Received: 15 January 2021 Revised: 28 February 2021 Accepted: 26 March 2021 DOI: 10.1002/gj.4142 RESEARCH ARTICLE Sedimentology of the Baluti Formation (Late Triassic) in the Warte area, northeastern Iraqi Kurdistan region Irfan Sh. Asaad1 | Sardar M. Balaky2 | 1 Department of Geology, College of Science, Salahaddin University-Erbil, Erbil, Iraq 2 Department of Petroleum Geosciences, Faculty of Science, Soran University, Erbil, Iraq 3 Scientific Research Center, Soran University, Erbil, Iraq Correspondence Irfan Sh. Asaad, Department of Geology, College of Science, Salahaddin University-Erbil, Erbil, Kurdistan region, Iraq. Email: irfan.asaad@su.edu.krd Handling Editor: I. Somerville Goran F. Hasan3 | Mahdi Kh. Aswad1 A detailed sedimentological investigation of the Baluti Formation (Late Triassic) in the Warte section, Imbricated Zone, northeastern Kurdistan region of Iraq has been undertaken for the first time. The formation is comprised of 34 m of dolomitic limestone, marly limestone, and marly dolomitic limestone which is partially brecciated and all interbedded with shale and several beds of marl in the lower part. Based on the field observations and petrographic inspections, four different lithostratigraphic units were identified in the studied section, which are, in ascending order: marly dolomitic limestone interbedded with marl and shale unit, brecciated marly dolomitic limestone interbedded with shale unit, fractured marly dolomitic limestone unit, and marly limestone interbedded with shale unit. The petrographic study of 19 thin sections of Baluti carbonates shows that the majority are composed of carbonate mud (micrite). The skeletal grains include ostracods, calcispheres, benthonic foraminifera, gastropods, bivalves, clasts, and bioclasts. While non-skeletal grains include peloids, intraclasts, and extraclasts. The results of X-ray diffraction (XRD) of five samples and scanning electron microscope (SEM) of three samples of the shale and marl of the studied formation show that the main clay mineral is illite, whereas non-clay mineral is dolomite. The carbonate rocks of the Baluti Formation were subjected to different diagenetic processes, such as micritization, dolomitization, cementation, compaction, solution, pyritization, neomorphism, and fracturing. Three main microfacies were identified in the Baluti carbonates and according to their environmental interpretation, they are grouped into one basic type of facies association—subtidal-semi restricted lagoon. Field observation, petrographic, microfacies, and textural analysis indicate that the Baluti Formation in the Warte section was deposited in a shallow marine, subtidal (lagoon) environment with semi-restricted conditions. KEYWORDS Baluti Formation, depositional environment, Kurdistan region of Iraq, Late Triassic, sedimentology 1 | I N T RO DU CT I O N green shales, calcareous, dolomitic, with intercalations of thin-bedded limestones, silicified limestones, and solution-recrystallization brec- The Baluti Formation was first described by Wetzel in 1950 and cias. The Baluti Formation crops out in limited surface sections along amended by Morton in 1951 (Bellen, Dunnigton, Wetzel, & the High Folded, Imbricate and Northern Thrust Zones from Zakho Morton, 1959) in its type section close to Baluti village, in the core of area in the northeast to Ranya region in the southeast (Buday, 1980). the Chia Gara anticline, south of Amadyia town. It comprises grey and In subsurface sections the Formation was identified in several wells Geological Journal. 2021;1–18. wileyonlinelibrary.com/journal/gj © 2021 John Wiley & Sons Ltd. 1 2 ASAAD ET AL. is regarded as one of the units of the middle part of the AP6 tectonostratigraphic megasequence. Because it is typified by rare fossil content, the Rhaetian (Late Triassic) age of the Baluti Formation Dashtak Fm. West of Iran Goff, 2006). According to Sharland et al. (2001), the Baluti Formation Early Jurassic Hiatus including: Jabal Kand-l, Khlesia-l, Atshan-l, and W Kifl-l (Jassim & Formation (Bellen et al., 1959; Jassim & Goff, 2006). The lateral equivalent unit of the Baluti Formation in the Iraqi western desert is the Zor Hauran Formation (Buday, 1980). While in surrounding countries, Minjur Fm. Kuwait & Saudi Arabia Upper Triassic Kurra Chine Formation and the overlying Liassic Sarki Early Jurassic Hiatus was determined by its stratigraphic position between the underlying and Northern Thrust Zones of Iraq (Al-Qayim, Omer, & Koyi, 2012). While, in subsurface sections, it found in different tectonic zones including the wells: Bakirman-1, Bjeel-1,2,3,7, Bekhma-1, Gulak-1, Jabal Kand-l, Khlesia-l, Atshan-l, and Wadi Kifl-l (Buday, 1980; Csató, Kiss, Toth, & Varga, 2014; Jassim & Goff, 2006) (Figure 1). In the Triassic period, the first tectonic event was the rifting of Gondwana which led to opening of Neo-Tethys Ocean along the line of the present Zagros Thrust Zone and separation of the Iranian Plate (Buday, 1980). In the Late Triassic, uplift occurred in the Rutba area in three common facies: (i) Inner shelf carbonates and clastics on the Stable Shelf (Mulussa and Zor Hauran