SPE 96896 A New Experimental Method To Determine Interval of Confidence for Capillary Pressure and Relative-Permeability Curves P. Egermann, J.-M. Lombard, C. Fichen, E. Rosenberg, E. Tachet, and R. Lenormand, Inst. Français du Pétrole Copyright 2005, Society of Petroleum Engineers This paper was prepared for presentation at the 2005 SPE Annual Technical Conference and Exhibition held in Dallas, Texas, U.S.A., 9 – 12 October 2005. This paper was selected for presentation by an SPE Program Committee following review of information contained in a proposal submitted by the author(s). Contents of the paper, as presented, have not been reviewed by the Society of Petroleum Engineers and are subject to correction by the author(s). The material, as presented, does not necessarily reflect any position of the Society of Petroleum Engineers, its officers, or members. Papers presented at SPE meetings are subject to publication review by Editorial Committees of the Society of Petroleum Engineers. Electronic reproduction, distribution, or storage of any part of this paper for commercial purposes without the written consent of the Society of Petroleum Engineers is prohibited. Permission to reproduce in print is restricted to a proposal of not more than 300 words; illustrations may not be copied. The proposal must contain conspicuous acknowledgment of where and by whom the paper was presented. Write Librarian, SPE, P.O. Box 833836, Richardson, TX 75083-3836, U.S.A., fax 01-972-952-9435. Abstract The saturation profiles are routinely measured during Special Core Analysis (SCAL experiments). Several ways exist to use this information in the inversion procedure of the relative permeability data. To date, the local saturation profiles are either included in a global objective function that is minimized during the inversion process, or smoothed and used as input data in the simulation, which leads to non smoothed simulated pressure drop. None of these methods permit to reproduce the local saturation fluctuations that are measured during coreflooding experiments. Our approach has the advantage to take benefit from these fluctuations to characterize the petrophysical properties for a given rock-type. In this paper, the methodology is first recalled and illustrated on a synthetic case. It is based on upscaling techniques applied in reservoir simulation. Both the stabilized and transient saturation profiles are analyzed to evaluate the local properties. The quality of the history matching is significantly improved. In addition, both kr and Pc-curves are obtained from only one experiment and the variability of these parameters with the heterogeneity is also investigated. This estimated interval of confidence for kr and Pc can be very useful to perform uncertainty studies at the reservoir scale. The Pc-curve interval of confidence determined with this method on a carbonate sample, is in good agreement with the variability observed with several centrifuge experiments performed on sister plugs. Finally an alternative approach derived of the heterogeneous method is proposed, which allows a very quick acquisition of all the information relative to kr and Pc during a multi-rate flow experiments. Introduction Petrophysical parameters assessment Both relative permeability (kr) and capillary pressure (Pc) curves are key factors for assessment and prediction of the hydrocarbon recovery of a field. Representative curves are routinely obtained through SCAL (Special Core Analysis Laboratory) studies, in operating conditions as close as possible of reservoir conditions. These conditions mainly concern the thermodynamic conditions (pressure, temperature), the reservoir stress (overburden pressure), the nature of the fluids (synthetic reservoir brine, live oil), the initial saturation state (low Swi value) and the in-situ wettability (preserved samples or restored wettability through an aging process at Swi). Relative permeabilities are usually determined from flow experiments performed on core samples using either the UnSteady-State (USS) or the Steady-State (SS) method, where either one or two fluids respectively are injected. The centrifuge technique can also be used but not at full reservoir conditions (Ruth, 1997; Chardaire et al., 1992). Whatever the method used, the experimental results must be interpreted using capillary pressure curves. Virnovsky et al. (1998) proposed an analytical method to correct the SS data for capillary pressure. However, numerical simulations are needed for both USS and SS because a complete analytical solution does not exist. The kr curves can either be optimized in order to history match the experimental data knowing the Pc curve (from another experiment) or both kr and Pc curves can be optimized simultaneously (Chardaire et al., 1992; Helset et al., 1998). More recently, it has been shown that both kr and Pc curves can be determined at reservoir conditions using the semidynamic approach (Lombard et al., 2002). The main advantage of this method is to establish several equilibrium