101-F-01 burner or the result of excess hydrocarbons in the acid feed gases to the SRU. • SRU converters 1st Stage Converter 9101-V-01 and 2nd Stage Converter 9101-V-02 catalyst deterioration can be partially reversed by carrying out a catalyst rejuvenation exercise. Failure of signs of improved catalyst activity following a series of rejuvenations will require the catalyst to be sulphur stripped. Note that soot/carbon deactivation can only be corrected by removal of the contaminated top layers of catalyst from the reactors and replenishment with new. f. SRU Steam Generators & Condensers The following points should be carried out to ensure good operation of the Steam Generators: • Regularly check the levels (as given below) of the SRU Reaction Furnace Boiler 9101-E-07 Steam Drum 9101-V-07, Reaction Furnace Condenser 9101-E-01, 1st Stage Condenser 9101-E-02 and Last Condenser 9101-E-04. These levels can vary on load change, especially during start-up, but will normally present no problem EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 329 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL unless there is evidence of water carryover in the steam systems. In that case, gradually lower the steam generators level by operating the intermittent blow down. Blowing down too quickly could result in the start of a cycling level in the steam generator by an over compensating level controller. Sl. # Column/Vessel Level Gauges Level Transmitters 1. Reaction Furnace Boiler 9101-E-07 Steam Drum 9101-V-07 91-LG-1003 91-LG-1008 91-LT-1005 2. Reaction Furnace Condenser 9101-E-01 91-LG-1004 91-LT-1008 3. 1st Stage Condenser 9101-E-02 91-LG-1005 91-LT-1011 • Keep a record of the analysis of the treated Boiler Feed Water that enters the unit. Also maintain a record of the analysis of each Steam Generator Boiler Feed Water. These samples are drawn from the vessels continuous blow down lines through the sample coolers. • Maintain total dissolved solids, TDS, in the boiler water to below 3000 ppm for the LP Steam Generators and 1500 ppm for the SRU Reaction Furnace Boiler 9101-E-07. Control the TDS in each Steam Generator by the setting of the continuous blow down valve. • Carry out an intermittent blow down of each Steam Generator periodically to remove any accumulated sludge in the bottoms of the vessels. The frequency of this blow down will depend upon the quality of the Boiler Feed Water; a Boiler Feed Water containing a high TDS content will require more frequent intermittent blow downs than a demineralised or condensate based Boiler Feed Water that has a lower TDS content. Not using these blow downs will result in solids carry over from the Steam Generators into the steam systems. The long term result will be is the failure of the Steam Generators tubes due to overheating and or water side corrosion. • Maintain the Reaction Furnace Boiler 9101-E-07 at its operating pressure of 24.0 barg and the Reaction Furnace condenser 9101-E-01 and 1st Stage Condenser 9101-E-02 at 5.0 barg. Operating the LP steam system pressure higher than advised will result in viscous sulphur leaving the condensers and high temperatures in the sulphur pit. • Normal Operating Parameters - SRU Tag. No. Description Value Unit 91-FI-1001 Acid gas flow to Reaction Furnace burner >10912 Sm3/hr 91-TI-1003 Acid gas from Acid Gas Preheater temperature 200 °C EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 330 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Tag. No. Description Value Unit 91-FIC-1002 Main Combustion Air flow to Reaction Furnace burner 21124.6 Sm3/hr 91-FIC-1002B Secondary Air flow to Reaction Furnace burner 5744.1 Sm3/hr 91-FIC-1003 Trim Air flow to Reaction Furnace burner 2057.59 Sm3/hr 91-TI-1004 Air Temperature from Air Preheater 200 °C 91-TI-1055/ 1056 Reaction Furnace temperature >1250 °C 91-TI-1005 Reaction Furnace Boiler oultlet process gas temperature 303 °C 91-TI-1006 Reaction Furnace Condenser outlet process gas temperature 185 °C 91-TICA-1007 1st stage auxiliary burner temperature 230 °C st 91-FIC-1019 acid gas flow to 1 stage auxiliary burner 282 Sm3/hr 91-FIC-1018 Combustion Air flow to 1st Stage Auxiliary burner 909 Sm3/hr 91-HIC-1018A air to fuel gas ratio in 1st stage auxiliary burner 8.35 91-HIC-1018B air to acid gas ratio in 1st stage auxiliary burner 3.23 91-TI-1017 1st Stage Converter outlet process gas temperature 315 °C 91-TI-1018 1st Stage Condenser outlet process gas temperature 182 °C 91-TICA-1019 2nd Stage Auxiliary burner temperature 210 °C nd 91-FIC-1026 acid gas flow to 2 stage auxiliary burner 156 Sm3/hr 91-FIC-1025 combustion air flow to 2nd stage auxiliary burner 520 Sm3/hr 91-HIC-1025A air to fuel gas ratio in 2nd stage auxiliary burner 8.35 91-HIC-1025B air to acid gas ratio in 2nd stage auxiliary burner 3.23 91-ARC-1001 H2S/SO2 analyzer ratio at Final Separator outlet, if TGTU is not in line 2:1 91-ARC-1001 H2S/SO2 analyzer ratio at Final Separator outlet, if TGTU is in line 4:1 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 331 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7.1.3 Tail Gas Treatment Unit The operation and monitoring of the TGTU includes the following activities: a. Hydrogenation Reactor 9102-V-11 Operation To maintain good operation of the Hydrogenation Reactor 9102-V-11 the following points should be noted: • Maintain the RGG outlet temperature at 290⁰C • Maintain the RGG process air to fuel gas at a sub-stoichiometric ratio of approximately 14.0:1.0 (by weight) • Maintain the RGG steam to fuel gas at a ratio of approximately 2.0:1.0 (by weight) • The chemical conversion of SO2 to H2S in the Hydrogenation Reactor 9102-V-11 is exothermic. Changes in the H2S and SO2 concentrations in the SRU tail gases will be seen by a temperature change across the Hydrogenation Reactor 9102-V-11. A change in the H2 content, normally 2.0-4.0%, in the Tail Gas Amine Absorber 9102-C-12 outlet vent gases will also be seen. An increase in ∆T across the reactor indicates an increase in SO2 and a decrease in H2S in the SRU tail gases, whilst an increase of H2S and decrease of SO2 in the SRU tail gases will results in a decrease in ∆T across the reactor. When a change in the H2 content of the Tail Gas Amine Absorber 9102-C-12 vent gases is seen, check the upstream amine unit operation and the SRU Reaction Furnace 9101-F-01 controllers operation. • Observe the Hydrogenation Reactor 9102-V-11 catalyst ∆T 91-TDI-1307; it should normally be approximately 32°C. • Reactor inlet (91-TIC-1307) and outlet (91-TI-1310) temperatures are to be maintained around 290°C and 322°C respectively, Provided the unit is operated correctly the reactor catalyst should last for several years. • Over long periods of operation a decrease in the activity of the Hydrogenation Reactor 9101-V-11 catalyst will be seen. In the Hydrogenation Reactor 9101-V-11 deterioration in catalyst activity is seen by the point of reaction temperature moving down the catalyst bed and/or the ∆T (91-TDI-1307) increase falling below the 32°C expected across the reactor and possibly by an increase in the concentration of hydrogen seen by the Hydrogen Analyser 91-AI-1301 in the Tail Gas Amine Absorber 9102-C-12 outlet vent gas line. • If the Hydrogenation Reactor 9102-V-11 catalyst activity has declined then an increase in reactor inlet temperature may temporarily restore some activity, however a catalyst regeneration exercise will be eventually be required followed by sulphiding the catalyst to fully restore catalyst activity. • Periodically, e.g. every 3 months, sample the reactor outlet process gas and analyse for SO2. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 332 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL b. De superheater Contact Condenser 9102-C-11 Operation The following points should be carried out to ensure good operation of the De superheater Contact Condenser 9102-C-11 tower: • Maintain the Desuperheater Contact Condenser 9102-C-11 tower top temperature (91-TI-1317) at 42°C. • Maintain the top (91-FIC-1307), bottom (91-FIC-1314) circulating water flows at 197 m3/hr and 199 m3/hr, respectively. • Control the Desuperheater circulating water pH between 9.0 and 10.0 by monitoring 91-AI-1302. Regularly check pH analyser probe for cleanliness and flow of sample to ensure it gives accurate readings. Daily samples to check the water pH using a portable pH meter or litmus paper should be used to verify the pH analyser accuracy. Failure of the analyser over a period of time could result in low pH circulation water and corrosion of equipment. Adjust Desuperheater circulating water pH by small injections, 1 - 2 litres of liquid caustic injection at a time. Over injection of caustic will result in free caustic in the circulating water with the potential for caustic deposition and possible fouling of equipment. • Note the times that caustic has to be injected. An increase in the frequency of caustic additon has to be added to the Desuperheater circulating water suggest that the Hydrogenation Reactor 9102-V-11 catalyst is not fully converting SO2 to H2S. • Regularly check the Desuperheater circulating water for colour. The water colour will change from brown to dark brown to black over time as it becomes contaminated by traces of SO2 which pass out of the Hydrogenation Reactor 9102-V-11 into the Desuperheater Contact Condenser 9102-C-11. Should a sudden breakthrough of SO2 from the Hydrogenation Reactor 9102-V-11 occur then a rapid change of the circulating water colour will take place, accompanied by a low pH. Should a sudden breakthrough of SO2 occur due to an upset in the SRU, and if the upset condition is likely to take some time to correct, then it is advised that the Desuperheater Contact Condenser 9102-C-11/Tail Gas Amine Absorber 9102-C-12, i.e. the TGTU wet section, are temporarily taken off line to minimise any low pH corrosion of the Desuperheater Contact Condenser 9102-C-11 and possible degradation to the Tail Gas Amine Absorber 9102-C-12 circulating amine. • Periodically change out the Desuperheater circulating water by manually bleeding off to the spent caustic system. Water from the top cooling section of the Desuperheater Contact Condenser 9102-C-11 automatically replenish the tower’s bottom Desuperheater section level. • Monitor the Desuperheater Contact Condenser 9102-C-11 tower packed sections differential pressure indicators 91-PDI-1323/1324. An increase in differential pressure >0.04 barg could indicate packing fouling or flooding whilst a decrease in EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 333 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL pressure could indicate low circulation water flow and/or poor distribution across the packing. c. Tail Gas Amine Absorber 9102-C-12 The absorption of H2S by the Methyl Di Ethanol Amine (MDEA) in the Tail Gas Amine Absorber 9102-C-12 is a function of the following: • The flow and distribution of MDEA falling down the Tail Gas Amine Absorber 9102-C-12 tower through the upward flow of process gases • The temperature of the lean MDEA entering the Tail Gas Amine Absorber 9102-C-12 • The concentration and condition of the lean MDEA entering the Tail Gas Amine Absorber 9102-C-12 Monitoring of the amine unit will include the following: • Regularly check the following Tail Gas Amine Absorber 9102-C-12 level gauges and compare with DCS indicated levels: Vessel Vessel Tag No. Tail Gas Amine Absorber • 9102-C-12 Level Gauge Tag No. 9102-LG-1304A 9102-LG-1304B 9102-LG-1304C 9102-LG-1304D Regularly check the function of the following level transmitters and alarms as given below to confirm correct operation: Vessel Vessel Tag No. Tail Gas Amine Absorber 9102-C-12 Level Transmitter Tag No. 9102-LT-1308 9102-LT-1301 9102-LT-1310 • Maintain lean amine flow (91-FIC-1301) to the amine absorber at the correct flow for efficient absorption of H2S in the towers. • Maintain amine and gas temperatures as given below. Flow Pressure, bar(a) Temp. °C Amine flow to Tail Gas Amine Absorber 9102-C-12 4.69 45 Process gas flow to Acid Gas Amine Absorber 9102-C-12 1.19 41 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 334 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Regularly test the concentration of the lean amine. Add fresh amine if the strength is <50%. • Regularly check the healthiness of the H2S/H2 analyser 91-AI-1301 for normal operation. • Monitor the Tail Gas Amine Absorber 9102-C-12 differential pressure indicator 9102-PDI-1327. A gradual increase in pressure differential in a tower over a period of time will indicate fouling, whilst an increase in pressure differential over a short period will indicate foaming or flooding of the tower. In this case antifoam should be injected into an injection point and the amine circulation flow should be temporarily reduced to reduce the liquid/vapour loadings across the towers packed sections. • Normal Operating Parameters - TGTU Tag. No. Description Value Unit Sm3/hr 91-FIC-1311 Fuel gas to RGG flow 263.7 91-HIC-1304 Fuel gas to air flow ratio 0.12 91-HIC-1311 LP steam to fuel gas flow ratio 1.52 91-FIC-1310 LP steam flow to RGG 400 Kg/hr 91-FIC-1304 Combustion air flow to RGG 2371.6 Sm3/hr 91-TIC-1307 Hydrogenation reactor inlet temperature 290 °C 91-TI-1310 Hydrogenation reactor outlet temperature 327 °C 91-TI-1311 Reactor Effluent Cooler outlet temperature 177 °C 91-FIC-1314 Circulating water flow to Desuperheater 199 m3/hr 91-AI-1302 Desuperheater circulating water pH 9-10 91-TI-1314 Desuperheater circulating water temperature 80 °C 91-FIC-1307 Circulating water from Contact Condenser Trim Cooler 197 m3/hr 91-TI-1312 Circulating water to Cooling Water Circulation Pump temperature 71 °C 91-TIC-1301 Cooling water temperature at Contact Condenser Trim Cooler outlet 47 °C 91-TI-1317 Tail gas to Tail Gas Amine Absorber temperature 42 °C 91-FI-1531 Lean Amine flow to Tail Gas Amine Absorber 135 m3/hr 91-FIC-1325 Rich Amine flow from Tail Gas Amine Absorber to Acid Gas Amine Absorber 136 m3/hr 91-TI-1316 Tail gas from Tail Gas Amine Absorber top temperature 46 °C EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 335 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Tag. No. Description Value Unit 91-PG-1301 Tail gas from Tail Gas Amine Absorber top pressure 0.06 barg 91-AE-1301 Tail gas from Tail Gas Amine Absorber top H2S content 300 ppm 91-TI-1302 Rich amine from absorber temperature 55.2 °C Alarm and trip values for the Combustion Air Blower 9102-K-11A/B to be monitored are tabulated below: • Sl. # Tag No. Service Unit Limit Values H L HH LL 1 91-VT-1457 Blower-A radial vibration(X) microns 23 NA 28 NA 2 91-VT-1458 Blower-A radial vibration(Y) microns 23 NA 28 NA 3 91-ZT-1451A/B Blower-A axial vibration microns 61 NA 152 NA 4 91-VT-1451 Motor-A DE, brg. vibration microns 4.5 NA 7.1 NA 5 91-VT-1456 Motor-A NDE, brg. vibration microns 4.5 NA 7.1 NA 6 91-TE-1471 Motor-A DE brg. temperature °C 95 NA 105 NA 7 91-TE-1472 Motor-A NDE brg. temperature °C 95 NA 105 NA 8 91-TE-1451 Blower-A brg. temperature °C 115 NA 120 NA 9 91-TI-1452A/B Blower-A bull brg. temperature °C 105 NA 115 NA 10 91-TE-1457 Blower-A thrust brg. temperature °C 115 NA 120 NA 11 91-TI-1460 Blower-A Oil return temperature °C 115 NA 120 NA 12 91-PT-1460 Blower-A Seal air pressure bar(g) NA NA NA 0.3 13 91-TT-1453 Blower-A Discharge air temp °C NA NA 170 NA 14 91-PT-1459 Blower-A Lube oil pressure bar(g) NA NA NA 1.49 15 91-TT-1473 Blower-A Reservoir temperature °C NA NA 90 NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 336 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Tag No. 16 91-TT-1459 Blower-A lube oil temperature 17 91-PDT1461 Blower-A inlet air DP 18 91-VT-1717 19 Service Unit Limit Values H L HH LL °C NA NA 71 NA mbar NA NA 110 NA Blower-B radial vibration(X) microns 23 NA 28 NA 91-VT-1718 Blower-B radial vibration(Y) microns 23 NA 28 NA 20 91-ZT-1711A/B Blower-B axial vibration microns 61 NA 152 NA 21 91-VT-1711 Motor-BDE, bearing vibration microns 4.5 NA 7.1 NA 22 91-VT-1716 Motor-B NDE, brg vibration microns 4.5 NA 7.1 NA 23 91-TE-1731 Motor-B DE brg temperature °C 95 NA 105 NA 24 91-TE-1732 Motor-B NDE brg temperature °C 95 NA 105 NA 25 91-TE-1711 Blower-B plain brg temperature °C 115 NA 120 NA 26 91-TE-1712A/B Blower-B bull brg temperature °C 105 NA 115 NA 27 91-TE-1717 Blower-B thrust brg temperature °C 115 NA 120 NA 28 91-TT-1720 Blower-B oil return temperature °C 115 NA 120 NA 29 91-PT-1720 Blower-B seal air pressure bar(g) NA NA NA 0.35 30 91-TT-1713 Blower-B discharge air temp °C NA NA 170 NA 31 91-PT-1719 Blower-B Lube oil pressure bar(g) NA NA NA 1.49 32 91-TT-1733 Blower-B Reservoir temperature °C NA NA 90 NA 33 91-TT-1719 Blower-B lube oil temperature °C NA NA 71 NA 34 91-PDT1721 Blower-B inlet air DP mbar NA NA 110 NA 35 91-FT-1309 Comb air flow to RGG Sm3/hr NA NA NA 1900 36 91-PT-1303 Fuel gas pressure to RGG bar(g) NA NA 0.7 NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 337 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Service Unit Limit Values H L HH LL 37 91-PT-1305 Fuel gas pressure to RGG bar(g) NA NA NA 0.267 38 91-TT-1305 RGG process O/L temperature °C NA NA 300 NA 39 91-PT-1341 Comb air pressure to RGG bar(g) NA NA 0.7 NA % NA NA NA 76 40 7.1.4 Tag No. 91-LT-1309 Reactor effluent cooler level Instrumentation The following actions should be carried out to ensure that all instrumentation is operating satisfactorily: • The SRU Reaction Furnace 9101-F-01 burner instruments and peep sight nozzles are purged by instrument air during normal operation and by nitrogen at times of unit shutdown. In all cases it is important to ensure the purge flows are in operation to ensure the process tapping points do not block with corrosion products and/or sulphur deposits. A daily check should be made to ensure that these purges are taking place, failure or an incorrect purge flow to an instrument or peep sight nozzle will result in the blockage of the tapping point or nozzle with sulphur vapours. • Set up a preventative maintenance programme to regularly check critical instrumentation. It is advised that all instrumentation which initiates a unit shutdown should be checked every three months. Monitoring instruments such as Tail Gas Analysers, H2/H2S and pH analysers should be checked weekly. 7.1.5 Process On-Stream Analysis and Testing The good operation of the AGEU, SRU and TGTU can be maintained by close observation of a number of analysers. The SRU tail gas H2S/SO2 analyser and the TGTU Tail Gas Amine Absorber vent gas H2/H2S analysers. The information seen on these analysers will inform the operator of the condition of the SRU and TGTU processes as follows: • The SRU tail gas analyser is the most important analyser within the SRU/TGTU. Failure of this analyser to control the correct volume of trim air to the SRU Reaction Furnace burner will result, in the event that there is a change in composition of the acid feed gas, in an abnormal ratio of H2S and SO2 passing from the SRU and into the TGTU. The consequences of high H2S concentrations in the SRU tail gases will result in a reduction in the reactions taking place in the TGTU Hydrogenation Reactor (reduced delta temperature across reactor) and potential overloading of the tail gas amine absorber amine solution ability to absorb the EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 338 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL higher than normal loading of H2S gases from the process gases. This will result in H2S slippage in the Tail Gas Amine Absorbers vent gases to the Incinerator and possibly an increase of SO2 to atmosphere via the Incinerator stack. The consequences of high SO2 concentrations in the SRU tail gas will result in higher than normal temperatures in the TGTU Hydrogenation Reactor (increased delta temperature across reactor) and the possible breakthrough of SO2 to the DCC tower and Tail Gas Amine Absorber. Severe SO2 breakthrough will result in excessive corrosion of the DCC and Tail Gas Amine Absorber and degradation of the circulating amine solution • The Tail Gas Amine Absorber process vent gas outlet H2/H2S analyser may be used as a guide to the operation of the SRU Reaction Furnace burner stoichiometry. A reduction in the H2 and H2S contents of the Tail Gas Amine Absorber vent gases will indicate that the SRU Reaction Furnace is off ratio producing a higher than normal concentration of SO2 in its tail gases; i.e. too much process air. This process change may be confirmed by an increase in the delta temperature across the Hydrogenation Reactor catalyst bed. If the H2 and H2S contents of the Tail Gas Amine Absorber outlet vent gas should increase then the SRU is off ratio producing too much H2S in its tail gas; i.e. too little process air. This process change may be confirmed by a decrease in the delta temperature across the Hydrogenation Reactor’s catalyst bed. In both cases an increase of SO2 to atmosphere via the Incinerator stack will occur • The pH analyser employed in the DCC Desuperheater circulating water stream will indicate a low pH when any SO2 breakthrough occurs from the upstream Hydrogenation Reactor. To avoid corrosion of the equipment the desuperheating circulating water pH must always be alkaline, ideally in the 9.0 – 10.0 range. In the event of a sudden reduction of the contact condenser’s desuperheating circulating water pH, due to a breakthrough of SO2 from the Hydrogenation Reactor, the process gas flow from the Reactor Effluent Cooler to the contact condenser should be temporarily redirected to the Incinerator until the process upset has been corrected • Regular testing of the lean amine solution must be carried out to determine solution strength and H2S loading. If the solution strength is <40% then add fresh amine to the system via the amine surge tank fill connection. If the lean amine arriving at the Acid Gas Amine Absorber and the Tail Gas Amine Absorber is only semi lean, i.e. part loaded with H2S, then it is not being fully regenerated in the Amine Regenerator and operating corrections are required at the Regenerator The following is a suggested program for the analysis of the AGEU, SRU and TGTU gas and liquid streams. This program may be modified following operating experience of the units: EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 339 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Daily: DCC Desuperheater section water for pH and colour Twice Weekly: • Steam Generators waters for TDS and treating chemicals • Lean amine for strength and H2S loading Weekly: • SRU tail gas for H2S and SO2 • Acid gas amine absorber vent gas for H2S • TGTU Tail Gas Amine Absorber vent gas for H2S Monthly: • DCC top cooling water for pH • TGTU Hydrogenation Reactor outlet for SO2 • Incinerator stack gas for O2 and SO2 Three Monthly: • SRU feed acid gas for H2S and hydrocarbons • Incinerator stack gas for H2S and NOX 7.1.6 Tail Gas Incinerator • For normal operation of the Incinerator the following parameters has to be monitored • The normal operation of Incinerator is controlled by stack temperature controller 91-TIC-1155, set at 817°C. • It can be adjusted by adjusting the air fuel gas ratio via 91-HIC-1155A, which in turn adjusts the fuel and combustion air control valves. • Ensure the Air/fuel gas ratio set point provided by the operator in the Incinerator is 19.85 (Range: 14-24). • Monitor the performance of Incinerator Air Blowers 9101-K-12A/B frequently • Maintain the fuel gas flow (91-FIC-1155) to the Incinerator at 2256.9 Sm3/hr • Maintain the combustion 46938.7 Sm3/hr • All the process variables are controlled by monitoring Oxygen and SOX/NOX contents in the flue gas from stack. The excess Oxygen, SOX and NOX are continuously monitored by 91-AT-1051, 91-AT-1052 and 91-AT-1053, respectively. air flow (91-FIC-1156) to the Incinerator at EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 340 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Following are the main parameters in the Incinerator which are to be monitored for normal operation of Incinerator: Normal Operating Parameters – Tail Gas Incinerator Tag No. Description Value Unit 800 °C 91-TI-1155 Incinerator stack temp 91-FI-1155 Incinerator Fuel gas flow 2256.9 Sm3/hr 91-FI-1156 Incinerator combustion air flow 46938.7 Sm3/hr 91-AI-1051 Stack O2 3.7 % Vol. dry 91-AI-1052 Stack SOX ≤ 996 mg/Nm3 91-AI-1053 Stack NOX ≤ 55 mg/Nm3 Alarm values to be monitored Tag No. Description Unit Alarm Values LL L H HH 91-PT-1156 Fuel Gas Pressure bar(g) 0 NA NA 4 91-PT-1158 Fuel Gas Pressure bar(g) NA NA 2.5 NA 91-PT-1155 Fuel Gas Supply Pressure bar(g) 2.75 NA NA NA 91-PT-1157 Fuel Gas Supply Pressure bar(g) NA 5 NA NA 91-PT-1159 Pilot Fuel Gas Supply Pressure bar(g) NA 0.5 NA NA 91-TT-1161 Incinerator Shell Temperature °C NA 350 600 NA 91-TT-1162 Incinerator Shell Temperature °C NA 350 600 NA 91-TT-1156 Incinerator Temperature °C 817 NA NA NA 91-TT-1160 Incinerator Temperature °C NA NA NA 900 91-TT-1163 Stack Inlet Flue Gas Temperature °C NA 350 600 NA 91-TT-1164 Stack Inlet Flue Gas Temperature °C NA 350 600 NA 91-TT-1159 Stack Bottom Temperature °C NA NA 850 NA 91-TT-1158 Stack Middle Temperature °C NA NA 850 NA 91-TT-1157 Stack Top Temperature °C NA NA 850 NA 91-AT-1051 Stack Flue Gas Oxygen Content Mol% NA 2.75 3.5 NA 91-AT-1052 Stack Flue Gas SOX Content Mg/Nm3 NA NA 850 NA 91-AT-1053 Stack Flue Gas NOX Content Mg/Nm3 NA NA 250 NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 341 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7.2 UTILITIES 7.2.1 Instrument Air & Plant Air The following are the important parameters to be monitored for steady operation of Instrument Air System: 1. Maintain the instrument Air pressure (68-PIC-1310) at Instrument Air header around 7.8 barg and (68-PI-1311) at instrument air receiver around 7.85 barg. 2. Monitoring of Lube Oil circuit 3. • Maintain Lube Oil Tank level at normal operating condition (more then 50%) by monitoring 68-LG-1401 • Check lube oil temperature (68-TI-1402) and ensure the temperature is not greater than 65°C • Check discharge pressure (68-PI-1402) of lube oil pump and ensure the pressure is not less than 1.5 barg • Ensure that the differential pressure (68-PDI-1403) across Lube Oil Filter is not more than 0.5 barg Monitoring of Compressor • Monitor and ensure the compressor outlet pressure (68-PT-1406) is maintained around 8.0 barg • Monitor and ensure the compressor outlet temperature (68-TI-1405) is maintained around 55°C • Monitor compressor air intake pressure (68-PDI-1401) and ensure the pressure is under limit • Monitor Compressor 1st Stage and 2nd stage outlet temperatures (68-TI-1401 and 68-TI-1404) and ensure it is maintained below 250°C • Monitor Main Motor winding temperatures and ensure the temperatures are below 125°C • Monitor Main motor bearing temperatures (68-TI-1410 & 68-TI-1411) are below 100°C • Monitor inter cooler & after cooler air fans are running normal • Ensure loading and unloading of compressor is functioning normal • Ensure changeover of compressor after every 24 hrs • Ensure proper working of water level indicators in inter and after cooler separators and ensure the proper working of automatic drain valves • Monitor Compressor motor amperes at regular intervals in LCP EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 342 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Normal operating parameters: Tag No. 68-LI-1401 68-PI-1402 68-TI-1402 68-PDI-1403 68-TI-1401 68-TI-1403 68-TI-1404 68-TI-1405 68-PI-1406 68-PIC-1310 68-PI-1311 Description Lube oil sump level Compressor Lube oil pressure Lube oil temperature DP across lube oil filter LP stage outlet transmitter HP stage inlet temperature transmitter HP stage outlet temperature transmitter Compressor outlet temperature transmitter Compressor outlet pressure transmitter Instrument air at header pressure Plant air flow to plant air distribution System Required Value Unit 60 % 1.5 barg 65 °C 1.5 barg 250 °C 65 °C 250 °C 55°C °C 8 7.8 barg barg 7.85 barg Alarm and trip values of main parameters in Instrument air compressor are tabulated below: Tag No. Description Unit 68-PDI-1401 Compressor air inlet pressure 68-PI-1406 Alarm LL L H HH bar(g) -0.065 -0.070 NA NA Compressor outlet pressure bar(g) NA NA 14 16 68-PI-1402 Compressor Oil pressure bar(g) 1 1.2 NA NA 68-PDI-1403 Compressor Oil filter DP bar(g) NA NA 0.9 1.0 68-TI-1401 LP stage outlet temperature °C NA NA 255 260 68-TI-1402 Compressor oil temperature °C NA NA 70 75 68-TI-1403 HP stage inlet temperature °C NA NA 70 80 68-TI-1404 HP stage outlet temperature °C NA NA 255 260 68-TI-1405 Compressor outlet temp. °C NA NA 70 80 68-TI-1406 Main motor winding temp. °C NA NA NA 155 68-TI-1407 Main motor winding temp. °C NA NA NA 155 68-TI-1408 Main motor winding temp. °C NA NA NA 155 68-TI-1410 Main motor DE bearing temp. °C NA NA NA 115 68-TI-1411 Main motor NDE bearing temp. °C NA NA NA 115 68-TI-1412 Main motor winding temp. °C NA NA NA 155 68-TI-1413 Main motor winding temp. °C NA NA NA 155 68-TI-1414 Main motor winding temp. °C NA NA NA 155 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 343 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4. Monitoring of Dryer • Monitor Dryer Inlet filter differential pressure 68-PDI-1407and ensure that it is <0.3 bar • Monitor Dryer outlet filter differential pressure 68-PDI-1410and ensure that it is <0.3 bar • Monitor Dryer outlet Dew point analyzer 68-AI-1401 reading and ensure that it is< (-) 40°C • Monitor Dryer outlet pressure in 68-PG-1412 • Monitor drying and regeneration sequence are working properly Details of alarm values of main parameters in the dryer system are tabulated below: Unit Low Alarm High Alarm Inlet filter Diff. pressure bar NA 0.36 68-PDI-1410 Outlet filter Diff. pressure bar NA 0.36 3. 68-PI-1408 Vessel A pressure bar 3.5 0.7 4. 68-PI-1409 Vessel B pressure bar 3.5 0.7 5. 68-AI-1401 Dew point °C NA -40 6. 68-TI-1409 Inlet temperature °C 1°C 60 Sl. # Tag No. 1. 68-PDI-1407 2. Description Note: 68-PI-1408/68-PI-1409 low alarm is active only during the drying cycle and 68-PI1408/68-PI-1409 high alarm is active only during regeneration cycle. 7.2.2 Effluent & Waste Water Treatment The following are the important parameters to be monitored for steady operation of Effluent & Waste Water Treatment System: • Regularly check the level being maintained in the Waste Water Degasser 6922-V-07 by comparing the indicated level 69-LT-1301 with the level gauge 69-LG-1302 • Routinely check the smooth running of the Waste Water Degasser Pumps 6922-P-08A/B. • Check the differential pressure 69-PDI-1320 across the Sour Water Filter 6922-S-06. If it reaches 1.0 barg, then the filter elements are to be cleaned. • Regularly check the Sour Water Stripper 6922-C-01 pressure is maintained at 1.0 barg through 69-PT-1315 • Regularly check the Sour Water Stripper 6922-C-01 top trays differential pressure 69-PDI-1321 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 344 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Regularly check the Sour Water Stripper 6922-C-01 bottom trays differential pressure 69-PDI-1322 • Check the Sour Water Stripper 6922-C-01 top temperature is maintained at 82ºC through 69-TI-1322 • Check the bottom temperature of the Sour Water Stripper 6922-C-01 is maintained at 126ºC through 69-TI-1313 • The Sour Water Stripper 6922-C-01 bottom level has to be maintained around 50%. Check the level through 69-LI-1306 and compare with the level gauge 69-LG-1306. • Regularly check the smooth running of the Stripped Water Pumps 6922-P-10A/B. • Routinely check the smooth running of the Stripper Overheads Circulation Pumps 6922-P-11A/B. • Check the temperature of the LP steam is being maintained at 148ºC through 69-TI-1327 • Regularly check the temperature of the Sour Water Stripper Reboiler outlet vapour temperature is being maintained at 126ºC through 69-TI-1314 • Check the level of the Reboiler Condensate Drum is maintained at around 50% through 69-LI-1327 • Normal operating parameters: Tag No. Description 69-LIC-1301 69-PIC-1307 69-FIC-1314 69-PDI-1320 69-PIC-1315 69-PDI-1321 69-PDI-1322 69-TI-1322 69-TI-1313 69-LIC-1306 69-TIC-1327 Waste Water Degasser 6922-V-07 level Waste Water Degasser 6922-V-07 pressure Sour water to sour water stripper flow DP across Sour Water Filter 6922-S-06 Sour Water Stripper 6922-C-01 Sour Water Stripper 6922-C-01 tray top DP Sour Water Stripper 6922-C-01 tray bottom DP Sour Water Stripper 6922-C-01 top temperature Sour Water Stripper 6922-C-01 bottom temperature Sour Water Stripper 6922-C-01 bottom level Temperature of the LP steam Sour Water Stripper Re-boiler outlet vapour temperature Re-boiler Condensate Drum level Sour Water Stripper top level CW to Stripper Overhead Cooler LP steam flow to the Stripper Re-boiler Stripper overheads cooler to sour water Stripped Water Cooler outlet flow 69-TI-1314 69-LI-1327 69-LIC-1325 69-FIC-1316 69-FIC-1315 69-TIC-1315 69-FIC-1317 Required Unit Value % 60 barg 1 m3/hr 8.72 barg 1 barg 1 barg <0.15 barg <0.15 °C 82 °C 126 % 50 °C 148 126 °C 50 50 13.6 2154 55 8 °C % m3/hr Kg/hr °C m3/hr EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 345 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7.2.3 Fuel gas system Surveillance of the Fuel Gas System includes the following: • Regularly check the Fuel Gas KOD 6236-V-05 level gauge 62-LG-1301 and compare with DCS indicated level 62-LI-1301. • Fuel Gas KOD 6236-V-05 level in 62-LG-1301 and 62-LI-1301is to be maintained below 50% • Routine checks to be made in the Fuel gas system to identify any leaks with the portable gas detectors and to be recorded • Fuel Gas KOD 6236-V-05 is to be checked for condensate collection and to be drained free of condensate • Routine sampling of the Fuel gas to be done and the quality has to be cross checked with the Laboratory • Consumption of fuel gas has to be monitored and mass balance study has to be carried out to find any abnormal loss • Differential pressure 62-PDI-1305 is maintained below 0.02 barg • Check the Fuel Gas KOD 6236-V-05 pressure controllers 62-PIC-1301, 62-PIC-1302 and 62-PIC-1303 are in AUTO mode and is steady with a set value of 7 barg. • Normal operating parameters: Tag No. Description Required Value Unit 62-PIC-1301 Fuel Gas KOD 6236-V-05 pressure 7 barg 62-PIC-1302 Fuel Gas KOD 6236-V-05 pressure 7 barg 62-PIC-1303 Fuel Gas KOD 6236-V-05 pressure 7 barg 62-PDI-1305 Fuel Gas KOD 6236-V-05 DP 0.02 barg 62-LI-1301 Fuel Gas KOD 6236-V-05 level 55 % 7.2.4 Sea Cooling Water System For normal operation of sea cooling water system following monitoring is required: • Sea cooling water common discharge 69-FI-1301 flow is to be maintained around 1500 m3/hr • Monitor the flow trend of the 69-FI-1301. In case of any increase or decrease in consumption, analyse the cause and take the corrective measures • Ensure the sea cooling water pumps (6932-P04A/B) (69-PI-1301/69-PI-1303) is maintained around 5 barg discharge pressure EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 346 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Periodic checking of the discharge headers has to be carried out for any leak • Ensure the vibrations 69-VI-1301/69-VI-1302 of sea cooling water pumps (6932-P04A/B) are below 12 mm/s • Ensure the thrust bearing temperatures 69-TI-1331A/69-TI-1338A of Sea Cooling Water Pump (6932-P04A/B) bearings are below 85ºC • Ensure the motor winding temperatures of Sea Cooling Water Pump (6932-P04A/B) are below 135ºC • Ensure the pump DE/NDE bearing temperatures of Sea Cooling Water Pump (6932-P04A/B) are below 110ºC • Sea Cooling Water system normal operating parameters with values is tabulated below: Tag No. 7.2.5 Description Required Value Unit 69-FI-1301 Sea Cooling Water Pumps common discharge 1500 m3/hr 69-PI-1301 Sea Cooling Water Pump-A discharge pressure 5 barg 69-PI-1303 Sea Cooling Water Pump-B discharge pressure 5 barg 69-VI-1301 Sea Cooling Water Pump-A vibration <12 mm/s 69-VI-1302 Sea Cooling Water Pump-B vibration <12 mm/s 69-TI-1331A Sea Cooling Water Pump-A thrust bearing temperature <85 °C 69-TI-1338A Sea Cooling Water Pump-B thrust bearing temperature <85 °C Electro Chlorination Package The following parameters are monitored during normal operation: • Maintain the sea water pressure to the electrolyser around 4barg by monitoring the pressure gauge 69-PG-1451. • Ensure the sea water flow to electrolyser is maintained around 10 m3/hr by monitoring the flow transmitters 69-FI-1451 (6932-G01A) and 69-FI-1452 (6932-G01B) • Ensure the differential pressure across the auto back wash filters is maintained below 0.3 barg by monitoring the differential pressure transmitter indications 69-PDI-1452 (6932-S-03A) and 69-PDI-1453 (6932-S-03B) • Ensure the filter Outlet pressure 69-PI-1463 is maintained around 3.5 barg • Maintain the Electrolyser outlet temperatures are below 42°C by monitoring the temperature indications 69-TI-1452 (6932-G01A) and 69-TI-1453 (6932-G01B) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 347 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Ensure the dilution blower (6932-K-01A/K-01B) pressure is maintained around 150 mmwc by monitoring 69-PI-1464 • Ensure the dosing pump (6932-P-05A/P05B) discharge flow (69-FI-1453) is maintained around 11m3/hr. General checks: 1. Check/monitor the electrolyser duty/standby switching over. 2. Check/monitor the auto back wash filter changeover. 3. Check the duty blower for noise, vibration and excessive temperatures. 4. Check the general integrity of the package for any leakages and loose connections. 5. Check the security of all supports, brackets and clips Details of alarm values of main parameters in the ECP are tabulated below: Sl. # Tag No. Service Unit Limit Values High Low 1. 69-PDI-1452 Diff pressure across 6932-S-03A barg 0.3 NA 2. 69-PDI-1453 Diff pressure across 6932-S-03B barg 0.3 NA 3. 69-PI-1463 Filter O/L pressure barg 4.0 3.0 4. 69-TI-1451 Electrolyser inlet temperature °C 40.0 NA 5. 69-FI-1451 Inlet flow to electrolyser 6932-G01A m3/hr 13.0 9.0 6. 69-FI-1452 Inlet flow to electrolyser 6932-G01B m3/hr 13.0 9.0 7. 69-TI-1452 Electrolyser outlet temperature °C 42.0 NA 8. 69-TI-1453 Electrolyser outlet temperature °C 42.0 NA 9. 69-PDI-1465 Degassing tank vent air flow mmwc 170.0 140.0 10. 69-PI-1464 Dilution blower pressure mmwc 170.0 140.0 11. 69-LI-1452 Degassing tank level mm 2900 924 m /hr 13.0 1.8 mm 1621 520 µS/cm 75000 NA 12. 