formations), (ii) Inner shelf carbonates and evaporates in the Foothill zone, and (iii) restricted lagoonal TABLE 1 western Iraq and the rest of the Stable Shelf was submerged creating Mulussa Fm. Mulussa-E Fm. Baluti Fm. Zor Hauran Fm. Mulussa-F Fm. Fm. Aladag Syria Note: Adopted after Al-Husseini (2008), Buday (1980), Fortuny et al. (2015), Jassim and Goff (2006), Ozkan and Dinç (2018) and Ozkan and Elmas (2012). and limbs of several anticlines in the Zagros High Folded, Imbricate, Kasimlar Fm. The Baluti Formation mainly crops out as isolated patches in the cores Norian G EO LO GI C SE TT I N G Menteşe Fm. | Rhaetian 2 Late previously. Triassic of its depositional environment in areas that have not been studied Early and subdivisions, in order to understand further the lateral continuity Jurassic lithostratigraphy, petrography, diagenesis, mineralogy, facies analysis, Mesozoic of the Baluti Formation in the studied section in terms of Southeast of Turkey of this article is a detailed investigation of the sedimentological aspect South of Turkey mentology and palaeontology of the studied formation. The main aim Southwest of Turkey Omer (2020), which have all focused mainly on the stratigraphy, sedi- Stage and Samarrai (2019), Azo, Hanna, and Edilbi (2020), and Asaad and Epoch and Abdul- Razzak (2017), Asaad (2019), Asaad and Omer (2019), Lunn, Miller, Period Naser (2016), Al-Mashaikie (2017), Al-Mashaikie Era and McCann (2015), Shingaly (2016), Al-Mashaikie, Abdul-Razzak, and Regions Hanna (2007), Aqrawi, Goff, Horbury, and Sadooni (2010), Al-Juboury Geologic Time Scale includes the works of Buday (1980), Jassim and Goff (2006), Lithostratigraphic divisions of Upper Triassic–Lower Jurassic successions in Iraq and surrounding countries articles on the Baluti Formation in the outcrops of Northern Iraq. This Ubaid Fm. et al. (1959) in it is type section, there have been several published Mulussa-G Fm. Since the first description of the Baluti Formation by Bellen Çanakli Fm. West of Iraq (Buday, 1980) (Table 1). Kiziloren Fm. Hoşgör, 2015) and Menteşe dolostone Formation in Turkey (Ozkan & Dinç, 2018), and the upper part of Dashtak Formation in Iran Alakilise Fm. of Çanakli Formation, Kozluca Formation (Fortuny, Steyer, & Hettangian North of Iraq lower part of Kiziloren Formation (Ozkan & Elmas, 2012), middle part Butmah Fm /Sarki Fm. Minjur Formation in Kuwait and Saudi Arabia (Al-Husseini, 2008), the Kurra Chine Fm. it is equated with Mulussa-F Formation in Syria (Jassim & Goff, 2006), 3 ASAAD ET AL. F I G U R E 1 Location map of the Warte section including other previous studied outcrops and wells of Baluti Formation in Kurdistan region with the tectonic divisions of Iraq after Al-Qayim et al. (2012) and Fouad (2015) [Colour figure can be viewed at wileyonlinelibrary.com] facies in the High Folded Zone (Kurra Chine and Baluti formations) out in the valley and overlain by Jurassic units toward the top of Chia (Jassim & Goff, 2006). In Northern Thrust Zone, the Baluti Formation Rashkan Mountain. The exposed stratigraphic units in Warte area are: exhibits shallow marine facies with tropical to subtropical humid cli- Baluti Formation (Upper Triassic) and Sarki, Sehkanian, Sargalu, mate conditions (Asaad, 2019). Naokelekan, and Barsarin formations of Jurassic age (Figure 2). The Baluti Formation in the Warte section is located within the Imbricate Zone in which a few NW–SE trending thrusts were found. These thrusts have led to a repetition of strata in the exposed succes- 3 | METHODS AND MATERIALS sion. Generally, the Imbricate Zone in Iraq is characterized by severe folds and faults in the Palaeozoic to Cenozoic sedimentary strata, Field work was performed in the Imbricate Zone in the area around which well progressed in the northern portion and becomes less Warte town (Figure 1) in order to study the general geology and struc- developed toward the Iranian border (Fouad, 2015). tural relations of the area to choose a suitable section for the Baluti The studied section runs along a seasonal stream in the Warte Formation. The Warte section has not been investigated according to valley. The general strike of the strata takes the direction of Zagros any previously published works and thus there are few geologic data Fold and Thrust Belts which is NW-SE trend. The oldest rocks related to the study area because of its remote location. The studied exposed in the studied section are of Upper Triassic age which crop section is located about 150 m northeast of Khwartalesh village, 3 km 4 ASAAD ET AL. F I G U R E 2 Geological map of east Erbil area includes the studied section, modified from (Sissakian & Fouad, 2014) [Colour figure can be viewed at wileyonlinelibrary.com] south of Warte town, 28 km southeast of Soran city in the foot of the were collected perpendicular to the strike of the beds. Vertical sec- Chia Rashkan Mountain in Warte Valley. The studied section is tions were logged at intervals along the succession, detailed sedimen- located on the main road between Warte to Ranya city (Figure 2). The tological data obtained including grain size, texture, sedimentary studied formation was described