states between the viscous and the capillary forces within the sample by injecting one fluid while the other circulates at the outlet face. These equilibrium states enable the determination of both the kr of the injected phase and the Pc curve. The kr of the displaced phase can also be obtained by history matching of transient evolution of the pressure drop. In-situ saturation monitoring, which is now widely implemented in SCAL studies, brings a significant added value to the interpretation process because it enables the direct identification of the influence of the capillary effects on the experimental data. Several ways exist to use this information in the inversion procedure of the kr data. To date, the local saturation profiles are either included in a global objective function (in addition to the production and the pressure drop data) that is minimized during the inversion process, or smoothed and used as input data in the simulation. Local saturation fluctuations often take place in carbonate samples 2 during coreflood experiments. These saturation fluctuations cannot be anticipated during the preliminary core selection process because they are due to small-scale local variations of the petrophysical properties. Therefore, none of the available methods permit the accurate reproduction of both the production data and the heterogeneous saturation profiles in an automatic way. Background on rock heterogeneities Because the core heterogeneities can severely affect the determination of the petrophysical parameters, a SCAL study always begins by a preliminary selection and sampling process in order to retain the best cores within a given rock type. Various techniques can be used and combined to finalize the selection of core samples: CT-scanner, NMR, HPMI, tracer tests (Dauba et al., 1999). Petrophysical parameters (k, φ, kr, Pc) are seldom uniform within the entire core. Graue (1994) reported a study on an eolian sandstone originally considered as homogeneous, which showed unexpected saturation profiles during coreflood experiments. The saturation fluctuations were successfully interpreted as a result of permeability and capillary pressure heterogeneities. Honarpour et al. (1994) showed through several displacement experiments conducted on cross or parallel bedding cores, that the structure of the heterogeneity itself played a major role in the shape of relative permeability curves. These conclusions were confirmed by Mannseth et al. (1998), who interpreted synthetic experimental data with different heterogeneity structures (tilted lamina, unstructured heterogeneity distribution, and flow barriers). Hamon and Roy (2000) explored the influence of the coreflood design as a function of heterogeneity type, along or across bedding samples. They generated numerical experiments through a finely well characterized model, and the interpreted kr curves were compared to the input curves. One of their conclusions was that the USS experiment is very sensitive to along-axis heterogeneities. Saad et al. (1995) succeeded in history matching both the production data and the heterogeneous saturation profiles presented by Honarpour et al. (1994) by introducing a limited number of kr, Pc curves in the simulation code. Fincham and Gouth (2000) analysed a multi-rate coreflood experiment, which showed heterogeneous saturation profiles. Because the stabilized profiles result from an equilibrium between the viscous and the capillary forces, they observed that the saturation profiles tend to become more homogeneous at the highest bump flow rates (higher viscous forces). It was possible to reproduce all the experimental data by implementing a single set of kr curves and two Pc curves accounting for low and high permeability facies. Outline This paper presents an innovative methodology to fully account for the local heterogeneity in the history matching procedure to determine kr and Pc. The proposed approach takes advantage of local saturation fluctuations to characterize the petrophysical property variability within a rock-type. The method is derived from upscaling techniques that are routinely applied in reservoir simulation and that are based on the pressure data, which are, contrary to the saturation data, SPE 96896 already a smooth function even when the heterogeneity level is significant. Both the stabilized and transient saturation profiles are analyzed to evaluate the local kr and Pc. The first part of the paper is devoted to the presentation of the proposed approach. A literature review on the use of local saturations in SCAL and the background about upscaling techniques in reservoir engineering is first presented. The principle of the approach is then illustrated through a synthetic case and the general workflow to interpret an USS experiment is described. The application of the method for the interpretation of a multi-rate gas/brine experiment performed on a carbonate sample is then detailed. The results are compared to centrifuge data obtained on companion plugs. Finally, a semi-analytical