1 Introduction This document will describe the experimental apparatus and procedure for conducting material creep testing. The apparatus will use a weight and lever to apply constant tensile load to the sample during testing. The necessary sample loads and forces applied to the test apparatus are estimated based on approximated sample sizes and material properties from similar materials. The first section will discuss the estimation of forces and loads. Then this document will discuss the test apparatus and instrumentation, test specimen specifications and fabrication, and the design of experiments and test procedure. 2 Forces and Loads The test specimens will be thin walled composite tubes with fiber winding angle as close to 90° as possible. The samples will be loaded axially to measure the transverse material properties. The thin samples are estimated to have a wall thickness of 2-3 mm and are constructed from glass fiber reinforced polymer (GFRP). Material properties for a similar GFRP published in literature (Ha et al. 2006) is used to estimate the load that must be applied to the sample, forces on the test apparatus, and possible deformation. Table 1 provides approximate sample sizes and material properties. Estimations will be made with the samples being tested at 40% and 60% of their tensile strength. Table 1: Values for various parameters necessary for stress and strain analysis. Parameter Inner radius Outer radius Length Elastic modulus Transverse tensile strength Value 25.4 mm 27.4 – 28.4 mm 101.6 mm 8.27 GPa 31 MPa Beginning with the stress applied to the sample is 40% or 60% of the tensile strength, 𝜎𝑠𝑎𝑚𝑝 = 12.4E6 MPa, or 18.6E6 MPa (1) Then the force associated with this stress is given by 𝐹𝑠𝑎𝑚𝑝 = 𝜎𝑠𝑎𝑚𝑝 𝐴𝑠𝑎𝑚𝑝 (2) where the sample area is between Alow = 0.331x10-3 m2 and Ahigh = 0.507x10-3 m2. Then the sample load is given in Table 2. Table 2: Creep stress for 40% and 60% load creep testing. Values are given for the lower and upper bound of the cross-sectional area. FSamp(%) 40% Alow 4,113.7 N Ahigh 6,287.5 N 60% 6,170 N 9,431.2 N The load is applied to the sample with the lever arm, connected to part 8 in the assembly, appendix A. Redrawing the lever as a free body diagram yields Figure 1. Figure 1: Free body diagram of the lever arm with applied load, Fapp, load from the sample, Fsamp, and the support load at the fulcrum, Fsup, sitting at an arbitrary angle θ. In this figure the fulcrum is a distance rA and rB from the sample, FSamp, and the applied load, FApp respectively. The fulcrum is a pin type support and therefore restricts movement in the horizontal and vertical directions, and rotations about the vertical, y, or horizontal, x, axis. It can rotate about the out of plane, z, axis. The applied load is caused by gravity and acts vertically, and the sample load is also vertical. Of these only the rotation about the z axis and forces in the vertical direction are non-trivial. Then to produce the desired sample load, the necessary applied load and required support at the fulcrum can be found as a function of the angle of the lever θ. ∑ 𝑀𝑆 = 0 = 𝐹𝐴𝑝𝑝 cos(𝜃) − 𝐹𝑆𝑎𝑚𝑝 cos (𝜃) 𝐹𝑆𝑎𝑚𝑝 𝑟𝐴 𝐹𝐴𝑝𝑝 = 𝑟𝐵 (3) (4) (5) ∑ 𝐹𝑦 = 0 = 𝐹𝑆𝑢𝑝 − 𝐹𝑆𝑎𝑚𝑝 − 𝐹𝐴𝑝𝑝 𝑟𝐴 𝐹𝑆𝑢𝑝 = 𝐹𝑆𝑎𝑚𝑝 (1 + ) (6) 𝑟𝐵 Using equation (2) and the sample load in Table 2, the required load can be applied to the end of the lever. Using the current solid model, available in appendix A, and assuming the total length of the lever is 1 m then 𝑟𝐴 𝑟𝐵 = 0.118. The applied load at the end of the lever, FApp, is given in Table 3 in N and kg. Table 3: Load required at the end of the lever arm to apply the appropriate sample stress. The applied load is given in N and kg for both cross sectional areas FApp(%) 40% 60% Alow 485.4 N 49.5 kg 728.1 N 74.2 kg Ahigh 741.9 N 75.6 kg 1,112.9 N 113.4 kg Based on this analysis the test apparatus must be able to support a load of approximately 𝐹𝑆𝑢𝑝 = 10,544.1 𝑁 (7) At the lever arm fulcrum and 9,431.2 N at the base of sample, part 6. Deformation is estimated using the values in equation (1). The initial deformation is calculated using Hooke’s law and the results are provided in the table below. Table 4: Instantaneous deformation of test samples when the creep load is first applied. FSamp(%) Instantaneous deformation 40% 152.3x10-3 mm 60% 228.5x10-3 mm Based on these results it is reasonable to expect creep deformation to be on the order of 10-5 m. The above analysis will be used to inform the design of the test apparatus and the selection of sensors to ensure subsequent equipment will meet the test requirements. 