and logged in detail, recording the structure, and fossil contents. lithology and texture, grain size, mineralogy, macrofossils, trace fossils, A total of 19 thin sections of carbonate samples was prepared and sedimentary structures. The main lithology in the studied at the Geology Department, College of Science, Salahaddin section is dolomitic limestone, marly limestone, and shale. A total of University-Erbil. The samples were cut perpendicular to bedding 25 samples from carbonate and shale were collected (Figure 3), in planes and stained with the Alizarin Red S solution (ARS) following addition to several samples were taken across the overlying boundary the procedure of Friedman (1959) for distinguishing between the with the Sarki Formation in order to check the nature and position of calcite and dolomite. Detailed petrographic study and microfacies its upper boundary in detail. Unfortunately, the lower boundary of the analysis were performed. The petrographic description was based Baluti Formation is not revealed because of poor exposure. Samples mainly on Dunham's (1962) limestone classification scheme using 5 ASAAD ET AL. F I G U R E 3 Columnar section of Baluti Formation in the Warte section, Imbricate Zone, Northeastern Iraqi Kurdistan region [Colour figure can be viewed at wileyonlinelibrary.com] the polarized microscope. Whereas, five shale and marl samples cho- 4 RE SU LT S | sen for XRD analysis, in order to identifying their mineralogy. In addition, three samples of shale were chosen for scanning electron 4.1 | Lithostratigraphy microscope (SEM) in order to identify the clay minerals and clarify their origin, using the apparatus Cam Scan electron optics LTD, The total thickness of the Baluti Formation in the Warte section is Quanta 450, England. The samples were coated with gold 15 before 34 m. The lower boundary of the formation is not exposed in the analysis with the coating instrument. The XRD and SEM analysis are studied section which is supposed to overlie the Late Triassic Kurra achieved at the laboratories of the Research Center of Soran Univer- Chine Formation, because it is exposed in Rania area southwest of the sity, Erbil Governorate. Warte section. Whilst based on the field investigations and 6 ASAAD ET AL. petrographic study, the upper boundary with the Early Jurassic Sarki to grey marly limestone interbedded with bluish dark grey shale Formation is determined as gradational and conformable (Figure 3). (Figure 5e) followed by 3 m of thick-bedded grey dolomitic limestone Following four interbedded with dark grey shale (Figure 5f). The sedimentary struc- lithostratigraphic subdivisions (units) were identified from the Baluti field observations and petrographic study, ture of this unit is only horizontal (planar) lamination Unit D. It is over- Formation in the studied section (Figure 3): lain by thick-bedded grey dolomitic limestone of Sarki Formation marked by changing the microfacies from lime mudstone of the Baluti Formation to medium to coarse crystalline dolomitized limestone of 4.1.1 | Marly dolomitic limestone interbedded with marl and shale unit (Unit A) Sarki Formation (Figure 5f1). This 7.5 m thick unit forms the lower part of the studied section and 4.2 Petrography and diagenesis | is overlain by brecciated marly dolomitic limestone interbedded with shale unit (Unit B). It consists of 4 m of thin- to medium-beds of frac- 4.2.1 | Petrographic components tured grey marly dolomitic limestone interbedded with yellow marl including a 0.25 m interval of thinly-bedded dark grey silicified lime- The petrographic investigations of 19 thin sections of carbonate rocks stone overlain by 3.5 m of thin- to medium-beds of yellow to grey of the Baluti Formation shows that there are few allochems observed marly dolomitic limestone interbedded with grey to yellow marl and and most were obliterated due to severe diagenetic processes affect- thin beds of yellow shale (Figure 4b). The main sedimentary structures ing the rocks of the studied formation. The identified skeletal grains in this unit are horizontal (planar) laminations and bending of carbon- involved ostracods (Figure 6a), benthonic foraminifera (Figure 6b), ate rocks (Figure 4c). gastropods (Figure 6c), calcispheres (Figure 6d), bivalves (Figure 6e), phosphatized bioclasts (Figure 6f), and other bioclasts (Figure 7a). Non-skeletal grains are comprised of peloids (Figures 6f and 7b), intra- 4.1.2 | Brecciated marly dolomitic limestone interbedded with shale unit (Unit B) clasts (Figures 6f and 7b), and extraclasts, which are mainly monocrystalline quartz (Figure 7c). Unit B thickness of 4.5 m, comprises of 1 m of medium-bedded yellow to grey brecciated marly limestone overlain by 2 m of medium- to 4.2.2 | Diagenetic processes thick-bedded grey brecciated dolomitic limestone followed by 1 m of dark grey shale and 0.5 m of medium-bedded yellow to grey brecci- The carbonate rocks of the Baluti Formation in the Warte area have ated marly limestone (Figure 4d).Unit B overlain by the fractured been affected by several diagenetic processes. The earliest diagenetic marly dolomitic limestone unit. It is characterized by calcite geodes processes recorded in the studied thin section are micritization in the (Figure 4e) and honeycomb sedimentary structures (Figure 5a). form of a micritic rim (or envelope) around molluscs (Figure 7d). Micritization is commonly formed by borer organisms such as endolithic algae or fungi (Reid & Macintyre, 2000). 