approach derived of this heterogeneous method is proposed to speed up the interpretation of any multi-rate experiments. The proposed heterogeneous approach As described in the introduction, the rock heterogeneity very often affects the experimental saturation profiles. Several experimental techniques exist to identify this heterogeneity, and results from these techniques can be accounted for in the numerical simulation. Nevertheless, the heterogeneity is seldom taken into account in the interpretation process although several studies demonstrated that significant improvements can be made using local petrophysical parameters. The mathematical approach based on numerical inversion of the problem is too complex and time consuming to be conducted. The trial-and-error method is too subjective and only applicable on a limited number of petrophysical parameters. Therefore there is a need to develop a physical approach to assess these parameters directly from the experimental data in a consistent manner. Use of local saturations Local saturation profiles can bring a significant improvement in the interpretation of coreflood experiments by accounting for capillary pressure effects during the relative permeabilities determination. The most conventional approach for including saturation data in the history matching process is to use a homogeneous numerical model, a single kr curve (for each fluid) and a single Pc curves. The saturation data are added to the production data to calculate the objective function. At each iteration step, this objective function is minimized by adjusting kr and Pc curves. Several papers showed that the inclusion of the saturation data considerably improved the determination of kr, Pc curves especially at low injected fluid saturation (Courtial and Ghalimi, 2000). Nevertheless, the optimized simulated saturation profiles pass through the experimental data in only an average sense but cannot reproduce the local heterogeneities. Mejia and Mohanty (1995) proposed to improve this procedure by incorporating local end-point saturation in the inversion procedure. They found a better match of the saturation profiles but the large number of parameters to be considered makes the optimization process very time consuming. Another approach consists in processing directly the local saturation data (Goodfield et al., 2001; Element and Goodyear, 2002). The particularity of their approach is to eliminate the SPE 96896 Numerical example The main finding of these upscaling studies is that the pressure profiles are less sensitive to the heterogeneity than the saturation profiles. Therefore, it suggests that the pressure can be reasonably approximated using the petrophysical properties determined with a homogeneous model. Consequently, the pressure can be calculated at every saturation measurement location without the need for local pressure taps. Synthetic data have been generated by simulation to illustrate this point on a conventional USS coreflood imbibition experiment. The IFP in-house simulation code has been used with a 1D geometry and 30 cells. The core properties are presented in Table 1. We consider a multi-rate brine injection in a core originally at Swi (10, 50, 200, 400 cm3/hr). The same viscosity was considered for both fluids (1 cP) and a unique set of kr curves was used. The Corey exponents and kr end- Table 1. Core properties Length Diameter 8 cm 5 cm Phi Kmin Kmax 25 % 11 md 47 md K average Swi Sorw 24.5 md 0.1 0.1 Two sets of data were generated using either a homogeneous or a 1D heterogeneous core with non-uniform permeability and Pc curves. The permeability values range between 11 and 47 md and distributed at random along the sample. The local Pc curves were obtained using the Leverett function. The set of Pc curves is shown in Figure 1 and corresponds to an oilwet case. The permeability of the homogeneous core is the harmonic average. A unique Pc curve based on this average permeability value is considered for the homogeneous core. Sw (fraction) 0 0.2 0.4 0.6 0.8 1 1 0 -1 Pc w/o (bar) Pressure based approach Upscaling techniques in reservoir engineering A tremendous amount of work has been published on flow in heterogeneous porous media in the reservoir numerical simulation community. The geological codes often provide fine description models of millions of cells, which account for the complexity and the heterogeneities of the reservoir. Because the fluid flow simulations cannot be conducted on these high resolution grid, an upscaling (or averaging) technique is needed to reach reasonable calculation times. The conventional method is to coarsen the grid by doing a static upscaling before the flow simulation but it can lead to significant errors due to the averaging of the saturation profile. The principle of the Dual Mesh Method (DMM) is to solve the pressure equation on the coarse grid and the saturation equation on the fine grid. The pressure data are then interpolated on the fine grid to better reproduce the saturation profile evolutions (Guerillot