69-FI-1453 Dosing pump discharge 13. 69-LI-1454 Acid tank level 14. 69-AI-1451 Conductivity of acid wash solution 3 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 348 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 7.2.6 DM Water Package Surveillance of the DM Water System includes the following: • Confirm that the new Drinking Water Feed Pumps 6834-P-23A/B are operating satisfactory with sufficient level in Potable Water Storage Tank 6834-T-01 A/B and providing potable water to De-mineralized Water Package 6834-A-07. • Confirm that the following pumps are operating satisfactory. Periodically run each spare pump to prove its operation. Sl. # Pump Pump Tag No. 1. DM Water Transfer Pumps 6834-P-23A/B 2. Neutralization Pumps 6834-P-38A/B 3. HCI Dosing Pumps 6834-P-35A/B/C 4. NaOH Dosing Pumps 6834-P-34A/B/C 5. Recycling pumps 6834-P-37A/B 6. Regeneration pumps 6834-P-36A/B • Check for the inventories of the chemicals like sulphuric acid & NaOH regularly and arrange for the specified quantity of chemicals storage drums to avoid shortage of chemicals at any time. • Monitor the differential pressure across the Cationic Exchangers Bed 6834-S-21A/B by reading the 68-PDI-1826/68-PDI-1829 and ensure that it is less than XX barg. • Monitor the differential pressure across the Anionic Exchangers Bed 6834-S-22A/B by reading the 68-PDI-1827/68-PDI-1831 and ensure that it is less than XX barg. • Routine sampling of HCI Storage Tank 6834-T-16 to be carried out to check the concentration (33%) using the sampler 68-SC-1840. • Close co-ordination between the units is to be maintained for monitoring the levels in the HCI Storage Tank during transfer of acid. Initial and final tank levels have to be recorded for tank and loss of acid if any during transfer. Investigation has to be done in case of abnormal values and the root cause has to be identified and attended. • Check and monitor the HCI Storage Tank 6834-T-16 level in 68-LG-1825 and 68-LI-1825. • Close co-ordination between the units is to be maintained for monitoring the levels in the NaOH Storage Tank 6834-T-15 during transfer of NaOH. Initial and final tank levels have to be recorded for tank and loss of NaOH if any during transfer. Investigation has to be done in case of abnormal values and the root cause has to be identified and attended. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 349 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Routine sampling of NaOH Storage Tank 6834-T-15 to be carried out to check the concentration (25%) using the sampler 68-SC-1841. • Check and monitor the NaOH Storage Tank 6834-T-15 level in 68-LG-1826 and 68-LI-1826. • Check and monitor the following normal operating parameters: • • • a. DM Water Storage Tank 6834-T-08 level 68-LIC-1305 (5200 mm) b. DM water flow 68-FIC-1828(7 m3/hr) to DM Water Storage Tank 6834-T-08 c. SiO2 content in the DM water from anionic exchanger 6834-S-22A/B to DM Water Storage Tank 6834-T-08 is monitored by 68-AI-1830 and ensure that it is < xxx ppm wt d. Conductivity in the DM water from anionic exchanger 6834-S-22A/B to DM Water Storage Tank 6834-T-08 is monitored by 68-AI-1829 and ensure that it is < xxx µs e. Regeneration waste water from DM Water Package 6834-A-07 has to be neutralised in Neutralisation Pit 6834-A-01-T17 prior to disposal. f. Neutralisation water to open drain pH is monitored by 68-AI-1831 is maintained around XXX. On daily basis check the following: a. Visual inspection of the entire package to detect any possible defects (leaking flanges, loose fixtures etc.) b. Check that no resin is flowing over into the drain header trench as a result of incorrect action when a train is started up. c. Make sure that good demineralization is accomplished. If the produced water quality is not satisfactory check the reagent (HCI/NaOH) dosage. On weekly basis check the following: a. If there are any leaks, tighten the flanges concerned, if that does not stop the leak; make arrangements to stop the installation for repair b. Whenever working on the chemical system H2SO4 & NaOH make sure that appropriate protective equipment is used On monthly basis check the following: a. Detailed inspection of the entire DM Water Treatment Plant should be made to detect any malfunctions and to lubricate HCI/NaOH Dosing pumps, motors and all other lubrication points EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 350 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL b. Check the level of resin bed in the Cationic/Anionic Beds, if necessary, make up the difference. Do remember that resin swells, and that after regeneration both cation and anionic resins are at their maximum expansion Alarm and trip values main parameters in DM Water Package are tabulated below: Tag No. Service Unit Limit Values L H LL HH 68-LI-1825 Acid storage tank level % NA NA XX NA 68-LI-1826 Acid storage tank level % XX XX NA NA 68-LI-1827 Caustic storage tank level % NA NA XX NA 68-LI-1828 Caustic storage tank level % XX XX NA NA 68-LI-1830 Neutralisation Pit level % NA NA XX NA 68-LI-1831 Neutralising Pit level % XX XX NA NA 68-LI-1305 DMW storage Tank level % XX XX NA NA 68-AI-1829 Outlet DMW conductivity µs NA NA NA XX 68-AI-1830 Outlet DM Water silica Sio2 NA NA NA XX 68-AI-1826 Train-A Anionic Exchangers outlet conductivity µs NA XX NA NA 68-AI-1828 Train-B Anionic Exchangers outlet conductivity µs NA XX NA NA 68-FI-1826 Train-A Recycle pump flow m3/hr 68-FI-1837 68-FI-1829 68-FI-1838 Train-A Recycle pump flow Train B Recycle pump Flow Train-B Recycle pump flow XX XX NA NA 3 NA NA XX NA 3 XX XX NA NA 3 NA NA XX NA 3 m /hr m /hr m /hr 68-FI-1830 DM water package outlet flow m /hr NA NA XX NA 68-FI-1828 DM water package outlet flow m3/hr XX XX NA NA 68-FI-1825 Train-A Cationic exchanger inlet flow m3/hr XX XX NA NA 68-FI-1827 Train-B Cationic exchangers inlet flow m3/hr XX XX NA NA 68-PDI-1825 Train-A Cationic exchangers bed differential pressure barg NA XX NA NA 68-PDI-1826 Train-A Resin trap differential pressure barg NA XX NA NA 68-PDI-1828 Train-A Anionic exchangers Bed differential pressure barg NA XX NA NA 68-PDI-1827 Train-A Anionic exchanger Resin trap differential pressure barg NA XX NA NA EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 351 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Tag No. Service Unit Limit Values L H LL HH 68-PDI-1830 Train-B Cationic exchangers differential pressure barg NA XX NA NA 68-PDI-1829 Train-B Resin Trap differential pressure barg NA XX NA NA 68-PDI-1832 Train-B Anionic exchangers differential pressure barg NA XX NA NA 68-PI-1825 6834-P-35A diaphragm failure barg NA XX NA NA 68-PI-1826 6834-P-35B diaphragm failure barg NA XX NA NA 68-PI-1827 6834-P-35C diaphragm failure barg NA XX NA NA 68-PI-1828 6834-P-34A diaphragm failure barg NA XX NA NA 68-PI-1829 6834-P-34B diaphragm failure barg NA XX NA NA 68-PI-1830 6834-P-34C diaphragm failure barg NA XX NA NA 68-AI-1831 Neutralisation pump discharge pH pH XX XX NA NA 68-FI-1831 Neutralisation pump discharge flow m3/hr XX XX NA NA 68-FI-1835 Static Mixer inlet DM Water flow m3/hr XX XX NA NA 68-AI-1832 Static Mixer-A outlet conductivity µs XX XX NA NA 68-AI-1833 Static Mixer-B outlet conductivity µs XX XX NA NA 68-FI-1836 Static Mixer inlet DM Water flow m3/hr XX XX NA NA 68-AI-1833 Static mixer outlet conductivity µs XX XX NA NA 7.2.7 Boiler feed water system Surveillance of the Boiler feed water System includes the following: • Ensure the Steam Condensate Flash Drum pressure is maintained around 0.1 barg by monitoring the 68-PG-1308. • Ensure the Steam Condensate Flash Drum level is maintained around 50 % by monitoring the level through 68-LI-1301. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 352 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Ensure De-aerator Feed Pumps 6834-P-20A/B is running normal by monitoring discharge flow (68-FIC-1301) maintained at 83 m3/hr • Ensure the Steam Condensate Cooler Fans are running normal • Monitor the De-aerator top pressure 68-PIC-1304 at 0.2 barg. • Ensure the De-aerator level is maintained at 50%. • Ensure the LP saturated steam flow 68-FI-1309 to De-aerator is maintained around 180 Kg/hr. • Ensure the BFW pumps 6834-P-22A/B/C are running normal with discharge pressure (68-PI-1307) of 20.8 barg • Routine analysis of Boiler Feed Water from De-aerator Vessel 6834-A-08 should be carried out and confirm that the Oxygen content is <0.007 ppm wt. • Check the inventories of the chemicals like Oxygen Scavenger and complex product regularly and arrange for the road Tankers to avoid shortage of chemicals at any time. • Normal operating parameters values are tabulated below: Tag No. 68-PG-1308 68-LI-1301 68-FIC-1301 68-PIC-1304 68-LIC-1302 68-FI-1309 68-PI-1307 68-TIC-1301 • • Steam condensate flash drum pressure Steam condensate flash drum level De-aerator feed pumps 6834-P-20A/B flow De-aerator top pressure De-aerator level LP saturated steam flow BFW pumps 6834-P-22A/B/C pressure Steam Condensate Flash Drum temperature Required Value Unit 0.1 barg 50 % 83 m3/hr 0.2 50 180 20.8 Barg % Kg/hr barg 102 °C On daily basis check the following: • Visual inspection of the entire plant to detect any possible defects (leaking flanges, loose fixtures, etc.) • Make sure that good de-aeration process is accomplished. If the Boiler Feed Water quality is not satisfactory, check the chemical injection flow rate. On Weekly basis check the following: • • Description If there are any leakages, tighten the flanges concerned, if that does not stop the leakage; make arrangements to stop the installation for repair. On monthly basis check the following: EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 353 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Detailed inspection of the entire plant should be made to detect any malfunctions of Boiler Feed Water pumps and Chemical Injection pumps. Monitor the pressure and flow trend of the Boiler Feed Water system through 68-PI1307 and 68-FIC-1305. In case of any increase or decrease in consumption, take the corrective action. 7.2.8 Steam Generation During normal operation of the boiler, attention should be paid to the proper operation of all the ancillaries and equipment in service. Safe and reliable operation of the steam generator depends on routine monitoring of the control and safety systems. Controls and checks must be done continuously, also if the system is operated automatically. Any variation in the operating parameters indicates a change in boiler performances and proper actions should be taken in order to restore the previous conditions. In fact variations in the selected and settled parameters can result in worsening of the auxiliary power consumption and/or boiler efficiency, or sometimes can indicate a risk of possible damage. For example, the increasing of the boiler flue gas exit temperature can indicate possible carbon fouling deposition on tube surfaces or improper flame position or missadjustment of the air-fuel ratio. In particular the following parameters shall be controlled carefully. a. Boiler Water Level Water level variations in the boiler take place in case of rapid increase or decrease in steam output, so the proper water level in the steam drum must be maintained. Boiler water level is maintained by the level controller 91-LIC-1522 (set at 50%). Monitor the Boiler water level by the level gauges 91-LG-1522 & 91-LG-1523 during normal operation. Regularly cross check the DCS indicated level with level gauge. b. Boiler Feed Water The Boiler Feed Water should be carefully treated and monitored during boiler operation as it is essential to assure boiler integrity. It is important that plant operators always maintain the quality of Boiler feed Water as given below. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 354 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Feed Water quality (Limit Values) Parameters Units of Measurements Appearance - Clear, colourless, no suspended solids Direct Conductivity @ 25°C µS/cm < 10 Acid Conductivity @ 25°C µS/cm < 0.2 - > 9.2 Total Hardness (Ca + Mg) mg/l Nil Sodium and Potassium (Na + K) mg/l < 0.010 Iron (Fe) mg/l < 0.020 Copper (Cu) mg/l < 0.003 Silica (SiO2) mg/l < 0.020 Oxygen (O2) mg/l < 0.02 Oil/Grease mg/l < 0.1 Organic Compounds (as TOC) mg/l < 0.2 pH @ 25°C Boiler Feed Water Quality (Limit Values) Parameters Units of Measurements - Clear, colourless, no foam Direct Conductivity @ 25°C µS/cm < 100 Acid Conductivity @ 25°C µS/cm < 50 pH @ 25°C - 9.5-10.5 Alkalinity mmol/l 0.05-0.3 Silica (SiO2) mg/l < 70 Phosphate (PO4) mg/l <6 Appearance The Steam Generator is provided with one sampling system, that allows to analyse the quality of the Boiler Feed Water. The Boiler Feed Water Conductivity is maintained by acting on the CBD control valve, whose position determines the conductivity of the Boiler Feed Water. In order to get quality Boiler Feed Water, the following actions to be taken: • Establish a strict control of Feed Water and Boiler Water parameters through a routine sampling and subsequent chemical analysis of the samples at least one for each working shift (8 hours) or more frequently. Record each analysis result to easily check all data comparing them with boiler load and injection amounts of EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 355 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL chemical additives. This database allows also to check immediately any possible data variation and consequently to take the necessary remedial actions. • Feed water quality: Maintain Feed Water quality continuously by acting on Continuous Blow Down. Generally the CBD flow rate, during a good and regular boiler operation, should be about 1% of boiler MCR (the most economic and best operation should be based on a target of 0.5%). However, in case of need, the CBD flow rate can be temporarily increased by 2-3%. • Operation at high CBD flow rates clearly indicates that boiler water quality is not under control and that necessary remedial action must be taken. • Chemicals dosing injection: Operator must check that chemical dosing system is available and that all chemicals are injected at the required rate and concentration in the Feed Water and in Boiler Feed Water. Attention: For water chemical conditioning, it’s absolutely forbidden to use strong alkali compounds, with particular reference to those containing caustic soda (Sodium Hydroxide) and caustic potash (Potassium Hydroxide). It’s allowed to use volatile alkali compounds, adequately dosed and in the recommended quantity and phosphate treatment. c. Blow down, Water Column and Glass Indicators The CBD flow rate is automatically adjusted by the system according to the measured value of boiler water conductivity. The sampling system dedicated to steam generator is provided also with manual sampling line for each sample that can be used to perform a complete analysis of the feed/boiler water. Typically the facilities of a qualified water treatment laboratory should be employed to establish the feed/boiler water chemical characteristics and the chemical reactants to be injected, their frequency and quantity. Note: As chemical corrosion attack or salt deposition on internal surfaces generally grows slowly on boiler internal pressure parts, BE recommends to sample and analyse periodically the feed water and boiler water and to record the chemical analysis results (as conductivity, pH, alkalinity, TDS and all the others) in a dedicated book. So during steam generator life, all variations can be immediately monitored and possible immediate corrective actions (if and when necessary) can be activated. Note: When the boiler is in normal operation and in any cases when the boiler water/steam pressure is higher than atmospheric pressure, no manual boiler pressure part drain valves shall be opened. The boiler water column and level glass indicator shall be periodically and very carefully purged at least one time a week, so to limit sludge or sediment accumulation in these devices. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 356 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL In fact all this kind of accumulated deposits could cause an erroneous indication of the water level. d. Flame Pattern It is important to assure a good flame pattern in order to get a stable and safe combustion, limiting possible impingement on furnace wall tubes or on burner throat refractory and limiting also any possible flame pulsation. A good combustion will allow achieving the expected boiler performance, both in terms of steam production and flue gas emissions. On the contrary improper flame pattern could result in carbon build-up on the external tube surfaces that could reduce the thermal heat transfer, and consequently could increase the flue gas temperatures at the stack, so creating an efficiency reduction. Flame instability can cause some dangerous vibration phenomena and possible unburned fuel zone accumulation into the furnace. This dangerous situation must be absolutely avoided: in such case all the combustion system parameters must be controlled again till to eliminate this disturbance. Steam Generation unit normal operating parameters with values are tabulated below: Tag No. 68-LIC-1522 Description Boiler drum level Required Value 50 Unit % 3 68-FIC-1522 Boiler Feed Water flow XXX m /hr 68-TIC-1522 SH steam temperature 163 °C 68-TIC-1820 LP Steam header temperature XX °C 68-PIC-1523A Boiler drum pressure 16.4 barg 68-FIC-1525 Fuel gas flow to boiler XXX Kg/hr 68-FIC-1526 Combustion air flow to boiler XXX Kg/hr 68-AIC-1522 Oxygen analyzer controller XXX % 68-ZIC-1524 Flue gas damper position controller XXX % 68-PIC-1523B Steam pressure vent 17.4 barg 68-PIC-1306 LP steam header pressure 5 barg EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 357 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION VIII START-UP AFTER EMERGENCY SHUTDOWN EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 358 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 8.1 GENERAL Restart after Emergency Shutdown is discussed for the following units: 8.2 • Tail Gas Incinerator • Acid Gas Enrichment Unit • SRU • TGTU TAIL GAS INCINERATOR RESTART After the Tail Gas Incinerator ESD shutdown is activated, the unit is restarted as follows: 8.3 • Confirm the root cause of the Incinerator shutdown and rectify the same problem. Reset the ESD by pressing 65-HS-4001R for ESD-0, 65-HS-001R for ESD-1 and 65-HS-1192 for ESD-2/3/4 • Check and confirm the availability of utilities for operation. • Start Incinerator as per procedure described in section 6.3.1 ACID GAS ENRICHMENT UNIT RESTART After an emergency shutdown of AGEU, the unit is still with liquid levels in Acid Gas Amine Absorber column bottoms, Amine Surge Tank, Amine Regenerator and Amine Regenerator Reflux Drum. • Confirm the root cause of the Acid Gas Enrichment Unit shutdown and rectify the same problem. Reset the ESD by pressing 65-HS-4001R for ESD-0, 65-HS-001R for ESD-1 and 65-HS-1192 for ESD-2/3/4 • Confirm that all the utility services are available and all rotating equipments are ready for operation • Confirm that the downstream units are ready to receive the acid gas • All instrumentation is confirmed as reading correctly on the DCS, against local instrumentation and local gauges • All shut-down devices have been tested • Confirm Tail Gas Incinerator is in line • Acid gas feed to AGEU is isolated from upstream units • Acid gas from Regenerator Reflux Drum to Sulphur Recovery Unit is isolated and LP Acid Gas flare is lined up • Start AGEU as per the procedure described in section 6.3.2 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 359 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 8.4 SULPHUR RECOVERY UNIT RESTART After an emergency shutdown of SRU, the unit is still with liquid levels in Reaction Furnace Boiler 9101-E-07, Reaction Furnace Condenser 9101-E-01, 1st Stage Condenser 9101-E-02 and Last Condenser 9101-E-04. • Confirm the root cause of the SRU shutdown and rectify the same problem. Reset the ESD by pressing 65-HS-4001R for ESD-0, 65-HS-001R for ESD-1 and 65-HS-1192 for ESD-2/3/4 • Confirm that all the utility services are available and all rotating equipments are ready for operation • Confirm that the downstream units are ready to receive the tail gas • All instrumentation is confirmed as reading correctly on the DCS, against local instrumentation and local gauges • All shut-down devices have been tested The restart is done considering that SRU converters 1st Stage Converter 9101-V-01 & 2nd Stage Converter 9101-V-02 contain sulphur compounds. To ensure that during this start-up, there is no ignition of any Sulphur compounds within the unit, the Reaction furnace burner is operated at slightly sub-stoichiometric firing condition. • Start SRU as per the procedure described in section 6.3.3. 8.5 TGTU RESTART After the TGTU unit ESD is activated, the unit is still with liquid levels in Reactor Effluent Cooler 9102-E-11 and Desuperheater/Contact Condenser 9102-C-11 top and bottom sections. • Confirm the root cause of the TGTU shutdown and rectify the same problem. Reset the ESD by pressing 65-HS-4001R for ESD-0, 65-HS-001R for ESD-1 and 65-HS-1192 for ESD-2/3/4. • Confirm that all the utility services are available and all rotating equipments are ready for operation • Confirm that the downstream units are ready to receive the tail gas • All instrumentation is confirmed as reading correctly on the DCS, against local instrumentation and local gauges • All shut-down devices have been tested The Hydrogenation Reactor catalyst is in sulphided state so sulphiding of the catalyst is not required. The start-up is carried out considering that unit contains Sulphur compounds and ensure that during this start-up there is no ignition of any Sulphur compounds within the unit; the RGG burner is operated at slightly sub-stoichiometric firing conditions from the start of ignition in the RGG. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 360 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Close XV-1332 on tail gas line from Reactor Effluent Cooler to Desuperheater/Contact Condenser and open XV-1331 on tail gas line from Reactor Effluent Cooler to Tail Gas Incinerator. • Start TGTU as per the procedure described in section 6.3.4. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 361 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION IX TROUBLE SHOOTING OPERATIONS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 362 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 9.1 PROCESS 9.1.1 Incinerator Sl. # Problem 1. High SO2 content in stack gas 2. Diagnosis Control Action SOX Analyser 91-AI-1052 indicates high alarm 91-AAH1052 Claus sulphur recovery unit Sulphur recovery is low Ensure all process parameters in Claus sulphur recovery unit are at normal operating condition High Oxygen content in stack gas O2 Analyzer, 91-AI1051 indicates high O2 alarm 91-AAH-1051 Excess Oxygen reacts with SO2 and form SO3, which makes high corrosion Reduce air flow to Incinerator through 91-HIC-1155A 3. Low Oxygen content in stack gas O2 Analyzer 91-AI1051 Indicates low O2 alarm 91-AAL-1051 Low Oxygen content indicates unburnt sulphur compound to environment Increase Air flow to Incinerator through 91-HIC-1155A 4. Reduction in Incinerator temperature Combustion air flow low alarm 91-FAL-1156C 1. Incinerator Air Blower 9101-K-12 A/B mechanical problem Check/rectify Incinerator Air Blower 9101-K12A/B 2. Incinerator Air Blower 9101-K-12 A/B VFD malfunction Check/rectify the Incinerator Air Blower 9101-K12A/B VFD parts Malfunction of fuel gas control valve 91-FV-1155 Check/rectify malfunction of fuel gas flow control valve 91-FV-1155 5. 9.1.2 Drop in Incinerator temperature Indication Fuel gas pressure low alarm 91PAL-1157 Acid Gas Enrichment Unit Sl. # Problem Indications Diagnosis Control Action 1. Acid gas feed to Acid Gas Amine Absorber 9103-C11 temperature is high Temperature indicator is provided 91-TI-1503 showing high temperature and initiation of high temperature alarm 91-TAH-1503 H2S content in treated gas will increase due to low absorption rate Check sea cooling water flow to the Acid Gas Coolers 9103-E-101A/B 2. Lean amine feed to Acid Gas Amine Absorber 9103-C-11 temperature is high Temperature gauge 91-TG-1505 is provided showing high temperature H2S content in treated gas will increase due to low absorption rate Check Lean Amine Cooler 9103-E-14 fans are running and sea cooling water flow for the Lean Amine Trim Cooler 9103-E-15 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 363 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Problem Indications Diagnosis Control Action 3. Less Amine concentration in MDEA solution Lab Sample analysis shows less amine concentration Absorption rate low Add fresh MDEA solution to reach the required concentration 4. High H2S content in treated acid gas from absorber to Incinerator H2S analyser indicator is provided 91-AI-1501 showing high H2S content and initiation of high H2S content alarm 91-AAH-1501 Absorption rate low Increase lean amine circulation rate 5. High pressure difference across the tray in absorber column Differential pressure indicator 91-PDI-1522 is provided showing high differential pressure and initiation of high differential pressure alarm 91-PDAH-1522 Absorption rate low, due to foaming Start Antifoam Injection to Absorber column 6. High pressure difference across the tray in Regenerator column Differential Pressure indicator is provided 91-PDI1523 showing high pressure difference and initiation of high pressure difference alarm 91-PDAH-1523 Regeneration rate low due to foaming Start Antifoam Injection to Regenerator column 7. Regenerator Reboiler steam flow low Ratio controller 91-HIC-1503 is provided for rich amine to Regenerator and steam to Reboiler. 91-FIC-1503 showing low steam flow and initiating low flow alarm 91-FAL-1503 Regeneration rate will decrease Increase LP steam flow to Regenerator Reboiler 8. Suspended solids in lean amine solution Amine solution is not clear, it has suspended solids Lean amine quality will reduce Isolate amine filters and check filters condition EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 364 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 9.1.3 Sl. # 1 Sulphur Recovery Unit Problem Acid gas flow is low Indications Flow transmitter 91FT-1140 is provided. On low low flow 91FALL-1140 shutdown is initiated Diagnosis Feed gas to Reaction Furnace is low Control Action Maintain the Reaction furnace temperature at normal operating temperature with help of fuel gas Divert tail gas to Incinerator from Tail gas treating unit 2 Purge air to Reaction furnace purging nozzle low pressure Pressure Indicator 91-PI-1002 is provided Sulphur condensation occurs in purge nozzle point Nitrogen purging to Reaction furnace instrument nozzle opens when incase of blower shutdown 3 Acid gas temperature is low due to MS steam failure Temperature indicator 91-TI-1003 is provided Reaction Furnace temperature is reduced Start fuel gas feed to Reaction furnace 4 Air temperature is low due to MS steam failure Temperature indicator 91-TI-1004 is provided Reaction furnace temperature is reduced Start fuel gas firing to Reaction furnace for maintaining temperature at normal operating condition 5 1st Stage Converter inlet and outlet temperature difference is low Manually calculate temperature difference between inlet temperature (91-TIC-1007) and outlet temperature (91-TI-1017) Conversion of H2S to Sulphur is less Start catalyst regeneration 6 2nd Stage Converter inlet and outlet temperature difference is low Manually calculate temperature difference between inlet temperature indicator 91-TIC-1019 and outlet temperature indicator Conversion of H2S to Sulphur is less Start catalyst regeneration EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 365 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Problem 7 High H2S content in liquid sulphur from degassing pit to storage compartment 9.1.4 Indications Lab sample analysis shows high H2S concentration, it is carried out as per sampling schedules Diagnosis Control Action High H2S content in sulphur make poly sulphite formation Increase catalyst injection rate Tail Gas Treating Unit Sl. # Problem Indications Diagnosis Control Action 1. Hydrogenation Reactor inlet and outlet temperature difference is low Calculated temperature difference between inlet 91-TIC-1307 and outlet temperature 91-TI-1310 is indicated by 91-TDI-1307 Conversion of sulphur to H2S is less Increase Reactor inlet temperature 2. 3. 4. Low pH in wash water High pressure difference across the Desuperheater packing Wash water filter 9102-S15 differential pressure high Analyser (pH) is provided 91-AI-1302 showing low pH and initiation of low pH alarm 91-AAL-1302 Pressure difference indicator is provided 91-PDI-1324 showing high pressure difference and initiation of high pressure difference alarm 91-PDAH-1324 Differential pressure indicator is provided. 91-PDI-1329 showing high pressure and initiation of high pressure difference alarm 91-PDAH-1329 High corrosion will occur due to acid gas SO2 content high More recirculation rate Deposition of impurities on surface of filter element Start caustic injection to Desuperheater Circulation Pumps 9102-P-11A/B suction Divert final sulphur condenser tail gas to Incinerator Decrease recirculation water flow to Desuperheater Open filter bypass valve and run the plant for short duration and clean the filter element EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 366 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Problem Indications 5. Tail gas to Tail Gas Amine Absorber temperature is high Temperature indicator is provided 91-TI-1317 showing high temperature and initiation of high temperature alarm 91-TAH-1317 H2S absorption rate will decrease Increase circulating cooling water to Desuperheater/Co ntact Condenser 6. Amine concentration is less in MDEA solution Lab sample analysis shows less amine concentration Absorption rate will be reduced Add fresh MDEA solution to the required concentration 7. High H2S/H2 ratio content in treated acid gas from Tail Gas Amine Absorber to Incinerator H2S/H2 analyser indicator is provided 91-AI-1301 showing high H2S/H2 content and initiation of high H2S/H2 content alarm 91-AAH-1301 Less absorption rate Increase lean amine feed rate Diagnosis Control Action 9.2 Diagnosis Control Action UTILITIES 9.2.1 Instrument air package a. Air Compressor Sl. # 1. 2. 3. 4. Problem Indications High Abnormal sound temperature in in compressor DE/NDE bearing. Indicated by Low lube oil 68-PI-1402 discharge Low level in lube pressure oil sump Low Abnormal sound High in inter and temperature in after cooler Air DE/NDE bearings Fans and Gear box Compressor starts running, but does not load after a 20 sec delay time Compressor loaded lamp 68-XL-1409 indication in Bearing is worn out Check and replace if required Choke in lube oil filter Clean the filter Actual level low Top-up lube oil Bearing are worn out Check and replace if required Net air pressure 68-PT-1311/ 68-PT-1406 is above the loading set point LCP Malfunction of Loading solenoid valve Compressor will load when pressure in air net drops to pre-set loading pressure Check and replace if required EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 367 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # 5. 6. 7. Problem Water separators condensate level increase Indications High high level indication (68-XA-1402/ 1406)in UCP Diagnosis Malfunction of level indicators Malfunction of automatic drain valves High differential 68-PDI-1403 high Filter choke pressure across alarm lube oil filter Consumption Exceeds air delivery of Low discharge compressor Low pressure pressure of indication at Instrument air 68-PI-1406 Choked air filters Compressor Air leakage b. Control Action Check and replace if required Check and replace if required Clean the filter Check equipment connected/vents/ drains Remove filter assembly, clean and check/Replace filters Check and arrest leaks Air Dryer Sl. # Problem Indications Diagnosis Free water in compressed air inlet 1. High dew point High dew point alarm (68-AI1401/1451) 2. Dryer outlet flow/pressure is low Low flow alarm 68-FI-1302/ 68-PI-1302 3. Dryer fails to shift Dryer fault alarm Temperature of compressed air too high Poor desiccant performance/ Desiccant has become over saturated for a longer period Control Action Check the condensate separators and drains upstream of the dryer if they are operative Check the compressor after-cooler fan is operative Replace desiccant. Check the maintenance schedule for normal replacement periods Check inlet filters of compressor and check the outlet pressure of Poor performance the compressor and of IA Compressor compare this with the inlet pressure of the dryer Check Instrument Air Instrument air Filter. Clean if pressure low necessary Check the valve, Failure on the actuator and the pilot inlet valves air pressure to the EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 368 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Problem Indications Diagnosis Leak in Instrument air tubes Leak in valve actuator 4. 9.2.2 Dryer fault alarm Replace tube Service or replace actuator Check instrument air Instrument air filter. Clean if pressure low necessary Check the valve, actuator and the Failure of the instrument air valve pressure to the actuator Solenoid does not Check and replace open defective parts Effluent & Waste Water Treatment Unit Sl. # 1. 2. 9.2.3 Regeneration valve fails to open Control Action actuator Problem Indications Diagnosis Control Action Stripper Reboiler steam failure Low steam flow alarm 69-FAL1315 Isolate sour water Stripping rate of feed to Sour Water H2S will decrease Stripper and divert to the Observation sump High H2S content in stripped water Lab sample analysis shows high H2S concentration, it is carried out as per sampling schedules High H2S content to Observation sump Increase steam flow to Sour Water Stripper Reboiler Electro Chlorination Package Sl. # Problem Indications Diagnosis Loss of sea water supply 1. Electrolyser inlet flow low 69-FI-1451/ 1452 Isolating valves low alarm partially closed Control Action Check for sea water supply pressure Check and adjust the manual position of valves Blockage in the cell Rectify the blockage 2. Degassing Tank 69-LI-1451 high overflows high alarm Tank outlet restricted Check manual outlet valves are opened Check the 69-FIExcessive flow in to 1451/1452 set at the tank 10 m3/hr EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 369 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Problem Indications No level in 69-LI-1451 low 3. degassing tank level alarm Duty Hydrogen Dilution 4. Blower not working Running indication and ampere indication Diagnosis Control Action Tank drain valve open Check and rectify Tank or associated piping leak Check and arrest the leaks Mechanical defect in blower Check and rectify as required Electrical fault Check blower power supply and associated protective devices Check the blower motor Do blower Duty blower changeover and performance is very check the poor abnormality 5. Dilution air pressure low 69-PT-1464 low alarm Phase failure Transformer 6. rectifier not working Thyristor fuse failure 9.2.4 Blocked suction filter on duty blower Remove and clean the filter Transmitter malfunction Check the impulse lines for any block and check the electronics Loss of phase on incoming supply Check incoming supply and fuses Monitoring defect inside the Transformer/ Rectifier Check and replace the phase failure relay Earth with in T/R Trace and identify Rectifier failed Check and replace the Rectifier Chemical Injection Packages a. Complex Product Injection Package Sl. # Problem 1 Low level in Complex Product Storage Tank 6834-T-18 Indication Low level alarm 68-LAL-1317 Diagnosis Corrective action Complex product is consumed during injection Make up with the Complex Product solution Malfunction of level transmitter 68-LT-1317 Verify with level gauge 68-LG-1307. Isolate the level transmitter and rectify EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 370 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Problem Indication Diagnosis Corrective action 2 High level in Complex Product Storage Tank 6834-T-18 High level alarm 68-LAH-1317 Continuous filling of Complex product from the drum/dilution Stop unloading from the drum Malfunction of level transmitter 68-LT-1317 Verify with level gauge 68-LG-1307. Isolate the level transmitter and rectify. High diaphragm pressure of Complex Product Pump 6834-P41A/B High pressure alarm 68-PAH-1326/ 68-PAH-1327 Diaphragm rupture Rectify the problem in diaphragm Malfunction of pressure transmitter 68-PT-1326/ 68-PT-1327 Rectify the problem in pressure transmitter Low flow at injection point Low injection rate Operating at low stroke Increase the stroke length Choke/obstruction in suction line Check and rectify NRV got struck in the discharge line Check and rectify Pump not developing pressure Check the Pump and rectify 3 4 b. Oxygen Scavenger Injection Package Sl. # 1 2 Problem Indication Diagnosis Corrective action Low level in Oxygen Scavenger Storage Tank 6834-T-17 Low level alarm 68-LAL-1315 Oxygen Scavenger is consumed during injection Make up with the Oxygen Scavenger Solution Malfunction of level transmitter 68-LT-1315 Verify with level gauge 68-LG-1306. Isolate the level transmitter and rectify High level in Oxygen Scavenger Storage Tank 6834-T-17 High level alarm 68-LAH-1315 Continuous filling of Oxygen Scavenger from the drum/ dilution Stop unloading from the drum Malfunction of level transmitter 68-LT-1315 Verify with level gauge 68-LG-1306. Isolate the level transmitter and rectify. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 371 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # 3 4 c. Problem Indication Diagnosis Corrective action High diaphragm pressure of Oxygen Scavenger Injection Pump 6834-P39A/B High pressure alarm 68-PAH1324/ 68-PAH-1325 Diaphragm rupture Rectify the problem in diaphragm Malfunction of pressure transmitter 68-PT-1324/ 68-PT-1325 Rectify the problem in pressure transmitter Low flow at injection point Low injection rate Operating at low stroke Increase the stroke length Choke/obstruction in suction line Check and rectify NRV got struck in the discharge line Check and rectify Pump not developing pressure Check the Pump and rectify Biocide Injection Package Sl. # Problem Indication Diagnosis 1 Low level in Biocide Storage tank 6932-T-04 Low level alarm 69-LAL-1328 Biocide is consumed during injection Make up with Biocide solution Malfunction of level transmitter 69-LT-1328 Verify with level gauge 69-LG-1309. Isolate the level transmitter and rectify High level in Biocide Storage Tank 6932-T-04 High level alarm 69-LAH-1328 Continuous filling of Biocide from the drum/dilution Stop unloading from the drum Malfunction of level transmitter 69-LT-1328 Verify with level gauge 69-LG-1309. Isolate the level transmitter and rectify. High diaphragm pressure of Biocide Injection Pump 6932-P07A/B High pressure Diaphragm rupture alarm 69-PAH-1344/ Malfunction of 1346/1328/ pressure transmitters 1345/1347/ 1329 Low flow at injection point Low injection rate 2 3 4 Corrective action Rectify the problem in diaphragm Rectify the problem in pressure transmitter Operating at low stroke Increase the stroke length Choke/obstruction in suction line Check and rectify EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 372 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # d. Problem Indication Diagnosis Corrective action NRV got struck in the discharge line Check and rectify Pump not developing pressure Check the Pump and rectify Scale Inhibitor Injection Package Sl. # 1 2 3 4 Problem Indication Low level in Scale Inhibitor Storage Tank 6932-T-05 Low level alarm 69-LAL-1330 High level in Scale Inhibitor Storage Tank 6932-T-05 High level alarm 69-LAH-1330 High diaphragm pressure of Scale Inhibitor Injection Pump 6932-P09A/B High pressure alarm 69PAH-1338/ 1348/1350/ 1339/1349/ 1351 Low flow at injection point Low injection rate Diagnosis Corrective action scale inhibitor is consumed during injection Make up with the Scale Inhibitor solution Malfunction of level transmitter 69-LT1330 Verify with level gauge 98-LG-1310. Isolate the level transmitter and rectify Continuous filling of Scale Inhibitor from the drum/dilution Stop unloading from the drum Malfunction of level transmitter 69-LT1330 Verify with level gauge 69-LG-1310. Isolate the level transmitter and rectify. Diaphragm rupture Rectify the problem in diaphragm Malfunction of pressure transmitters Rectify the problem in pressure transmitter Operating at low stroke Increase the stroke length Choke/obstruction in suction line Check and rectify NRV got struck in the discharge line Check and rectify Pump not developing pressure Check the Pump and rectify EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 373 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. Catalyst Injection Package Sl. # Problem 1 Low level in Catalyst Storage Tank 9101-T-01 Low level alarm 91-LAL1127 High level in Catalyst Storage Tank 9101-T-01 High level alarm 91-LAH-1127 High diaphragm pressure of catalyst injection Pump 9101-P11A/B High pressure Diaphragm rupture alarm 91PAH-1128/ Malfunction of 91-PAH-1129 pressure transmitter 91-PT-1128/91-PT1129 Low flow at injection point Low injection rate 2 3 4 f. Indication Diagnosis Corrective action Catalyst solution is consumed during injection Make up with the catalyst solution Malfunction of level transmitter 91-LT1127 Verify with level gauge 91-LG-1127. Isolate the level transmitter and rectify Continuous filling of Catalyst from the drum/dilution Stop unloading from the drum Malfunction of level transmitter 91-LT1127 Verify with level gauge 91-LG-1127. Isolate the level transmitter and rectify. Rectify the problem in diaphragm Rectify the problem in pressure transmitter Operating at low stroke Increase the stroke length Choke/obstruction in suction line Check and rectify NRV got struck in the discharge line Check and rectify Pump not developing pressure Check the Pump and rectify Antifoam Injection Package Sl. # 1 Problem Low level in Antifoam Storage Tank 9103-T-12 Indication Low level alarm 91-LAL1521 Diagnosis Corrective action Antifoam is consumed during injection Make up with Antifoam solution Malfunction of level transmitter 91-LT1521 Verify with level gauge 91-LG-1510. Isolate the level transmitter and rectify EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 374 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # 2 3 4 g. Problem Indication High level in Antifoam Storage Tank 9103-T-12 High level alarm 91LAH-1521 High diaphragm pressure of Antifoam Injection Pump 9103-P16A/B Low flow at injection point Diagnosis Corrective action Continuous filling of Antifoam from the drum/dilution Stop unloading from the drum Malfunction of level transmitter 91-LT1521 Verify with level gauge 91-LG-1510. Isolate the level transmitter and rectify. High pressure alarm 91PAH-1565/91PAH-1566 Diaphragm rupture Rectify the problem in diaphragm Malfunction of pressure transmitter 91-PT-1565/91-PT1566 Rectify the problem in pressure transmitter Low injection rate Operating at low stroke Increase the stroke length Choke/obstruction in suction line Check and rectify NRV got struck in the discharge line Check and rectify Pump not developing pressure Check the Pump and rectify Corrosion Inhibitor Injection Package Sl. # Problem Indication Diagnosis 1 Low level in Corrosion Inhibitor Storage Tank 9103-T-13 Low level alarm 91-LAL1523 Corrosion Inhibitor is consumed during injection Make up with Corrosion Inhibitor solution Malfunction of level transmitter 91-LT1523 Verify with level gauge 91-LG-1511. Isolate the level transmitter and rectify High level in Corrosion Inhibitor Storage tank 9103-T-13 High level alarm 91LAH-1523 Continuous filling of Corrosion Inhibitor from the drum/ dilution Stop unloading from the drum Malfunction of level transmitter 91-LT1523 Verify with level gauge 91-LG-1511. Isolate the level transmitter and rectify. 2 Corrective action EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 375 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # Problem Indication 3 High diaphragm pressure of corrosion inhibitor injection Pump 9103-P101A/B High pressure alarm 91PAH-1567/ 91-PAH-1568 Diaphragm rupture Rectify the problem in diaphragm Malfunction of pressure transmitter 91-PT-1567/91-PT1568 Rectify the problem in pressure transmitter Low flow at injection point Low injection rate Operating at low stroke Increase the stroke length Choke/obstruction in suction line Check and rectify NRV got struck in the discharge line Check and rectify Pump not developing pressure Check the Pump and rectify 4 h. Sl. # 1 2 3 Diagnosis Corrective action Caustic Injection Package Problem Indication Low level in Caustic Storage Tank 9103-T-14 Low level alarm 91-LAL1525 High level in caustic storage tank 9103-T-14 High level alarm 91-LAH-1525 High diaphragm pressure of Caustic Injection Pump 9103-P103A/B High pressure alarm 91PAH-1569/ 91-PAH-1570 Diagnosis Corrective action Caustic product is consumed during injection Make up with caustic solution Malfunction of level transmitter 91-LT1525 Verify with level gauge 91-LG-1512. Isolate the level transmitter and rectify Continuous filling of Caustic product from the drum Stop unloading from the drum Malfunction of level transmitter 91-LT1525 Verify with level gauge 91-LG-1512. Isolate the level transmitter and rectify. Diaphragm rupture Rectify the problem in diaphragm Malfunction of pressure transmitter 91-PT-1569/91-PT1570 Rectify the problem in pressure transmitter EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 376 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # 4 9.2.5 Problem Low flow at injection point Indication Low injection rate Diagnosis Operating at low stroke Choke/obstruction in suction line NRV got struck in the discharge line Pump not developing pressure Corrective action Increase the stroke length Check and rectify Check and rectify Check the Pump and rectify DM Water Package Sl. # Problem 1 High Pressure drop across the cationic bed 2 High Pressure drop across the cationic bed 3 High silica content in DM water 9.2.6 Indications High differential pressure alarm 68-PDAH-1825/ 68-PDAH-1830 across the bed Diagnosis Too many fines and broken resins High differential pressure alarm 68-PDAH-1828/ 68-PDAH-1832 across the bed Silica content high alarm in DM water, 68-AAH-1830 Too many fines and broken resins Organic matter in fresh water feed Control Action Adjust flow rates for backwash the resins to remove fines and broken resins Inform Water Treatment unit to check Adjust flow rates for backwash the resins to remove fines and broken resins Less caustic strength during regeneration Increase Caustic strength during regeneration Diagnosis Failure of Supply of DM Water or Condensate to steam condensate flash drum Fluctuation in Steam Flow to De-aerator, De-aerator Level and De-aerator Pressure. Control Action Check the DM water unit and LP Condensate system header and normalize the system Tune the controller and maintain the steady Pressure, Level and Temperature as per the design conditions Diagnose and attend the problem of Oxygen Scavenger Injection Boiler Feed Water System Sl. # Problem 1 Boiler Feed Water level low in De-aerator 6834-A-08 2 Indications Level low indication in 68-LI-1302 Boiler Feed Lab Result Water quality is not meeting with design specification Problem in Oxygen Scavenger Injection EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 377 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # 3 9.2.7 Problem BFW header pressure low Indications Pressure low indication in 68- PI-1307 Diagnosis Control Action Tripping of running Boiler Feed Water pump Start the standby pump (if not started on Auto) and line-up as per the normal start-up procedure. Analyze the reason for trip and rectify before starting back the pump which is tripped. Low level in the De aerator. Refer Problem No #1. Steam Generation Package Sl. # 1 Problem Leakage/Tube rupture Indications Presence of Steam at stack outlet. Diagnosis High furnace pressure 68-PI-1528 Flue gas Temperature low 68-TI-1523 Control Action Shutdown and Inspect the Boiler. Tube substitution/ Repair Feed water flow 68-FIC-1522 and Main steam flow 68-FI-1524 variations. Drum level low 68-LI-1523 2 Improper Combustion Black smoke appears at stack outlet Insufficient Combustion Air 68-FIC-1526 Adjust the airflow rate. Adjust the Burner air register, if required. Check the FD fan is functioning correctly. 3 Pulsated/ Spontaneous Combustion 1. Flame is not stable 2. Vibrations in furnace area and Burner floor area. Insufficient combustion air flow 68-FIC-1526 Adjust the airflow rate. Adjust the Burner air register, if required. Check that the FD fan is functioning correctly. Insufficient draft EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 378 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # 4 Problem Drum Water Level-too high or Low Indications Diagnosis Control Action 1. Drum level 68-LI-1523 Fluctuations. 2. Feed water flow 68-FIC1522 fluctuations Malfunction of feed water control loop Check and rectify the feed water flow and steam flow controls. Malfunction of feed water system Check and rectify the feed water system Leakage from piping Check and attend the leakages 5 Main steam flow low SH main Steam flow alarm 68-FSL1524 Main SH steam stop valve failed in close position or any other struck-up. Trip the Boiler immediately. Check and rectify the problem. 6 Outlet main steam SH steam low temperature Low temperature alarm 68-TAH-1820 Problem in Desuperheater feed water control valve 68-TV-1522 Check and set the DSH control valve in manual mode to close the valve if opened fully. Faulty Instrument Check and rectify the faulty Instruments SH temperature control failure Check and rectify the Instrument control loops. Problem in Desuperheater feed water control valve 68-TV-1522 Check and set the DSH control valve in manual mode to open the valve if closed Faulty Instrument Check and rectify the faulty Instruments SH temperature control failure Check and rectify the Instrument control loops. 7 Outlet main steam SH steam high temperature High temperature alarm in 68-TAH-1820 8 High flue gas temperature High temp. alarm 68-TAH-1523 Too much excess air - Oxygen analyser 68-AIC-1522 Reduce the excess air. 9 Combustion Air Duct vibration Vibrations/Ab normal noises Expansion Joint failure Check the expansion joint, stop the fan and rectify the joint Support damaged/failure Check and Rectify the support FD fan surge Stop the FD fan, inspect the wind box and refer to the FD fan manual, check and rectify EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 379 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sl. # 10 Problem Pipe vibration/ Water hammering Indications Diagnosis Control Action Vibrations/ab normal noises Two phase flow in pipeline. Pipeline not supported properly. Open the drain valve and drain the water/condensate, warm up/charge the pipeline slowly. Check the pipeline supports and rectify the problem. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 380 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION X PLANNED SHUTDOWN EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 381 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10.1 Planned Shutdown - Process The shutdown of the AGEU, SRU, TGTU and the Incinerator is explained below. The shutdown of the Incinerator will only take place following the shutdown of the AGEU, SRU and the TGTU. The planned shutdown of the process units take place in the following sequence: 10.1.1 • TGTU • SRU • AGEU • Incinerator TGTU Shutdown Shutdown of the TGTU will proceed as follows: TGTU Wet Section Shutdown The shutdown of the TGTU wet section, the DCC and Tail Gas Amine Absorber tower, may take place before or after acid feed gases are removed and replaced with fuel gas in the SRU Reaction Furnace burner. It is advised to stop the flow of SRU tail gas to the TGTU wet section before acid feed gas is removed from the SRU Reaction Furnace burner, rather than after the burner is operating on fuel gas; this action will minimise the possibility of an upset condition during the acid gas to fuel gas change over in the SRU Reaction Furnace burner, that could result in high concentrations of SO2 in the process gas causing corrosion of equipment in the TGTU wet section and degradation of the amine solution in the Tail Gas Amine Absorber. Shutdown of the TGTU DCC and absorber tower will proceed as follows: • Open Reactor Effluent Cooler process outlet gas valve 91-XV-1331 to route Hydrogenation section process gases to the Incinerator • Close Reactor Effluent Cooler process outlet gas valve 91-XV-1332 to the DCC tower • Continue DCC Desuperheater and cooling waters circulations until column has cooled to near ambient temperatures, then stop pumps • Continue circulation of lean amine to the Tail Gas Amine Absorber for a period of time, e.g. 30 minutes, to ensure all rich amine solution has been removed to the Amine Regenerator for regeneration, then stop lean amine flow to the Tail Gas Amine Absorber and stop the Tail Gas Rich Amine Pump • If the DCC is to be opened for inspection then: EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 382 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Before stopping the DCC tower top section cooling water pump, pump all possible water from the top chimney tray to the Effluent Water Treatment • Pump out the bottom Desuperheater section of the DCC to the spent caustic system • Through the condensate line to the cooling water pumps suction line, introduce condensate to establish a level in the contact condenser tower top chimney tray cooling section • Start a Cooling Water Recirculation Pump 9102-P-12A/B to establish water circulation through the Contact Condenser Cooler to the top of the DCC tower • Open the DCC bottom level control valve 91-LV-1307 to transfer condensate from the top cooling water system to establish a condensate level in the bottom of the tower. Continue adding condensate via the Cooling Water Recirculation Pumps suction line to maintain a water level in the top chimney tray • When a water level is established in the bottom of the DCC, start a Desuperheater Circulation Pump 9102-P-11A/B and start circulation around the bottom of the tower • Again pump out the bottom Desuperheater section to the spent caustic system • Sample the water whilst it is being pumped out to the spent caustic system, if the pH of the water is near to the pH of condensate, then the Desuperheater section has been flushed clean. Repeat filling and circulating the Desuperheater section if further flushing is required • When flushed clean, drain any remaining water in the top cooling water and bottom Desuperheating sections of the DCC tower to the drains system • After water washing, final cleaning and gas freeing of the DCC tower should be carried out by steaming. The DCC process gas outlet valve to the Tail Gas Amine Absorber is first closed and LP steam is introduced into the tower via its utility connection. • The DCC tower is initially steamed to flare, via the towers PSV open bypass line, and then to atmosphere before the steam is stopped, and air allowed to enter the equipment. Steam out of the tower should be for a minimum of 4 hours to flare followed by a minimum of 4 hours to atmosphere. • If the Tail Gas Amine Absorber is to be opened for inspection then: • Restart a Tail Gas Rich Amine Pump 9102-P-16A/B and pump out all amine from the bottom of the Tail Gas Amine Absorber to the Acid Gas Amine Absorber • After water washing, final cleaning and gas freeing of the Tail Gas Amine Absorber should be carried out by steaming. LP steam is introduced into the tower via its utility connection and steamed to the Incinerator for a minimum of 8 hours EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 383 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Note: The Incinerator must be in operation when steam out of the Tail Gas Amine Absorber is taking place. TGTU BSR Section Shutdown • Stop the Sour gas from Effluent and Waste Water Treatment Unit by closing 69-PV1315A and open 69-PV-1315B to LP Acid Gas Flare. • Open SRU tail gas outlet valve 91-XV-1097 to route tail gas directly to the Incinerator • Close SRU tail gas outlet valve 91-XV-1098 to the TGTU • Simultaneously while the SRU tail gas valve to the TGTU is being closed; shutdown the RGG burner via the RGG manual shutdown switch 91-HS-1403. • Confirm that the action of the shutdown switch has closed or opened the following RGG shutdown valves: • Nitrogen valve 91-XV-1307 to the RGG process air line is opened (valve will remain open for ~15 minutes) • Nitrogen valve 91-XV-1301 to the RGG instrument nozzles is opened (valve will remain open for ~15 minutes) • Instrument air valve 91-XV-1302 to the RGG instrument nozzles is closed • Process air valve 91-XV-1306 is closed • Fuel gas shutoff valves 91-XV-1303 and 91-XV-1304 is closed and vent valve 91-XV-1308 is opened • LP steam ON/OFF valve 91-XV-1305 is closed • After a set time of 15 minutes, confirm that the nitrogen purge valves to the RGG process air line 91-XV-1307 and to the RGG instrument nozzles 91-XV-1301 have closed. • Close manual valves in the RGG process air, instrument air, fuel gas and LP steam lines to the RGG. • The TGTU BSR section and hydrogenation reactor may then be left to cool naturally until a re-start is required. • Observe the Reactor Effluent Cooler steam side pressure after unit shutdown and open the vessel’s steam side vent valve when steam side pressure falls to <1.0 barg to avoid a vacuum being formed in the vessel. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 384 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10.1.2 SRU Shutdown Shutdown of the SRU will proceed as follows: • If time permits, prior to reducing acid feed gas to the SRU it is advised that the SRU converters catalyst beds undergo a rejuvenation exercise, refer to Section 12.4.5. • Reduce acid gas feed to the SRU Reaction Furnace to the unit minimum design flow of 6628 kg/hr, (2169 am3/hr) When acid gas feed flows to the SRU reaction furnace burner are at the unit’s minimum: • Open SRU tail gas line valve 91-XV-1097 to the Incinerator • Close SRU tail gas line valve 91-XV-1098 to the TGTU • Confirm process air and acid gas controllers are in automatic operating mode • Switch acid gas to the Reaction Furnace Control valve 91-PV-1503B to manual operating mode and slowly reduce acid gas to the SRU Reaction Furnace • Switch trim air controller 91-FIC-1003 to manual mode and close trim air control valve. • Confirm the stoichiometric air requirements for the fuel gas • Confirming the fuel gas shutdown valves are open, in manual operating mode, slowly open fuel gas control valve 91-FV-1009 to introduce fuel gas to the SRU Reaction Furnace burner to replace the acid gas. • Observe adjustment of the process air flow as fuel gas flow to the Reaction Furnace burner increases. • Simultaneously whilst increasing fuel gas flow 91-FT-1009, decrease acid gas flow 91-FI-1001 to the reaction furnace burner to ensure the fuel gas is being burned at slightly substoichiometric firing conditions. • Simultaneously switch 1st Stage Auxiliary Burner and 2nd Stage Auxiliary Burner from acid gas to fuel gas • When acid gas flow has stopped close manual valve in acid gas line to Reaction Furnace burner. • Close MS steam to the Acid Gas Pre-heater • Observe adjustment of the process air as fuel gas flow to the Reaction Furnace burner increases and acid gas flow decreases. • Introduce LP steam to the fuel gas line through 91-XV-1079 to prevent soot being formed at sub-stoichiometric firing conditions. Set steam controller to control the EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 385 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL steam flow at a ratio to natural gas of 1:1 (by wt). Before opening steam valves ensure steam lines are fully drained of condensate. • Introduce LP steam to the burner process air line through 91-XV-1078 to moderate the furnace temperature and prevent overheating of the furnace refractory. Note that the furnace temperature will dictate the amount of steam used, too much steam could result in interference of the burners flame detectors sensing the flame resulting in a burner trip. Before opening steam valves ensure steam lines are fully drained of condensate. • Continue operating the SRU Reaction Furnace burner in slightly sub-stoichiometric firing conditions to produce a hot inert flow of combustion gas through the unit to sweep all possible sulphur from the SRU converters catalyst beds. Continue this operation until the flow of sulphur is seen to have stopped from all sulphur condenser seals. • When all possible sulphur has been removed from the SRU converters, if the intent is not to open the SRU to carry out maintenance, then shutdown the unit via its emergency stop switch. If the SRU is not to be opened for a maintenance overhaul then a catalyst sulphur stripping exercise is not required and the shutdown of the unit can proceed as follows: • Close MS steam to the process air pre-heater • Through the SRU shutdown switch 91-HS-1213 from LCP, shutdown the unit • Confirm that action of the shutdown switch has closed or opened the following shutdown valves to the reaction furnace burner: • Acid gas valve 91-XV-1102 to reaction furnace is closed • Fuel gas shutoff valves 91-XV-1099 & 91-XV-1048 are closed and vent valve 91-XV-1100 is opened. • Combustion air to reaction furnace valve 91-XV-1101 is closed • Nitrogen valve 91-XV-1127 to the process air line, open (valve will remain open for ~15 minutes) • Nitrogen valve 91-XV-1110 to burner instrument nozzles, open (valve will remain open for ~15 minutes) • Purge air to burner instrument nozzles, closed • LP steam valve 91-XV-1078 is closed • After a set time of 15 minutes, confirm that the nitrogen purge valves to the Reaction Furnace process air line and to the Reaction Furnace burner instrument nozzles have closed • SRU may then be left to cool naturally until a re-start is required EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 386 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Close manual valves in the process air, instrument air, fuel gas, acid gas and LP steam lines to the reaction furnace • Observe all steam generators steam side pressures after unit shutdown. When pressures have decayed to <1.0 barg on the steam side of the WHB, condensers and reactor effluent cooler, open atmospheric vents to prevent a vacuum being formed in the vessels • The SRU may then be left to cool naturally until a re-start is required • If the intent is to open the unit to carry out an internal inspection and maintenance then a sulphur stripping/regeneration exercise will first have to be carried out to remove all hazardous sulphur compounds from the unit, refer to Section 12.4.6 10.1.3 Acid Gas Enrichment Unit Shutdown The unit shutdown is performed as detailed below: • Inform NGL-1, 2 & 3 to slowly reduce the acid gas feed to AGEU to the unit turndown flow of 12241 kg/hr When the acid gas feed is at the turndown flow: • Close acid gas to Acid Gas KO Drum by closing 91-PV-1503B manually • Open 91-PV-1503A and send the acid gas to LP Acid Gas Flare • Inform NGL-1, 2 & 3 to fully stop the acid gas feed to AGEU • Close the acid gas feed to amine absorber by closing the inlet block valve • Close the treated gas outlet from Acid Gas Amine Absorber 9103-C-11 to Incinerator pressure control valve 91-PV-1502 and the upstream and downstream isolation valves. • The amine solution is to be circulated until the solution is completely regenerated. Take samples from Amine Regenerator bottom and confirm. • When the solution is completely regenerated, slowly close the LP Steam to Regenerator Reboiler 9103-E-13 by closing the inlet flow control valve 91-FV-1503. • Close the condensate outlet from Regenerator Reboiler Condensate Pot 9103-V-13 and open the pot vent to avoid pulling vacuum when the pressure is reduced. • Stop the Regenerator Reflux drum pumps 9103-P-11A/B when the level in the Regenerator Reflux Drum 9103-V-12 reaches low and close the discharge isolation valves. • Open 91-PV-1539 to supply nitrogen to the Amine Regenerator. • Continue MDEA circulation till the solution is cooled down. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 387 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Slowly reduce the amine circulation rate and stop the Lean Amine Pumps 9103-P13A/B. • Stop Rich Amine Pumps 9103-P-12A/B and Hot Lean Amine Pumps 9103-P-17A/B after transferring the solution to the Amine Surge Tank 9103-T-11. • Stop Regenerator Condenser Cooler 9103-E-12 fans and Lean Amine Cooler 9103-E14 fans. • Drain the MDEA solution from Acid Gas Amine Absorber 9103-C-11 through the Acid Gas Rich Amine Pumps casing drain to the Amine Sump 9103-V-10 and transfer the solution from the Amine Sump to the Amine Surge Tank 9103-T-11 • Drain the Lean/Rich Amine Exchanger 9103-E-11A/B by opening the drains on the Lean and Rich amine side to the Amine Sump 9103-V-10 and transfer the solution from the Amine Sump to the Amine Surge Tank 9103-T-11 • Drain the Amine Regenerator 9103-C-12 through the Hot Lean Amine Pumps 9103P-17A/B casing drain to the Amine Sump 9103-V-10 and transfer the solution from the Amine Sump to the Amine Surge Tank 9103-T-11 • Drain the solution from the Regenerator Condenser Cooler 9103-E-12 and Regenerator Condenser Trim Cooler 9103-E-16 by draining through the upstream and downstream drain valves of 91-TV-1502 to the Amine Sump 9103-V-10 and transfer the solution from the Amine Sump to the Amine Surge Tank 9103-T-11 • Drain the Regenerator Reboiler through the vessel drains to the Amine Sump 9103-V-10 and transfer the solution from the Amine Sump to the Amine Surge Tank 9103-T-11 • Drain the Lean Amine Cooler and Lean Amine Trim Cooler through the drains to the Amine Sump 9103-V-10 and transfer the solution from the Amine Sump to the Amine Surge Tank 9103-T-11 • Drain the Lean Amine Filters through the drains to the Amine Sump 9103-V-10 and transfer the solution from the Amine Sump to the Amine Surge Tank 9103-T-11 • Depressurise the system by opening the vents to flare • Steam out of the unit has to be carried out for vessel entry 10.1.4 Incinerator Shutdown The Incinerator will only be shutdown following the shutdown of the TGTU, SRU and AGEU. The shutdown of the unit may proceed as follows: Confirm that all process gases from the upstream AGEU, SRU and TGTU have stopped and that the following process gas valves to the incinerator are isolated: • Treated vent gas line from the Acid Gas Amine Absorber is blind isolated • Treated vent gas line from the Tail Gas Amine Absorber is blind isolated EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 388 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • SRU tail gas line valve 91-XV-1097 • TGTU Reactor Effluent Cooler outlet process gas valve 91-XV-1331 • TGTU wet section start-up vent gas valve • Sulphur Degassing Pit ejector vent gases If the incinerator is not to be opened for inspection, then: • Press the Incinerator emergency shutdown switch 91-HS-1167 in LCP to shutdown the unit. • An emergency shutdown will cause all valves to revert to their fail safe positions. The valve positions are as follows: • Fuel gas control valve 91-FV-1155 at low fire position • Fuel gas upstream block valve 91-XV-1155 in close position • Fuel gas vent valve 91-XV-1156 in open position • Fuel gas downstream block valve 91-XV-1157 in close position • Pilot gas upstream block valve 91-XV-1158 in close position • Pilot gas vent valve 91-XV-1159 in open position • Fuel gas downstream block valve 91-XV-1160 in close position • After 15 minutes air supply valve 91-XV-1161 is closed Note: Local ESD pushbutton 91-HS-1167 and remote ESD signal shutdown the blower’s 9101-K-12A/B directly. If the Incinerator is to be opened for inspection, then it should be slowly cooled to protect its refractory from shock cooling as follows: • Place the temperature controller 91-TIC-1155 to “Manual mode” • slowly reduce, at an advised rate (e.g. 50°C/hr), the Incinerator combustion chamber temperature by reducing fuel gas flow to the burner until the burner is at its minimum turndown and the combustion chamber is at as low a temperature as possible before stopping fuel gas to the burner • At 250°C, stop the combustion by pressing Normal stop pushbutton “91-HS-1166” on LCP • Following are the sequence of action when stop pushbutton is activated: • A 5 minute timer is started • Fuel gas control valve 91-FV-1155 at low fire position • Fuel gas upstream block valve 91-XV-1155 in close position EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 389 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10.2 • Fuel gas vent valve 91-XV-1156 in open position • Fuel gas downstream block valve 91-XV-1157 in close position • Pilot gas upstream block valve 91-XV-1158 in close position • Pilot gas vent valve 91-XV-1159 in open position • Fuel gas downstream block valve 91-XV-1160 in close position • Continue operating the Incinerator Air Blower to cool the unit by combustion air until as near to ambient temperatures as possible are seen in the combustion chamber and stack; after 5 minutes, pilot and purge air supply valve 91-XV-1161 is closed and then stop the Incinerator Air Blower 9101-K-12A/B manually • Blind isolate the unit for in readiness for opening and inspection UTILITIES 10.2.1 Steam Generation Package Shutdown The shutdown sequence of the boiler 6848-A-02A is as follows: • Before stopping the boiler increase the blow down rate to remove as much sediments as possible • Reduce the boiler load to 75% • Reduce the firing rate gradually to its minimum • Reduce the boiler load to 20%, by taking all boiler controls in manual • Start to open the start-up vent valve 68-PV-1523 until the steam drum pressure begins to decrease • Close the 68-MOV-1522 to stop the steam supply to the header • Stop the burner by pressing the normal stop push button 68-HSC-1527 in local boiler panel Following are the sequence in BMS when burner stop pushbutton is pressed: • Pilot burner vent valve 68-XV-1533 opens • Pilot burner shutoff valves 68-XV-1531 and 68-XV-1532 closes • Main burner vent valve 68-XV-1530 opens • Main burner shutoff valves 68-XV-1528 and 68-XV-1529 closes • Close the start-up vent valve 68-PV-1523 Following is the post purge sequence executed by BMS in boiler: • BMS sets the air purge request and post purge in progress signal • Combustion air flow damper (68-FV-1526) will be opened to threshold limit EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 390 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Ensure the presence of 68-FZSO-1526 limit switch • After 1 minute delay if the flue gases recirculation controller is enabled then BMS will set flue gas purge request and BCS will open the recirculation damper (68-FV1524) • After receiving the 68-FV-1524 open feedback BMS sets flue gas purge in progress signal • After 30 seconds BMS resets post-purge in progress, air purge request signal, air purge in progress and flue gas purge request and flue gas purge in progress signal • BMS sets the flue gas purge end and air purge end signal • Stop the Forced Draft Fan 6848-K-02A and Flue Gas Recirculation Fan 6848-K-03A • Allow the boiler to cool down and monitor the drum pressure via 68-PI-1523 • When Drum Pressure reaches 1.5- 2.0 barg, open the saturated steam vent valves • Cool down the unit naturally until the ambient temperature is reached • Close the Boiler feed water control valve 68-LV-1522 • Drain the Boiler with the drum vent valves in open position • Isolate the other utility pipelines Follow the same sequence for stopping of another running boiler. 10.2.2 Boiler Feed Water System Shutdown During Planned Shutdown of Boiler Feed Water system, the scheduled maintenance activity on Deaerator, Boiler Feed Water Pumps, chemical Injection Pumps and the auxiliary equipment can be carried out as per company maintenance schedule. Other maintenance activity that may be carried out includes checking of PSV and calibration of instruments, etc. Jobs like Deaerator Internal work, equipment overhauls will be planned in long Shutdown. But in case if the Deaerator internal work is not planned during long Shutdowns, preservation procedures as per the company procedure has to be followed. Get clearance from all process units before taking the shutdown of the Boiler Feed Water System. Ensure steam generation units are stopped, before taking shutdown of boiler feed Water system. Following steps are to be followed for shutdown of Boiler Feed Water System: • Stop Oxygen Scavenger injection to Deaerator package 6834-A-08 • Stop the boiler feed water Pumps 6834-P-22 A/B/C and close the pump suction & discharge valves. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 391 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10.2.3 • Stop the Deaerator Feed Pumps 6834-P-20A/B • Isolate the LP saturated steam to Deaerator vessel by taking 68-PIC-1304 in manual and close the control valve 68-PV-1304 • Isolate the DM Water supply to Steam Condensate Flash Drum 6834-V-05. • Isolate the LP Condensate supply to Steam Condensate Flash Drum 6834-V-05 • Isolate the steam condensate from Steam Condensate Coolers 6834-E-02 by taking 68-TIC-1301 in manual and close the control valve 68-TV-1301 • Ensure Deaerator Feed Pumps recirculation flow controller 68-FIC-1301 is in manual and the steam condensate to flash drum minimum flow control valve 68-FV-1301 is fully closed. • Stop all the running Steam Condensate Cooler Fans 6834-E-02. DM water package Shutdown During Planned Shutdown of DM Water system, the scheduled maintenance activity on anionic, cationic Exchanger and the auxiliary equipment can be carried out as per company maintenance schedule. Other maintenance activity that may be carried out includes checking of PSV, calibration of instruments, cleaning of filters and replacement of resin, etc. Jobs like Resin replacement, Equipment overhauls will be planned in this Long Shutdown. But in case if the resin replacement is not planned during Long Shutdowns, Preservation procedures as per the vendor has to be followed. For details of these preservation procedures refer the Vendor Operation and Maintenance Manual. To stop the DM water train, place the respective AUTO/MAN/OFF selector in OFF position. When OFF mode is selected, all valves involved in the respective sequence is closed, phase duration timers are stopped at the current status, and the sequence is ‘freeze’ in the current phase, with all outputs inhibited. The procedure for normal shutdown of DM Water Package unit is given below: 1. Get clearance from all process units before taking the shutdown of the DM Water System. 2. Isolate the fresh Water supply to both the trains. 3. If the regeneration is in progress in one of the train continue regeneration and stop the train after the completion of regeneration by placing the respective AUTO/ MAN/OFF selector in OFF position. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 392 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 4. Select the train which is in online to manual, use the step advance button to start the regeneration and after completion of regeneration, stop the train by placing the respective AUTO/MAN/OFF selector in OFF position. 5. Isolate the product DM Water to DM Water Storage Tank. 6. If the Resins are to be preserved for a long time, follow the Preservation procedures as given in the Vendors Manual. 7. Based on the requirement, isolate and hand over the equipments as per the equipment hand over procedure. 