4.1.3 | (Unit C) Fractured marly dolomitic limestone The other diagenetic process in the Baluti carbonates is dolomitization which occurs in both early and late phases. The early dolomitization is characterized by very fine crystals which are abundant in the The total thickness of the unit is 5 m. The lower 2 m consists of thin- lower part of the studied section and formed before the lithification bedded grey fractured marly limestone (Figure 5b) and upper 3 m is com- of sediments when still in connect with Mg-rich marine water prised of thin-bedded grey fractured dolomitic limestone (Figure 5c). (Tucker, 1981). The late dolomitization differs from the early diage- Sedimentary structures of this unit involve only horizontal (planar) lami- netic dolomite by its coarser crystals, formed in the stage of post- nation. Zoophycos brianteus trace fossils of Zoophycos ichnofacies was lithification of sediments by the influence of Mg-rich solutions which observed on the marly limestone beds of the unit (Figure 5d) which pre- mostly destroyed the original texture of the rocks (Chilingar, Bissell, & fer fine-grained siliciclastic and carbonate rocks and common on the shelf Wolf, 1967; Tucker, 1981). According to the Randazzo and setting in Mesozoic rocks (Knaust, 2017). The unit C is overlain by marly Zachos (1984) classification, three dolomite textures were identified; limestone interbedded with shale unit (Unit D). aphanotopic and sieve mosaic in the lower part (Figure 7c,e) and fogged mosaic in the middle and upper parts of the studied section (Figure 7f). 4.1.4 | Marly limestone interbedded with shale unit (Unit D) Cementation also occurred in the carbonates of the Baluti Formation and the main types are granular cement (Figure 6a) and blocky calcite cement (Figure 8a) reflecting a specific diagenetic environment. This unit comprises the uppermost part of the Baluti Formation in the Granular cement formed in the vadose zone (marine and meteoric) studied section. It consists of 14 m of thin- to medium-bedded yellow while blocky calcite mostly formed in meteoric (phreatic and vadose) ASAAD ET AL. F I G U R E 4 Photographs showing: (a) Studied section of Baluti Formation with overlying Sarki Formation. (b) Marly dolomitic limestone interbedded with marl and shale unit. (c) Bending (red arrows) of marly dolomitic limestone unit interbedded with marl. (d) Brecciated marly dolomitic limestone interbedded with shale unit. (e) Calcite geodes in the brecciated marly limestone beds. Scales: hammer 30 cm; pen 14 cm [Colour figure can be viewed at wileyonlinelibrary.com] 7 8 ASAAD ET AL. F I G U R E 5 Photographs showing: (a) Honeycomb sedimentary structure in brecciated marly limestone beds. (b) Thin-bedded grey fractured marly limestone. (c) Thin-bedded grey fractured dolomitic limestone. (d) Zoophycos brianteus trace fossils (red arrow) on the marly limestone bed. (e) Thin- to medium-bedded yellow to grey marly limestone interbedded with bluish dark grey shale. (f) Thick-bedded grey dolomitic limestone (red arrow) interbedded with dark grey shale underlying dolomitic limestone beds of Sarki Formation. (f1) Microphotograph showing the medium to coarse crystals of zoned dolomite in Sarki Formation. Scales: hammer 30 cm; pen 14 cm [Colour figure can be viewed at wileyonlinelibrary.com] ASAAD ET AL. F I G U R E 6 Photomicrographs of Baluti Formation in the Warte section showing: (a) Ostracod lime mudstone, Ostracode carapace filled by granular cement (red arrow). WB24., (p).P. (b) Benthonic foraminifera (red arrow)-peloidal lime wackestone, the benthonic foraminifera broken by fractures and affected by neomorphism. WB1, P.P. (c) Gastropod (red arrow) lime wackestone affected by neomorphism. WB1., P.P. (d) Calcisphere (red arrows)- peloidal (black arrows) lime wackestone submicrofacies. WB.4., P.P. (e) Intraclastic (red arrow)- bivalve (black arrows)- peloidal lime packstone. WB.10., X.N. (f) Phosphatic bioclast lime mudstone, the clast is supposed to be the destroyed part of a conodont (red arrow). WB19., P.P. WB: Warte-Baluti, P.P: plane-polarized light. A.S: alizarin stained: X.N: crossed-nicols [Colour figure can be viewed at wileyonlinelibrary.com] 9 10 ASAAD ET AL. F I G U R E 7 Photomicrographs of Baluti Formation in the Warte section showing: (a) Bioclastic packstone subjected to neomorphism and affected by fracturing (red arrow). WB17., P.P (b) Intraclastic (red arrow)-peloidal lime packstone.WB1., P.P. (c) Early stage dolomitization composed of very fine dolomite crystals forming aphanotopic fabric with some fine grains of monocrystalline quartz. Dolomitized lime mudstone microfacies. B6., X.N. (d) Brecciated intraclasts (red arrow)- molluscs had micrite envelops (black arrow) and subjected to dissolution (white arrow) dolomitized lime wackestone. WB9, X.N. (e) Sieve