and Verdière, 1995). From a mathematical point of view, the DMM approach is justified by the parabolical (or elliptical) nature of the pressure equation (long range forces) compared with the hyperbolical nature of the saturation equation. It makes the pressure profiles to be smoother than the saturation profiles (Verdière et al., 1996). point values are equal to 2 and 0.6 for the water phase, and, 4 and 0.9 for the oil phase respectively. -2 -3 -4 -5 -6 Figure 1 : Synthetic case with small-scale heterogeneities: the set of Pc curves implemented in the simulator at each location 5000 30 4500 25 4000 Pressure drop (mbar) local heterogeneity effects by smoothing the saturation profiles and to use them as input data for the numerical simulator. This leads to simulated pressure profiles that are not smooth, which is not consistent with the experimental pressure drop responses that exhibit always a smooth, strictly monotonous decreasing behavior after breakthrough, whatever the level of heterogeneity inside the core. Therefore, this approach permits the reproduction of the saturation data in all the cases (input data in the model) but it fails to take into account the heterogeneity and produces non-physical pressure drop responses. The latest approach is the one followed by Graue (1994), Fincham and Gouth (2000) and Saad et al. (1995). It consists in implementing several kr, Pc curves in the simulator to account for the local heterogeneities. These existing studies demonstrated that this approach permits significant improvements in the quality of the history match but is only applicable with a limited number of curves. 3 3500 Oil pro du cti 15 on (c m3 10 ) 20 3000 2500 2000 1500 Pressure drop 1000 Oil production 5 500 0 0 50 100 150 0 200 Time (h) Figure 2 : Synthetic case with small-scale heterogeneities: production data The production data (Figure 2) are very similar to real experiments performed in the laboratory in an oil-wet core. Each increase of the injection rate (bump) leads to production 4 SPE 96896 1 Hete 10 cm3/hr 0.9 Hete 50 cm3/hr 0.8 Hete 200 cm3/hr Hete 400 cm3/hr Sw (fraction) 0.7 Homo 10 cm3/hr 0.6 Homo 50 cm3/hr 0.5 Homo 200 cm3/hr Homo 400 cm3/hr 0.4 0.3 0.2 0.1 0 0 2 4 6 8 10 Core length (cm) Figure 3 : Saturation profiles for the homogeneous (solid or dotted lines) and the heterogeneous cores (points) descriptions Principle of the "pressure based" method First, the experiments are interpreted as if the sample were homogeneous using standard methods used in SCAL, and pressure profiles at each injection step are calculated using a numerical simulator. When stabilization is reached, the pressure in the displaced phase is uniform along the sample and equal to the outlet pressure (no flow rate implies no pressure gradient). The local pressure of the injected phase corresponds to the capillary pressure (plus the outlet pressure) as in a semi-dynamic experiment. The saturation Sw is known at any location of the in-situ measurement and the corresponding capillary pressure Pc is derived from the calculated pressure profile. The capillary curve is determined by all the points Pc(Sw) measured at the various locations along the sample and the various flow rates. The above described approach will be referred as “pressure based” approach in the following. 600000 Hete 10 cm3/hr Hete 50 cm3/hr Hete 200 cm3/hr 500000 Hete 400 cm3/hr Water pressure (Pa) of additional oil due to the increase of the viscous forces. As expected, many fluctuations are observed in the saturation profiles with the heterogeneous core (Figure 3) due to local variations of oil trapping. The amplitude of the saturation fluctuations (10-15 % saturation units) is in good agreement with real experimental data. The fluctuations also tend to minimize at higher rates because the viscous forces are higher, leading to saturation close to the asymptotic value (= 1 – Sor). This behavior is also observed in experimental data (Egermann et al., 2003; Fincham and Gouth, 2000). The saturation profiles obtained with the homogeneous core pass on average through the heterogeneous saturation points but the saturation differences can be locally as high as 10 % (Figure 3). This is completely different for the pressure profiles. Some small amplitude fluctuations can be detected on the profiles derived from the heterogeneous core but they remain very comparable to the homogeneous case (Figure 4). This example illustrates and confirms that the pressure profiles are less prone to fluctuations due to small-scale heterogeneity (on the order of the centimeter scale) compared to the saturation profiles. Homo 10 cm3/hr 400000 Homo 50 cm3/hr Homo 200 cm3/hr Homo 400 cm3/hr 300000 200000 100000 0 0 2 4 6 8 10 Core length (cm) Figure 4 : Pressure profiles for the homogeneous (solid or dotted lines) and the heterogeneous core (points) descriptions General workflow for interpretation In this part, the general methodology to account progressively for heterogeneities is described. The general workflow is given in Figure 5 and includes