10.2.4 Chemical Injection System Shutdown a. Antifoam Injection Package 9103-A-11 Antifoam Injection System shutdown is carried out as described below: • Stop the Antifoam Injection Pumps 9103-P-16A/B from LCP • Stop the Antifoam Tank Agitator in the Antifoam Storage Tank • Close the isolation valve at the Antifoam Storage Tank outlet to the suction of the pumps • Close the suction and discharge isolation valves of the Antifoam Injection Pumps • Close the Antifoam injection line isolation valve at the injection point • Drain the Antifoam from the lines and the pumps to the drain pit and flush the lines with water and deenergise the pumps if required for any maintenance. • If the Antifoam Storage Tank has to be handed over for maintenance, then the tank level has to be reduced to the level possible before stopping the Injection pumps. The tank has to be drained fully to the drain pit and washed thoroughly with water. b. Caustic Injection Package 9103-A-13 Caustic Injection System shutdown is carried out as described below: • Stop the Caustic Injection Pumps 9103-P-103A/B from LCP • Stop the Caustic Tank Agitator in the Caustic Storage Tank • Close the isolation valve at the Caustic Storage Tank outlet to the suction of the pumps • Close the suction and discharge isolation valves of the Caustic Injection Pumps • Close the Caustic injection line isolation valve at the injection point • Drain the Caustic from the lines and the pumps to the drain pit and flush the lines with water and deenergise the pumps if required for any maintenance. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 393 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • c. If the Caustic Storage Tank has to be handed over for maintenance, then the tank level has to be reduced to the level possible before stopping the Injection pumps. The tank has to be drained fully to the drain pit and washed thoroughly with water. Corrosion Inhibitor Injection Package 9103-A-12 Corrosion Inhibitor Injection System shutdown is carried out as described below: • Stop the Corrosion Inhibitor Injection Pumps 9103-P-101A/B from LCP • Stop the Corrosion Inhibitor Tank Agitator in the Corrosion Inhibitor Storage Tank • Close the isolation valve at the Corrosion Inhibitor Storage Tank outlet to the suction of the pumps • Close the suction and discharge isolation valves of the Corrosion Inhibitor Injection Pumps • Close the Corrosion Inhibitor injection line isolation valve at the injection point • Drain the Corrosion Inhibitor from the lines and the pumps to the drain pit and flush the lines with water and deenergise the pumps if required for any maintenance. • If the Corrosion Inhibitor Storage Tank has to be handed over for maintenance, then the tank level has to be reduced to the level possible before stopping the Injection pumps. The tank has to be drained fully to the drain pit and washed thoroughly with water. d. Complex Product Injection Package 6834-A-09 Complex Product Injection System shutdown is carried out as described below: • Stop the Complex Product Injection Pumps 6834-P-41A/B from LCP • Stop the Complex Product Tank Agitator in the Complex Product Storage Tank • Close the isolation valve at the Complex Product Storage Tank outlet to the suction of the pumps • Close the suction and discharge isolation valves of the Complex Product Injection Pumps • Close the Complex Product injection line isolation valve at the injection point • Drain the Complex Product from the lines and the pumps to the drain pit and flush the lines with water and deenergise the pumps if required for any maintenance. • If the Complex Product Storage Tank has to be handed over for maintenance, then the tank level has to be reduced to the level possible before stopping the Injection pumps. The tank has to be drained fully to the drain pit and washed thoroughly with water. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 394 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. Oxygen Scavenger Injection Package 6834-A-09 Oxygen Scavenger Injection System shutdown is carried out as described below: • Stop the Oxygen Scavenger Injection Pumps 6834-P-39A/B from LCP • Stop the Oxygen Scavenger Tank Agitator in the Oxygen Scavenger Storage Tank • Close the isolation valve at the Oxygen Scavenger Storage Tank outlet to the suction of the pumps • Close the suction and discharge isolation valves of the Oxygen Scavenger Injection Pumps • Close the Oxygen Scavenger injection line isolation valve at the injection point • Drain the Oxygen Scavenger from the lines and the pumps to the drain pit and flush the lines with water and deenergise the pumps if required for any maintenance. • If the Oxygen Scavenger Storage Tank has to be handed over for maintenance, then the tank level has to be reduced to the level possible before stopping the Injection pumps. The tank has to be drained fully to the drain pit and washed thoroughly with water. f. Biocide Injection Package 6932-A-06 Biocide Injection System shutdown is carried out as described below: • Stop the Biocide Injection Pumps 6932-P-07A/B from LCP • Close the isolation valve at the Biocide Storage Tank outlet to the suction of the pumps • Close the suction and discharge isolation valves of the Biocide Injection Pumps • Close the Biocide injection line isolation valve at the injection point • Drain the Biocide from the lines and the pumps to the drain pit and flush the lines with water and deenergise the pumps if required for any maintenance. • If the Biocide Storage Tank has to be handed over for maintenance, then the tank level has to be reduced to the level possible before stopping the Injection pumps. The tank has to be drained fully to the drain pit and washed thoroughly with water. g. Scale Inhibitor Injection Package 6932-A-07 Scale Inhibitor Injection System shutdown is carried out as described below: • Stop the Scale Inhibitor Injection Pumps 6932-P-09A/B from LCP • Close the isolation valve at the Scale Inhibitor Storage Tank outlet to the suction of the pumps EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 395 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Close the suction and discharge isolation valves of the Scale Inhibitor Injection Pumps • Close the Scale Inhibitor injection line isolation valve at the injection point • Drain the Scale Inhibitor from the lines and the pumps to the drain pit and flush the lines with water and deenergise the pumps if required for any maintenance. • If the Scale Inhibitor Storage Tank has to be handed over for maintenance, then the tank level has to be reduced to the level possible before stopping the Injection pumps. The tank has to be drained fully to the drain pit and washed thoroughly with water. h. Catalyst Injection Package 9101-A-01 Catalyst Injection System shutdown is carried out as described below: • Stop the Catalyst Injection Pumps 9101-P-11A/B from LCP • Close the isolation valve at the Catalyst Storage Tank outlet to the suction of the pumps • Close the suction and discharge isolation valves of the Catalyst Injection Pumps • Close the Catalyst injection line isolation valve at the injection point • Drain the Catalyst from the lines and the pumps to the drain pit and flush the lines with water and de-energise the pumps if required for any maintenance. • If the Catalyst Storage Tank has to be handed over for maintenance, then the tank level has to be reduced to the level possible before stopping the Injection pumps. The tank has to be drained fully to the drain pit and washed thoroughly with water. 10.2.5 Electro Chlorination Package Shutdown • The plant is stopped in a controlled manner by operating the system stop pushbutton on the HMI. • If the plant is in remote control mode then a stop signal from the DCS will initiate the controlled shutdown. • Following are the sequence events in controlled shutdown: • Give stop command • System shutdown sequence flag shown • Duty transformer/Rectifiers 6932-RC-101A/B are de-energised to 0 amps. • After a 1 minute delay: • The duty Sea Cooling Water Pump 6932-P-04 A/B is stopped • The Auto Back Wash Filter 6932-S-03A cycle operation completes the backwash EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 396 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10.2.6 • After 5 minutes of time delay duty Hydrogen Dilution Blower 6932-K-01A/B is stopped • The duty Continuous Chlorination Pump/Shock Chlorination Pump 6932-P05A/B is stopped • All actuated valves will close • The system Stop is indicated Sea cooling water Shutdown The shutdown of the Sea Cooling Water Pumps 6932-P-04A/B will proceed as follows: • Ensure that the Electro Chlorination Package is already stopped • Close the outlet valve and ensure that the pump runs in this condition for no more than a few seconds • Stop the Sea Cooling Water Pumps 6932-P-04A/B • Close the flushing/cooling fluid supply at a time appropriate to the process • For prolonged shutdowns and especially when ambient temperatures are likely to drop below freezing point, the pump and the cooling and flushing arrangements to be drained. 10.2.7 Fuel Gas system Shutdown Shutdown of the fuel gas system is carried out as described below: • Ensure that there is no requirement for fuel gas from the New Steam Boiler Package 6848-A-02A/B/C • Ensure that the Boiler Package 6848-A-02A/B/C fuel gas inlet XVs 68-XV-1302, 68-XV-1303 & 68-XV-1304 and the isolation valves are closed • Isolate the backup fuel gas supply from 6103-K-01A/B by closing the isolation valves of 62-PV-1301B • Isolate the backup fuel gas supply from 30” existing line by closing the isolation valves of 62-PV-1302 • Close the fuel gas supply from first stage Booster Compressor 6701-K-10/20/30 by closing the isolation valves of 62-PV-1301A • Open 62-PV-1303 to LP Flare Header and depressurise the system • Open the drain valves of the LP Fuel gas KO Drum and drain the liquids to the LP Flare Header • Purge the Fuel gas system with nitrogen to reduce the HC content to 0% LEL and depressurise the system EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 397 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Reverse to close the spectacle blinds on the fuel gas lines from Booster Compressor 6701-K-10/20/30 upstream of 62-XV-1301, spectacle blind on the back up fuel gas supply from 6103-K-01A/B upstream of 62-XV-1302 and spectacle blind on the back up fuel gas supply from 30” existing line upstream of 62-XV-1303 • Reverse to close the spectacle blinds on the fuel gas lines to the New Steam Boiler Package 6848-A-02A/B/C upstream of XV-1302/XV-1303/XV-1304 • The fuel gas system is to be preserved under nitrogen till maintenance activities are taken up. 10.2.8 Effluent & Waste Water Unit Shutdown The Effluent & Waste Water Unit shutdown is carried out in the following steps: • Slowly reduce the waste water feed to the Waste Water Degasser 6922-V-07 and stop the flow from the upstream units • Close 69-PV-1315A and open 69-PV-1315B and send the sour gas from Sour Water Stripper to LP Acid Gas Flare Header • Gradually reduce the level in the Waste Water Degasser 6922-V-07 by pumping the waste water to the Sour Water Stripper. • Stop Waste Water Degasser Pumps 6922-08A/B • Stop the Stripper Overheads Circulation Pump 6922-P-11A/B • Reduce the steam flow to the Sour Water Stripper Reboiler and fully close 69-FV1315 • Close the Reboiler Condensate Drum 6922-V-09 level control valve 69-LV-1327 and open vent in the drum when the pressure reaches 1.0 barg • Reduce the level in the Sour Water Stripper 6922-C-01 and stop the Stripped Water Pump 6922-P-10 A/B when the level is low • Stop the Stripper Overheads Cooler 6922-E-03 fans and the Stripped Water Cooler 6922-E-02 fans • Close 69-PV-1307 and stop the nitrogen supply to the Waste Water Degasser 6922-V-07 • Drain the Waste Water Degasser 6922-V-07 to the waste water distribution header through the Waste Water Degasser Pumps 6922-P-08A/B casing drains • Drain the Sour Water Filter 6922-S-06 to the waste water distribution header • Drain the Sour/Stripped Water Exchanger 6922-E-01 to the waste water distribution header • Drain the Sour Water Stripper 6922-C-01 to the waste water distribution header through the bottom drain EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 398 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10.2.9 • Drain the Stripped Water Pumps 6922-P-10A/B to the waste water distribution header through the casing drain • Drain the Stripper Overhead Circulation Pumps 6922-P-11A/B to the waste water distribution header through the casing drain • Drain the Sour Water Stripper Reboiler 6922-E-04A/B to the waste water distribution header through the low point drain • Drain the Stripper Overheads Cooler 6922-E-03 and Stripped Water Cooler 6922-E02 to the waste water distribution header through the low point drain • Depressurise the system to LP Acid Gas Flare Header • Steam out of the system is necessary to carry out maintenance activities. Instrument air Shutdown 10.2.9.1 Shutdown of Instrument Air Compressor The Instrument Air Compressor is normally kept in ‘Remote-Auto’ mode during normal operation. Hence, depending on the demand of instrument air, the Compressor will get stopped automatically. Auto Stop In Remote mode, if the Compressor runs unloaded for a period of time (maximum 20 minutes idling delay), the Compressor gets stopped. The Compressor will restart only when the air is required. Compressor Manual stop A compressor can be taken for planned shutdown after ensuring the healthiness of Stand-by Compressor In remote mode compressor can be stopped by the operator from ICSS/UCP. In local mode Compressor can be stopped by pressing the ‘STOP’ pushbutton in Local Control Panel. The following steps to be followed for stopping the Compressor 6837-K-02A from LCP: 1. Turn the selector switch 68-HS-1403 to Local position in LCP. 2. Initiate the stop command (68-HSCA-1415) from LCP. 3. Confirm the Compressor 6837-K-02A gets unloaded by de-energizing both SOV’s. 4. After 10 seconds main motor and the fan cooler motors will be stopped. Note: Follow the above steps for shutdown of Instrument Air Compressor 6837-K-02B. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 399 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 10.2.9.2 Planned Shutdown of Dryer Package The Dryer Package can be taken planned shutdown for carrying out the scheduled maintenance activities like cleaning of Filters, replacement of desiccant, calibration of instruments, servicing of ON-OFF valves may be carried out as per QP maintenance schedule. The following steps are to be followed for shutdown of the Instrument Air Dryer Package (Train – A) and release for maintenance: • Initiate ‘STOP’ command 68-HSCA-1408 from DCS/UCP after completion of drying cycle Note: The dryer will stop after completion of the present cycle. The command de-energises the purge solenoids to close the purge valves 68-XV-1416 & 68-XV-1417. • Ensure that inlet 68-XV-1418 & 68-XV-1419 is closed • Close the manual isolation valves 68-BV-2236 & 68-BV-2238 at the upstream of Pre-Filters 6837-S07A/B • Close the manual isolation valves 68-BV-2249 & 68-BV-2251 at the outlet of After Filter 6837-S08A/B • Open the condensate drain valves of Pre-Filters 6837-S-07A/B • Depressurise the system by opening the vent valves Note: Follow the above procedure for shutdown of Instrument Air Dryer Package (Train-B). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 400 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION XI EMERGENCY SHUTDOWN EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 401 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.1 GENERAL In general, Emergency Shutdowns (ESD) causes the affected equipment to be blocked in and isolated from other systems, or process areas, where upset conditions have not occurred. ESD system is designed to implement safe and dependable emergency shutdown of the process and utility systems, and their associated equipment in order to prevent the development of a hazardous condition, which may be caused by a process upset or by an external event. The operator can manually initiate emergency shutdown when required or in response to external events such as fire and gas detection. The ESD System is designed to achieve the following objectives listed in order of priority: • Protection of personnel (highest priority) • Protection of equipment • Protection of the environment • Continuity of production (by minimizing spurious shutdowns) The ESD system in SRU Upgrade is divided into five shutdown levels: 1. ESD Level 0 Shutdown- Total Plant Shutdown with depressurization. 2. ESD Level 1 Shutdown - Shutdown with Depressurization to safe level. 3. ESD Level 2 Shutdown - Shutdown without depressurization (manual depressurization is allowed). 4. ESD level 3-Process system/subsystem shutdown without depressurization. 5. ESD level 4-Individual equipment system shutdown without depressurization. Emergency shutdown, which can occur in the unit, must be recognized and acted upon immediately. In case of activation of any one unit ESD, the activated ESD performs the other unit shutdown, according to the sequence given in Cause & Effect Matrix & P&ID. ESD Level 0 Shutdown ESD level-0 shutdown is a total plant shutdown which includes a number of related level 3 unit/sub unit/zones which can also be shutdown on an individual basis with depressurization. ESD Level 1 Shutdown ESD level-1 shutdown includes a number of related level 3 unit/sub-unit/zones which can also be shutdown on an individual basis with depressurization to safe level. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 402 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL ESD Level 2 Shutdown ESD level-2 shutdown includes a number of related level 3 unit/sub-unit/zones which can also be shutdown on an individual basis without depressurization, but permissive for manual depressurization is available. ESD Level 3 Shutdown This level of shutdown is without depressurization, which normally protects a complete process unit. A system or subsystem shutdown typically comprise of a process system, such as TGTU or a RGG package. ESD Level 4 Shutdown This is the lowest level of shutdown, without depressurization and involves shutdown of an individual piece of equipment or a zone, which is immediately affected by an upset condition, but not affecting other equipment or zones. ESD Zones The SRU safeguarding based on ESD Zone is defined as below: Process: • Acid Gas Enrichment Unit • Sulphur Recovery Unit • TGTU • Incinerator Utilities: • Steam Generation System • Boiler Feed Water System • DM Water System • Chemical Injection System • Electro Chlorination System • Sea Cooling Water System • Fuel Gas System • Effluent and Waste Water System • Instrument Air Compressor EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL 11.2 PROCESS 11.2.1 Acid Gas Enrichment Unit Equipments in this ESD Zone are as follows: • Acid Gas Coolers (9103-E-101A/B) • Lean Acid Gas KO Drum (9103-V-14) • Acid Gas Amine Absorber (9103-C-11) • Acid Gas KO Drum Return Pumps (9103-P-14 A/B) • Acid Gas Rich Amine Pumps (9103-P-12A/B) • Lean/Rich Amine Exchanger (9103-E-11A/B) • Amine Regenerator (9103-C-12) • Hot Lean Amine Pumps (9103-P-17A/B) • Regenerator Condenser Coolers (9103-E-12) • Regenerator Condenser Trim Cooler (9103-E-16) • Regenerator Reflux Drum (9103-V-12) • Regenerator Reflux Drum Pumps (9103-P-11A/B) • Regenerator Re-Boiler Condensate Pot 9103-V-13) • Regenerator Re-Boiler (9103-E-13) • Lean Amine Cooler (9103-E-14) • Lean Amine Trim Cooler (9103-E-15) • Amine Surge Tank (9103-T-11) • Lean Amine Pumps (9103-P-13A/B) • Lean Amine Filter (9103-S-11) • Activated Carbon Filter (9103-S-12) • Fines Filter (9103-S-13) • Amine Sump (9103-V-10) • Amine Sump Pump (9103-P-15) • Amine Sump Filter (9103-S-14) Rev.: 0 Date: 03/09/2012 Page: 403 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 404 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.2.1.1 ESD Level-0 Shutdown in Acid Gas Enrichment Unit ESD Level-0 is activated only by pressing emergency pushbutton 65-HS-4001 in CCR. Following are the effects of ESD Level-0 Shutdowns in AGEU: • Acid gas ON/OFF valve 91-XV-1502 to flare opens • Acid gas ON/OFF valve 91-XV-1501 to 9103-E-101 closes • Acid Gas KO Drum Return Pumps 9103-P-14A/B trips • Liquid from Acid Gas KO Drum Return Pump ON/OFF valve 91-XV-1503 closes • Acid Gas Rich Amine Pump 9103-P-12A/B trips • Lean amine valve 91-XV-1504 to acid gas amine absorber closes • Hot Lean Amine Pumps 9103-P-17A/B trips • Hot lean amine valve 91-XV-1507 to Lean/Rich Exchanger closes • Regenerator Reflux Drum Pumps 9103-P-11A/B trips • DM water valve 91-XV-1517 to Regenerator Reflux Drum closes • Acid gas from Regenerator Reflux Drum ON/OFF valve 91-XV-1516 to SRU closes • Regenerator Reboiler steam valve 91-XV-1505 closes • Tail Gas Rich Amine Pumps 9102-P-16A/B trips • Lean amine to Tail Gas Amine Absorber valve 91-XV-1310 closes • Tail gas rich amine valve from Tail Gas Rich Amine Pump discharge 91-XV-1309 closes • Lean Amine Pumps 9103-P-13A/B trips • Amine sump pump 9103-P-15 trips • Acid gas drain outlet valve 91-XV-1109 from pipe separator closes. • Regenerator condenser cooler fans trip • Lean amine cooler fans trip • Lean Amine Pumps 9103-P-13A/B trips 11.2.1.2 ESD Level-1 Shutdown in Acid Gas Enrichment Unit ESD Level-1 shutdown in AGEU is activated on the following causes: • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4) • Fire detection alarm (68-XS-02-1801) from utility area (LER-6) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 405 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Fire detection alarm (68-XS-03-1801) from utility boiler area (LER-6) • Fire detection alarm (66-XS-01-1801) from new substation area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from utility area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from utility boiler area (LER-6) • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from new substation area • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR Following are the effects of ESD Level 1 Shutdowns in AGEU & Amine section: • Acid gas ON/OFF valve 91-XV-1502 to flare opens • Acid gas ON/OFF valve 91-XV-1501 to 9103-E-101 closes • Acid Gas KO Drum Return Pumps 9103-P-14A/B trips • Liquid from Acid Gas KO Drum Return Pump ON/OFF valve 91-XV-1503 closes • Acid Gas Rich Amine Pump 9103-P-12A/B trips • Lean amine valve 91-XV-1504 to acid gas amine absorber closes • Hot Lean Amine Pumps 9103-P-17A/B trips • Hot lean amine valve 91-XV-1507 to Lean/Rich Exchanger closes • Regenerator Reflux Drum Pumps 9103-P-11A/B trips • DM water valve 91-XV-1517 to Regenerator Reflux Drum closes • Acid gas from Regenerator Reflux Drum ON/OFF valve 91-XV-1516 to SRU closes • Regenerator Reboiler steam valve 91-XV-1505 closes • Tail Gas Rich Amine Pumps 9102-P-16A/B trips • Lean amine to Tail Gas Amine Absorber valve 91-XV-1310 closes • Tail gas rich amine valve from Tail Gas Rich Amine Pump discharge 91-XV-1309 closes • Lean Amine Pumps 9103-P-13A/B trips • Amine sump pump 9103-P-15 trips • Acid gas drain outlet valve 91-XV-1109 from pipe separator closes. • Regenerator condenser cooler fans trip EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 406 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Lean amine cooler fans trip • Lean Amine Pumps 9103-P-13A/B trips 11.2.1.3 ESD Level 2 Shutdown in Acid Gas Enrichment Unit Following are the causes for ESD level-2 shutdown: • Activation of ESD-2 Level-2 shutdown pushbutton 61-HS-006 • Power failure signal (65-XS-1024) from ESD system at LER-4 • Instrument air pressure low low (2oo3) alarm 65-PALL-1003 (existing) • Instrument air pressure low low (2oo3) alarm 68-PALL-1312 (SRU Upgrade) • Steam Generator Package shutdown signal 68-XS-1580/68-XS-1680/68-XS-1780 • Existing SRU shutdown signal 65-XA-1001 from ESD system at LER-4 • Incinerator shutdown signal (91-XS-1186) from UCP at LER-4 • BFW/Steam failure signal 65-XS-1021 from ESD system at LER-4 • High high level alarm (91-LAHH-1504) in Acid Gas Amine Absorber bottom (9103-C-11) • High high level alarm (91-LAHH-1509) in Amine Regenerator bottom (9103-C-12) • Low low flow alarm (91-FALL-1515) from Lean Amine Pumps (9103-P-13A/B) discharge Following are the effects of ESD Level 2 Shutdowns in AGEU: • Operator Permissive is available for operating Acid gas ON/OFF valve 91-XV-1502 to flare • Acid gas ON/OFF valve 91-XV-1501 to 9103-E-101 closes • Acid Gas KO Drum Return Pumps 9103-P-14A/B trips • Liquid from Acid Gas KO Drum Return Pump ON/OFF valve 91-XV-1503 closes • Acid Gas Rich Amine Pump 9103-P-12A/B trips • Lean amine valve 91-XV-1504 to acid gas amine absorber closes • Hot Lean Amine Pumps 9103-P-17A/B trips • Hot lean amine valve 91-XV-1507 to Lean/Rich Exchanger closes • Regenerator Reflux Drum Pumps 9103-P-11A/B trips • DM water valve 91-XV-1517 to Regenerator Reflux Drum closes • Acid gas from Regenerator Reflux Drum ON/OFF valve 91-XV-1516 to SRU closes • Regenerator Reboiler steam valve 91-XV-1505 closes • Tail Gas Rich Amine Pumps 9102-P-16A/B trips EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 407 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Lean amine to Tail Gas Amine Absorber valve 91-XV-1310 closes • Tail gas rich amine valve from Tail Gas Rich Amine Pump discharge 91-XV-1309 closes • Lean Amine Pumps 9103-P-13A/B trips • Amine sump pump 9103-P-15 trips • Acid gas drain outlet valve 91-XV-1109 from pipe separator closes. • Regenerator condenser cooler fans trip • Lean amine cooler fans trip • Lean Amine Pumps 9103-P-13A/B trips 11.2.1.4 ESD Level 3 Shutdown in AGEU ESD Level-3 is activated in AGEU only by pressing pushbutton 91-HS-1011 in CCR. Following are the effects of ESD Level 3 Shutdown in AGEU & Amine section: • Acid gas ON/OFF valve 91-XV-1501 to 9103-E-101 closes • Acid Gas KO Drum Return Pumps 9103-P-14A/B trips • Liquid from Acid Gas KO Drum Return Pump ON/OFF valve 91-XV-1503 closes • Acid Gas Rich Amine Pump 9103-P-12A/B trips • Lean amine valve 91-XV-1504 to Acid Gas Amine Absorber closes • Hot Lean Amine Pumps 9103-P-17A/B trips • Hot lean amine valve 91-XV-1507 to Lean/Rich Exchanger closes • Regenerator Reflux Drum Pumps 9103-P-11A/B trips • DM water valve 91-XV-1517 to Regenerator Reflux Drum closes • Acid gas from Regenerator Reflux Drum ON/OFF valve 91-XV-1516 to SRU closes • Regenerator Re-boiler steam valve 91-XV-1505 closes • Tail Gas Rich Amine Pumps 9102-P-16A/B trips • Lean amine to Tail Gas Amine Absorber valve 91-XV-1310 closes • Tail gas rich amine valve from Tail Gas Rich Amine Pump discharge 91-XV-1309 closes • Lean Amine Pumps 9103-P-13A/B trips • Amine Sump Pump 9103-P-15 trips • Acid gas drain outlet valve 91-XV-1109 from Pipe Separator closes. • Regenerator Condenser Cooler Fans trip EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 408 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Lean Amine Cooler Fans trip • Lean Amine Pumps 9103-P-13A/B trips 11.2.1.5 ESD Level 4 Shutdown in Acid Gas Enrichment Unit Following are the ESD Level 4 Shutdowns (equipment wise) in AGEU & Amine section: Lean Acid Gas KO Drum (9103-V-14) • High high level alarm 91-LAHH-1502 in Lean Acid Gas KO Drum (9103-V-14) closes the acid gas block valve 91-XV-1501 to Acid Gas Coolers • Low low level alarm 91-LALL-1503 in lean acid gas KO drum (9103-V-14) closes the liquid block valve 91-XV-1503 from lean acid KO drum Acid Gas Amine Absorber (9103-C-11) • Low low level alarm 91-LALL-1516 in Acid Gas Amine Absorber bottom trips the Acid Gas Rich Amine Pumps 9103-P-12A/B • Low low rich amine flow alarm 91-FALL-1510 in Acid Gas Amine Absorber trips the Acid Gas Rich Amine Pumps 9103-P-12A/B Amine Regenerator • Low low level alarm 91-LALL-1517 in Amine Regenerator bottom trips the Hot Lean Amine Pumps 9103-P-17A/B and closes the hot lean amine valve 91-XV-1507 to Lean Rich Exchanger • Low low hot lean amine flow alarm 91-FALL-1509 trips the Hot Lean Amine Pumps 9103-P-17A/B and closes the hot lean amine valve 91-XV-1507 to Lean Rich Exchanger Regenerator Reflux Drum • Low low level alarm 91-LALL-1518 in Regenerator Reflux Drum trips the regenerator reflux drum pumps 9103-P-11A/B • High high level alarm (91-LAHH-1507) in Regenerator Reflux Drum closes the DM water block valve 91-XV-1517 • Low low flow alarm (91-FALL-1506) trips the Regenerator Reflux Pumps 9103-P11A/B Tail Gas Absorber • High high level alarm (91-LAHH-1310) in Tail Gas Absorber bottom closes the lean amine inlet valve 91-XV-1310 to Tail Gas Amine Absorber • Low low level alarm (91-LALL-1301) in Tail Gas Absorber bottom trips the Tail Gas Absorber Bottom Pumps (9102-P-16A/B) and closes the Tail Gas Rich Amine On/OFF valve 91-XV-1309 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 409 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Low low flow alarm (91-FALL-1305) in Tail Gas Rich Amine Pump discharge trips the Tail Gas Absorber Bottom Pumps (9102-P-16A/B) and closes the tail gas rich amine On/OFF valve 91-XV-1309 Amine Surge Tank • Low low level alarm (91-LALL-1511) in Amine Surge Tank trips the lean amine pump (9103-P-13A/B) • Low low level alarm (91-LALL-1513) in Amine Sump trips the amine sump pump (9103-P-15) Pipe Separator Low low level alarm (91-LALL-1054) closes the acid gas outlet valve 91-XV-1109 in the Pipe Separator Regenerator Condenser Coolers Regenerator Condenser Coolers 9103-E-12AA to 9103-E-12DC trips, due to high high vibration alarms sensed by their respective cooler fan vibration probes. Detail list of coolers and vibration alarms are as listed below: Vibration Tag No. Cooler Tag No. 91-VAHH-1537 9103-EM-12AA 91-VAHH-1538 9103-EM-12AB 91-VAHH-1539 9103-EM-12AC 91-VAHH-1540 9103-EM-12BA 91-VAHH-1541 9103-EM-12BB 91-VAHH-1542 9103-EM-12BC 91-VAHH-1543 9103-EM-12CA 91-VAHH-1544 9103-EM-12CB 91-VAHH-1545 9103-EM-12CC 91-VAHH-1546 9103-EM-12DA 91-VAHH-1547 9103-EM-12DB 91-VAHH-1548 9103-EM-12DC Lean Amine Coolers Lean amine coolers 9103-E-14AA to 9103-E-14JC trips due to high high vibration alarms sensed by their respective cooler fan vibration probes. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 410 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Detail list of coolers and vibration alarms are as listed below: Vibration Tag No. Cooler Tag No. 91-VAHH-1501 9103-EM-14AA 91-VAHH-1502 9103-EM-14AB 91-VAHH-1503 9103-EM-14AC 91-VAHH-1504 9103-EM-14BA 91-VAHH-1505 9103-EM-14BB 91-VAHH-1506 9103-EM-14BC 91-VAHH-1507 9103-EM-14CA 91-VAHH-1508 9103-EM-14CB 91-VAHH-1509 9103-EM-14CC 91-VAHH-1510 9103-EM-14DA 91-VAHH-1511 9103-EM-14DB 91-VAHH-1512 9103-EM-14DC 91-VAHH-1513 9103-EM-14EA 91-VAHH-1514 9103-EM-14EB 91-VAHH-1515 9103-EM-14EC 91-VAHH-1516 9103-EM-14FA 91-VAHH-1517 9103-EM-14FB 91-VAHH-1518 9103-EM-14FC 91-VAHH-1519 9103-EM-14GA 91-VAHH-1520 9103-EM-14GB 91-VAHH-1521 9103-EM-14GC 91-VAHH-1522 9103-EM-14HA 91-VAHH-1523 9103-EM-14HB 91-VAHH-1524 9103-EM-14HC 91-VAHH-1525 9103-EM-14IA 91-VAHH-1526 9103-EM-14IB 91-VAHH-1527 9103-EM-14IC 91-VAHH-1528 9103-EM-14JA 91-VAHH-1529 9103-EM-14JB 91-VAHH-1530 9103-EM-14JC EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 411 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Lean Amine Pumps Lean Amine Pump 9103-P-13A trips due to the following causes: Tag No. Description 91-TAHH-1569 High high temperature alarm in lean amine motor NDE bearing 91-VAHH-1591 High high radial vibration alarm in lean amine pump motor DE end 91-VAHH-1592 High high radial vibration alarm in lean amine pump motor NDE end 91-VAHH-1593 High high radial vibration alarm in lean amine pump DE side 91-VAHH-1594 High high radial vibration alarm in lean amine pump NDE side 91-VAHH-1595 High high axial vibration alarm in lean amine pump NDE side 91-VAHH-1596 High high axial vibration alarm in lean amine pump NDE side Lean Amine Pump 9103-P-13B trips due to the following causes: Tag No. Description 91-TAHH-1579 High high temperature alarm in lean amine motor NDE bearing 91-VAHH-1599 High high radial vibration alarm in lean amine pump motor DE end 91-VAHH-1600 High high radial vibration alarm in lean amine pump motor NDE end 91-VAHH-1601 High high radial vibration alarm in lean amine pump DE side 91-VAHH-1602 High high radial vibration alarm in lean amine pump NDE side 91-VAHH-1603 High high axial vibration alarm in lean amine pump NDE side 91-VAHH-1604 High high axial vibration alarm in lean amine pump NDE side • High high temperature alarm (91-TAHH-1589) in Acid Gas Rich Amine Pump motor drive NDE bearing, trips the acid gas rich amine pump 9103-P-12A. • High high temperature alarm (91-TAHH-1593) in Acid Gas Rich Amine Pump motor drive NDE bearing, trips the acid gas rich amine pump 9103-P-12B. • High high temperature alarm (91-TAHH-1597) in Hot Lean Amine Pump motor drive NDE bearing, trips the acid gas rich amine pump 9103-P-17A. • High high temperature alarm (91-TAHH-1601) in Hot Lean Amine Pump motor drive NDE bearing, trips the acid gas rich amine pump 9103-P-17B. 11.2.2 Sulphur Recovery Unit Equipment in this ESD Zone is as follows: • Acid Gas KO drums (9101-V-04) • Process Air Blowers (9101-K-01A/B) • Process Air Pre-heater (9101-E-05) • Reaction Furnace (9101-F-01) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL • Steam Drum (9101-V-07) • Reaction Furnace Condenser (9101-E-01) • 1st Stage Condenser (9101-E-02) • 1st Stage Converter (9101-V-01) • Last Condenser (9101-E-04) • Boiler Feed Water Heater (9101-E-08) • Acid Water Pumps (9101-P-01A/B) • Acid Gas Pre-Heater (9101-E-06) • HP Condensate Drums (9101-V-06). • Reaction Furnace Boiler (9101-E-07) • Boiler Blow Down Pit (9101-T-04) • 1st Stage Auxiliary Burner (9101-F-02) • 2nd Stage Auxiliary Burner (9101-F-03) • 2nd Stage Converter (9101-V-02) • Final Separator (9101-V-05) • New Catalyst Tank (9101-T-09) • New Sulphur Degassing Pumps (9101-P-09A/B) • New Sulphur Degassing Pit (9101-T-01B) • Existing Catalyst Tank (9101-T-03) • Existing Sulphur Degassing Pumps (9101-P-03A/B) • Existing Sulphur Degassing Pit (9101-T-01) • Sulphur Storage Tank (9101-T-02) • Steam Ejector (9101-X-02) • New Steam Ejector (9101-X-03) • New Catalyst Metering Pumps (9101-P-11A/B) • New Sulphur Product Pumps (9101-P-10A/B) • Catalyst Metering Pumps (9101-p-02A/B) • Existing Sulphur Product Pumps (9101-P-04A/B) • Sulphur Tank Pumps (9101-P-15A/B) Rev.: 0 Date: 03/09/2012 Page: 412 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 413 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.2.2.1 ESD –Level 1 Shutdown in Existing SRU Following are the causes which initiates ESD level-1 shutdown in existing SRU: • General plant shutdown activation by pushbutton 65-HS-001 • Total power shutdown signal 65-XS-1024 • Instrument air pressure low low alarm 65-PALL-1003A/B/C • BFW steam failure signal 68-XS-1015 • Unit -91 general shutdown activation by pushbutton 91-HS-1011 Above mentioned ESD level-1 shutdown causes closes the following valves in existing SRU: • Acid gas inlet valve 91-XV-1001 to acid gas KO drum 9101-V-04 • Acid water outlet valve 91-XV-1022 to MEDA storage tank • Combustion air discharge valve 91-XV-1046 to pre-heater 9101-E-05 • Fuel gas to Reaction Furnace valve 91-XV-1099 • Fuel gas to Reaction Furnace valve 91-XV-1048 • Acid gas to Reaction Furnace valve 91-XV-1102 • Combustion air to Reaction Furnace valve 91-XV-1101 • Combustion air to Reaction Furnace valve 91-FV-1002 • Secondary air to Reaction Furnace valve 91-FV-1002B • Trim air to Reaction Furnace valve 91-FV-1003 • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1028 • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1131 • Fuel gas to 1st Stage Auxiliary Burner valve 91-FV-1020 • Combustion air to 1st Stage Auxiliary Burner valve 91-FV-1018 • Acid gas to 1st Stage Auxiliary Burner valve 91-FV-1019 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1031 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1133 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-FV-1027 • Combustion air to 2nd Stage Auxiliary Burner valve 91-FV-1025 • Acid gas to 2nd Stage Auxiliary Burner valve 91-FV-1026 • Tail gas valve 91-XV-1098 to RGG EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 414 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Above mentioned ESD level-1 shutdown causes opens the following valves in existing SRU: • Fuel gas to atmosphere from 1st Stage Auxiliary Burner valve 91-XV-1132 • Fuel gas to atmosphere from 2nd Stage Auxiliary Burner valve 91-XV-1134 • Fuel gas to atmosphere from Reaction Furnace valve 91-XV-1100 • Nitrogen valve 91-XV-1127 to Reaction Furnace instruments • LP steam in air valve 91-XV-1076 to Acid Gas Burner • LP steam valve 91-XV-1079 to acid gas gun open • Tail gas valve 91-XV-1097 to Incinerator Above mentioned ESD level-1 shutdown causes trips the following in existing SRU: Equipment Tag No. Description Trip Signal 9101-K-01A/B Process Air Blower 91-XS-1004/91-XS-1005 9101-P-01A/B Acid Water Pump 91-XS-1002/91-XS-1003 9101-P-02A/B Catalyst Metering Pumps 91-XS-1034/91-XS-1035 9101-P-03A/B Sulphur Degassing Pumps 91-XS-1036/91-XS-1037 9101-P-11A/B Catalyst Metering Pumps 91-XS-1129/91-XS-1130 9101-P-09A/B Sulphur Degassing Pumps 91-XS-1138/91-XS-1139 9101-P-04A/B Sulphur Product Pumps 91-XS-1038/91-XS-1039 9101-P-10A/B Sulphur Product Pumps 91-XS-1140/91-XS-1141 9101-P-15A/B Sulphur Tank Pumps 91-XS-1051/91-XS-1052 Note: 1. Steam supply valve 91-XV-1045 to Ejector 9101-X-02 and Steam supply valve 91-XV1092 to Ejector 9101-X-03 is closed only on the following ESD level-1 causes: • BFW steam failure signal 68-XS-1015 • Unit-91 general shutdown activation by pushbutton 91-HS-1011 2. Incinerator is tripped only due to following ESD level-1 causes: • General plant shutdown activation by pushbutton 65-HS-001 • Total power shutdown signal 65-XS-1024 • Instrument air pressure low low alarm 65-PALL-1003A/B/C EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 415 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.2.2.2 ESD–Level 2 Shutdown in Existing SRU Following is the only cause which initiates ESD level-2 shutdowns in existing SRU: Confirmed gas detection alarm (91-GF-1001/1029) 91-XS-1901 in existing SRU. Above mentioned ESD level-2 shutdown cause closes the following valves in existing SRU: • Acid gas inlet valve 91-XV-1001 to Acid Gas KO Drum 9101-V-04 • Acid water outlet valve 91-XV-1022 to MDEA storage tank • Combustion air discharge valve 91-XV-1046 to Pre-Heater 9101-E-05 • Fuel gas to Reaction Furnace valve 91-XV-1099 • Fuel gas to Reaction Furnace valve 91-XV-1048 • Acid gas to Reaction Furnace valve 91-XV-1102 • Combustion air to Reaction Furnace valve 91-XV-1101 • Combustion air to Reaction Furnace valve 91-FV-1002 • Secondary air to Reaction Furnace valve 91-FV-1002B • Trim air to Reaction Furnace valve 91-FV-1003 • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1028 • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1131 • Fuel gas to 1st Stage Auxiliary Burner valve 91-FV-1020 • Combustion air to 1st stage auxiliary burner valve 91-FV-1018 • Acid gas to 1st Stage Auxiliary Burner valve 91-FV-1019 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1031 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1133 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-FV-1027 • Combustion air to 2nd Stage Auxiliary Burner valve 91-FV-1025 • Acid gas to 2nd Stage Auxiliary Burner valve 91-FV-1026 • Tail gas valve 91-XV-1098 to RGG • Steam supply valve 91-XV-1045 to Ejector 9101-X-02 • Steam supply valve 91-XV-1092 to Ejector 9101-X-03 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 416 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Above mentioned ESD level -2 shutdown cause opens the following valves in existing SRU: • Fuel gas to atmosphere from 1st Stage Auxiliary Burner valve 91-XV-1132 • Fuel gas to atmosphere from 2nd Stage Auxiliary Burner valve 91-XV-1134 • Fuel gas to atmosphere from reaction furnace valve 91-XV-1100 Nitrogen valve 91-XV-1127 to Reaction Furnace instruments • LP steam in air valve 91-XV-1076 to acid gas burner • LP steam ON/OFF valve 91-XV-1079 to acid gas gun • Tail gas valve 91-XV-1097 to Incinerator Above mentioned ESD level -2 shutdown causes trips the following in existing SRU: Equipment Tag No. Description Trip Signal 9101-K-01A/B Process air blower 91-XS-1004/91-XS-1005 9101-P-01A/B Acid water pump 91-XS-1002/91-XS-1003 9101-P-02A/B Catalyst metering pumps 91-XS-1034/91-XS-1035 9101-P-03A/B Sulphur degassing pumps 91-XS-1036/91-XS-1037 9101-P-11A/B Catalyst metering pumps 91-XS-1129/91-XS-1130 9101-P-09A/B Sulphur degassing pumps 91-XS-1138/91-XS-1139 9101-P-04A/B Sulphur product pumps 91-XS-1038/91-XS-1039 9101-P-10A/B Sulphur product pumps 91-XS-1140/91-XS-1141 9101-P-15A/B Sulphur tank pumps 91-XS-1051/91-XS-1052 Note: Incinerator is tripped through the signal 91-XS-1169. 