mosaic composed of coarse euhedral dolomite rhombs, with high intercrystalline porosity filled by granular calcite cement (red arrows). WB9., P.P., A.S. (f) Fogged mosaic dolomite with cloudy center and clear rims (red arrows). WB23., X.N [Colour figure can be viewed at wileyonlinelibrary.com] ASAAD ET AL. 11 F I G U R E 8 Photomicrographs of Baluti Formation in the Warte section showing: (a) Blocky calcite cement filled the vein (red arrow) in microspar groundmass subjected to solution (yellow arrow)., WB24. X.N. (b) Fractures filled by blocky calcite cement (red arrow). WB10., X.N. (c) Benthonic foraminifera (red arrow) lime mudstone influenced by fracturing (black arrow). WB23. X.N. (d) Peloidal lime packstone affected by stylolitization (red arrow). WB11. P.P. (e) Peloidal-bioclast lime packstone include framboidal pyrites (white arrow). WB10., P.P. (f) Authigenic minerals evaporites (red arrows). WB5. X.N [Colour figure can be viewed at wileyonlinelibrary.com] 12 ASAAD ET AL. and burial environments (Flügel, 2010). Compaction in both mechani- and on the surface of the detrital grains (Figure 10a–d). Dolomite also cal and chemical types was observed in the studied section. The is of authigenic origin from calcite during meteoric diagenesis of the mechanical compaction indicators are fractures that ordinarily are Baluti rocks in the studied section and this is indicated by euhedral filled by sparry calcite cement (Figure 8b,c), breaking of grains carbonate grains of the shales of the studied section (Figure 10b). The (Figure 6b) and deformation of allochems (Figure 6f). Chemical com- high concentration of selenium mineral within the dark grey shale in paction is exhibited by stylolitization which mainly is sutured seam the lower part of the studied section (Figure 9a) is supposed to have stylolite, irregular type with peaks of low amplitude type (Figure 8d). come from magmatic intrusions, especially where it is found with sul- Solution process have highly influenced the groundmass fides (pyrites) (Stillings, 2017). Apatite which occurred in the middle (Figure 8a) and most types of fossil shells of the Baluti Formation part of the Baluti shale (Figure 9b) has a cauliflower-like aggregate (Figure 7d) which is supposed to be the result of dissolution of meta- nature (Figure 10d), which proves that it formed by bacteria from stable minerals such as high-Mg calcite and aragonite and fresh water direct precipitation from solutions (Lucas & Prevot-Lucas, 1997). has been more efficient than marine water in this diagenesis (Asaad & The occurrence of detrital quartz (Figure 10e,f) with feldspar Balaky, 2020). Authigenic minerals (pyrite) also had a good imprint on (Figure 9a,b) in studied samples of the Baluti carbonates indicate that the studied rocks of the Baluti Formation and the most common type they were transported from an area near to the depositional basin of is framboidal pyrite (Figure 8e) which occurred in the lower and upper the formation because they have a lower mechanical stability than parts of the studied section. Whereas, evaporites are observed in the quartz (Morad, 2003). lower part of the studied formation (Figure 8f). The other diagenetic process is neomorphism (Figure 6b) affected in variable percentage on the Baluti carbonates in the studied section. 4.4 Microfacies analysis | Three main microfacies types were recognized in the carbonate rocks 4.3 | Mineralogy of the Baluti Formation in the Warte section based on the classification of Dunham (1962), which is based mainly on the original texture The results of the XRD analysis are shown in Figure 9. Based on the of carbonate rocks. Each microfacies was later subdivided into several X-ray diffraction (XRD) analysis for selected shale and marl samples, submicrofacies according to the significant fossils' types (Table 2). the main constituents are dolomite, feldspar, calcite, quartz, apatite, and selenium (Figure 9a,b). While, clay minerals are represented by illite only. The majority of illite is of authigenic origin in the studied 4.4.1 | Lime mudstone microfacies section and this is indicated by morphology of illite seen in SEM microphotographs which involves: illite rim cements (pore lining illite This facies is characterized by a mud-supported fabric consisting of fibres), which occur mainly in intergranular pores around the grains more than 90% lime mud while the rest is composed of allochems F I G U R E 9 X-ray diffractograms of the bulk clay samples of the Baluti Formation from the Warte section, Imbricated Zone. (a) WB3. (b) WB12 [Colour figure can be viewed at wileyonlinelibrary.com] ASAAD ET AL. 13 F I G U R E 1 0 Scanning electron microphotographs (SEM) showing: (a) anhedral carbonate grains (red arrows), diagenetic illite (black arrow). WB12. (b) Well-developed euhedral, authigenic pyrite crystal (yellow arrow), euhedral dolomite rhombs (black arrows), white diagenetic illites (red arrow). WB25. (c) Branched and rod-like cyanobacteria fossils (red arrow), illite (black arrows). WB25. (d) Diagenetic illite (red arrow), cauliflower-like forms made by apatite (yellow arrow). WB25. (e) Detrital quartz grain (red arrow). WB12. (f) Bladed fragment of the cyanobacteria composed of mineralized filaments (Red arrow), organic matter filling pores (white arrow), detrital quartz grain (Q). WB12 [Colour figure can be viewed at wileyonlinelibrary.com] 14 TABLE 2 ASAAD ET AL. Microfacies subdivisions of Baluti Formation in the Warte section Main microfacies Dunham (1962) Subdivision of Dunham (1962) Lime Mudstone Dolomitized lime mudstone Lime Wackestone Lime Packstone SMF Flügel (1982) Environment of deposition It characterized by fine crystals of dolomite distributed on the micritic groundmass of the submicrofacies with rare grains of fine monocrystalline quartz. It commonly occurs in the lower part of studied section. 