3 Material Creep Testing 3.1 Design of Experiments Table 5: Treatment combinations table showing all the combinations of creep load and testing temperature. Applied Load 40% YS 60% YS Test Temperature 25 40 65 80 105 25 40 65 80 105 o Blocking 3.2 Test apparatus Technical drawings for the testing apparatus can be found in appendix A. The primary components of the test apparatus are the frame, mounting fixtures, and instrumentation. The frame is constructed from standard sized T-slotted aluminum bars 1.5 inches square and either 1 foot or eight inches long. These are held together with L-brackets. These components are readily available from commercial suppliers such as McMaster-Carr (USA). Instrumentation will be discussed in greater detail in the next section. The lower mounting fixture is a solid steel bar held in place with pipe brackets. The middle of the bar has a coupling which slides inside the test sample tab and is held in place with a 12 mm steel pin. This provides a ridged support structure to hold the sample in place and can be adjusted to line up with the upper fixture ensuring the sample is loaded purely in the axial direction. The cross bar is constructed from solid steel to ensure it is significantly more ridged than the sample to minimize deflection of this part. The upper fixture is constructed from a short steel bar that acts as a coupling between the end of the lever arm and the test sample. Again, these components are constructed from steel to minimize deformation and are held in place with 12 mm steel pins A tensile load sensor added to the test apparatus to replace part 7 to continuously record the creep load on the test specimen. The strain gauge will be surface mounted to the specimen using an epoxy adhesive. A silicone heater will then be wrapped around the sample and set to the appropriate temperature. Electrical leads from these sensors then run to controllers then computer to be recorded. These sensors are discussed in greater detail in the following sections. 3.3 Instrumentation 3.3.1 Heater The heating elements necessary for elevated temperature testing will be required to maintain temperatures from 25°C to 120°C for between 1 and 12 hours depending on the specific experimental requirements. The heating elements will also have to wrap around the cylindrical shaped samples and provide uniform heating of the sample. The silicone rubber strip heater, part number STR001, is an example of an appropriate heater is produced by Wattco Inc. (Lachine, Quebec, Canada). This type of heater has a maximum rated operating temperature of 200°C, rated input voltage of 120V, and a built in adjustable thermostat. The heater is available in a strip 5” wide and 12” long, appropriately sized for the test samples, with Velcro attachments on the short edge to facilitate application to the samples. When contacted the company made clear that this heater will be able to maintain the set temperature within 1°C as required. As a premanufactured component this heater would easily integrate into the test apparatus. Cost: Quantity 1 = ~400CAD, 10 = 186CAD/unit Commented [MS1]: Will have to change for a less expensive load sensor. New sensor Omega LCM111-1k 3.3.2 Strain gauge 3.3.3 Load sensor Omega LCM111-1k: • • • • S type load sensor will be placed under the sample, replacing part 6. Fixed between two plate. Sample applies tensile load to top plate, sensor records load. 3” x 2” x 1” Compatible Meters: DP41-S, DP25B-S Sensor: ~525CAD, Meter: DP25-S = ~425CAD 3.3.4 Data Acquisition 3.4 Sample Fabrication 3.4.1 Shape and dimensions 3.4.2 Filament winding 3.4.3 Cutting/post processing/documentation 3.5 Test procedure To begin an experiment 1. 2. 3. 4. 5. 6. 7. 8. Install sample Connect strain gauges and load sensors Calibrate sensors Set temperature and begin heating Check sensors are functioning properly, reached correct temperature Begin recording Apply load Begin timer After completion 1. Remove load and turn off heat 2. Stop data recording 3. Remove sample from apparatus