several steps. Determination of the "homogeneous" curves As a "first guess" for the calculation, a first set of curves noted <kr> and <Pc> are determined as if the sample were homogeneous, using standard methods in SCAL. For a multi-rate unsteady-state (USS) experiment, the <kr> and <Pc> curves can be determined analytically using the procedure followed in a semi-dynamic experiment and described in a previous SCA paper (Lombard et al., 2002). The following analytical expressions with full account for capillary effects are used : dS (1) S inlet (∆Pi ) = S + q dq µL dq (2) kr inj = KA d∆Pi The capillary pressure points correspond to the ∆Pi, Sinlet(∆Pi) values because the stabilized pressure drop is measured at the inlet. ∆Pi can be considered as the capillary pressure because the displaced phase is no longer mobile when stabilization state is reached, leading to an uniform profile in this phase. Therefore, the pressure drop that is measured across the sample corresponds to the pressure difference between the injected and the displaced phases at the inlet, which is the definition of the capillary pressure. If there is only one or a limited number of flow rates, the previous method cannot be used (need to calculate the derivative of saturation and pressure versus flow rate). In this case, the capillary pressure must be measured on a separate experiment, and the relative permeability determined from the displacement (JBN + numerical simulation accounting for capillary pressure). SPE 96896 5 Using the homogeneous curves <kr> and <Pc>, a pressure profile is numerically calculated at each step (Figure 5). Step 1: determination of the local Pc(x) In this part the “pressure based” approach is applied by combining the experimental saturation measurements with the simulated pressure profiles at the equilibrium points. This enables derivation of several values of Pc at all locations where a saturation measurement was performed. These calculated values are then used to obtain the local Pc(x) curves for each position. These different Pc(x) curves are introduced as inputs in the simulator in addition to <kr> obtained through the homogeneous approach (Figure 5). This procedure can be repeated several times to improve also the simulated pressure profiles, but our experience shows that one iteration is often enough to considerably improve the match of all the data. This approach results in a very fast calculation since only a direct simulation is involved. Experimental data multi rate injection Analytical interpretation JBN Semi-dynamic method (Pc and kr analytical values) Pc curve on companion plug Homogeneous approach Inputs : Pc, first guess krs Coreflood simulator krs Application case and comparison with conventional measurements In a previous publication, the proposed methodology has been successfully applied to interpret USS experiments conducted on heterogeneous samples with a gas-oil and a water-oil systems (Egermann and Lenormand, 2004). The simulated saturation profiles were in very good agreement with the experimental profiles. The same approach was also adopted for the interpretation of semi-dynamic water/oil experiments performed on carbonate samples from several rock types (Lombard et al, 2004). This section is focused on the comparison between the variability of the Pc data that can be obtained from only one experiment using the proposed approach, and the spreading that can be obtained within the same rock-type from Pc curves obtained on several companion plugs (centrifuge technique). Experimental procedures and results The experiments were conducted at ambient conditions, on carbonate samples cored at several locations and directions in a quarry bloc: one sample for the multi-rate experiment, three plugs for the centrifuge drainage experiments. Their main properties are gathered in Table 2. Table 2. Plug properties Outputs : krs, Psim(x,t) Stabilized Simulated data Gravity is neglected in the above expression. Swexp(x,t) Heterogeneous approach step1 Inputs : Pc(x), homogeneous krs Samples Multi-rate centri 1 centri 2 centri 3 K (mD) 402 528 79 52 Porosity 0.31 0.35 0.29 0.34 Outputs : krs, all data matched Heterogeneous approach step2 Inputs : Pc(x), Transient Swexp(x,t) Output : local kr values Figure 5. General workflow to interpret an USS multi-rate experiment Step 2: determination of the local kr(x) The determination of local kr(x) does not require simulations. The relative permeability of the injected fluid is derived by using Darcy's law and assuming a uniform permeability. When steady-state is reached, the pressure gradient in the injected fluid is equal to the gradient in capillary pressure (derived from step 1): k kw ∂Pc (3) qw = µ w ∂x The relative permeability of the displaced fluid is derived from the transient evolution of the saturation profiles. The displaced phase relative permeability is derived from the general expression of the fractional flow, calculated using the mass balance (Craig, 1993): k kro ∂Pc 1− ut µo ∂x (4) fw = µ w ko 1+ µo k w For the