23 Subtidal (lagoon) Benthonic foraminiferal lime mudstone Benthonic forams in micritic matrix, characterized by fracturing which filled by granular cement. Commonly exist in the upper part of the formation. 19 Subtidal (lagoon) Phosbioclast lime mudstone Bioclasts of different phosphatized walled bioclast is the main skeletal grain in micritic matrix subjected to severe neomorphism. It occurred in the upper part of the studied formation. 14 Subtidal (lagoon) Ostracod lime mudstone Ostracods filled by granular calcite cement, observed in the micritic matrix which faced to neomorphism. 8 Shelf lagoon with circulation Gastropoda lime wackestone Microgastropda is the main skeletal grain among bioclasts and and calcispheres in micritic matrix. It characterized by neomorphism and observed in the lower part of studied section. 9 Shelf lagoon with circulation Benthonic foraminiferalpeloidal lime wackestone Benthonic forams with peloids and bioclasts in micriitc matrix which affected by severe neomorphism and fracturing and found in the lower portion of the studied formation. 8 Shelf lagoon with circulation Brecciated intraclast -molluscs dolomitized lime wackestone This subdivision characterized by macro and micro breccia having both molluscs and intraclasts grains in dolomitized micritic matrix. Late dolomitization and dissolution are the main diagenetic criteria and occurred in the lower part of studied section. 14 Shelf lagoon with circulation Calcisphere-peloidal lime wackestone Calcispheres and peloids are observed in the micritic matrix. Peloid non-skeletal grains also found in this microfacies. It common in the lower part of the Baluti carbonate. 9 Shallow lagoon with open circulation Bioclastic lime packstone It includes unidentified bioclasts affected by neomorphism and fracturing and found in the middle part of studied section. 9 Shallow lagoon with open circulation Peloidal-bioclast lime packstone It characterized by common peloidal grains with bioclasts and subjected to neomorphism and pyritization. It is present in the middle part of the studied section. 8 Shelf lagoon with circulation Intraclast-peloidal lime packstone Main allochems involves intraclasts and peloids which affected by dissolution. It is observed in the lower part of the studied formation. 8 Shelf lagoon with circulation Peloidal lime packstone Peloids grains in spary calcite matrix characterized by stylolitization are common in middle part of the formation. 18 Shelf lagoon with open circulation Intraclast -bivalve peloidal lime packstone It observed in the middle part of the studied section and include more than 90% of grains which are mainly intraclasts, peloids, bivalves with rare monocrystalline quartz. 18 Shelf lagoon with open circulation Diagnostic features (Dunham, 1962). It is a common microfacies and found in the lower (Figure 9a), phosphatised bioclast lime mudstone (Figure 9b), and and upper parts of the studied section. It includes dolomitized lime ostracod lime mudstone submicrofacies (Figure 9c). The main diage- mudstone (Figure 6a), benthonic foraminiferal lime mudstone netic processes observed in this facies are dolomitization in addition 15 ASAAD ET AL. to cementation and neomorphism. It is equivalent to the standard bearing lime mudstone, overlain by 3 m of thick-bedded grey dolo- microfacies SMF 8,14 and 19 of Flügel (1982) and facies zone FZ mitic limestone within lime mudstone microfacies. The association is 7 and 8 of Wilson (1975). also characterized by bearing authigenic mineral (pyrite) in the lower and upper parts of studied section. 4.4.2 | Lime wackestone microfacies 5 | DI SCU SSION This microfacies is the second commonest microfacies of the Baluti carbonates in the studied section. It is observed in the lower part of The Baluti Formation was deposited in a shallow marine lagoonal envi- the section. It has a texture composed of grains ranging between ronment in the Late Triassic, corresponding to the second stage of the 10 and 50% in a mud-supported matrix (Dunham, 1962). It includes opening of the Neo-Tethys Ocean, when further extensions formed gastropod lime wackestone (Figure 9d), benthonic foraminiferal- around the northern and eastern margins of the Arabian Plate peloidal lime wackestone (Figure 9e), brecciated-intraclast-mollusc (Sadooni & Al-Sharhan, 2004). In the Warte area, the dominance of dolomitized lime wackestone (Figure 9f), and calcisphere-peloidal