11.2.2.3 ESD–Level 3 Shutdown in Existing SRU Following are the causes which initiates ESD level-3 shutdowns in existing SRU: • Fuel gas low low pressure alarm 65-XS-1020 • AGR S/D (2 trains) 65-XS-1008 • Process air blowers flow low low alarm 91-FALL-1006 • Steam Drum 9101-V-07 level low low alarm 91-LALL-1006 • Reaction Furnace Condenser level low low alarm 91-LALL-1009 • 1st Stage Condenser level low low alarm 91-LALL-1012 • Acid gas inlet pressure low low alarm 91-PALL-1025 • Process Air Blower 9101-K-01A/B shutdown signals 91-XS-1063 and 91-XS-1064 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 417 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Air for acid gas burner pressure high high alarm 91-PAHH-1054A/B/C • Acid gas to reaction furnace flow low low alarm 91-FALL-1140 • Combustion air to acid gas burner flow low low alarm 91-FALL-1129 • Fuel gas to reaction furnace flow low low alarm 91-FALL-1130 • Reaction Furnace shutdown pushbutton 91-HS-1012A from CCR • Reaction Furnace shutdown pushbutton 91-HS-1213 from LCP • Reaction furnace flame failure alarm 91-BALL-1055A/B • Rupture pin failure alarm 91-TAHH-1050 Above mentioned ESD level-3 shutdown causes closes the following valves in existing SRU: • Acid gas inlet valve 91-XV-1001 to Acid Gas KO Drum 9101-V-04 • Acid water outlet valve 91-XV-1022 to MDEA storage tank • Combustion air discharge valve 91-XV-1046 to Air Pre-Heater 9101-E-05 • Fuel gas to Reaction Furnace valve 91-XV-1099 • Fuel gas to Reaction Furnace valve 91-XV-1048 • Acid gas to Reaction Furnace valve 91-XV-1102 • Combustion air to Reaction Furnace valve 91-XV-1101 • Combustion air to Reaction Furnace valve 91-FV-1002 • Secondary air to Reaction Furnace valve 91-FV-1002B • Trim air to Reaction Furnace valve 91-FV-1003 • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1028 • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1131 • Fuel gas to 1st Stage Auxiliary Burner valve 91-FV-1020 • Combustion air to 1st Stage Auxiliary Burner valve 91-FV-1018 • Acid gas to 1st Stage Auxiliary Burner valve 91-FV-1019 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1031 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1133 • Combustion air to 2nd Stage Auxiliary Burner valve 91-FV-1025 • Acid gas to 2nd Stage Auxiliary Burner valve 91-FV-1026 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-FV-1027 • Tail gas valve 91-XV-1098 to RGG EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 418 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Above mentioned ESD level-3 shutdown causes opens the following valves in existing SRU: • Fuel gas to atmosphere from 1st Stage Auxiliary Burner valve 91-XV-1132 • Fuel gas to atmosphere from 2nd Stage Auxiliary Burner valve 91-XV-1134 • Fuel gas to atmosphere from Reaction Furnace valve 91-XV-1100 • Nitrogen valve 91-XV-1127 to Reaction Furnace instruments • LP steam in air valve 91-XV-1076 to Acid gas burner • LP steam valve 91-XV-1079 to acid gas gun open • Tail gas valve 91-XV-1097 to Incinerator Above mentioned ESD level-3 shutdown causes trips the following in existing SRU: • Process air blower’s 9101-K-01A/B • Acid Water Pumps 9101-P-01A/B Note: Incinerator is tripped only on Fuel gas pressure low low alarm 65-XS-1020. 11.2.2.4 ESD–Level 4 Shutdown in Existing SRU 1st Stage Auxiliary Burner Following are the causes in SRU 1st Stage Auxiliary Burner which initiates ESD Level 4 Shutdown: • Activation of 1st Stage Auxiliary Burner stop pushbutton 91-HS-1227 from LCP • Combustion air flow to 1st Stage Auxiliary Burner low low alarm 91-FALL-1133 • Acid gas flow to 1st Stage Auxiliary Burner low low alarm 91-FALL-1134 • Fuel gas flow to 1st Stage Auxiliary Burner low low alarm 91-FALL-1135 • Flame failure alarm 91-BALL-1003A/B in 1st Stage Auxiliary Burner Effects of ESD Level 4 Shutdown in SRU-1st stage auxiliary burner: • 1st Stage Auxiliary Burner fuel gas valve 91-XV-1028 close • 1st Stage Auxiliary Burner fuel gas valve 91-XV-1131 close • 1st Stage Auxiliary Burner combustion air valve 91-FV-1018 close • 1st Stage Auxiliary Burner acid gas valve 91-FV-1019 close • 1st Stage Auxiliary Burner fuel gas valve 91-FV-1020 close • 1st Stage Auxiliary Burner fuel gas to atmosphere valve 91-XV-1132 opens EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 419 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 2nd Stage Auxiliary Burner Following are the causes in SRU 2nd Stage Auxiliary Burner which initiates ESD Level 4 Shutdown: • Activation of 2nd Stage Auxiliary Burner stop pushbutton 91-HS-1196 from LCP • Combustion air flow to 2nd Stage Auxiliary Burner low low alarm 91-FALL-1136 • Acid gas flow to 2nd Stage Auxiliary Burner low low alarm 91-FALL-1137 • Fuel gas flow to 2nd Stage Auxiliary Burner low low alarm 91-FALL-1138 • Flame failure alarm 91-BALL-1004A/B in 2nd Stage Auxiliary Burner Effects of ESD Level 4 Shutdown in SRU 2nd stage auxiliary burner: • 2nd Stage Auxiliary Burner fuel gas valve 91-XV-1031 close • 2nd Stage Auxiliary Burner fuel gas valve 91-XV-1133 close • Combustion air to 2nd Stage Auxiliary Burner valve 91-FV-1025 close • 2nd Stage Auxiliary Burner acid gas valve 91-FV-1026 close • 2nd Stage Auxiliary Burner fuel gas valve 91-FV-1027 close • 2nd Stage Auxiliary Burner fuel gas to atmosphere valve 91-XV-1134 opens Sulphur Pit Following are the causes in SRU which initiates ESD Level 4 Shutdown in Sulphur pit 9101-T-01: • High high H2S alarm 91-AHA-1002 alarm in 9101-T-01 • Sweeping air flow low low alarm 91-FALL-1032 Effects of ESD Level 4 Shutdown in SRU - Sulphur pit 9101-T-01: • Catalyst Metering Pumps 9101-P02A/B trip • Sulphur Degassing Pumps 9101-P03A/B trip • Sulphur Product Pumps 9101-P-04A/B trip New Sulphur Pit Following are the causes in SRU which initiates ESD Level 4 Shutdown in New Sulphur Pit 9101-T-01B: • High high H2S alarm 91-AHA-1002 alarm in 9101-T-01B • Sweeping air flow low low alarm 91-FALL-1056 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 420 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Effects of ESD Level 4 Shutdown in SRU – New Sulphur Pit 9101-T-01B area: • New Catalyst Metering Pumps 9101-P11A/B trip • New Sulphur Degassing Pumps 9101-P09A/B trip • New Sulphur Product Pumps (9101-P-10A/B) trip Acid Gas KO Drum High high level alarm 91-LAHH-1003 alarm in Acid Gas KO Drum 9101-V-04 closes the following valves: • Acid gas inlet valve 91-XV-1001 to Acid Gas KO Drum 9101-V-04 • Combustion air discharge valve 91-XV-1046 to Pre-heater 9101-E-05 • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1028 • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1131 • Combustion air to 1st Stage Auxiliary Burner valve 91-FV-1018 • Acid gas to 1st Stage Auxiliary Burner valve 91-FV-1019 • Fuel gas to 1st Stage Auxiliary Burner valve 91-FV-1020 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1031 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1133 • Combustion air to 2nd Stage Auxiliary Burner valve 91-FV-1025 • Acid gas to 2nd Stage Auxiliary Burner valve 91-FV-1026 • Fuel gas to 2nd Stage Auxiliary Burner valve 91-FV-1027 • Fuel gas to Reaction Furnace valve 91-XV-1099 • Fuel gas to Reaction Furnace valve 91-XV-1048 • Combustion air to Reaction Furnace valve 91-XV-1101 • Acid gas to Reaction Furnace valve 91-XV-1102 • Combustion air to Reaction Furnace valve 91-FV-1002 • Secondary air to Reaction Furnace valve 91-FV-1002B • Trim air to Reaction Furnace valve 91-FV-1003 • Tail gas valve 91-XV-1098 to RGG High high level alarm 91-LAHH-1003 alarm in Acid Gas KO Drum 9101-V-04 opens the following valves: • Fuel gas to atmosphere from 1st Stage Auxiliary Burner valve 91-XV-1132 • Fuel gas to atmosphere from 2nd Stage Auxiliary Burner valve 91-XV-1134 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 421 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Fuel gas to atmosphere valve 91-XV-1100 • Nitrogen valve 91-XV-1127 to Reaction Furnace instruments • LP steam in air valve 91-XV-1076 to Acid Gas Burner • LP steam valve 91-XV-1092 to Acid gas gun • Tail gas valve 91-XV-1097 to Incinerator • High high level alarm 91-LAHH-1003 alarm in Acid Gas KO Drum 9101-V-04 trips the Process air blower’s 9101-K-01A/B. • Low low level alarm 91-LALL-1002 alarm in Acid Gas KO Drum 9101-V-04 activates the following: • Acid Water Pumps 9101-P-01A/B trip • Acid water outlet valve 91-XV-1022 to MDEA storage tank closes Sulphur Degassing Unit • Low low level alarm 91-LALL-1015 alarm in Sulphur Degassing Unit 9101-T-01 trips the following: • Sulphur Degassing Pumps 9101-P-03A/B • Sulphur Product Pumps 9101-P-04A/B • Low low level alarm 91-LALL-1017 alarm in Sulphur Storage Tank 9101-T-02 trips the Sulphur Tank Pumps 9101-P-15A/B. • Low low level alarm 91-LALL-1052 alarm in Sulphur Degassing Unit 9101-T-01B trips the following: • • Sulphur Degassing Pumps 9101-P-09A/B • Sulphur Product Pumps 9101-P-10A/B High high level alarm 91-LAHH-1017 alarm in Sulphur Storage Tank 9101-T-02 trips the following: • Sulphur Product Pumps 9101-P-10A/B • Sulphur Product Pumps 9101-P-04A/B Sulphur Degassing Pit • High high temperature alarm 91-TAHH-1033 in Sulphur Degassing Pit 9101-T-01 closes the steam supply valve 91-XV-1045 to Steam Ejector 9101-X-02. • High high temperature alarm 91-TAHH-1104 in Sulphur Degassing Pit 9101-T-01B closes the steam supply valve 91-XV-1092 to Steam Ejector 9101-X-03 and opens the LP steam valve 91-XV-1078 to Acid Gas Burner,91-XV-1079 to Acid Gas Gun. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 422 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • High high pressure alarm 91-PAHH-1055 in Final Separator 9101-V-05 opens the tail gas valve 91-XV-1097 to Incinerator and closes the tail gas valve 91-XV-1098 to RGG. • Gas detected alarm 91-XS-1902(91-GF-1001 to 91-GF-1003) in air intake of 9101-K01A trips the Combustion Blower 9101-K-01A. • Gas detected alarm 91-XS-1903 (91-GF-1004 to 91-GF-1006) in air intake of 9101-K-01B trips the Combustion Blower 9101-K-01B. Inter trips RGG shutdown signals 91-XS-1350 to existing SRU unit opens the tail gas valve 91-XV1097 to Incinerator and closes the tail gas valve 91-XV-1098 to RGG Incinerator shutdown signal 91-XS-1104 initiates the following in SRU: • Acid gas inlet valve 91-XV-1001 to Acid Gas KO Drum 9101-V-04 close • Combustion air discharge valve 91-XV-1046 to Pre-Heater 9101-E-05 close • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1028 close • Fuel gas to 1st Stage Auxiliary Burner valve 91-XV-1131 close • Combustion air to 1st Stage Auxiliary Burner valve 91-FV-1018 close • Acid gas to 1st Stage Auxiliary Burner valve 91-FV-1019 close • Fuel gas to 1st Stage Auxiliary Burner valve 91-FV-1020 close • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1031 close • Fuel gas to 2nd Stage Auxiliary Burner valve 91-XV-1133 close • Combustion air to 2nd Stage Auxiliary Burner valve 91-FV-1025 close • Acid gas to 2nd Stage Auxiliary Burner valve 91-FV-1026 close • Fuel gas to 2nd Stage Auxiliary Burner valve 91-FV-1027 close • Fuel gas to Reaction Furnace valve 91-XV-1099 close • Fuel gas to Reaction Furnace valve 91-XV-1048 close • Combustion air to Reaction Furnace valve 91-XV-1101 close • Acid gas to Reaction Furnace valve 91-XV-1102 close • Combustion air to Reaction Furnace valve 91-FV-1002 close • Secondary air to Reaction Furnace valve 91-FV-1002B close • Trim air to Reaction Furnace valve 91-FV-1003 close • Tail gas valve 91-XV-1098 to RGG close EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 423 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.2.3 • Steam supply valve 91-XV-1045 to Ejector 9101-X-02 close • Steam supply valve 91-XV-1092 to Ejector 9101-X-03 close • Fuel gas to atmosphere from 1st Stage Auxiliary Burner valve 91-XV-1132 open • Fuel gas to atmosphere from 2nd Stage Auxiliary Burner valve 91-XV-1134 open • Fuel gas to atmosphere from reaction furnace valve 91-XV-1100 open • Nitrogen valve 91-XV-1127 to Reaction Furnace instruments open • LP steam in air valve 91-XV-1076 to Acid Gas Burner open • LP steam valve 91-XV-1092 to Acid Gas Gun open • Tail gas valve 91-XV-1097 to Incinerator open • Combustion Air Blowers 9101-K-01A/B trip • Catalyst Metering Pumps 9101-P-02A/B, 9101-P-11A/B trip • Sulphur Degassing Pumps 9101-P-03A/B, 9101-P-09A/B trip • Sulphur Product Pumps 9101-P-10A/B trip • Sulphur Tank Pumps 9101-P-15A/B trip Tail Gas Treatment Unit Equipment in this ESD Zone is as follows: • RGG (9102-F-11) • Hydrogenation Reactor (9102-V-11) • Reactor Effluent Cooler (9102-E-11) • Start-up Gas Steam Ejector (9102-X-11) • De-super Heater/Contact Condenser (9102-C-11) • Wash Water Filter (9102-S-15) • Contact Condenser Trim Coolers (9102-E-13A/B) • Contact Condenser Cooler (9102-E-12) 11.2.3.1 ESD Level 0 Shutdown in TGTU system ESD level-0 is activated only by pressing emergency pushbutton 65-HS-4001 in CCR. Following are the effects of ESD Level 0 Shutdowns in TGTU section: • Combustion air block valve 91-XV-1306 to RGG closes • Fuel gas block valve 91-XV-1303 to RGG closes • Fuel gas vent valve 91-XV-1308 to RGG opens EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 424 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Fuel gas block valve 91-XV-1304 to RGG closes • Steam block valve 91-XV-1305 to RGG closes • Nitrogen purge block valve 91-XV-1307 to RGG opens • Nitrogen purge block valve 91-XV-1301 to RGG opens • Instrument air purge block valve 91-XV-1302 to RGG closes • De-super Heater Circulation Pump 9102-P-11A/B trip • Cooling Water Circulation Pump 9102-P-12A/B trip • Combustion Air Blowers 9102-K-11A/B is trip • Contact Condenser Cooler Fans trip • Tail gas bypass block valve 91-XV-1331 to Incinerator opens • Tail gas block valve 91-XV-1332 to Contact Condenser closes • Sour Water Stripper 6922-C-01 overhead block valve 69 XV-1313 closes 11.2.3.2 ESD Level 1 Shutdown in TGTU system Following causes initiates ESD level1 shutdown in TGTU: • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4). • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4). • Fire detection alarm (68-XS-02-1801) from Utility area (LER-6) • Fire detection alarm (68-XS-03-1801) from Utility Boiler Area (LER-6) • Fire detection alarm (66-XS-01-1801) from New Substation Area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from Utility Area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from Utility Boiler area (LER-6) • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from New Substation Area • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR Following are the effects of ESD Level 1 Shutdowns in TGTU section: • Combustion air block valve 91-XV-1306 to RGG closes • Fuel gas block valve 91-XV-1303 to RGG closes EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 425 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Fuel gas vent valve 91-XV-1308 to RGG opens • Fuel gas block valve 91-XV-1304 to RGG closes • Steam block valve 91-XV-1305 to RGG closes • Nitrogen purge block valve 91-XV-1307 to RGG opens • Nitrogen purge block valve 91-XV-1301 to RGG opens • Instrument air purge block valve 91-XV-1302 to RGG closes • De-super Heater Circulation Pump 9102-P-11A/B trip • Cooling Water Circulation Pump 9102-P-12A/B trip • Combustion Air Blowers 9102-K-11A/B is trip • Contact Condenser Cooler Fans trip • Tail gas bypass block valve 91-XV-1331 to Incinerator opens • Tail gas block valve 91-XV-1332 to Contact Condenser closes • Sour Water Stripper 6922-C-01 overhead block valve 69 XV-1313 closes 11.2.3.3 ESD Level 2 Shutdown in TGTU system ESD Level 2 Shutdown is activated by the following causes: • High high level alarm (91-LAHH-1504) in Acid Gas Amine Absorber bottom (9103-C-11) • High high level alarm (91-LAHH-1509) in Amine Regenerator bottom (9103-C-12) • Low low flow alarm (91-FALL-1515) in Lean Amine Pumps (9103-P-13A/B) discharge • Incinerator shutdown signal (91-XS-1186) from Incinerator UCP • Unit-91 (SRU+AGEU+TGTU) shutdown activation by pushbutton 91-HS-1011 • Total power failure signal (65-XS-1024) • Instrument air pressure low low (2oo3) alarm 65-PALL-1003 • Steam failure signal 65-XS-1021 • Existing SRU shutdown signal 65-XA-1001 • Steam generator package shutdown signal 68-XS-1580/68-XS-1680/68-XS-1780 • Instrument air pressure 2oo3 low low alarm (68-PALL-1312A/B/C) Following are the effects of ESD Level 2 Shutdowns in TGTU section: • Combustion air block valve 91-XV-1306 to RGG closes • Fuel gas block valve 91-XV-1303 to RGG closes EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 426 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Fuel gas vent valve 91-XV-1308 to RGG opens • Fuel gas block valve 91-XV-1304 to RGG closes • Steam block valve 91-XV-1305 to RGG closes • Nitrogen purge block valve 91-XV-1307 to RGG opens • Nitrogen purge block valve 91-XV-1301 to RGG opens • Instrument air purge block valve 91-XV-1302 to RGG closes • De-super heater Circulation Pump 9102-P-11A/B trip • Cooling Water Circulation Pump 9102-P-12A/B trip • Combustion Air Blowers 9102-K-11A/B is trip • Contact Condenser Cooler Fans trip • Tail gas bypass block valve 91-XV-1331 to Incinerator opens • Tail gas block valve 91-XV-1332 to Contact Condenser closes • Sour Water Stripper 6922-C-01 overhead block valve 69 XV 1313 closes 11.2.3.4 ESD–Level 3 Shutdown in TGTU System Following are the causes which initiates ESD-3 shutdown in TGTU: • Activation of RGG burner manual shutdown pushbutton 91-HS-1336 at NGL-3 CCR • Activation of RGG burner manual shutdown pushbutton 91-HS-1404 at local • RGG burner flame detection failure alarm 91-BALL-1304 • Combustion air flow to RGG low low alarm 91-FALL-1309 • Fuel gas pressure to RGG high high alarm 91-PAHH-1303 • Fuel gas pressure to RGG low low alarm 91-PALL-1305 • RGG process outlet gas temperature high high alarm 91-TAHH-1305 • Combustion air to RGG high high pressure alarm 91-PAHH-1341 • Reactor Effluent Cooler level low low alarm 91-LALL-1309 Above mentioned ESD level -3 shutdown causes closes the following valves in TGTU: • Combustion air block valve 91-XV-1306 to RGG burner • Fuel gas block valve 91-XV-1303 to RGG burner • Fuel gas block valve 91-XV-1304 to RGG burner • Steam block valve 91-XV-1305 to RGG burner EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 427 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Instrument air purge block valve 91-XV-1302 to RGG instruments • Tail gas to Contact Condenser valve 91-XV-1332 • Sour Water Stripper Overhead valve69-XV-1313 Above mentioned ESD level-3 shutdown causes opens the following valves in TGTU: • Fuel gas vent valve 91-XV-1308 from RGG • Nitrogen purge block valve 91-XV-1307 to RGG burner • Nitrogen purge block valve 91-XV-1301 to RGG instruments • Tail gas bypass valve 91-XV-1331 to Incinerator Also above mentioned ESD level-3 shutdown causes trips the Combustion Air Blower’s 9102-K-11A/B in TGTU. ESD level-3 is also activated by pressing emergency pushbutton 91-HS-1011 in CCR. Following are the effects of above shutdown in TGTU section: • Combustion air block valve 91-XV-1306 to RGG closes • Fuel gas block valve 91-XV-1303 to RGG closes • Fuel gas vent valve 91-XV-1308 to RGG opens • Fuel gas block valve 91-XV-1304 to RGG closes • Steam block valve 91-XV-1305 to RGG closes • Nitrogen purge block valve 91-XV-1307 to RGG opens • Nitrogen purge block valve 91-XV-1301 to RGG opens • Instrument air purge block valve 91-XV-1302 to RGG closes • De-super heater Circulation Pump 9102-P-11A/B trip • Cooling Water Circulation Pump 9102-P-12A/B trip • Combustion Air Blowers 9102-K-11A/B is trip • Contact Condenser Cooler Fans trip • Tail gas bypass block valve 91-XV-1331 to Incinerator opens • Tail gas block valve 91-XV-1332 to Contact Condenser closes • Sour Water Stripper 6922-C-01 overhead block valve 69 XV-1313 closes • Combustion Air Blowers 9102-K-11A/B trip EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 428 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.2.3.5 ESD–Level 4 Shutdown in TGTU System Following are the ESD-4 shutdowns (equipment wise) in TGTU: Contact Condenser: • Low low level alarm (91-LALL-1306) in de-super heater/contact condenser bottom trips the de-super heater circulation pumps 9102-P-11A/B • De-super heater/contact condenser bottom water circulation low low flow alarm (91-FALL-1306) trips the de-super heater circulation pumps 9102-P-11A/B • Low low level alarm (91-LALL-1304) in De-super Heater/Contact Condenser water draw off tray trips the Cooling Water Circulation Pumps 9102-P-12A/B • Low low cooling water circulation flow alarm (91-FALL-1316) trips the Cooling Water Circulation Pumps 9102-P-12A/B • De-super Heater Condenser Cooler Fans 9102-E-12AA to 9102-E-12BC trips due to high high vibration alarms sensed by their respective cooler vibration probes. Detail list of coolers and vibration alarms are as listed below: Vibration Tag No. Cooler Tag No. 91-VAHH-1301 9102-EM-12AA 91-VAHH-1302 9102-EM-12AB 91-VAHH-1303 9102-EM-12AC 91-VAHH-1504 9102-EM-12BA 91-VAHH-1307 9102-EM-12BB 91-VAHH-1308 9102-EM-12BC RGG (9102-F-11) Combustion Blower Combustion air blower 9102-K-11A trips due to the following causes: Tag No. Description 91-VAHH-1457 High high radial vibration alarm 91-ZAHH-1451 High high axial vibration alarm 91-VAHH-1451 High high vibration alarm in motor bearing DE side 91-VAHH-1456 High high vibration alarm in motor bearing NDE side 91-TAHH-1451 High high temperature alarm in compressor bearing 91-TAHH-1452 High high temperature alarm in bull gear bearing 91-PALL-1459 Low low lube oil pressure alarm 91-TAHH-1459 High high lube oil temperature alarm 91-PALL-1460 Low low seal air pressure alarm EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 429 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Tag No. Description 91-TAHH-1453 High high discharge air temperature alarm 91-HS-1453 Emergency stop pushbutton 91-TAHH-1460 High high lube oil return line temperature alarm 91-PDAHH-1461 High high differential pressure alarm 91-TAHH-1473 High high lube oil reservoir temperature alarm 91-VAHH-1458 High high radial vibration alarm 91-TAHH-1457 High high temperature alarm in thrust bearing 91-VAHH-1454 High high vibration alarm in compressor lube oil cooler fan-1 91-VAHH-1455 High high vibration alarm in compressor lube oil cooler fan-1 91-TAHH-1471 High high temperature alarm in motor DE bearing 91-TAHH-1472 High high temperature alarm in blower motor NDE bearing Combustion Air Blower 9102-K-11B trips due to the following causes: Tag No. Description 91-VAHH-1717 High high radial vibration alarm 91-ZAHH-1711 High high axial vibration alarm 91-VAHH-1711 High high vibration alarm in motor bearing DE side 91-VAHH-1716 High high vibration alarm in motor bearing NDE side 91-TAHH-1711 High high temperature alarm in compressor bearing 91-TAHH-1712 High high temperature alarm in bull gear bearing 91-PALL-1719 Low low lube oil pressure alarm 91-TAHH-1459 High high lube oil temperature alarm 91-PALL-1720 Low low seal air pressure alarm 91-TAHH-1713 High high discharge air temperature alarm 91-HS-1713 Emergency stop pushbutton 91-TAHH-1720 High high lube oil return line temperature alarm 91-PDAHH-1721 High high differential pressure alarm 91-TAHH-1733 High high lube oil reservoir temperature alarm 91-VAHH-1716 High high radial vibration alarm 91-TAHH-1717 High high temperature alarm in thrust bearing 91-VAHH-1714 High high vibration alarm in compressor lube oil cooler fan-1 91-VAHH-1715 High high vibration alarm in compressor lube oil cooler fan-1 91-TAHH-1731 High high temperature alarm in motor DE bearing 91-TAHH-1732 High high temperature alarm in blower motor NDE bearing EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 430 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.2.4 Incinerator 11.2.4.1 ESD Level 0 Shutdown in Incinerator system ESD level-0 activated by pressing emergency pushbutton 65-HS-4001 in CCR, directly trips the Incinerator through UCP. 11.2.4.2 ESD Level 1 Shutdown in Incinerator system ESD level 1 shutdown is activated on the following causes: • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4) • Fire detection alarm (68-XS-02-1801) from Utility area (LER-6) • Fire detection alarm (68-XS-03-1801) from Utility Boiler area (LER-6) • Fire detection alarm (66-XS-01-1801) from New Substation area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from Utility area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from Utility boiler area (LER-6) • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from New Substation area • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR All the above mentioned ESD Level-1 causes directly trips the Incinerator through UCP. 11.2.4.3 ESD Level 2 Shutdown in Incinerator system ESD Level 2 Shutdown is activated by the following causes: • Total power failure signal (65-XS-1024) • Instrument air pressure low low (2oo3) alarm 65-PALL-1003 • Instrument air pressure 2oo3 low low alarm (68-PALL-1312A/B/C) • Activation of ESD-2 shutdown pushbutton 61-HS-006 in CCR All the above mentioned ESD Level-2 causes directly trips the Incinerator through UCP. Also incinerator is tripped due to the activation of Incinerator manual shutdown pushbutton 91-HS-1169 in CCR. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 431 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.2.4.4 Incinerator Emergency Shutdown from UCP UCP checks all trip and alarm condition for healthy status before start-up and during operation. Alarm conditions are flagged on display of UCP but the Incinerator remains running. Trip conditions initiate a shutdown and a reset is required before the unit is available. Following are the causes that initiates the Incinerator trip action in UCP: • Remote ESD signal 91-XS-1185 • Local ESD (PB on LCP) 91-HS-1167 • Combustion Air flow Low low alarm 91-FALL-1156B • Fuel gas to burner pressure Low low alarm 91-PALL-1155 • Fuel gas to burner pressure Low low alarm 91-PALL-1156 • Fuel gas to burner pressure High high alarm 91-PAHH-1156 • Flame fail (2oo3) alarm 91-BSLL-1155 • Incinerator Temperature high high alarm 91-TAHH-1160 Following are the effects of trips in Incinerator: • Fuel gas control valve 91-FV-1155 at low fire position • Fuel gas upstream block valve (91-XV-1155) in close position • Fuel gas vent valve (91-XV-1156) in open position • Fuel gas downstream block valve (91-XV-1157) in close position • Pilot gas upstream block valve (91-XV-1158) in close position • Pilot gas vent valve (91-XV-1159) in open position • Fuel gas downstream block valve (91-XV-1160) in close position • After 15 minutes air supply valve (91-XV-1161) will close Note: Blower’s 9101-K-12A/B to be stopped manually. Local ESD pushbutton (91-HS-1167) and remote ESD signal (91-XS-1185) shutdown the blowers directly. Also above mentioned causes in UCP initiates ESD Level-2 trip signal to 91-XS-1186 to plant ESD system. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 432 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.3 11.3.1 UTILITIES Steam Generation System 11.3.1.1 ESD Level 0 Shutdown in Steam Generator Package ESD level-0 activated by pressing emergency pushbutton 65-HS-4001 in CCR, directly trips all the running Steam Generation Packages (6848-A02A/B/C) through UCP. 11.3.1.2 ESD Level 1 Shutdown in Steam Generator Package ESD level1 is activated on the following causes: • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4) • Fire detection alarm (68-XS-02-1801) from Utility area (LER-6) • Fire detection alarm (68-XS-03-1801) from Utility boiler area (LER-6) • Fire detection alarm (66-XS-01-1801) from New Substation area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from Utility area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from Utility boiler area (LER-6) • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from New Substation area All the above mentioned ESD Level-1 causes directly trips all the running Steam Generation Packages (6848-A02A/B/C) through UCP. 11.3.1.3 ESD Level 2 Shutdown in Steam Generator Package ESD Level 2 Shutdown is activated by the following causes: • Total power failure signal (65-XS-1024) • Instrument air pressure low low (2oo3) alarm 65-PALL-1003 • Instrument air pressure 2oo3 low low alarm (68-PALL-1312A/B/C) • Activation of ESD level-2 shutdown pushbutton 61-HS-006 • Fuel gas header pressure high high alarm 62-PAHH-1304 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 433 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL All the above mentioned ESD Level-2 causes directly trips all the running Steam Generation Packages (6848-A02A/B/C) through UCP. 11.3.1.4 ESD Level 3 Shutdown in Steam Generator Package • Activation of Manual Shutdown pushbutton 68-HS-1580 from CCR console trips the Steam Generation Package6848-A02A. • Activation of Manual Shutdown pushbutton 68-HS-1680 from CCR console trips the Steam Generation Package6848-A02B. • Activation of Manual Shutdown pushbutton 68-HS-1780 from CCR console trips the Steam Generation Package6848-A02B. • Main LP steam header pressure low low alarm 68-PALL-1303A/B/C and De-aerator level low low alarm 68-LALL-1310 trips all the running Steam Generation Packages (6848-A02A/B/C) through UCP. 11.3.1.5 Steam Generator Package Trip through UCP Causes Emergency trip causes in UCP are given below: Sl. # Description Tag No. 1 Combustion chamber pressure high-high 68-PAHH-1528A/B/C 2 Boiler level low low 68-LALL-1523A/B/C 3 Boiler level high high 68-LAHH-1523A/B/C 4 Saturated steam pressure high-high 68-PAHH-1522A/B/C 5 Upstream burner gas pressure low-low 68-PALL-1525A/B/C 6 Downstream burner gas pressure high-high 68-PAHH-1526A/B/C 7 Combustion air flow low-low 68-FALL-1526B/C/D 8 Natural gas flow High-High 68-FAHH-1525B/C/D 9 Instrument air pressure low-low 68-PALL-1527A/B/C 10 ESD from boiler control panel 68-HS-1523 11 ESD from boiler local control panel 68-HS-1524 12 Emergency shutdown 68-HS-1525 13 Forced draft fan not running 68-ZI-1548 14 Emergency shutdown from ESD 68-XS-1327 If a trip condition is present, an emergency shutdown is performed and burners will not be allowed to restart until the cause is recognized and corrective actions are taken for logic reset. During the ESD trip the following actions are performed: • Close main burner shut-off valve 68-XV-1528 & open vent valve 68 XV-1530 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 434 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Close igniters main shut-off valve 68-XV-1531if the pilot is lighted • Perform a boiler post firing purge Note: only Steam Generation Package 6848-A02A tags are considered. 11.3.2 Boiler Feed Water System Equipment in this ESD Zone is as follows: • Steam Condensates Flash Drum (6834-V-05) • De-aerator Feed Pumps (6834-P-20A/B) • Steam Condensate Coolers (6834-E-02) • BFW De-aerator Package (6834-A-08) • Boiler Feed Water Pumps (6834-P-22A/B/C) • Steam Generation Package (6848-A-02A/B/C) • Boiler Blow Down Pit (6848-T-02) • Drinking Water Pumps (6834-P-23A/B) • BFW Chemical Injection Package (6834-A-09) 11.3.2.1 ESD Level 0 Shutdown in Boiler Feed Water System ESD level-0 is activated only by pressing emergency pushbutton 65-HS-4001 in CCR. Following are the effects of ESD Level 0 Shutdowns in Heating System: • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1302 close • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1303 close • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1304 close • Drinking Water Pumps (68-P-23A/B) trip • DM Water Feed Pumps (68-P-24A/B) trip • De-aerator Feed Pumps (68-P-20A/B) trip • Steam Condensate Coolers trip • Boiler Feed Water Pumps 68-P-22A/B/C trip • De aerator inlet ESD valve 68-XV-1301 close 11.3.2.2 ESD Level 1 Shutdown in Boiler Feed Water System ESD level 1 is activated on the following causes: • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 435 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Fire detection alarm (68-XS-02-1801) from Utility Area (LER-6) • Fire detection alarm (68-XS-03-1801) from Utility Boiler area (LER-6) • Fire detection alarm (66-XS-01-1801) from New Substation area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from Utility area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from Utility boiler area (LER-6) • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from New substation area • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR Following are the effects of ESD Level 1 Shutdowns in Heating System: • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1302 close • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1303 close • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1304 close • DM Water Feed Pumps (68-P-24A/B) trip • De-aerator Feed Pumps (68-P-20AA/B) trip • Steam Condensate Coolers trip • De aerator inlet ESD valve 68-XV-1301 close • Boiler Feed Water Pumps 68-P-22A/B/C trip 11.3.2.3 ESD Level 2 Shutdown in Boiler Feed Water System ESD Level 2 Shutdown is activated by the following causes: • Total power failure signal (65-XS-1024) • Instrument air pressure low low (2oo3) alarm 65-PALL-1003 • Instrument air pressure 2oo3 low low alarm (68-PALL-1312A/B/C) • Activation of ESD level-2 shutdown pushbutton 61-HS-006 • Steam Generation Packages trip (68-XS-1580/68-XS-1680/68-XS-1780) Following are the effects of ESD Level 2 Shutdowns in Heating System: • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1302 close • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1303 close EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 436 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1304 close • DM Water Feed Pumps (68-P-24A/B) trip • De aerator Feed Pumps (68-P-20A/B) trip • Steam Condensate Coolers trip • De aerator inlet ESD valve 68-XV-1301 close • Boiler Feed Water Pumps 68-P-22A/B/C trip 11.3.2.4 ESD Level 3 Shutdown in Boiler Feed Water System 1. Main LP steam header pressure low low alarm 68-PALL-1303A/B/C and de-aerator level low low alarm 68-LALL-1310 causes the following effects in heating system: • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1302 close • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1303 close • Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1304 close • De aerator feed pumps (68-P-20A/B) trip • Steam Condensate Coolers trip • De-aerator inlet ESD valve 68-XV-1301 close • Boiler Feed Water Pumps 68-P-22A/B/C trip 2. Steam Generation Package 6848-A-02A trip signal 68-XS-1580 closes the Boiler 6848-A-02A fuel gas ON/OFF valve 68-XV-1302 3. Steam Generation Package 6848-A-02B trip signal 68-XS-1680 closes the Boiler 6848-A-02B fuel gas ON/OFF valve 68-XV-1303. 4. Steam Generation Package 6848-A-02C trip signal 68-XS-1780 closes the Boiler 6848-A-02C fuel gas ON/OFF valve 68-XV-1304. 11.3.2.5 ESD Level 4 Shutdown in Boiler Feed Water System Following are the ESD-4 shutdowns (equipment wise) in BFW/Steam Generation Packages: Steam Condensate Coolers • High high vibration alarm 68-VAHH-1301 in steam condensate cooler 6834-E-02A trips the steam condensate cooler motor 6834-EM-2A1 • High high vibration alarm 68-VAHH-1302 in steam condensate cooler 6834-E-02A trips the steam condensate cooler motor 6834-EM-2A2 • High high vibration alarm 68-VAHH-1303 in steam condensate cooler (6834-E-02B trips the steam condensate cooler motor 6834-EM-2B1 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 437 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • High high vibration alarm 68-VAHH-1304 in steam condensate cooler 6834-E-02B trips the steam condensate cooler motor 6834-EM-2AB2 • High high vibration alarm 68-VAHH-1305 in steam condensate cooler 6834-E-02C trips the steam condensate cooler motor 6834-EM-2C1 • High high vibration alarm 68-VAHH-1306 in steam condensate cooler 6834-E-02C trips the steam condensate cooler motor 6834-EM-2C. Drinking Water • Low low level alarm 68-LALL-006 in existing Drinking Water Storage Tank 6834-T01A trips the Drinking Water Pumps 6834-P-23A/B. • Low low level alarm 68-LALL-007 in existing Drinking Water Storage Tank 6834-T01B trips the Drinking Water Pumps 6834-P-23A/B. • Low low level alarm 68-LALL-1307 in DMW storage tank 6834-T-08 trips the DMW Water Feed Pumps 6834-P-24A/B. • High high level alarm 68-LAHH-1306 in DMW storage tank 6834-T-08 trips the DMW package. Steam Condensate Flash Drum • Low low level alarm 68-LALL-1309 in Steam Condensate Flash Drum 6834-V-05 trips the De-aerator Water Feed Pumps 6834-P-20A/B. • High high level alarm 68-LAHH-1308 in Steam Condensate Flash Drum 6834-V-05 trips the DMW Water Feed Pumps 6834-P-24A/B. BFW De-aerator Package High high level alarm 68-LAHH-1312 in BFW De-aerator Package 6834-A-08 closes the De-aerator inlet ESD valve 68-XV-1301. 