multi-rate experiment, the sample was set in a core holder transparent to X-ray, to enable local saturation measurements with the CT-scanner. The experiment consisted in injecting nitrogen (N2) in the core fully saturated with brine (salinity: 20g/l). N2 was injected at a constant pressure using a pressure regulator. Three steps of injection were considered : 115, 230 and 620 mbar. Pressure was changed from one step to another when no water production was detected at the outlet. The local saturation profiles were measured during the whole experiment to follow the transient evolutions and also to check the stabilization at the end of each step. The three periods of injection can be clearly distinguished on the production data, especially for water production curve (Figure 6). Due to the heterogeneity of the studied sample, the stabilized saturation profiles exhibit large fluctuation (Figure 11). The fluctuation can reach 6-7 saturation units, which is in agreement with other experimental works reported in the litterature (first part of the manuscript, example: Graue, 1994). 6 SPE 96896 18 100000 16 1400 12 10 8 6 Experimental Numerical simulation 4 Pc centri 2 1200 Local Pc: step 1 1000 100 Experimental 10 Numerical simulation 2 0 0 100 200 300 1 400 0 Tim e (m in) 100 200 Tim e (m in) 300 800 600 400 Interpretation of the local Pc values The interpretation of the USS experiment with the heterogeneous approach led to the capillary pressure points plotted in Figure 7. For each pressure, local Pc data were calculated at the equilibrium. The connection between the points calculated from three different stabilized saturation profiles is satisfactory and, thanks to large capillary end effects, a wide range of saturation was investigated (Sw varies from 1 to 0.3) 1000 Local Pc: step 1 Local Pc: step 2 800 Local Pc: step 2 Local Pc: step 3 400 Figure 6 : Production data (gas-water experiment) 900 Pc centri 3 1000 Pc gaz/eau (mb Gaz Production (cm3) Water Production (cm3) Pc centri 1 10000 14 Local Pc: step 3 200 0 0 0.2 0.4 0.6 0.8 1 Sw (fraction) Figure 8 : Comparison between local Pc points and a set of Pc curves from companion plugs Alternative approach using the saturation profile In the above-described method, the pressure profile is numerically calculated using the homogeneous values <kr> and <Pc>. However, when the homogeneous value <Pc> is not known, a determination of local values is still possible using the saturation profile. We will demonstrate this approach using the example described in the previous section. Pc g/w (mba 700 Linear interpolation of the pressure profile The simplest approach consists in a linear interpolation of the pressure between the inlet and outlet of the porous medium (Figure 9). As the capillary end effects are not taken into account with this approach, the local Pc points calculated are not satisfactory, especially at the plateau level (Figure 10). However, this curve can be used as a first guest for iteration. 600 500 400 300 200 100 0 700 0 0.2 0.4 0.6 0.8 1 Sw (fraction) Figure 7 : Local Pc data derived from the USS experiment 500 Pressure (mbar) Comparison with Pc data from companion plugs In Figure 8, the Pc data obtained from the "heterogeneous" interpretation of the USS experiment are compared to the data measured on the three companion plugs using the centrifuge technique. For this comparison, the centrifuge Pc curves were corrected using Leverett function to account for the different permeability and porosity of the samples and for IFT variation. Each centrifuge curve is located in the area delimited by the local Pc points of the USS experiment. The interval of confidence drawn by the three centrifuge curves is comparable to the one obtained from the USS experiment. At ambient conditions, a centrifuge screening on several samples as well as a USS experiment interpreted with the heterogeneous approach can be used to study the variability of Pc-curve within a given rock type. The main advantage of the heterogeneous approach is its possible application for the interpretation of experiments (USS or semi-dynamic) performed at reservoir conditions, using only one sample. step 1 : simulated step 2 : simulated step 3 : simulated step 1 : linear step 2 : linear step 3 : linear 600 400 300 200 100 0 0 10 20 30 40 50 60 70 80 90 Length from the inlet (mm) Figure 9 : Simulated (lines) and extrapolated (dots) stabilized pressure profiles SPE 96896 7 The local capillary pressure are then calculated using these pressure profiles, and the results are very similar to the first approach (Figure 13). The local capillary pressure points can be accurately determined from these profiles and the application of step 2 of the heterogeneous approach leads finally to the local relative permeability values. Consequently this method allows to obtain quickly most of the information on capillary pressure and relative permeability variability. 