lime mudstone microfacies within the Baluti Formation infers that sea wackestone submicrofacies (Figure 10a). Cementation, dissolution, bottom was stagnant and calm enough for lime mud to accumulate. fracturing, and neomorphism are the main diagenetic processes Dolomitized lime mudstone indicates a restricted platform environment affected this microfacies. This facies corresponds to the standard (Al-Hammdani, Al-Naqib, & Al-Youzbaki, 2005). The laminated grey microfacies SMF 8, 9 and 14 of Flügel (1982) and facies zone FZ 7 of shale of the Baluti Formation may refer to very slow motion of water Wilson (1975). and are often occurred in lagoonal deposits (Blatt & Tracy, 1996). The occurrence of benthic foraminifera within the micritic-supported microfacies refers to a shallow water environment (Balaky, Abdula, & 4.4.3 | Lime packstone microfacies Perot, 2016; Bismuth & Bonnefous, 1981). Peloid, bioclast, and intraclast wackestone and packstone microfacies are common in the This microfacies is composed of more than 60% grains leaving minor lagoonal environment (Wadood, Khan, Li, Ahmad, & Jiao, 2021). micrite between grain-supported limestones (Dunham, 1962). It is Calcispheres can occur in both shallow warm and deep waters widespread in the lower and middle parts of the studied formation. (Masters & Scott, 1978). The association of calcispheres, ostracods, and The petrographic investigation of this facies led to identifying the gastropods with benthonic foraminifers indicates a lagoonal shallow bioclast lime packstone, peloidal-bioclast lime packstone, intraclast- marine environment (Asaad & Balaky, 2018). Phosphatised bioclast lime peloidal lime packstone, peloidal lime packstone, and intraclast- mudstone which forms from the remains of phosphate fossils such as bivalve-peloidal lime packstone submicrofacies. The significant teeth, bones, and conodonts occurs in the upper part of the studied diagenetic processes affected upon this microfacies are neomorphism, section and is characteristic of lag deposits that originating during pyritization, fracturing and stylolitization. It corresponds to the stan- periods of reduced sedimentation or non-deposition in a depositional dard microfacies SMF 8, 9 and 18 of Flügel (1982) and facies zone FZ regime (Flügel, 2010). Zoophycos ichnofacies refers to a very shallow 7 of Wilson (1975). lagoonal, quiet water environment of the Baluti Formation in the studied section. This is indicated by the low diversity of skeletal grains inferring stressful conditions related to significant salinity variations and/or 4.5 | Facies association a restricted setting of the basin (Giannetti, Tent-Manclús, & BaezaCarratalá, 2017), confirmed by the presence of evaporites recognized in The recognized microfacies of Baluti carbonates in the Warte thin sections from the formation. On the other hand, cyanobacteria section can be grouped according to their environmental interpreta- which is present in the shale of the upper part of the Baluti Formation tion into a subtidal (semi-restricted lagoon) facies association. are phototrophic bacteria that can grew in different aquatic environ- This facies association is equivalent to facies zone 7 and 8 of Wil- ments, both marine and fresh waters, and tolerate a wide range of son (1975). It is present in the whole succession of the Baluti Forma- water temperature, pH, redox potential, and salinity (Al-Bassam & tion in the studied section. The lower part consists mainly of 12 m of Halodová, 2018) in association with the above-mentioned criteria that yellow to grey marly dolomitic limestone partially brecciated within may indicate a shallow marine environment for the Baluti Formation. lime mudstone, wackestone, and packstone microfacies interbedded The common existence of authigenic pyrite in the lower and upper with grey to yellow marl and thin beds of yellow and grey shale char- parts of the Baluti carbonates indicates a restricted-lagoonal condition acterized by calcite geodes and honeycomb sedimentary structures. (Asaad & Balaky, 2018; Kauffman & Sageman, 1990). Calcite geodes The middle part comprises 5 m of thin-bedded grey fractured marly which are observed in the lower part of the studied section are thought dolomitic limestone within lime mudstone to wackestone microfacies to have formed in cavities by evaporate dissolution, which developed bearing Zoophycos brianteus trace fossils of Zoophycos ichnofacies. during periodic hypersaline conditions in the shallow restricted lagoon The upper part consists of 14 m of grey and blue shale interbedded environment (Flügel, 2010) and confirmed by the presence of remnant with thin- to medium-bedded yellow to grey of marly limestone authigenic evaporites in thin sections. 