11.3.3 DM water system 11.3.3.1 ESD Level 0 Shutdown in DM water package ESD level-0 is activated by pressing emergency pushbutton 65-HS-4001 in CCR which directly trips the DM water package through UCP. 11.3.3.2 ESD Level 1 Shutdown in DM Water Package ESD level1 is activated on the following causes: • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 438 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Fire detection alarm (68-XS-02-1801) from Utility area (LER-6) • Fire detection alarm (68-XS-03-1801) from Utility boiler area (LER-6) • Fire detection alarm (66-XS-01-1801) from New substation area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from utility area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from utility boiler area (LER-6) • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from New Substation Area All the above mentioned ESD Level-1 causes directly trips the running DM water package through UCP. 11.3.3.3 ESD Level 2 Shutdown in DM Water Package ESD Level 2 Shutdown is activated by the following causes: • Total power failure signal (65-XS-1024) • Instrument air pressure low low (2oo3) alarm 65-PALL-1003 • Instrument air pressure 2oo3 low low alarm (68-PALL-1312A/B/C) • Activation of ESD level-2 shutdown pushbutton 61-HS-006 All the above mentioned ESD Level-2 causes directly trips the DM water package through UCP. 11.3.3.4 ESD Level 4 Shutdown in DM Water Package ESD Level 4 Shutdown is activated by the following causes: • DM Water Storage Tank level low low alarm (68-LALL-1307) • DM Water Storage Tank level high high alarm (68-LAHH-1306) All the above mentioned ESD Level-4 causes directly trips the DM Water Package through UCP. 11.3.3.5 DM Water Package Trip through UCP Causes • Low low Level alarm 68-LALL-1825 in Acid Storage Tank 6834-T-16 trips the Acid Dosing Pump 6834-P-35A/B/C in DM water package • Low low Level alarm 68-LALL-1827 in Caustic Storage Tank 6834-T-15 trips the Caustic Dosing Pump 6834-P-34A/B/C in DM water package EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 439 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Low low Level alarm 68-LALL-1830 in Neutralisation Pit 6834-A-01 trips the Neutralisation Pump 6834-P-38A/B in DM water package • Low low Level 68-LALL-1307 in De-mineralized Water Storage Tank 6834 T-08 trips the following in DM water package: • Regeneration Pumps 6834-P-36A/B • Acid Dosing Pumps 6834-P-35A/B • Caustic Dosing Pump 6834-P-34A/B • High Conductivity Concentration 68-AHH-1829 in outlet of De mineralized Water and trip the De mineralized Package 6834-A-07 • High Silica Concentration 68-AHH-1830 in outlet of De mineralized Water trips the De-mineralized Package 6834-A-07 • Recycling Pump 6834-P-37A discharge flow low low alarm 68-FALL-1837 trips the Recycling Pump 6834-P-37A • Recycling Pump 6834-P-37B discharge flow low low alarm 68-FALL-1838 trips the Recycling Pump 6834-P-37B • Regeneration Pump 6834-P-36A/B discharge flow low low alarm 68-FALL-1839 trips the following: 1. Regeneration Pump 6834-P-36A/B 2. Acid Dosing Pump 6834-P-35A/B 3. Caustic Dosing Pump 6834-P-34A/B DM Package flow low low alarm 68-FALL-1830 trips recycling Pump 6834-P-37A/B. 11.3.4 Chemical Injection System Equipment in this ESD Zone is as follows: • Complex Product Tank (6834-T-18) • Complex Product Pumps (6834-P-41A/B) • Oxygen Scavenger Tank (6834-T-17) • Oxygen Scavenger Pumps (6834-P-39A/B) • Corrosion Inhibitor Tank (9103-T-13) • Corrosion Inhibitor Pumps (9103-P-101A/B) • Caustic Injection Tank (9103-T-14) • Caustic Injection Pumps (9103-P-103A/B) • Antifoam Injection Tank (9103-T-12) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 440 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Antifoam Injection Pumps (9103-P-16A/B) • Catalyst Injection Pumps (9101-P-01A/B) 11.3.4.1 ESD Level 0 Shutdown in Chemical Injection System ESD level-0 is activated only by pressing emergency pushbutton 65-HS-4001 in CCR. Following are the effects of ESD Level 0 Shutdowns in chemical injection system: • Complex Product Pumps (6834-P-41A/B) • Complex Product Tank Agitator (6834-M-04) • Oxygen Scavenger Injection Pumps (6834-P-39A/B) • Oxygen Scavenger Product Tank Agitator (6834-M-03) • Corrosion Inhibitor Tank Agitator (9103-M-13) • Corrosion Inhibitor Pumps (9103-P-101A/B) • Caustic Injection Pumps (9103-P-103A/B) • Caustic Injection Tank Agitator (9103-M-14) • Antifoam Injection Pumps (9103-P-16A/B) • Antifoam Injection Tank Agitator (9103-M-12) • Catalyst Injection Pump (9101-P-01A/B) 11.3.4.2 ESD Level 1 Shutdown in Chemical Injection System ESD level1 is activated on the following causes: • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4) • Fire detection alarm (68-XS-02-1801) from utility area (LER-6) • Fire detection alarm (68-XS-03-1801) from utility boiler area (LER-6) • Fire detection alarm (66-XS-01-1801) from new substation area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from utility area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from utility boiler area (LER-6) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 441 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from new substation area Following are the effects of ESD Level 1 Shutdowns in chemical injection system: • Complex Product pumps (6834-P-41A/B) • Complex Product Tank Agitator (6834-M-04) • Oxygen Scavenger Injection Pumps (6834-P-39A/B) • Oxygen Scavenger Product Tank Agitator (6834-M-03) • Corrosion Inhibitor Tank Agitator (9103-M-13) • Corrosion inhibitor Pumps (9103-P-101A/B) • Caustic Injection Pumps (9103-P-103A/B) • Caustic injection Tank Agitator (9103-M-14) • Antifoam injection Pumps (9103-P-16A/B) • Antifoam Injection Tank Agitator (9103-M-12) • Catalyst Injection Pump (9101-P-01A/B) 11.3.4.3 ESD Level 2 Shutdown in Chemical Injection System ESD Level 2 Shutdown is activated by the following causes in chemical injection systems: • Total power failure signal (65-XS-1024) • Instrument air pressure low low (2oo3) alarm 65-PALL-1003 • Instrument air pressure 2oo3 low low alarm (68-PALL-1312A/B/C) • Activation of ESD level-2 shutdown pushbutton 61-HS-006 Following are the effects of ESD Level 2 Shutdowns in Chemical Injection System: • Complex Product Pumps (6834-P-41A/B) • Complex Product Tank Agitator (6834-M-04) • Oxygen Scavenger Injection pumps (6834-P-39A/B) • Oxygen Scavenger Product Tank Agitator (6834-M-03) • Corrosion Inhibitor Tank Agitator (9103-M-13) • Corrosion Inhibitor Pumps (9103-P-101A/B) • Caustic Injection Pumps (9103-P-103A/B) • Caustic Injection Tank Agitator (9103-M-14) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 442 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Antifoam Injection Pumps (9103-P-16A/B) • Antifoam Injection Tank Agitator (9103-M-12) • Catalyst Injection Pump (9101-P-01A/B) 11.3.4.4 ESD–Level 3 Shutdown in Chemical Injection System Following are the ESD-3 shutdowns in Chemical Injection Package: Complex Product Low low level alarm (68-LALL-1316) in Complex Product Tank trips the Complex Product Injection Pumps (6834-P-41A/B) and Complex Product Tank Agitator (6834-M-04) Oxygen Scavenger Low low level alarm (68-LALL-1315) in Oxygen Scavenger Tank 6834-T17 trips the Oxygen Scavenger Injection Pumps (6834-P-39A/B) and Oxygen Scavenger Product Tank Agitator (6834-M-03) Corrosion Inhibitor Low low level alarm (91-LALL-1522) in Corrosion Inhibitor Tank 9103-T-13 trips the Corrosion Inhibitor Pumps (9103-P-101A/B) and Corrosion Inhibitor Tank Agitator (9103-M-13) Caustic Injection Low low level alarm (91-LALL-1524) in Caustic Injection Tank 9103-T-14 trips the Caustic Injection Pumps (9103-P-103A/B) and Caustic Injection Tank Agitator (9103-M-14) Antifoam Injection Low low level alarm (91-LALL-1520) in Antifoam Injection Tank 9103-T-12 trips the Antifoam Injection Pumps (9103-P-16A/B) and Antifoam Injection Tank Agitator (9103-M-12) Catalyst Injection Low low level alarm (91-LALL-1128) in Catalyst Injection Tank 9101-T-901 trips the Antifoam Injection Pumps (9103-P-16A/B) 11.3.4.5 ESD–Level 4 Shutdown in Chemical Injection System Following are the ESD-4 shutdowns (equipment wise) in Chemical Injection Package: Complex Product • Low low level alarm (68-LALL-1316) in complex product tank trips the Complex Product Pumps (6834-P-41A/B) • High high diaphragm pressure alarm (68-PAHH-1326) in Complex Product Injection Pump 6834-P-41A trips the pump EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 443 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • High high diaphragm pressure alarm (68-PAHH-1327) in Complex Product Injection Pump 6834-P-41B trips the pump Oxygen Scavenger • Low low level alarm (68-LALL-1315) in Oxygen Scavenger Tank 6834-T17 trips the Oxygen Scavenger Injection Pumps (6834-P-39A/B) • High high diaphragm pressure alarm (68-PAHH-1324) in Oxygen Scavenger Injection Pump 6834-P-39A trips the pump • High high diaphragm pressure alarm (68-PAHH-1325) in Oxygen Scavenger Injection Pump 6834-P-39B trips the pump Corrosion Inhibitor • Low low level alarm (91-LALL-1522) in Corrosion Inhibitor Tank 9103-T-13 trips the corrosion inhibitor pumps (9103-P-101A/B) • High high diaphragm pressure alarm (91-PAHH-1567) in Corrosion Inhibitor Pump 9103-P-101A trips the pump • High high diaphragm pressure alarm (91-PAHH-1568) in Corrosion Inhibitor Pump 9103-P-101B trips the pump Caustic Injection • Low low level alarm (91-LALL-1524) in Caustic Injection Tank 9103-T-14 trips the caustic injection pumps (9103-P-103A/B) • High high diaphragm pressure alarm (91-PAHH-1567) in Caustic Injection Pump 9103-P-103A trips the pump • High high diaphragm pressure alarm (91-PAHH-1568) in Caustic Injection Pump 9103-P-103B trips the pump Antifoam Injection • Low low level alarm (91-LALL-1520) in Antifoam Injection Tank 9103-T-12 trips the Antifoam Injection Pumps (9103-P-16A/B) • High high diaphragm pressure alarm (91-PAHH-1565) in Antifoam Injection Pump (9103-P-16A trips the pump • High high diaphragm pressure alarm (91-PAHH-1566) in Antifoam Injection Pump 9103-P-16B trips the pump Catalyst Injection • Low low level alarm (91-LALL-1128) in Catalyst Injection Tank 9101-T-901 trips the Antifoam Injection Pumps (9103-P-16A/B) • High high diaphragm pressure alarm (91-PAHH-1128 in Catalyst Injection Pump (9103-P-16A) trips the pump EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 444 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • 11.3.5 High high diaphragm pressure alarm (91-PAHH-1130) Catalyst Injection Pump (9103-P-16B) trips the pump Electro Chlorination System Electro Chlorination System UCP trip If an emergency Shutdown is commenced then the immediate shutdown of the complete package takes place, without a run on time for electrolyser flushing and tank venting. Causes responsible for emergency shutdown are tabulated below: Sl. # 11.3.6 Tag No. Description 1 69-HS-1451 Emergency stop in UCP 2 69-HS-1452 Emergency stop in ECP skid 3 69-HS-1453 Emergency stop in ECP skid 4 69-XS-1336 Sea cooling water pump (6932-P-04A/B) trip 5 66-GF-02-1801 Hydrogen gas high-high alarm 6 66-GF-02-1801 Hydrogen gas high-high alarm Sea Cooling Water System Equipment in this ESD Zone is as follows: • Sea Cooling Water Pumps (6932-P-04A/B) • Sea Cooling Water Filters (6932-S-02A/B) • Electro Chlorination Package (6932-A-05) • Biocide Injection Package (6932-A-06) • Scale Inhibitor Package (6932-A-07) • Local Chemical Drain Pit (6932-T-01) ESD–Level 4 shutdown in Sea Cooling Water System Following are the ESD-4 shutdowns (equipment wise) in Sea Cooling Water System: • High high vibration alarm (69-VSHH-1301) in Sea Cooling water Pump 6932-P04A trips the sea cooling water pump 6932-P-04A • High high vibration alarm (69-VSHH-1302) in Sea Cooling Water Pump 6932-P04B trips the sea cooling water pump 6932-P-04B Sea Cooling Water Pumps 6932-P-04A/B trip signals (69-XZA-1311/69-XZA-1322) trips the following packages: • Electro chlorination Package (6932-A-05) EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 445 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.3.7 • Biocide Injection Package (6932-A-06) • Scale Inhibitor Package (6932-A-07) Fuel Gas System 11.3.7.1 ESD Level 0 Shutdown in Fuel Gas System ESD level-0 is activated only by pressing emergency pushbutton 65-HS-4001 in CCR. Following are the effects of ESD Level 0 Shutdowns in Fuel Gas System: • Fuel gas from 1st Stage Booster Compressor ON/OFF valve 62-XV-1301 close • Fuel gas from 6103-K-01A/B ON/OFF valve 62-XV-1302 close • Fuel gas from 30” existing main line inlet ON/OFF valve 62-XV-1303 close 11.3.7.2 ESD Level 1 Shutdown in Fuel Gas System ESD level1 is activated on the following causes: • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4) • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4) • Fire detection alarm (68-XS-02-1801) from utility area (LER-6) • Fire detection alarm (68-XS-03-1801) from utility boiler area (LER-6) • Fire detection alarm (66-XS-01-1801) from new substation area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from utility area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from utility boiler area (LER-6) • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from new substation Following are the effects of ESD Level 1 Shutdowns in fuel gas system: • Fuel gas from 1st Stage Booster Compressor ON/OFF valve 62-XV-1301 close • Fuel gas from 6103-K-01A/B ON/OFF valve 62-XV-1302 close • Fuel gas from 30” existing main line inlet ON/OFF valve 62-XV-1303 close EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 446 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.3.7.3 ESD Level 2 Shutdown in Fuel gas system ESD level2 is activated by high high fuel gas header pressure alarm 62-PAHH-1304 and following are the effects of level-2 shutdown: 11.3.8 • Fuel gas from 1st Stage Booster Compressor ON/OFF valve 62-XV-1301 close • Fuel gas from 6103-K-01A/B ON/OFF valve 62-XV-1302 close • Fuel gas from 30” existing main line inlet ON/OFF valve 62-XV-1303 close Effluent Waste Water System Equipment in this ESD Zone is as follows: • Waste Water Degasser (6922-V-07) • Sour Water Filter (6922-S-06) • Sour/stripped Water Exchanger (6922-E-01) • Stripped Water Cooler (6922-E-02) • Sour water Stripper (6922-C-01) • Sour water Stripper Re-boiler (6922-E-04) • Stripper Overheads Cooler (6922-E-03) • Re-boiler Condensate Drums (6922-V-09) • De-super Heater (6922-X-01) • Waste Water Degasser Pumps (6922-P-08A/B) • Stripped Water Pumps (6922-P-10A/B) • Stripped Overhead Circulation Pumps (6922-P-11A/B) 11.3.8.1 ESD-Level 0 Shutdown in Effluent Waste Water System ESD level-0 is activated (cause) only by pressing emergency pushbutton 65-HS-4001 in CCR. Following are the effects of ESD Level 0 Shutdown in Effluent Waste Water System: • Waste Water Degasser Pump (6922-P-08A/B) trip • Stripper Overhead Circulation Pumps (6922-P-11A/B) trip • Stripper Overhead Cooler Fan motor (69-EM-03AA/AB) trip • Stripped Water Pumps (6922-P-10A/B) trip • Stripper Water Cooler Fan motor (69-EM-02AA/AB) trip • 6922-V-07 inlet ON/OFF valve 69-XV-1312 close EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 447 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Stripper overhead ON/OFF valve 69-XV-1313 close • LP steam supply ON/OFF valve 69-XV-1314 close • LP fuel gas supply ON/OFF valve 69-XV-1315 close • 6922-V-07 outlet ON/OFF valve 69-XV-1316 close • 6922-C-01 outlet ON/OFF valve 69-XV-1339 close • Sour water to Waste Water Degasser ON/OFF valve 91-XV-1575 close 11.3.8.2 ESD-Level 1 Shutdown in Effluent Waste Water System Following are the causes of ESD level1 shutdown: • Fire detection alarm (91-XS-01-1801) from AGEU/TGTU unit (LER-4). • Fire detection alarm (91-XS-02-1801) from Incinerator area (LER-4). • Fire detection alarm (68-XS-02-1801) from utility area (LER-6) • Fire detection alarm (68-XS-03-1801) from utility boiler area (LER-6) • Fire detection alarm (66-XS-01-1801) from new substation area • Fire detection alarm (66-XS-03-1801) from LER-6 • Flammable gas detection alarm (91-XS-01-1802) from AGEU/TGTU unit (LER-4) • Flammable gas detection alarm (91-XS-02-1802) Incinerator area (LER-4) • Flammable gas detection alarm (68-XS-02-1802) from utility area (LER-6) • Flammable gas detection alarm (68-XS-03-1802) from utility boiler area (LER-6) • Flammable gas detection alarm (66-XS-03-1802) from LER-6 • Flammable gas detection alarm (66-XS-01-1802) from new substation area • Activation of ESD Level-1 shutdown pushbutton 65-HS-001 in CCR Following are the effects of ESD Level 1 Shutdown in effluent waste water system: • Waste Water Degasser pump (6922-P-08A/B) trip • Stripper Overhead Circulation Pumps (6922-P-11A/B) trip • Stripper Overhead Cooler Fan motor (69-EM-03AA/AB) trip • Stripped Water Pumps (6922-P-10A/B) trip • Stripper Water Cooler Fan motor (69-EM-02AA/AB) trip • 6922-V-07 inlet ON/OFF valve 69-XV-1312 close • Stripper overhead ON/OFF valve 69-XV-1313 close • LP steam supply ON/OFF valve 69-XV-1314 close EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 448 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • LP fuel gas supply ON/OFF valve 69-XV-1315 close • 6922-V-07 outlet ON/OFF valve 69-XV-1316 close • 6922-C-01 outlet ON/OFF valve 69-XV-1339 close • Sour water to Waste Water Degasser ON/OFF valve 91-XV-1575 close. 11.3.8.3 ESD Level 2 Shutdown in Effluent Waste Water System ESD Level 2 Shutdown is activated by the following causes: • High high level alarm 91-LAHH-1504 in Acid Gas Amine Absorber bottom 9103-C-11 • High high level alarm 91-LAHH-1509 in Amine Regenerator bottom 9103-C-12 • Low low flow alarm 91-FALL-1515 in Lean Amine Pumps 9103-P-13A/B discharge • Incinerator shutdown signal 91-XS-1186 from Incinerator UCP • Unit -91 general shutdown activation by pushbutton 91-HS-1011 • Total power failure signal (65-XS-1024) • Instrument air pressure low low (2oo3) alarm 65-PALL-1003 • Steam failure signal 65-XS-1021 • Existing SRU shutdown signal 65-XA-1001 • De-aerator drum level low low signal 68-XS-1310 • Steam Generator Package shutdown signal 68-XS-1580/68-XS-1680/68-XS-1780 • Fuel gas header pressure high high alarm 62-PAHH-1304 • Instrument air pressure 2oo3 low low alarm 68-PALL-1312A/B/C Following are the effects of ESD Level 2 Shutdown in effluent waste water system: • Waste Water Degasser Pump 6922-P-08A/B trip • Stripper Overhead Circulation Pumps 6922-P-11A/B trip • Stripper Overhead Cooler Fan motor 69-EM-03AA/AB trip • Stripped Water Pumps 6922-P-10A/B trip • Stripper Water Cooler Fan motor 69-EM-02AA/AB trip • 6922-V-07 inlet ON/OFF valve 69-XV-1312 close • Stripper overhead ON/OFF valve 69-XV-1313 close • LP steam supply ON/OFF valve 69-XV-1314 close • LP fuel gas supply ON/OFF valve 69-XV-1315 close EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 449 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • 6922-V-07 outlet ON/OFF valve 69-XV-1316 close • 6922-C-01 outlet ON/OFF valve 69-XV-1339 close • Sour water to Waste Water Degasser ON/OFF valve 91-XV-1575 close 11.3.8.4 ESD–Level 4 Shutdown in Effluent Waste Water System Following are the ESD-4 shutdowns (equipment wise) in effluent waste water system: Waste Water Degasser • Low low level alarm 69-LALL-1311 in Waste Water Degasser 6922-V-07 trips the Waste Water Degasser Pumps (6922-P-08A/B) • High high level alarm 69-LAHH-1311 in Waste Water Degasser 6922-V-07 closes the waste water degasser inlet valve 69-XV-1312, LP fuel gas supply valve 69-XV-1315 and sour water to Waste Water Degasser valve 91-XV-1575. • High high pressure alarm 69-PAHH-1311 in Waste Water Degasser 6922-V-07 Sour Water Stripper • Low low level alarm 69-LALL-1315 in Sour Water Stripper 6922-C-01 trips the Stripper overhead Circulation Pumps 6922-P-11A/B • Low low level alarm 69-LALL-1316 in Sour Water Stripper 6922-C-01 bottom section trips the Stripper Water Pumps (6922-P-10A/B) and closes the Sour Water Stripper outlet ON/OFF valve 69-XV-1339 • High high level alarm 69-LAHH-1316 in Sour Water Stripper 6922-C-01 bottom section trips Waste Water Degasser Pumps 6922-P-08A/B and closes the 6922-V-07 outlet ON/OFF valve 69-XV-1316 Stripper Overheads Cooler • High high vibration alarm 69-VSHH-1304 in Stripper Overheads Cooler Fan 6922-E-03AA trips the Stripper Overheads Cooler Fan motor 69-EM-03AA • High high vibration alarm 69-VSHH-1303 in Stripper Overheads Cooler Fan 6922-E-03AB trips the Stripper Overheads Cooler Fan motor 69-EM-03AB • High high vibration alarm 69-VSHH-1305 in Stripper Overheads Cooler Fan 6922-E-02AA trips the Stripper Overheads Cooler Fan motor 69-EM-02AA • High high vibration alarm 69-VSHH-1306 in Stripper Overheads Cooler Fan 6922-E-02AB trips the Stripper Overheads Cooler Fan motor 69-EM-02AB • TGTU shutdown signal 91-XS-1335 closes the Stripper overhead ON/OFF valve 69-XV-1313. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 450 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.3.9 Instrument Air Compressors 11.3.9.1 ESD Level 0 Shutdown in Instrument Air Compressor (6837-K-02A/B) ESD level-0 is activated (cause) only by pressing emergency pushbutton 65-HS-4001 in CCR which trips both the instrument air packages in UCP through the signal 68-XS-1424. 11.3.9.2 Emergency Shutdown from UCP UCP checks all trip and alarm condition for healthy status before start-up and during operation. Alarm conditions are flagged on display of UCP but the compressor remains running. Trip conditions initiate a compressor shutdown and a reset is required before the unit is available. Following causes initiates the Compressor trip in UCP: 11.4 • Compressor outlet pressure high-high (68-PT-1406) • Compressor air inlet pressure low-low (68-PDT-1401) • Compressor oil pressure low-low (68-PT-1402) • Compressor oil filter DP high-high (68-PDT-1403) • LP stage outlet temperature high-high (68-TT-1401) • Compressor oil temperature high-high (68-TT-1402) • LP stage inlet temperature high-high (68-TT-1403) • Compressor outlet temperature high-high (68-TT-1405) • Over load relays of main motor, inter external after cooler motors • Main motor winding temperatures high-high • Emergency stop at LCP (68-HS-1401) UTILITY FAILURE While every emergency situation must be handled individually, depending upon the existing conditions when the emergency originates. The following recommended procedures provide sequences of major steps which must be taken for the most likely emergency situations. The extent to which the plant has to be shut down depends on the specific emergency. In any emergency, determine the extent of the emergency condition, and decide how to cope with it. Then proceed with one of the following actions as warranted by the emergency: • Handle the emergency as a localized condition without shutting down the rest of the plant. For example, in case of a faulty control valve. Block in and bypass the malfunctioning item until repairs can be made. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 451 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Shut down the unit using the normal shutdown procedure described in Section 10.2. • Shut down the unit using the emergency procedures given below for a specific emergency. 11.4.1 LP Steam Failure Consequence Generally, steam failure is for long duration. Due to loss of LP steam, the stripping of the amine solution in Amine Regenerator, Reducing Gas Generator, BFW Preheater 9101-E-08, Sulphur Degassing Pit 9101-T-01B, Sour Water Stripper Reboiler and Steam tracing of fuel gas lines are affected. The lack of steam to AGEU Regenerator Reboiler produce off spec gas to Sulphur Recovery Unit, it affects the sulphur quality which is produced by Sulphur Recovery Unit. So, the off spec gas is lined up to acid gas flare. When the temperature reaches below Sulphur melting temperature, solid formation occurs inside Sulphur transfer lines. Hence, the SRU unit shutdown is necessary until steam flow reaches normal flow of plant running. Action • Shutdown AGEU, SRU and TGTU unit due as the LP steam is not available for Reboilers, Preheating and heat tracing. • Isolate sulphur transfer lines and drain all the sulphur to collection area. 11.4.2 Sea Cooling Water Failure Consequence • In the event of Sea Cooling Water failure, there is no cooling water supply to coolers and condensers. • AGEU Acid Gas Coolers 9103-E-101A/B, Regenerator Condenser Trim Cooler 9103-E-16, Lean Amine Trim Cooler 9103-E-15, Contact Condenser Trim Cooler 9102-E-13A/B process gas/liquid temperature rises. Action • Shutdown the AGEU and TGTU unit by initiating ESD level-1 shutdown. • If Sulphur Recovery Unit upstream unit shutdown duration is short-time <24 hrs there is no need to take shutdown of Claus sulphur recovery and Incinerator units. Maintain the Reaction Furnace temperature and maintain the Incinerator temperature with the help of fuel gas firing. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 452 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 11.4.3 Instrument Air Failure Consequence In case, the instrument air supply to SRU upgrade is stopped, all the control valves position is kept on fail safe position as per the position indicated in P&ID. If the instrument air is not immediately restored, the SRU Upgrade units must be shut down. Action Shut down the AGEU, SRU, TGTU and Incinerator units as instrument air supply to SRU is not available for operating control valves and ESD valves. 11.4.4 Power Failure In case of power failure, all pumps and compressors are stopped due to loss of power. Only UPS power is available for DCS, F&G panel and emergency light. Generally, the power failure affects all the units. Consequence The plant has to be shut down as: Power failure trips all the pumps, blowers, compressors and air cooler fans. Action Shut down all the units of SRU Upgrade facilities due to unavailability of feed for running the plant. 11.4.5 Boiler Feed Water Failure In the general boiler feed water failure, all the Steam Generators, SRU Reaction Furnace Boiler, Reaction Furnace Condensers, 1st Stage Condenser and Reaction Effluent Cooler in TGTU initiates shutdown to respective unit, due to loss of boiler feed water. Consequence The plant has to be shut down as: SRU Upgrade Reaction Furnace Boiler & Last condenser and TGTU unit Reactor Effluent Cooler tubes will be damaged due to loss of boiler feed water. Action Shutdown the AGEU, SRU and TGTU units as the boiler feed water is not available for recovering heat from the above equipment. 11.4.6 Fuel Gas Failure Consequence • Steam Generation from the Boilers is affected EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 453 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Complete burning of Sulphur and hydrocarbon compound are not possible when Incinerator temperature is less than normal operating temperature. • Hydrogenation reaction rate is reduced due to low temperature in RGG. Action Shutdown AGEU, SRU, TGTU and Incinerator units of SRU units as fuel gas is not available. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 454 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION XII MAINTENANCE EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 455 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 12.1 GENERAL Maintenance is an activity which helps to keep the plant and equipments in running condition for a longer period of time. It is the work performed on an equipment, vessel, column or piping to preserve it in as near to its original condition as is practical and to realize its normal life expectancy. Types of Maintenance Maintenance is classified as below: a. Preventive maintenance (PM) Preventive maintenance is a routine maintenance (cleaning, inspection, oiling and retightening) design to retain the healthy condition of equipment and prevent failure through the prevention of deterioration, periodic inspection or equipment condition diagnosis, to measure deterioration. Preventive maintenance (PM) is the practice of maintaining equipment on a regular schedule, based on elapsed time, run-time meter readings, or number of operations. The intent of PM is to “prevent” maintenance problems or failures before they take place by following routine and comprehensive maintenance procedures. The goal is to achieve fewer, shorter, and more predictable outages. b. Shutdown Maintenance Shutdown maintenance consists of those activities that can be carried out only during the shutdown of the plant/equipments. In order to ensure that a process plant continues to run at peak efficiency, it is prudent to do shutdown maintenance for huge sections of the plant at specific intervals. During this shutdown period, the plant is stopped, cleaning and repairing of equipments is carried out and then the plant is started back. The plant has to be carefully and safely shutdown for this activity. For handing over to maintenance the plant has to be depressurised, drained of liquids, purged with nitrogen, steaming out is carried out if necessary, chemicals disposed of safely. Refer section–X for safe shutdown and handing over of the plant for maintenance. 12.2 12.2.1 PREVENTIVE MAINTENANCE Process Regular inspection and maintenance of the rotary equipment pays rich dividends. Potentially hazardous situations can be avoided and costly delays in production can be minimized. QP standard maintenance schedules and procedures shall be followed for the regular maintenance of the mechanical equipment (blowers, pumps, etc.) electrical equipment and instruments. Refer to the vendor O & M manuals for detailed maintenance procedures of package equipment (Instrument Air Compressors, Electrical Equipment, etc.). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 456 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 12.2.1.1 Acid Gas Enrichment Unit a. Centrifugal Pumps Equipment Description Acid Gas KO Drum Return Pump 9103-P-14A/B, Acid Gas Rich Amine Pumps 9103-P-12A/B, Hot Lean Amine Pumps 9103-P-17A/B, Regenerator Reflux Drum Pumps 9103-P-11A/B, Lean Amine Pumps 9103-P-13A/B, Amine Sump Pump 9103-P-15 Activity Area Activity Description Frequency Joints/ Flanges, Mechanical Seal Check all joints/flanges/gaskets for amine/liquid leakage. Report to maintenance any leakage. Operator Rounds Abnormal Noises Pumps Check for unusual noises or noise levels. Report to maintenance. Operator Rounds Strainers/ Filters Differential Pressures. Pump Suction Report to Maintenance for further actions. Operator Rounds Loose Component Checks All Component Check entire skid for loose nuts & bolts. Report to maintenance any abnormality. Operator Rounds Lube Oil Level Checks Pumps Bearings DE & NDE Check the oil levels (Top-up Lube Oil as required) Operator Rounds Excessive Vibration Pumps Check the Pumps for any abnormal vibrations and report to maintenance. Operator Rounds Excessive Bearing Temperature Bearings Check the oil system and inform to maintenance. Operator Rounds Test Run Stand by Pump Ensure readiness for Operation As per QP schedule Coupling Guard Checks Pumps Coupling Check the security of Coupling guards. As per QP schedule Holding Down Bolts Checks Pump Units Check the security of all holdingdown bolts As per QP schedule Pump Units Carry out logging of key parameters of Pump Units required As per QP schedule Leakage Logging EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 457 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL b. Vessels Equipment Description Lean Acid Gas KO Drum 9103-V-14 Regenerator Reflux Drum 9103-V-12 Regenerator Reboiler Condensate Pot 9103-V-13 Amine Sump 9103-V-10 Amine Sump Filter 9103-S-14 Activity Area Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check vessels for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Vessels Carry out logging of key parameters required As per QP schedule c. Filter Equipment Description Lean Amine Filter 9103-S-11 Activated Carbon Filter 9103-S-12 Fines Filter 9103-S-13 Activity Area Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts. Report to maintenance any abnormality. Operator Rounds Filter Cleaning Filter Clean the filter and reinstall as required Dictated by pressure drop Logging Sour Water Filter Carry out logging of key parameters required. As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 458 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL d. Columns Equipment Description Activity Area Acid Gas Amine Absorber 9103-C-11 Amine Regenerator 9103-C-12 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check the columns for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Logging Columns Carry out logging of key parameters required. As per QP schedule e. Heat Exchanger Equipment Description Activity Area Acid Gas Coolers 9103-E-101A/B Regenerator Reboiler 9103-E-13 Lean/Rich Amine Exchangers 9103-E-11A/B Regenerator Condenser Trim Cooler 9103-E-16 Lean Amine Trim Cooler 9103-E-15 Activity Description Frequency Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Heat Exchangers Carry out logging of key parameters required. As per QP schedule Leakage f. Tank Equipment Description Amine Surge Tank 9103-T-11 Activity Area Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for amine leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check the Tank for loose nut & bolts, cable trays and report to maintenance for any abnormality Operator Rounds Logging Tank Carry out logging of Key Parameters required. As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 459 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL g. Air Coolers Equipment Description Activity Area Regenerator Condenser Cooler 9103-E-12 Lean Amine Cooler 9103-E-14 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check air coolers for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Motor Bearing Check lubricant levels, and top up as and when required. Operator Rounds Motor Check for abnormal motor vibrations and report to maintenance Operator Rounds Temperature Motor Check for abnormal motor Temperature and report to maintenance Operator Rounds Logging Air Coolers Carry out logging of key parameters required. As per QP schedule Grease/ Oil Level 12.2.1.2 Sulphur Recovery Unit a. Blower Equipment Description Activity Area Process Air Blowers 9101-K-01A/B Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. During Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. During Operator Rounds Oil Level Lube Oil Tank, Bearings and Gear Box Check the oil levels (Top-up lube oil as and when required.) As per QP schedule Condensate Draining Lube Oil Tank Draining condensed water from the Lube Oil Tank As per QP schedule Lube Oil Circuit Check whether the Lube Oil Filters differential pressure across the oil filters exceed the limit value. If exceeded, inform Maintenance to change the oil filter element. Daily Lube Oil Pressure too Low EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 460 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Activity Abnormal Noise Vibrations Temperature Logging Area Activity Description Frequency Blower Check the blower for abnormal noise. If abnormal, report to maintenance. Operator Rounds Motor Check the motor for abnormal noise. If abnormal, report to maintenance. Operator Rounds Lube oil Cooler Fan/ Motor Check the fan/motor for abnormal noise. If abnormal, report to maintenance. Operator Rounds Blower Check the blower for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Motor Check the motor for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Lube oil Cooler Fan/ Motor Check the fan/motor for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Motor Check for abnormal motor winding temperature. If abnormal, report to maintenance. Operator Rounds Lube oil Cooler Fan Motor Check for abnormal fan motor winding temperature. If abnormal, report to maintenance. Operator Rounds Blower Carry out logging of key parameters of the blower required Operator Rounds b. Vessels Equipment Description Activity Area Acid Gas KO Drum 9101-V-04 HP Condensate Drum 91014-V-06 Final Separator 9101-V-05 Activity Description Frequency Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Vessels Carry out logging of key parameters required As per QP schedule Leakage EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 461 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL c. Pumps Equipment Description Activity Acid Water Pump 9101-P-01A/B, Sulphur Product Pumps 9101-P-10A/B Sulphur Degassing Pumps 9101-P-09A/B Sulphur Tank Pumps 9101-P-15A/B Catalyst Metering Pumps 9101-P-11A/B Sulphur Product Pumps 9101-P-10A/B Sulphur Degassing Pumps 9101-P-09A/B Area Activity Description Joints/Flanges Mechanical Seal Check all joints/flanges/ gaskets for leakage. Report to maintenance any leakage. Operator Rounds Pumps Check for unusual noises or noise levels. Report to maintenance. Operator Rounds Strainers Differential Pressure Pump Suction Check the Differential Pressures, if it is abnormal, report to Maintenance for further actions. Operator Rounds Loose Component Check All Component Check for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Lube Oil Level Checks Pumps Bearings DE & NDE, Motor Bearings DE & NDE. Check the oil levels (Top-up Lube Oil as required) Operator Rounds Excessive Vibration Pumps Check the Pumps for any abnormal vibrations and report to maintenance. Operator Rounds Excessive Bearing Temperature Bearings Check the oil supply system and inform to maintenance. Operator Rounds Test Run Stand by Pump Ensure readiness for Operation As per QP schedule Coupling Guard Checks Pumps Coupling Check the security of Coupling guards. As per QP schedule Holding Down Bolts Checks Pump Units Check the security of all holding-down bolts As per QP schedule Logging Pump Units Carry out logging of key parameters of Pump Units required As per QP schedule Leakage Abnormal Noise Frequency EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 462 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL d. Boiler Equipment Description Reaction Furnace Boiler 9101-E-07 Activity Area Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/ gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Carry out logging of key parameters required. As per QP schedule Loose Component Logging Boiler e. Heat Exchanger Equipment Description Activity Area Process Air Preheater 9101-E-05 Acid Gas Preheater 9101-E-06 Reaction Furnace Condenser 9101-E-01 1st Stage Condenser 9101-E-02 Last Condenser 9101-E-04 BFW Preheater 9101-E-08 Activity Description Frequency Joints/ Flanges Check all joints/flanges/ gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Heat Exchangers Carry out logging of key parameters required. As per QP schedule Leakage EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 463 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL f. Combustion Chamber Reaction Furnace 9101-F-01 1st Stage Auxiliary Burner 9101-F-02 2nd Stage Auxiliary Burner 9101-F-03 Equipment Description Activity Area Activity Description Frequency Joints/Flanges Check all joints/flanges/ gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Reaction Furnace, 1st Stage Auxiliary Burner, 2nd Stage Auxiliary Burner Carry out logging of key parameters required As per QP schedule Leakage g. Reactor Equipment Description Activity Area 1st Stage Converter 9101-V-01 2nd Stage Converter 9101-V-02 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging 1st Stage Converter, 2nd Stage Converter Carry out logging of key parameters required As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 464 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL h. Tank Equipment Description Activity Area Catalyst Tank 9101-T-03/09 Sulphur Degassing Pit 9101-T-01/01B Activity Description Frequency Joints/ Flanges Check all joints/flanges/ gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds Level Tank Monitor the level in Storage Tank. Operator Rounds Leakage 12.2.1.3 Tail Gas Treatment Unit a. Blowers Equipment Description Activity Area Combustion Air Blowers 9102-K-11A/B Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. During Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. During Operator Rounds Oil Level Lube Oil Tank, Bearings and Gear Box Check the oil levels (Top-up lube oil as and when required.) As per QP schedule Condensate Draining Lube Oil Tank Draining condensed water from the Lube Oil Tank As per QP schedule Lube Oil Pressure too Low Lube Oil Circuit Check whether the Lube Oil Filters differential pressure across the oil filters exceed the limit value. If exceeded, inform Maintenance to change the oil filter element. As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 465 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Activity Abnormal Noise Vibrations Area Frequency Blower Check the blower for abnormal noise. If abnormal, report to maintenance. Operator Rounds Motor Check the motor for abnormal noise. If abnormal, report to maintenance. Operator Rounds Lube oil Cooler Fan/ Motor Check the fan/motor for abnormal noise. If abnormal, report to maintenance. Operator Rounds Blower Check the blower for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Motor Check the motor for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Lube oil Cooler Fan/ Motor Check the fan/motor for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Motor Check for abnormal motor winding temperature. If abnormal, report to maintenance. Operator Rounds Lube oil Cooler Fan Motor Check for abnormal fan motor winding temperature. If abnormal, report to maintenance. Operator Rounds Blower Carry out logging of key parameters of the blower required As per QP schedule Temperature Logging Activity Description b. Combustion Chamber Equipment Description Activity Area Reducing Gas Generator 9102-F-11 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/ gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Reducing Gas Generator Carry out logging of key parameters required As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 466 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL c. Reactor Equipment Description Activity Area Hydrogenation Reactor 9102-V-11 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Hydrogenation Reactor Carry out logging of key parameters required As per QP schedule d. Boiler Equipment Description Activity Area Reactor Effluent Cooler 9102-E-11 Activity Description Frequency Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Reactor Effluent Cooler Carry out logging of key parameters required. As per QP schedule Leakage e. Heat Exchanger Equipment Description Activity Area Contact Condenser Trim Cooler 9102-E-13A/B Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays, earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Heat Exchanger Carry out logging of key parameters required. As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 467 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL f. Pumps Equipment Description Activity Area Cooling Water Circulation Pump 9102-P-12A/B Desuperheater Circulation Pumps 9102-P-11A/B Tail Gas Rich Amine Pumps 9102-P-16A/B Activity Description Frequency Leakage Joints/ Flanges Mechanical Seal Check all joints/flanges/gaskets for any leak. Report to maintenance any leakage. Operator Rounds Abnormal Noises Pumps Check for unusual noises or noise levels. Report to maintenance. Operator Rounds Strainers Differential Pressure Pump Suction Check the Differential Pressures, if it is abnormal, report to Maintenance for further actions. Operator Rounds Loose Component Checks All Component Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Lube Oil Level Checks Pumps Bearings DE & NDE, Motor Bearings DE & NDE. Check the oil levels (Top-up Lube Oil as required) Operator Rounds Excessive Vibration Pumps Check the Pumps for any abnormal vibrations and report to maintenance. Operator Rounds Excessive Bearing Temperature Bearings Check the oil supply system and inform to maintenance. Operator Rounds Test Run Stand by Pump Ensure readiness for Operation As per QP schedule Coupling Guard Checks Pumps Coupling Check the security of Coupling guards. As per QP schedule Holding Down Bolts Checks Pump Units Check the security of all holdingdown bolts As per QP schedule Logging Pump Units Carry out logging of key parameters of Pump Units required Once per Shift EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 468 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL g. Air Coolers Equipment Description Activity Area Contact Condenser Cooler 9102-E-12 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Motor Bearing Check lubricant levels, and top up as and when required. Operator Rounds Motor Check for abnormal motor vibrations and report to maintenance Operator Rounds Temperature Motor Check for abnormal motor Temperature and report to maintenance Operator Rounds Logging Air Coolers Carry out logging of key parameters required. As per QP schedule Grease/ Oil Level h. Columns Equipment Description Activity Area Desuperheater/Contact Condenser 9102-C-11 Tail Gas Amine Absorber 9102-C-12 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire unit for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Logging DCC Carry out logging of key parameters required. As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 469 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL i. Filter Equipment Description Activity Area Wash Water Filter 9102-S-15 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Wash Water Filter Carry out logging of key parameters required As per QP schedule 12.2.1.1 Tail Gas Incinerator a. Combustion Chamber Equipment Description Activity Area Leakage Joints/ Flanges Loose Component All Components Logging Incinerator Incinerator 9101-F-14 Activity Description Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Carry out logging of key parameters required Frequency Operator Rounds Operator Rounds As per QP schedule b. Blowers Equipment Description Activity Area Incinerator Air Blowers 9101-K-12A/B Activity Description Frequency Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. During Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. During Operator Rounds Oil Level Bearings Check the oil levels (Top-up lube oil as and when required.) As per QP schedule Leakage EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 470 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Activity Area Frequency Blower Check the blower for abnormal noise. If abnormal, report to maintenance. Operator Rounds Motor Check the motor for abnormal noise. If abnormal, report to maintenance. Operator Rounds Blower Check the blower for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Motor Check the motor for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Temperature Motor Check for abnormal motor winding temperature. If abnormal, report to maintenance. Operator Rounds Logging Blower Carry out logging of key parameters of the blower required Operator Rounds Abnormal Noise Vibrations 12.2.2 Activity Description UTILITIES 12.2.2.1 Plant and Instrument Air Compressor Description Comments Maintenance Frequency Daily Overall Visual Inspection Complete overall visual inspection to be sure all equipment is operating & safety systems are in place. X Leakage Assessment Look for and report any system leakage X Compressor Operation Monitor operation for run time and temperature variance from trended norms X Dryers Dryers should be observed for proper function X Compressor Ventilation Make sure proper ventilation is available for compressor inlet X Condensate Drains Drain condensate from tanks, legs, and/or traps X Operating Temperature Verify operating temperature is per manufacturer specification X Weekly Monthly Annually EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 471 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Description Maintenance Frequency Comments Daily Weekly Pressure Relief Valves Verify all pressure relief valves are functioning properly X Air Consuming Device Check All air consumer devices need to be inspected on a regular basis for leakage X Drain Traps Clean out debris and check operation X Monthly Annually 12.2.2.2 Chemical Injection System The following maintenance procedures are applicable to the all the chemical injection systems listed below. 1. Antifoam Injection Package 9103-A-11 2. Caustic Injection Package 9103-A-13 3. Corrosion Inhibitor Injection Package 9103-A-12 4. Complex Product Injection Package 6834-A-09 5. Oxygen Scavenger Injection Package 6834-A-09 6. Biocide Injection Package 6932-A-06 7. Scale Inhibitor Injection Package 6932-A-07 8. Catalyst Injection Package 9101-A-01 Equipment Description a. Chemical Unloading Pump Activity Area Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire Skid for loose nuts & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 472 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL b. Chemical Storage Tank Activity Area Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds Logging Tank Carry out logging of Key Parameters required. As per QP schedule c. Chemical Storage Tank Agitator (If applicable) Equipment Description Activity Area Chemical Dosing Pumps Activity Description Frequency Oil level Gear Box Check lubricant levels, and top up as and when required. Operator Rounds Vibration Motor Check for abnormal motor Vibrations and report to maintenance Operator Rounds Abnormal Temperature Motor Bearings Check for abnormal motor Bearings temperature and report to maintenance Operator Rounds Loose Component All Components Check agitator Operator Rounds Logging Agitator Carry out logging of key parameters required As per QP schedule d. Chemical Injection Pumps Equipment Description Activity Area Chemical Dosing Pumps Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Oil level Pumps Check lubricant levels, and top up as and when required. Operator Rounds Pump Check pump Vibrations and report to maintenance Operator Rounds Motor Check for abnormal motor Vibrations and report to maintenance Operator Rounds Pump Bearings Check for abnormal Pump Bearings temperature and report to maintenance Operator Rounds Vibration Abnormal Temperature EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 473 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Activity Area Activity Description Frequency Pressure Drop Suction Strainer Check for any choke in Suction Strainer. Strainer to be cleaned periodically. Dictated by Pump Discharge Pressure Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds Logging Pumps Carry out logging of key parameters required As per QP schedule 12.2.2.3 LP Fuel Gas System Equipment Description Activity LP Fuel Gas KO Drum 6236-V-05 Area Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging LP Fuel Gas KO Drum Carry out logging of key parameters required As per QP schedule 12.2.2.4 Waste Water Treatment System a. Vessels Equipment Description Activity Area Waste Water Degasser 6922-V-07 Sour Water Stripper Reboiler 6922-E-04 Reboiler Condensate Drum 6922-V-09 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire unit for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Logging Waste Water Treatment System Carry out logging of key parameters required. As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 474 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL b. Columns Equipment Description Activity Area Sour Water Stripper 6922-C-01 Activity Description Frequency Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire unit for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Logging Sour Water Stripper Carry out logging of key parameters required. As per QP schedule Leakage c. Heat Exchanger Equipment Description Activity Area Sour/Stripped Water Exchanger 6922-E-01 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Sour/ Stripped Water Exchanger Carry out logging of key parameters required. As per QP schedule d. Filter Equipment Description Activity Area Sour Water Filter 6922-S-06 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts. Report to maintenance any abnormality. Operator Rounds Filter Cleaning Filter Clean the filter and reinstall as required Dictated by 69-PDIA-1320 Logging Sour Water Filter Carry out logging of key parameters required. As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 475 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. Pumps Equipment Description Activity Area Waste Water Degasser Pumps 6922-P-08A/B Stripped Water Pumps 6922-P-10A/B Stripper Overheads Circulation Pumps 6922-P-11A/B Activity Description Frequency Leakage Joints/ Flanges Mechanical Seal Check all joints/flanges/gaskets for process flow/oil leakage. Report to maintenance any leakage. Operator Rounds Abnormal Noises Pumps Check for unusual noises or noise levels. Report to maintenance. Operator Rounds Strainers Differential Pressure Pump Suction Check the suction Pressure, if it is abnormal, Change over the pump or report to Maintenance for further actions. Operator Rounds Loose Component Checks All Component Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Lube Oil Level Checks Pumps Bearings DE & NDE Check the oil levels (Top-up Lube Oil as required) Operator Rounds Excessive Vibration Pumps Check the Pumps for any abnormal vibrations and report to maintenance. Operator Rounds Excessive Bearing Temperature Bearings Check the oil supply system and inform to maintenance. Operator Rounds Test Run Stand by Pump Ensure readiness for Operation As per QP schedule Coupling Guard Checks Pumps Coupling Check the security of Coupling guards. As per QP schedule Holding Down Bolts Checks Pumps Check the security of all holdingdown bolts As per QP schedule Logging Pumps Carry out logging of key parameters As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 476 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL f. Air Coolers Equipment Description Activity Area Stripper Overheads Cooler 6922-E-03 Stripped Water Cooler 6922-E-02 Activity Description Frequency Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Motor Bearing Check lubricant levels, and top up as and when required. Operator Rounds Motor Check for abnormal motor vibrations and report to maintenance Operator Rounds Temperature Motor Check for abnormal motor Temperature and report to maintenance Operator Rounds Logging Air Coolers Carry out logging of key parameters required. As per QP schedule Leakage Loose Component Grease/ Oil Level 12.2.2.5 Sea Cooling Water System Equipment Description Activity Leakage Area Joints/ Flanges Mechanical Seal Sea Cooling Water Pumps 6932-P-04A/B Activity Description Check all joints/flanges/gaskets for any leakage. Report to maintenance any leakage. Check for unusual noises or noise levels. Report to maintenance. Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Check the Pumps for any abnormal vibrations and report to maintenance. Frequency Operator Rounds Abnormal Noises Pumps Operator Rounds Loose Component Checks All Component Excessive Vibration Pumps Excessive Bearing Temperature Bearings Check the oil supply system and inform to maintenance. Operator Rounds Test Run Stand by Pump Ensure readiness for Operation As per QP schedule Operator Rounds Operator Rounds EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 477 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Activity Coupling Guard Checks Holding Down Bolts Checks Logging Area Activity Description Frequency Pumps Coupling Check the security of Coupling guards. As per QP schedule Pumps Check the security of all holdingdown bolts As per QP schedule Pumps Carry out logging of key parameters As per QP schedule 12.2.2.6 Electro Chlorination a. Filters Equipment Description Activity Area Auto Backwash Filters 6932-S-03A/B Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts. Report to maintenance any abnormality. Operator Rounds Logging Auto Backwash Filter Carry out logging of key parameters required. As per QP schedule b. Electrolyser Equipment Description Activity Area Electrolyser 6932-G-01A/B Degassing Tank 6932-T-02 Acid Wash Tank 6932-T-03 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Electrolyser/ Degassing Tank Carry out logging of key parameters required As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 478 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL c. Tanks Equipment Description Activity Area Degassing Tank 6932-T-02 Acid Wash Tank 6932-T-03 Activity Description Frequency Leakage Joints/Flang es Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds Logging Tank Carry out logging of Key Parameters required. As per QP schedule d. Blowers Equipment Description Activity Area Hydrogen Dilution Blowers 6932-K-01A/B Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. During Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. During Operator Rounds Blower Check the blower for abnormal noise. If abnormal, report to maintenance. Operator Rounds Motor Check the motor for abnormal noise. If abnormal, report to maintenance. Operator Rounds Blower Check the blower for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Motor Check the motor for abnormal vibrations. If abnormal, report to maintenance. Operator Rounds Temperature Motor Check for abnormal motor winding temperature. If abnormal, report to maintenance. Operator Rounds Logging blower Carry out logging of key parameters of the blower required. Operator Rounds Abnormal Noise Vibrations EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 479 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. Pumps Equipment Description Activity Dosing Pumps 6932-P-05A/B Acid Wash Pump 6932-P-06 Area Activity Description Frequency Leakage Mechanical Seal/Gland/ Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Oil level Pumps Check lubricant level, and top up as and when required. Operator Rounds Pump Check pump Vibration and report to maintenance Operator Rounds Motor Check for abnormal motor Vibration and report to maintenance Operator Rounds Pump Bearings Check for abnormal Pump Bearings temperature and report to maintenance Operator Rounds Pressure Drop Suction Strainer Check for any choke in Suction Strainer. Strainer to be cleaned periodically. Dictated by Pump Discharge Pressure Gauge Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds Logging Water Carry out logging of key parameters required. As per QP schedule Vibration Abnormal Temperature 12.2.2.7 Demineralized Water System a. Pumps Equipment Description Activity Leakage Regeneration Pumps 6834-P-36A/B Recycling Pumps 6834-P-37A/B Neutralisation Pit Pumps 6834-P-38A/B HCl Injection Pumps 6834-P-35A/B/C NaOH Injection Pumps 6834-P-34A/B/C Demineralized Water Feed Pumps 6834-P-24A/B Area Activity Description Mechanical Seal/Gland/ Joints/ Flanges Check all joints/flanges/ gaskets for process flow leakage. Report to maintenance for any leakage. Frequency Operator Rounds EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 480 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Activity Area Activity Description Frequency Pumps Check lubricant level, and top up as and when required. Operator Rounds Pump Check pump Vibration and report to maintenance Operator Rounds Motor Check for abnormal motor Vibration and report to maintenance Operator Rounds Pump Bearings Check for abnormal Pump Bearings temperature and report to maintenance Operator Rounds Pressure Drop Suction Strainer Check for any choke in Suction Strainer. Strainer to be cleaned periodically. Dictated by Pump Discharge Pressure Gauge Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds Logging Pumps Carry out logging of key parameters required. As per QP schedule Oil level Vibration Abnormal Temperature b. Tanks Equipment Description Activity Area Demineralised Water Storage Tank 6834-T-08 HCl Storage Tank 6834-T-16 NaOH Storage Tank 6834-T-15 Neutralisation Pit 6834-A-01 Activity Description Frequency Leakage Joints/ Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds Logging Tank Carry out logging of Key Parameters required. As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 481 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL c. Vessels Equipment Description Activity Cation Exchangers 6834-S-21A/B Anion Exchangers 6834-S-22A/B Area Activity Description Frequency Joints/Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire unit for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Logging Cation Exchangers 6834-V-02A/B, Anion Exchangers 6834-V-03A/B Carry out logging of key parameters required. As per QP schedule Leakage 12.2.2.8 Boiler Feed Water System a. Pumps Equipment Description Activity Area Deaerator Feed Pumps 6834-P-20A/B Boiler Feed Water Pumps 6834-P-22A/B/C Activity Description Frequency Leakage Mechanical Seal/Gland/ Joints/Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Oil level Pumps Check lubricant level, and top up as and when required. Operator Rounds Pump Check pump Vibration and report to maintenance Operator Rounds Motor Check for abnormal motor Vibration and report to maintenance Operator Rounds Pump Bearings Check for abnormal Pump Bearings temperature and report to maintenance Operator Rounds Suction Strainer Check for any choke in Suction Strainer. Strainer to be cleaned periodically. Dictated by Pump Discharge Pressure Gauge Vibration Abnormal Temperature Pressure Drop EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 482 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Activity Area Activity Description Frequency Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing Operator wire. and report to maintenance Rounds for any abnormality Logging Water Carry out logging of key parameters required. b. Vessels Equipment Description Activity Area Leakage Joints/Flanges Loose Component All Components Logging Steam Condensate Flash Drum 6834-V-05, BFW Deaerator Package 6834-A-08 c. As per QP schedule Steam Condensate Flash Drum 6834-V-05 BFW Deaerator Package 6834-A-08 Activity Description Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Check entire unit for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Carry out logging of key parameters required. Frequency Operator Rounds Operator Rounds As per QP schedule Air Coolers Equipment Description Activity Area Leakage Joints/Flanges Loose Component All Components Motor Bearing Grease/ Oil Level Motor Temperature Motor Logging Steam Condensate Cooler Steam Condensate Cooler 6834-E-02 Activity Description Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Check lubricant levels, and top up as and when required. Check for abnormal motor vibrations and report to maintenance Check for abnormal motor Temperature and report to maintenance Carry out logging of key parameters required. Frequency Operator Rounds Operator Rounds Operator Rounds Operator Rounds Operator Rounds As per QP schedule EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 483 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 12.2.2.9 Steam Generation System a. Fans Equipment Description Activity FD Fan 6848-K-02A Flue Gas Recirculation Fan 6848-K-03A Area Leakage Joints/Flanges Loose Component All Components Oil Level Bearings and Gear Box Fan Abnormal Noise Motor Blower Vibrations Motor Temperature Motor Logging Fan b. Activity Description Check all joints/flanges/gaskets for process flow leakage. Report to maintenance any leakage. Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Check the oil levels (Top-up lube oil as and when required) Check the blower for abnormal noise. If abnormal, report to maintenance. Check the motor for abnormal noise. If abnormal, report to maintenance. Check the blower for abnormal vibrations. If abnormal, report to maintenance. Check the motor for abnormal vibrations. If abnormal, report to maintenance. Check for abnormal motor winding temperature. If abnormal, report to maintenance. Carry out logging of key parameters Frequency During Operator Rounds During Operator Rounds Daily Operator Rounds Operator Rounds Operator Rounds Operator Rounds Operator Rounds Each shift Drums Equipment Description Activity Area Steam Drum 6848-V-02A Activity Description Frequency Joints/ Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire unit for loose nuts & bolts, cable trays & earthing wire. Report to maintenance for any abnormality. Operator Rounds Logging Steam Drum 6848-V-02A Carry out logging of key parameters required. As per QP schedule Leakage EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 484 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL c. Combustion Chamber Equipment Description Activity Steam Generation System Area Activity Description Frequency Joints/Flanges Check all joints/flanges/gaskets for any leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire skid for loose nuts & bolts, cable trays & earthing wire. Report to maintenance any abnormality. Operator Rounds Logging Steam Generation System Carry out logging of key parameters required As per QP schedule Leakage d. Phosphate Dosing Package Phosphate Storage Tank Equipment Description Activity Area Phosphate Storage Tank 6848-T-01A Activity Description Frequency Gland/ Joints/Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Operator Rounds Logging Tank Carry out logging of Key Parameters required. As per QP schedule Leakage Phosphate Dosing Pumps Equipment Description Activity Area Phosphate Dosing Pumps 6848-P-01A/02A Activity Description Frequency Leakage Mechanical Seal/Gland/ Joints/Flanges Check all joints/flanges/gaskets for process flow leakage. Report to maintenance for any leakage. Operator Rounds Oil level Pumps Check lubricant levels, and top up as and when required. Operator Rounds Pumps Check pump Vibrations and report to maintenance Operator Rounds Motor Check for abnormal motor Vibrations and report to maintenance Operator Rounds Vibration EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 485 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Activity 12.3 Area Activity Description Loose Component All Components Check entire Skid for loose nut & bolts, cable trays & earthing wire. and report to maintenance for any abnormality Logging Pumps Carry out logging of key parameters required Frequency Operator Rounds As per QP schedule SHUTDOWN MAINTENANCE a. Plant and Instrument Air Compressor & Dryer For detailed Maintenance Procedures, refer vendor “Installation, Operation and Maintenance Manual” 2970-0006-5-26-0002 b. Steam Generation Package 6848-A-02A/B/C For detailed Maintenance Procedures, refer vendor “Installation, Operation and Maintenance Manual” 2970-0025-5-26-0002 c. Electrochlorination Package 6932-A-05 For detailed Maintenance Procedures, refer vendor “Technical Installation, Operating and Maintenance Manual” 2970-0008-5-26-0003 d. Sea Cooling Water Pumps 6932-P-04A/B For detailed Maintenance Procedures, refer vendor “Installation, Operation and Maintenance Manual” 2970-0028-5-26-0002 e. Chemical Injection Package For detailed Maintenance Procedures, refer vendor “Installation, Operation and Maintenance Manual” 2970-0102-5-26-0006 f. Combustion Air Blowers 9102-K-11A/B For detailed Maintenance Procedures, refer vendor “Installation, Operation and Maintenance Manual” 2970-0101-5-00-0004 12.4 CATALYST LOADING & SPECIAL PROCEDURES Catalyst loading has to be carried out for the following reactors: 1. SRU 1st Stage & 2nd Stage Converters 2. Hydrogenation Reactor EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 486 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SRU 1st Stage & 2nd Stage Converters/Hydrogenation Reactor 12.4.1 a. Catalyst loading This operation is carried out taking precautions highlighted hereafter: Note: The catalyst is a sophisticated product and should be handled carefully, avoiding any hazardous loss. • Before loading, it is recommended to check that all reactors are dry, clean and that all internals are in the proper place and installed as recommended in the various drawings and process data sheets • Covers must be installed at the top of each reactor on temporary structures to protect against rain • Loading of catalyst shall not be done during a period of rain or of great level of humidity b. Preliminary operations • When the reaction section drying out is complete and nitrogen has been replaced by air, the reactors can be opened for inspection of the internals. All damaged internal parts must be replaced or repaired • If needed, the reactors will be brushed and vacuum cleaned before catalyst loading starts • Catalyst loading will be interrupted in case of rain or snow, or efficient protection must be set in place c. Equipment and personnel The list below is based on the following assumption: catalyst loading will be carried out with one crane. • One telescopic crane capable of lifting about 3 tons, 5 meters above the reactor upper manhole (see Fig. 33) • One forklift to handle the catalyst drum pallets • Stationary hopper equipped with 8 to 10" nozzles to be installed on the reactor upper manhole (see Fig. 38) • Two mobile hoppers, each having a capacity of about 5 to 6 catalyst drums (see Fig. 37) • One structure (scaffolding and timbers) to unload the drums into the mobile hoppers (see Fig. 35) • One safety harness, rope ladders, portable oxygen analyzer, low voltage lighting, dust masks, air masks, goggles, plastic sheets to protect drums and reactor in case of rain EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 487 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • To serve the above mentioned equipment the following personnel is necessary: • One foreman • One crane operator • One fork lift operator • One team of 4 riggers at ground level for catalyst handling and loading into the mobile hoppers • One team of 6 fitters for vessels opening closing and for catalyst loading, • One sock loading operator inside the reactor. Note: These personnel shall be permanently present during the loading operation. The total number of personnel will be obtained by multiplying by the number of shifts, if the loading takes place on 24 hours basis. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 488 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 33 – Catalyst handling with drums EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 489 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 34 – Catalyst handling with big bags EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 490 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 35 – Filling up the hopper at ground level from drums EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 491 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 36 – Ground level preparation for big bag lifting EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 492 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 37 – Catalyst Loading – Mobile Hopper EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 493 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 38 – Catalyst Loading – Stationary Hopper EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 494 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 39 – Catalyst Loading – Slide Valve EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 495 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Fig. 40 – Sock loading under air EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 496 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL d. Catalyst loading procedure • Check that the quality of the catalyst and the amount available are as specified. • The following guideline for the reactor loading assumes a single catalyst bed. It also assumes that the internals have been, first inspected in position and then dismantled to speed up the loading process. When there is only one catalyst bed, internals (except the bottom collector) would be installed and inspected after the catalyst loading. • Refer to the loading drawing for the various heights of catalyst and alumina layers etc., and to the detail drawings for the installation of the internals. Inside the reactor measures will be taken from the welding line. Manufacturer's vessels measurements are generally shown from tangent lines. • Make the necessary adjustment. Materialize the various levels with chalk marks on the reactor wall. • Before loading catalyst ensure that operators have available wooden boards upon which to stand when inside the reactor, to spread their weight and avoid crushing of catalyst with the feet. Ensure also that the boards are counted into the reactor and from time to time during loading and as they are taken out of the reactor. Boards left in the reactor will interfere with pressure drop and flow distribution. • The reactor to be loaded should be placed under a reverse air flow to remove any dust generated during the loading process, out of the reactor. Ideally, the dust should be collected in bag filters installed at the outlet man-way. • Lift down the required volume of inert support balls, or active supports as appropriate, and build up the bottom layer. Carefully level the surface, before loading catalyst • Start loading the catalyst bed according to the loading diagram. The person inside the reactor shall build a level of catalyst as uniformly as possible • During the catalyst loading a sample shall be taken in each drum/big bag in order to prepare a composite sample of the reactor load. • when the upper level of the catalyst bed is reached stop loading the catalyst and carefully level the surface • Add the layer of ½” or ¾” hold down balls on top of the active catalyst if required. Note: Vendor does recommend loading inert ceramic balls to hold down the active catalyst if no deflector is installed in the vessel, and/or if the active catalyst bed height is lower than 90 cm. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 497 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL If deflector is installed and if the catalyst bed height is comprised in between 0.9 and 1 m, Vendor advises to load ceramic balls, when the height difference in between the deflector and the top of the active catalyst is lower than 1 m. According to what Vendor commonly sees, hold down ceramic balls can be avoided if a deflector is installed and if the active catalyst bed height is larger than 1 m. Loading hold down balls may also be avoided if a deflector is installed and if the active catalyst bed height is comprised in between 0.9 and 1m, providing that the height difference in between the deflector and the top of the active catalyst is larger than 1 m. • Install the inlet distributor and the top flange A loading report must be carefully filled with: • Number of drums or big bags loaded in each layer • Catalyst batch and drum/big bag reference numbers The loading density is checked at the end of the loading. e. Leak test After closure of the reactor and prior to catalyst activation, leak tests will be conducted. f. Catalyst Handling The SRU first and second Claus converters are part filled with alumina and titanium dioxide catalysts, the titanium dioxide catalyst being located in the bottom of the converter with the alumina on top. The titanium dioxide catalyst is supported on the ceramic balls support material. The TGTU hydrogenation reactor contains a special CoMo catalyst which is supported on ceramic balls support material. A layer of ceramic balls material is also located on the top of the catalyst to protect the catalyst from refractory dust and debris that may be carried forward from the upstream SRU. All catalysts and ceramic ball support material will be delivered to site in either one tonne big bags or 220 litre drums. Until the time of loading into a converter/reactor all catalyst should be kept in a covered heated warehouse to ensure no contamination from rain, sand, dust or low temperature damage can occur. 12.4.2 Catalyst Activity & Life Expectancy a. SRU Converters Provided the acid feed gases being processed in the SRU compositions are near to design then the converters catalysts can be expected to operate satisfactorily for a minimum of three years before replacement is necessary. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 498 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Catalyst life can be prolonged by maintaining a low hydrocarbon content in the acid gas feed, by preventing carryover of amine solutions to the SRU, by ensuring that ammonia salts are not being formed in the process, by avoiding emergency shutdown conditions during which the catalyst beds may be exposed to high temperatures caused by burning sulphur, and by operating care to avoid water condensation on the catalyst. The first catalyst bed generally accounts for most of the conversion. Therefore, the life expectancy of the second bed will almost always exceed that of the first. A shift of the primary activity from the first to second bed is a reliable indication that the first bed requires attention. The best measure of a SRU converters catalyst activity is the percentage of H2S conversion to sulphur obtained in normal operation. This activity will decrease over a period of time, depending on the quality of acid gas feed used and the care with which the SRU is operated. Normally a loss of activity will be seen in the first converter with the point of reaction and temperature increase, moving down the catalyst bed. The activity of the catalyst is observed by watching the temperature change across the converter bed. Good activity is observed when a significant temperature increase is seen in the top/upper portion of the catalyst bed. Record the bed temperature differentials at the initial start-up, during, and at the end of a run as a reference for operation of the unit. A permanent decrease in temperature differential usually indicates catalyst deactivation. Normally, this is an accumulation of carbon, sulphates, or other contaminants on the bed. An indication of sulphate formation in the catalyst is by the increased concentrations of COS, CS2 and CO in the treated gas from the upstream amine absorbers. Some catalyst activity may be restored by carrying out the catalyst management procedures. Since catalyst life expectancy cannot be predicted accurately in advance for any given SRU, it is a good practice to maintain a full replacement supply of catalyst for the converters of one SRU in the refinery warehouse, or be able to acquire the catalyst quickly from the catalyst supplier should a replacement charge of catalyst be required. After sufficient data has been accumulated on the catalysts conversion performance, it is generally advisable to replace all or part of the catalyst on a regular time schedule. b. TGTU Hydrogenation Reactor Under normal operations this catalyst is expected to maintain its activity for a minimum of six years. A hydrogen gas concentration of >1.5% is required to ensure conversion of the sulphur compounds in reactors feed gases to hydrogen sulphide. Catalyst life will be prolonged if a hydrogen concentration of approximately 3% is recorded by the amine absorber vent gas outlet analyser. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 499 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Similarly to the SRU converters catalysts the TGTU Hydrogenation Reactor catalyst activity is observed by watching the temperature change across the reactor bed. Good activity is observed when a significant temperature change occurs in the top/upper portion of the catalyst bed. Also records of the catalyst bed temperature differentials should be taken at the initial start-up, during, and at the end of a run as a reference for operation of the unit. Although the Hydrogenation Reactor catalyst is not likely to be fouled and deactivated by contaminants as the SRU converters catalysts may be it is advised to maintain a full replacement supply of catalyst for one TGTU Hydrogenation Reactor in the refinery warehouse or be able to acquire the catalyst quickly from the catalyst supplier should a replacement charge of catalyst be required. Some catalyst activity may be restored by carrying out the catalyst management procedures. 12.4.3 Catalyst Preparation When preparing to inspect and/or replace a SRU or TGTU reactors catalyst the SRU/TGTU must first follow the normal shutdown and sulphur stripping and regeneration procedures. Following the shutdown of the unit no vessel should be entered until it has been cooled and all process gas utility streams to the SRU/TGTU have been isolated. Prior to entry to a converter/reactor the vessel must be tested to determine if it is free of noxious gases. Even when a satisfactory oxygen reading is recorded in the vessel it is advised that persons entering the vessel should be supplied with an air mask and a safety belt and that a safety attendant/standby person is continually stationed outside the vessel to monitor the person(s) in the vessel. a. Catalyst Sampling When a SRU converter or the TGTU hydrogenation reactor is first opened it is advised that samples of the catalysts are taken and sent to the catalyst supplier for analysis. Samples should be taken from various levels in the beds. b. Catalyst Inspection The inspection of the catalyst will determine if part, or the complete, catalyst bed is to be replaced because of catalyst contamination, fusion with other products, loss of granular size or evidence of reduced activity. c. Catalyst Replacement Catalyst replacement alternatives are described in the following sub-sections: d. Top Layer Replacement If the deactivation of the catalyst is caused by fusion or some condition affecting only the top layer, carefully remove this layer, rake and smooth the top of the remaining catalyst bed and replace with new catalyst to the design bed depth. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 500 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL e. Full Bed Replacement with Old and New Catalyst If the contamination and deterioration extends deeper into the catalyst bed it is advised to remove and screen the remainder of the catalyst and then recharge the usable portion. If the entire catalyst bed is to be removed proceed as follows: If installed, carefully remove any top layer of ceramic balls followed by the catalyst and catalyst support layer ceramic balls. Screen the ceramic balls. Examine the process gas outlet pipe and screens. Replace the catalyst support ceramic balls in the bottom of the vessel. Screen the catalyst that was removed, discard the fines and reserve the usable portion. Add enough new catalyst to compensate for the amount discarded and spread this in an even layer over the catalyst support ceramic balls. Add the screened used catalyst to bring the bed to full depth. If required add the top layer of ceramic balls. f. Full Bed Replacement with New Catalyst If inspection shows the whole catalyst bed is of questionable value, replace all the old catalyst with new. Follow the applicable steps for a full bed replacement above. Inspect the physical condition of the new catalyst to determine if screening is required to remove fines. Do not screen unless necessary and avoid excessive handling. g. Catalyst Unloading Methods A gravity method or a vacuum method may be used to remove catalyst from a converter/reactor. If the catalyst is to be reused then the gravity method is advised so that a minimum of damage and the production of catalyst fines and dusts are produced during the unloading operation. Unloading is carried out through temporary chutes connected to the converter/reactor side manways with the catalyst collected in clean dry drums or other suitable containers. During the unloading process care should be taken to separate the ceramic balls support material from the catalyst. For the SRU first and second converter care will have to be taken to separate the titanium dioxide catalyst from the alumina catalyst during the unloading operations. If only the top section of catalyst in a converter has to be replaced then this layer is normally removed by hand through the converters top manways; alternatively if care is EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 501 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL taken, then the catalyst may be removed through the converters top manways by means of the vacuum method. If the catalyst is not to be reused then vacuum method is advised as this method minimises the unloading time and does not require the opening of the converters side manways. h. Catalyst Disposal Regenerated alumina catalyst may be disposed of to a land fill site. Titanium dioxide and hydrogenation catalysts should be disposed of via a catalyst reclamation company. At the end of the life of each catalyst it is advised that the supplier is consulted regarding its disposal. 12.4.4 Catalyst Management a. SRU Reactor Catalyst The alumina catalyst in the SRU converters consists of small spheres that have very small pores. The H2S and SO2 gases enter into these pores and emerge as sulphur and water vapour. Some sulphur in the liquid phase may collect in the catalyst and over a period of time will lower the sulphur conversion efficiency making it necessary for the catalyst beds to be given a rejuvenation or heat soak. A loss of catalyst activity is seen by the temperature increase and start of the exothermic reaction moving further down the converters catalyst beds. To improve converters catalyst activity a rejuvenation of the catalyst is carried out with the SRU and TGTU in normal operation processing acid feed gas. If no improvement in conversion is seen, a sulphur stripping procedure will then be necessary. A sulphur stripping procedure may also be required if the catalyst is contaminated by carbon laydown from hydrocarbons carried in the unit’s acid feed gas or because of contamination by liquid carryover with the acid gas from the Amine Regenerator which is so severe that a SRU shutdown is required and the converters opened to replace the contaminated catalyst. Prior to sulphur stripping, the catalyst beds and the SRU will contain potentially hazardous and contaminating materials such as H2S, SO2, sulphur and other sulphurous compounds. The object of the sulphur stripping exercise is to remove these contaminants under controlled conditions. At the conclusion of the sulphur stripping operations the catalyst should be clean and the plant should be free of harmful gases and deposits. A sulphur stripping operation will also be carried out before the plant is opened for any maintenance work, where there is a possibility of air entering the system, which could cause the ignition of any sulphurous compounds in the catalysts or process gas stream side of the unit. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 502 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Sulphur stripping is carried out with the SRU Reaction Furnace burner operating on fuel gas only, initially at stoichiometric firing conditions. Sulphur stripping should only be carried out for the requirements stated above, since the operation can be potentially hazardous to both catalyst and equipment. b. TGTU Hydrogenation Reactor Catalyst Under normal operations this catalyst is expected to maintain its activity for many years, much longer than the SRU catalysts. A hydrogen gas concentration normally of >1.5% is advised to ensure efficient conversion of the sulphur compounds in reactor’s feed gas to hydrogen sulphide. Catalyst life will be prolonged if a hydrogen concentration of approximately 2-4% is seen by the Tail Gas Amine Absorber outlet vent gas H2 analyser. The activity of the catalyst is observed by watching the temperature change across the reactor bed. Good activity is observed when a significant change occurs in the upper portion of the bed. A decrease in activity will be seen by the point of start of temperature increase moving down the catalyst bed. A permanent decrease in temperature differential usually indicates catalyst deactivation. Normally, this is an accumulation of carbon, sulphates or other contaminants on the catalyst bed. Sulphation of the catalyst will be increased if concentrations of COS, CS2 and CO in the acid feed gas increase. Increasing the Hydrogenation Reactor inlet temperature by a few degrees above normal will help to restore some catalyst activity. Oxidation of the Hydrogenation Reactor catalyst will restore some activity. Oxidation must be carried out prior to the TGTU being opened for maintenance and inspection. Prior to unit restart the catalyst will require sulphiding. 12.4.5 SRU Converter Catalyst Rejuvenation: A catalyst rejuvenation is carried out whilst the SRU and TGTU are in normal operation processing acid gas. The rejuvenation will proceed as follows: • Slowly increase the SRU converters auxiliary burners outlet temperatures as high as possible above normal operating temperatures for the first auxiliary burner, ~260°C, and to ~235°C for the second auxiliary burner. • Hold these temperatures for 24 hours to allow any sulphur contained in the catalyst pores to flow out of the pores. • After 24 hours, still holding the higher than normal auxiliary burners outlet temperatures, go off ratio at the SRU Reaction Furnace to decrease the volume of air to the reaction furnace burner to produce a H2S:SO2 ratio of approx. 5.0:1.0 in the unit's tail gases as indicated by the tail gas analyser. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 503 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Maintain this rich in H2S ratio for 24/36 hours. • Following this hold period return to normal operations with a tail gas H2S:SO2 ratio of 4.0:1.0. • Reduce auxiliary burners outlet temperatures of 230°C and 210°C. • If following a number of rejuvenation exercises, no temperature increase is seen across the converters then a stripping exercise will have to be carried out in an attempt to re-establish catalyst activity. 12.4.6 temperatures to their normal operating SRU Converter Catalyst Stripping To carry out this exercise the TGTU is first taken out of service and the SRU tail gas routed directly to the Incinerator. The procedure for sulphur stripping the SRU converters catalyst may be broken down into three sub-procedures: I. • Hot inert gas sweep • Sulphur stripping • Cool down Hot Inert Gas Sweep A hot inert gas sweep of the SRU converters catalyst will commence as soon as acid gas feed to the Reaction Furnace burner has been stopped and the burner is operating only on fuel gas at slightly sub-stoichiometric firing conditions with LP steam injection to the fuel gas and process air lines to the Reaction Furnace burner. During the hot inert gas sweep note the following: • Monitor the converters temperatures closely and increase the flow of fuel gas if an unexpectedly high temperature, (indicating burning of sulphur compounds), is seen in the converters catalyst beds. • Hold this hot inert gas sweep of the converters catalyst beds for a period that includes four hours after the flow of sulphur is seen to cease from all condensers sulphur seals, before proceeding with a sulphur stripping operation. II. Sulphur Stripping Sulphur stripping will commence immediately following the completion of the hot inert gas sweep of the unit as described above. Sulphur stripping will proceed as follows: • Confirm that the auxiliary burners outlet and converters catalyst bed temperatures are at 230°C and 210°C. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 504 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • With process air and fuel gas controllers in manual operating mode, very slowly increase process air flow to the Reaction Furnace burner by adjustments to process air controller. • Maintain the auxiliary burners temperature outlet controllers in automatic operating mode throughout the sulphur stripping operation set at their normal operating temperatures of 230°C and 210°C. • Every few minutes increase process air flow in very small increments until there is evidence of burning of sulphur compounds within the SRU. Note that the trim air control valve may be used to allow a fine control of excess process air is achieved. • Observe all temperature points across the SRU. • The first sign of the burning of sulphur compounds in the SRU should be seen by a temperature increase in the top layer of catalyst in the first converter. A temperature increase may also be seen in the Reaction Furnace Condenser process gas outlet or 1st Stage Condenser process gas outlet as sulphur compounds in these sections commence burning. • Hold the process air flow at its present flow when a temperature front is seen in the first converter. • Note the flows of fuel gas and process air. • Closely observe the converters catalyst bed temperatures, if temperatures approach 400°C, reduce the amount of process air to the Reaction Furnace burner. Note: Under no circumstances should converter catalyst temperatures exceed 425°C (or other temperature advised by the catalyst supplier). • In the event of a sudden increase in temperature in a converter catalyst bed, immediately increase fuel gas flow to allow the fuel gas to consume any excess oxygen and to stop the temperature rise. This action will ensure a flow of hot combustion gas through the unit at a high flow rate to displace any pockets of gas which contain high oxygen content. • Once the temperature front has passed through the first converter it will move into the second converter. There may be some overlapping of temperature fronts between the first and second converters due to the possibility of channelling of gases through the first converter catalyst. • When the temperature front has moved through the second converter catalyst, over a period of eight hours, gradually reduce the flow of fuel gas to the reaction furnace burner leaving the process air flow unchanged to allow an excess of oxygen to appear in the process gas stream. • Closely observe all temperature points across the unit for any secondary burning of sulphur compounds. If secondary burning is seen, immediately increase fuel gas EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 505 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL flow to the reaction furnace burner to consume the excess oxygen in the process gases and halt the temperature increase in the area of burning. III. Cool Down Cool down will commence immediately after sulphur stripping of the converters catalyst is completed as follows: • Close MS steam control valve to the process air pre-heater. • Start increasing process air flow to the Reaction Furnace burner whilst holding fuel gas flow constant. The Reaction Furnace temperature will slowly fall. • With process air at a fairly high flow, start lowering process temperatures by reducing fuel gas flow to the Reaction Furnace burner. • Start reducing converters catalyst bed temperatures by reducing auxiliary burners outlet temperatures at 50°C/hr. • When <400°C is seen in the Reaction Furnace, stop LP steam injection to the fuel gas and combustion lines to the Reaction Furnace burner and manually isolate. Also close LP steam to the acid gas bypass line to the reaction furnace. • Continue reducing fuel gas flow to the Reaction Furnace burner until the lowest temperature possible is seen on the reaction furnace and converters temperature indicators, ideally ~100°C, then stop fuel gas flow to the Reaction Furnace burner. • Isolate fuel gas to the auxiliary burners. • Continue process air flow through the SRU to further cool the equipment to near blower discharge/ambient temperature. The SRU converter catalyst regeneration procedure is now complete. 12.4.7 TGTU Hydrogenation Reactor Catalyst Oxidation: If the SRU and TGTU are to be opened for inspection and maintenance at the same time then the sulphur stripping of the SRU converters and the oxidation of the TGTU Hydrogenation Reactor may be carried out in the same operation. In this case the oxidation of the Hydrogenation Reactor catalyst would be carried out in series with the sulphur stripping of the SRU converters catalyst as described in Section 12.4.7-I If the TGTU is to be opened for inspection and maintenance independently of the SRU then the TGTU Hydrogenation Reactor oxidation is carried out as a stand alone procedure as described in Section 12.4.7-II I. TGTU Hydrogenation Reactor Catalyst Oxidation – (In series with the SRU converters sulphur stripping operation): Oxidation of the Hydrogenation Reactor in series with the sulphur stripping of the SRU converters will proceed as follows: EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 506 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Confirm that the RGG outlet/Hydrogenation Reactor inlet temperature is at 290°C • Open the Reactor Effluent Cooler 9102-E-11 outlet process gas valve to the Incinerator and close the Reactor Effluent Cooler outlet valve to the Contact Condenser to take the TGTU wet section out of service. • Proceed with the sulphur stripping of the SRU converters catalyst beds as described in section 12.4.6. • When the second SRU converter catalyst bed sulphur stripping is complete, or near complete the excess oxygen in the SRU process air that was used to sulphur strip the SRU converters catalysts will pass through to the TGTU to commence the oxidation of the Hydrogenation Reactor catalyst. Note that there may be some overlapping of sulphur stripping of the third SRU converter and the oxidation of the Hydrogenation Reactor. • Closely observe the Hydrogenation Reactor catalyst temperatures, if temperatures approach 400°C then reduce the amount of process air to the SRU Reaction Furnace burner. Note: Under no circumstances should the Hydrogenation Reactor catalyst temperatures exceed 425°C (or other temperature advised by the catalyst supplier). • When the catalyst oxidation is complete as seen by the temperature front having passed through the Hydrogenation Reactor catalyst bed the fuel gas flow to the SRU Reaction Furnace burner is slowly decreased, leaving the process air flow unchanged so allowing an excess of oxygen in the process gases passing through the SRU converters and TGTU Hydrogenation Reactor. • Maintain close observation of all temperature points across the SRU converters and the TGTU Hydrogenation Reactor for any secondary burning. If secondary burning is seen then increase fuel gas flow to the SRU Reaction Furnace burner to consume the excess oxygen in the process gases and halt the temperature increase in the area of burning. • Following oxidation of the Hydrogenation Reactor hydrogenation section is cooled down with the SRU. • Reduce RGG outlet temperatures at approx. 50°C/hr to cool the Hydrogenation Reactor catalyst. Note that the RGG process air to fuel gas ratio may now be adjusted so that the RGG burner is operating in excess air conditions. • When ~100°C is seen in the Hydrogenation Reactor catalyst, via the shutdown switch, stop the RGG. catalyst, the TGTU EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 507 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Confirm that the action of the shutdown switch has closed or opened the following RGG shutdown valves: • Nitrogen valve to the RGG combustion air line, open (valve will remain open for ~15 minutes) • Nitrogen valve to the RGG instrument nozzles, open • Instrument air to the RGG instrument nozzles, closed • Combustion air valve, closed • Fuel gas, two valves closed and vent valve open • LP steam, closed • After a set time of ~15 minutes, confirm that the nitrogen purge valves to the RGG combustion air line and to the RGG instrument nozzles have closed. • Close manual valves in the RGG combustion air, instrument air, fuel gas and LP steam lines to the RGG. The TGTU Hydrogenation Reactor may now be opened for inspection and maintenance. Note: Complete oxidation of a TGTU Hydrogenation Reactor catalyst and the elimination of all pyrophoric material in the reactor can sometimes be difficult to fully carry out in a catalyst oxidation exercise. Care should therefore be taken when opening a Hydrogenation Reactor as ignition of any pyrophoric material in pockets of sulphided catalyst may result. II. TGTU Hydrogenation Reactor Catalyst Oxidation – (Independent of the SRU converters sulphur stripping operation): In the event that the TGTU is taken out of service independently of the SRU and has to be opened for inspection and maintenance then all sulphur compounds in the Hydrogenation Reactor catalyst must be first removed by regeneration of the catalyst. This is achieved by recycling nitrogen gases around the RGG, Hydrogenation Reactor, Reactor Effluent Cooler and the DCC tower by means of the start-up gas steam ejector and by adjusting the amount of excess air to the RGG burner to burn off all sulphur compounds on the Hydrogenation Reactor catalyst. This procedure should be carried out immediately after the TGTU is shutdown when the Hydrogenation Reactor catalyst is still near its normal operating temperature. Regeneration of the Hydrogenation Reactor catalyst may proceed as follows: • Shutdown the TGTU as described in Section 10.1.1 leaving the DCC top and bottom circulating waters in service and a BFW level in the Reactor Effluent Cooler • Confirm that the SRU tail gas valve to the TGTU is closed • Confirm that the process gas valve from the Reactor Effluent Cooler to the DCC is open EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 508 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Close the DCC process gas outlet valve to the Tail Gas Amine Absorber • Open manual valve in gas recycle line from the DCC outlet process gas line to the RGG inlet line • Set vent gas pressure control valve from the DCC vent gas outlet line to the Incinerator at 0.25 barg • Introduce a flow of nitrogen into the RGG inlet line • Observe the start-up pressure control valve opening to control the excess nitrogen gases to the Incinerator • Open start-up gas steam ejector process gas inlet and outlet manual valves • Open LP steam to the start-up gas steam ejector to start circulating nitrogen gases around the TGTU BSR section. Nitrogen gases will flow through and around the RGG, Hydrogenation Reactor, Reactor Effluent Cooler and DCC with excess gases being vented to the Incinerator via the recycle gas pressure control valve. • Ignite the RGG burner on fuel gas at normal slightly sub-stoichiometric firing conditions and set RGG outlet temperature controller set point at 250ºC. • Open LP steam shutdown valve to the RGG and introduce steam to the RGG fuel gas line to suppress the formation of carbon and soot at stoichiometric firing conditions. Set the steam flow in a ratio of 2:1 (by wt) to fuel gas. Notes: 1. As the Hydrogenation Reactor now contains sulphur compounds the RGG burner must be operated at its normal, slightly sub-soichiometric, firing conditions. 2. If the Hydrogenation Reactor catalyst has cooled then slowly raise temperatures at 50°C/hr to 250ºC. • Slowly adjust the RGG combustion air to fuel gas ratio controller to allow a small excess of combustion air at the RGG burner. • Observe all temperature points across the Hydrogenation Reactor • The first sign of the burning of sulphur compounds in the Hydrogenation Reactor should be seen by a temperature increase in the top layer of catalyst. • Hold the RGG excess combustion air conditions when a temperature front is seen in the Hydrogenation Reactor. Note the flow of combustion air and fuel gas. • Closely observe the Hydrogenation Reactor’s catalyst temperatures, if temperatures approach 400°C, adjust the RGG combustion air to fuel gas ratio controller to reduce the flow of combustion air to the RGG. Note: Under no circumstances should catalyst temperatures exceed 425°C (or other temperature advised by the catalyst supplier). EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 509 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • In the event of a sudden increase in temperature in a reactor catalyst bed, immediately adjust the RGG combustion air to fuel gas ratio controller to stoichiometric firing conditions to stop excess air in the RGG combustion gases Note: This action will ensure a flow of hot recycle gas through the Hydrogenation Reactor at the start-up gas steam ejector flow rate to displace any pockets of gas in the Hydrogenation Reactor which contain high oxygen content. In this case under no circumstance should the start-up gas steam ejector be stopped. • When the temperature front has moved through the Hydrogenation Reactor catalyst, over a period of approx. two hours, gradually adjust the RGG combustion air to fuel gas ratio controller to increase excess air flow and an excess of oxygen to appear in the recycle process gas stream. • Closely observe all temperature points across the Hydrogenation Reactor for any secondary burning of sulphur compounds. If secondary burning is seen, immediately reset the RGG combustion air to fuel gas ratio controller to reduce excess combustion air flow to the RGG to reduce the excess oxygen in the recycle gas and halt the temperature increase in the area of burning within the Hydrogenation Reactor catalyst bed. Proceed to cool down the Hydrogenation Reactor as follows: • Start reducing the RGG outlet temperature controller set point at 50°C/hr to cool the Hydrogenation Reactor • Slowly adjust the RGG combustion air to fuel gas ratio controller to increase excess combustion air flow to the RGG • When the RGG outlet temperature is 200°C, close LP steam to the RGG fuel gas line • Continue reducing RGG outlet temperature controller set point until ~100°C is seen in the hydrogenation reactor catalyst bed • Stop fuel gas to the RGG burner leaving combustion air flow to cool the Hydrogenation Reactor to combustion air temperature • Close nitrogen to the RGG process gas inlet line • Activate the RGG shutdown switch to close all shutdown valves • Confirm that the action of the shutdown switch has closed or opened the following RGG shutdown valves: • Nitrogen valve to the RGG combustion air line, open (valve will remain open for ~15 minutes) • Nitrogen valve to the RGG instrument nozzles, open • Instrument air to the RGG instrument nozzles, closed EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 510 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL • Combustion air valve, closed • Fuel gas, two valves closed and vent valve open • LP steam, closed • Close LP steam to the start-up gas steam ejector • Close process gas inlet valve to and outlet valve from the start-up steam gas ejector • Close BSR section start-up vent gas pressure control valve and manual valve • Observe the Reactor Effluent Cooler steam generator steam side pressure after unit shutdown. When pressure has decreased to <1.0 barg on the steam side of the vessel, open atmospheric vent to prevent a vacuum being formed in the vessel. The TGTU hydrogenation reactor catalyst regeneration procedure is now complete. Note: Complete oxidation of a TGTU hydrogenation reactor catalyst and the elimination of all pyrophoric material in the reactor can sometimes be difficult to fully carry out in a catalyst oxidation exercise. Care should therefore be taken when opening a hydrogenation reactor as ignition of any pyrophoric material and pockets of sulphided catalyst may result. 12.4.8 Hydrogenation Reactor Sulphiding in Series with the SRU The following text is a guide only to the sulphiding of the hydrogenation reactor catalyst. The catalyst manufacturer/supplier should advise the catalyst temperature required at the start of sulphiding operations and the rate of temperature increase and any temperature hold periods etc. during the operation. Prior to the start of sulphiding operations, the SRU reaction furnace burner and the RGG burner will be operating on fuel gas, and SRU tail gases will be routed through the TGTU BSR section. TGTU process gases will be routed to the Incinerator from the outlet of the Reactor Effluent Cooler and will be valve isolated to the contact condenser. Sulphiding operations will proceed as follows: • Confirm that the SRU Reaction Furnace burner is operating on fuel gas at slightly sub-stoichiometric firing conditions. • Confirm that the RGG burner is operating on fuel gas at slightly sub-stoichiometric firing conditions. • Confirm that the Hydrogenation Reactor catalyst bed is fully heated through to a temperature of 200°C. • Using the acid gas sulphiding line from the Regenerator Reflux Drum 9103-V-12 to the Hydrogenation Reactor inlet line, slowly open manual valve at the EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 511 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Hydrogenation Reactor to introduce a small flow of H2S acid gas into the Hydrogenation Reactor. Aim initially for 1% - 2% vol. of H2S in process gases. Notes: 1. The intention is to aim initially for a 1% - 2% vol. of H2S in process gases. 2. The reaction of H2S in the Hydrogenation Reactors catalyst is exothermic. For every 1% vol. of H2S entering the reactor a catalyst temperature increase of approximately 15°C can be expected. • Slowly increase Hydrogenation Reactor inlet temperatures at a rate of approximately 15°C/hr to 290°C whilst keeping the catalyst bed delta temperature <25°C. • If the exothermic reactions produce a catalyst bed delta temperature >25°C then reduce the flow of H2S acid gas into the Hydrogenation Reactor. Note: Under no circumstances should catalyst temperatures be allowed to exceed 425°C as damage to the catalyst and equipment will occur. • As soon as acid gases are introduced into the Hydrogenation Reactor inlet line start sampling the reactor’s inlet and outlet process gas Note: A hand-held Drager tube type sampling system is suggested where an immediate read out of H2S concentration in % or ppm can be seen. • At one hour intervals, continue sampling the reactor outlet gas until the H2S concentration in process gases are stable; then increase the RGG outlet temperature at 25°C/hr to 390°C, or other advised temperature. Note: Closely observe all temperature points across the Hydrogenation Reactor. If temperatures approach 400°C reduce and/or temporarily stop acid gas flow to the reactor. Under no circumstances should the reactor catalyst exceed 425°C as damage to the catalyst will occur. • Hold the reactor catalyst bed temperature at 390°C with the H2S rich acid gas flow passing through the reactor for a minimum of 4 hours to ensure the catalyst is fully sulphided. • Following the 4 hours hold period, stop the flow of the H2S rich acid gas to the inlet of the Hydrogenation Reactor. • Via the double block valves vent point valve, nitrogen purge the acid gas sulphiding line to the Hydrogenation Reactor and then back to the SRU acid gas feed line; then valve and blind isolate the line. • Reduce reactor inlet temperature to 240°C Sulphiding of the hydrogenation reactor is now complete and amine acid feed gas may be introduced to the SRU. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 512 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL 12.5 COMBUSTION AIR BLOWER 9102-K-11A LUBE OIL REPLACEMENT 1. The lube oil to be replaced every 8760 hours of blower running 2. Start Combustion Air Blower 9102-K-11B 3. Stop Combustion Air Blower 9102-K-11A 4. Allow sufficient time to cool the lube oil in the tank 5. Drain the spent lube oil and collect in drums 6. Close the drain valve fully after draining the spent oil 7. After draining the spent oil remove the oil drums to the designated place 8. Open the top man way of the lube oil tank 9. Check the internals of the tank 10. If the inside of the tank is dirty it should be manually cleaned 11. After thorough cleaning of the inside of the tank close the top man way 12. Bring the new lube oil drums near to the tank 13. Transfer lube oil to the tank through a hand pump 14. Transfer 2222 litres of oil to the tank 15. If any oil is spilled in the drain pan it has to be collected and disposed of in the same way as mentioned above. EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 513 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION XIII ANNEXURE EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 TITLE: OPERATION AND MAINTENANCE MANUAL 13.1 PFD/P&ID 13.2 HEAT AND MATERIAL BALANCE 13.3 CAUSE AND EFFECT DIAGRAM 13.4 DESIGN BASIS 13.5 MSDS Rev.: 0 Date: 03/09/2012 Page: 514 of 517 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 515 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL SECTION XIV REFERENCE DOCUMENTS EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 516 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Description Document No. Design Basis Memorandum 2970-6-29-0001 Process Description 2970-6-11-0001 Instrumentation Control Philosophy 2970-6-03-0001 Operating, Control and Safeguarding Philosophy - Utility Systems 2970-6-03-0002 Equipment List - Process Systems 2970-6-30-0001 Equipment List - Utility Systems 2970-6-30-0002 Line List - Process Systems 2970-6-33-0001 Line List - Utility Systems 2970-6-33-0002 Electrical Design Basis – SRU 2970-2-29-0001 Instrumentation Control Philosophy 2970-4-03-0001 Telecommunication Design Basis 2970-8-29-0001 Commissioning Execution Plan 2970-0-04-0031 Operating Guidelines for Sulphur Recovery Upgrade (Worley Parsons) 2365-0100 Process Control Narrative & Philosophy 2365-0098 Punch List Procedure 2970-0-05-0051 Process Flow Diagram 2970-6-52-0001 to 10 Utility Flow Diagram 2970-6-53-0001 to 10 Piping and Instrumentation Diagram (Process) 2970-6-50-0002 to 53 Piping and Instrumentation Diagram (Utility) 2970-6-51-0001 to 46 Mass Balance AGEU/SRU/TGTU 2970-6-42-0003 Cause and Effect Chart – ESD – NGL 3 2970-3-55-0001 Cause and Effect Chart – ESD – NGL 1/2 2970-3-55-0002 ESD Cause and Effect Matrix – Modifications of Existing Drawings – NGL 3 2970-3-55-0003 Instrument Air Compressor & Dryer Package – Control Narrative 2970-0006-4-03-0001 Instrument Air Compressor & Dryer Package – IOM Manual 2970-0006-5-26-0002 Instrument Air Compressor & Dryer Package – P&IDs 2970-0006-6-50-0001-3 Instrument Air Compressor & Dryer Package PFD 2970-0006-6-52-0001 Electro-Chlorination Package - Control Philosophy 2970-0008-4-03-0001 Electro-Chlorination Package – Alarm and Trip Schedule 2970-0008-4-67-0001 Electro-Chlorination Package – IOM Manual 2970-0008-5-26-0003 Electro-Chlorination Package – P&IDs 2970-0008-6-50-0001-0001-005 EPIC for Gas Sweetening Facilities Project (GSF) at Mesaieed & Dukhan Part-1 SRU (Mesaieed) Doc. No.: 2970-0-22-0001 Rev.: 0 Date: 03/09/2012 Page: 517 of 517 TITLE: OPERATION AND MAINTENANCE MANUAL Description Document No. Electro-Chlorination Package - PFD 2970-0008-6-52-0001 Steam Generation Package – BMS Functional Specification 2970-0025-4-14-0001 Steam Generation Package – BCS Functional Specification 2970-0025-4-14-0002 Steam Generation Package - Alarm and Trip Schedule 2970-0025-4-30-0005 Steam Generation Package - IOM Manual 2970-0025-5-26-0002 Steam Generation Package – P&IDs 2970-0025-6-50-0001-001-004 2970-0025-6-50-0002-001/002 2970-0025-6-50-0003 Steam Generation Package - PFD 2970-0025-6-52-0001 Sea Cooling Water Pumps - IOM Manual 2970-0028-5-26-0002 Sea Cooling Water Pumps – P&IDs 2970-0028-6-50-0001 Demineralization Water Treatment Package – Control Philosophy 2970-0048-4-03-0001 Demineralization Water Treatment Package – P&IDs 2970-0048-6-50-0001-001-005 Combustion Air Blower 9102-K-11A/B – Control Philosophy