1000 Pc centri 1 900 Pc centri 2 800 Pc centri 3 Local Pc: step 1 Pc gaz/eau (mb 700 Local Pc: step 2 600 Local Pc: step 3 500 400 300 200 700 100 step 1 : simulated 0 0 0.2 0.4 0.6 0.8 step 2 : simulated 600 1 step 3 : simulated step 1 : calculated Sw (fraction) step 1 : experimental 0.8 step 2 : experimental step 3 : experimental 0.7 step 1 : analytical Sg (fraction 0.6 Pressure (mba Analytical calculation of the pressure profile A more accurate approach consists in using homogeneous saturation profiles <Sw> together with homogeneous <kr> to determine the pressure profiles when steady-state is reached. The first step is the parametrization of the displacing fluid relative permeability, using a standard analytical function (Corey exponent for example). The saturation profiles are also approximated by a smooth function such as: λ ⎛ ⎛ L − x ⎞ ⎞⎟ (5) S g ( x ) = S ginlet ⎜1 − ⎜ exp− ⎟ ⎜ ⎝ H ⎠ ⎟⎠ ⎝ where, Sginlet, L, H and λ are adjusting parameters to be fitted according to the experimental data points. Sginlet nearly corresponds to the gas saturation at the inlet, L is the total core length and the other parameters control the shape of the profile. step 2 : calculated step 3 : calculated 400 300 200 100 0 0 20 40 60 80 100 Length from the inlet (mm) Figure 12 : Comparison between analytical and simulated pressure profiles 1400 Local Pc: step 1 Local Pc: step 2 1200 Local Pc: step 3 Pc centri 1 1000 Pc gaz/eau (mb Figure 10 : Local Pc data with linear interpolation of the pressure – bad agreement especially in the plateau region 500 Pc centri 2 Pc centri 3 800 600 step 2 : analytical step 3 : analytical 0.5 400 0.4 200 0.3 0 0 0.2 0.2 0.4 0.6 0.8 1 Sw (fraction) 0.1 0 0 20 40 60 80 100 Figure 13 : Comparison between local Pc points obtained using the homogeneous saturation profiles and a set of Pc curves from companion plugs Length from the inlet (mm) Figure 11 : Stabilized gas saturation profiles obtained experimentally and with the analytical parametrization Then the pressure profile in the displacing phase is numerically calculated using an explicit scheme since saturation is known. The pressure difference in each grid is derived using either the liquid or gas Darcy's equation. The total profile is then calculated by integrating from the exit where the pressure is known. The result is in good agreement with the profiles calculated by using the homogeneous capillary pressure (Figure 12). Conclusions Within a same rock type, Pc and kr can vary significantly. The study of the influence of heterogeneity on these petrophysical parameters is of primary importance for the estimation of field production. A novel approach was successfully developed and tested to take into account the rock heterogeneities that impact the coreflood experimental data mainly in terms of saturation profiles. The methodology is based on the inclusion of local capillary pressure curves determined analytically by combining experimental saturation profiles obtained during stabilization states and simulated pressure profiles. The 8 SPE 96896 proposed approach takes advantage from previous works on upscaling techniques for reservoir engineering, which showed that pressure distribution is much less affected than saturation distribution by the presence of heterogeneity. Multi-rate injection experiments are recommended to get analytically both Pc and kr data prior to the start of the simulation process. The method enables the reproduction of the saturation fluctuations by calculating analytically the local Pc attributes using the stabilized saturation profiles. The local values of kro can be obtained using the transient profiles between two consecutive rates. The overall method was successfully applied on experimental data related to intermediate permeability carbonate samples (composite or single plug) for a gas/oil system. The interpretation of the local Pc attributes was also successfully applied on several carbonate rock types, for a water/oil system. This method can be used to reinterpret existing experiments that were affected by small-scale heterogeneties. The spreading of the kr, Pc data due to the heterogeneity within a given rock-type can be assessed from only one experiment and can be very helpful to prove the coherency between different experiments performed on different samples, with different methods in a SCAL program. An alternative approach derived of this heterogeneous method and based on the explicite determination of the pressure profiles can also be applied to speed up the interpretation of any multi-rate experiments. in SPE Annual Technical Conference: Proceedings, Washington, DC. 3. Courtial, R., and Ghalimi, S., 2000, Techniques for Relative Permeability Calculations : A Closer Look, SCA 2000-47, in the Society of Core Analysts Symposium: Proceedings, Abu-Dhabi. 4. Craig, F.F. :"The reservoir engineering aspects of waterflooding", Monograph Series, SPE, Richardson, Texas (1993), vol. 3. 5. Dauba, C., Hamon, G., Quintard, M., and Cherblanc, F., 1999, Identification of Parallel Heterogeneities with Miscible Displacement, SCA 9933, in the Society of Core Analysts Symposium: Proceedings, Denver, Colorado. 