16 ASAAD ET AL. F I G U R E 1 1 The depositional model of the Baluti Formation at Warte section and other localities in Iraqi Kurdistan Region. (Galley Derash and Sararu sections after Asaad and Omer (2020) and Bakerman, Bekhme, Bjeel, and Gulak wells after Csató et al. (2014)) [Colour figure can be viewed at wileyonlinelibrary.com] Summarizing all the petrographic, facies, and textural analyses, it consisting of clay and siltstone with little carbonate deposited in a flu- is concluded that the Baluti Formation at the Warte section was vial and lagoonal environment (Yousef, Al-Kadi, & Morozov, 2016) deposited in a shallow marine environment, subtidal (lagoon) with and marked the beginning of a regional transgression that continued semi-restricted conditions, as depicted in the proposed model for the through to the Early Jurassic (Brew, Barazangi, Al-Maleh, & inferred palaeoenvironmental conditions of the Baluti Formation in Sawaf, 2001). Northeastern Kurdistan region of Iraq (Figure 11). The depositional environment of the Baluti Formation in the Warte section is relatively shallower compared to other localities 6 | CONC LU SIONS toward the west of the Iraqi Kurdistan region, for example, at Galley Derash in the High Folded Zone and Sararu area in the Northern 1. Four different lithostratigraphic units were identified from the Thrust Zone, which were deposited in a shallow marine environment Baluti Formation in the Warte section based on field observation including and petrographic study, which are, in ascending order: unit lagoonal, shoal, and fore-shoal settings (Asaad & Omer, 2020). The stressed shallow water environment of the Baluti A—Marly dolomitic limestone interbedded with marl and shale, unit Formation in the studied section is indicated by the absence of ooids, B—Brecciated marly dolomitic limestone interbedded with shale, coated grains, dasycladacean green algae, red algae, ammonoids, and unit C—Fractured marly dolomitic limestone unit, and unit ripple marks, which were observed in both the Galley Derash and Sararu sections (Asaad & Omer, 2020).Whereas, in Bakirman-1, Bjeel- D—Marly limestone interbedded with shale. 2. Petrographically, the Baluti carbonates in the studied 1,2,3,7, Bekhma-1, and Gulak-1 wells toward the southwest of Warte section comprise of a variety of shallow water skeletal fauna area, it was deposited in a tidal flat, lagoonal, and evaporitic environ- including ostracods, calcispheres, benthonic foraminifers, gastro- ment, which formed from dolomite and dolomitic, silicified and oolitic pods, bivalves, phosphatised bioclasts, and bioclasts. While non- limestones with green shales and anhydrite replacements (Csató skeletal grains include peloids, intraclasts, and extraclasts. The et al., 2014) that refers to a shallower and more restricted setting than dominant groundmass in the studied section is micrite. The main the Warte area. Regional correlation of the Baluti Formation with sur- non-clay minerals in the shales and marls of the Baluti Formation rounding areas shows that the Late Triassic Dashtak Formation which are dolomite and the clay mineral is illite. is mainly comprised of shallow water carbonate–evaporite sediments 3. The carbonate rocks of Baluti Formation were subjected to differ- consisting of dolomite, evaporite, and shale rare in fossil content was ent diagenetic processes such as micritization, dolomitization, deposited in a supratidal and tidal flat to lagoonal environment within cementation, compaction, solution, pyritization, neomorphism, and the Neo-Tethys Ocean in the eastern Zagros Fault and Thrust belt in fracturing. Iran (Rahmani, Khoshnoodkia, Mohseni, & Hajian, 2018). It differs 4. Following Dunham's (1962) classification, and detailed microscopic from the Baluti Formation in the Warte Section by containing multiple investigation, three main microfacies were identified in the Baluti evaporate intervals which were thought to have been deposited dur- carbonates in the studied section, which are grouped into one ing basic type of facies association relating to their environmental the second Triassic infilling-subsidence event (Rahmani et al., 2018). While in southeastern Turkey, the Çanakli Formation interpretation of a subtidal-semi-restricted lagoon. which forms the base of Cudi Group is mainly comprised of dolomite (Fortuny et al., 2015), which was deposited in a lagoonal shallow AC KNOWLEDG EME NT S marine carbonate environment during the Late Triassic age The authors would like to extend their appreciations to the Geology (Ziegler, 2001). In northwestern Syria the Mulussa-F (Serjelu) Forma- Department of Salahaddin University-Erbil for their help in preparing tion is relatively dissimilar in facies than Baluti Formation by thin sections and also the Research Center of Soran University is 17 ASAAD ET AL. appreciated for their help in XRD and SEM analyses. The gratitude to Prof. Dr. Faraj Tobia from Geology Department Salahaddin University-Erbil, for his helping in interpretation of XRD results. Thanks to Mr. Bzhar A. Manaf, geologist from Petroleum Geoscience Department in Soran University, for his help during the field work. Mr. Peyman Aspoukeh, assistant lecturer of particle physics in Scientific Research Center of Soran University, is also thanked for his laboratory help. Mr. Waad Sh. Asaad and Mr. Miran K. Abduljalil are thanked for computer facilities. P EE R R EV I E W The peer review history for this article is available at https://publons. com/publon/10.1002/gj.4142. 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