6. Egermann, P., Robin, M., Lombard, J.-M., Modavi, A., and Kalam, M. Z., 2003, Gas Process Displacement Efficiency Comparisons on a Carbonate Reservoir, SPE 81577 in the SPE Middle East Oil Show: Proceedings, Bahrain. 7. Egermann, P., and Lenormand, R., 2004, A New Methodology to evaluate the impact of local heterogeneity on Petrophysical Parameters (Kr, Pc): Application on Carbonate Rocks, SCA 2004-18, in the Society of Core Analysts Symposium: Proceedings, Abu Dhabi, UAE. 8. Element, D. J., and Goodyear, S. G., 2002, New Coreflood Simulator Based on Independent Treatment of In-Situ Saturation and Pressure Data, SCA 2002-07, in the Society of Core Analysts Symposium: Proceedings, Monterey, CA. 9. Fincham, A., and Gouth, F., 2000, Improvements of Coreflood Design and Interpretation using a New Software, SCA 2000-19, in the Society of Core Analysts Symposium: Proceedings, Abu-Dhabi. Acknowlegments The author acknowledge O. Vizika and F. Kalaydjian for their useful comments and fruitful discussions. Nomenclature A : ∆Pi : fw : K : : kri krinj : L : µi : Pc : Q : : Swi : S : Si : Sinlet ut : lateral core area total pressure drop measured at the inlet watercut absolute permeability relative permeability of phase i relative permeability of the injected phase core length viscosity of phase i capillary pressure flow rate irreducible water saturation average saturation saturation of phase i saturation at the inlet face of the core total fluid velocity (Q/A) References 1. Chardaire-Rivière, C., Chavent, G., Jaffré, J., Liu, J., Bourbiaux, B., 1992, Simultaneous Estimation of Relative Permeabilities and Capillary Pressure, SPE Formation Evaluation, December, p. 283-289. 2. Chardaire-Rivière, C., Forbes, P., Zhang, J. F., Chavent, G., and Lenormand, R., 1992, Improving the Centrifuge Technique by Measuring Local Saturations, SPE 24882, 10. Goodfield, M., Goodyear, S. G., and Townsley, P. H., 2001, New Coreflood Interpretation Method for Relative Permeabilities Based on Direct Processing of In-Situ Saturation Data, SPE 71490 in SPE Annual Technical Conference: Proceedings, New Orleans, LO. 11. Graue, A., 1994, Imaging the Effects of Capillary Heterogeneities on Local Saturation Development in Long Corefloods, SPE Drilling & Completion, March, p. 57-64. 12. Guerillot, D., and Verdière, S., 1995, Different Pressure Grids for Reservoir Simulation in Heterogeneous Reservoirs, SPE 29148 in the 13th SPE Symposium on Reservoir Simulation: Proceedings, San Antonio, TX. 13. Hamon, G., and Roy, C., 2004, Influence of Heterogeneity, Wettability and Coreflood Design on Relative Permeability Curves, SCA 2000-23 in the Society of Core Analysts Symposium: Proceedings, Abu Dhabi. 14. Helset, H.M., Nordtvedt, J.E., Skoeveland, S.M., Virnovsky, G.A., 1998, Relative Permeabilities From Displacement Experiments With Full Account for SPE 96896 Capillary Pressure, SPE Reservoir Engineering, April, p. 92-98. 9 Evaluation & 15. Honarpour, M.M., Cullick, A. S., and Saad, N., 1994, Influence of Small-Scale Rock Laminations on Core Plug Oil/Water Relative Permeability and Capillary Pressure, SPE 27968, in SPE Centennial Petroleum Engineering Symposium: Proceedings, Tulsa, OK. 16. Lombard, J.-M., Egermann, P., and Lenormand, R., 2002, Measurement of Capillary Pressure Curves at Reservoir Conditions, SCA 2002-09, in the Society of Core Analysts Symposium: Proceedings, Monterey, CA. 17. Lombard, J.-M., Egermann, P., and Lenormand, R., Bekri, S., Hajizadeh, M., Hafez, H., Modavi, A., and Kalam, M.Z., 2004, Heterogeneity Study Through Representative Capillary Pressure Measurements - Impact on Reservoir Simulation and Field Predictions, SCA 2004-32, in the Society of Core Analysts Symposium: Proceedings, Abu Dhabi, UAE. 18. Mannseth, T., Mykkeltveit, J., Nordtvedt, J. E., and Sylte, A., 1998, Effects of Rock Heterogeneities on Capillary Pressure and Relative Permeabilities, SPE 50574, in the SPE European Petroleum Conference: Proceedings, The Hague, The Netherlands. 19. Mejia, G.M., Mohanty, K.K., Watson, A.T., 1995, Use of In-Situ Saturation Data in Estimation of Two-Phase Flow Functions in Porous Media, Journal of Petroleum Science and Engineering, vol. 12, p. 233-245. 20. Ruth, D., 1997, Analysis of centrifuge relative permeability data, SCA 9711, in the Society of Core Analysts Symposium: Proceedings, Calgary, Canada. 21. Saad, N., Cullick, A. S., and Honarpour, M. M., 1995, Immiscible Displacement Mechanisms and Scale-up in the Presence of Small-Scale Heterogeneities, SPE 30779, in the SPE Annual Technical Conference: Proceedings, Dallas, TX.. 22. Verdière, S., Guérillot, D., and Thomas, J.-M., 1996, Dual Mesh Method for Multiphase Flows in Heterogeneous Porous Media, in the 5th European Congress on the Mathematical of Oil Recovery: Proceedings, Leoben, Austria. 23. Virnovsky, G. A., Vatne, K. O., Skoeveland, S. M., and Lohne, A., 1998, Implementation of Multirate Technique to Measure Relative Permeabilities Accounting for Capillary Effects, SPE 49321, in the SPE Annual Technical Conference: Proceedings, New Orleans, LO.