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Filtration

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Filtration
Filtration is a process used to separate solids from liquids or gases using a filter medium
that allows the fluid to pass, but not the solid. The term "filtration" applies whether the
filter is mechanical, biological, or physical. The fluid that passes through the filter is
called the filtrate. The filter medium may be a surface filter, which is a solid that traps
solid particles, or a depth filter, which is a bed of material that traps the solid.
Filtration is typically an imperfect process. Some fluid remains on the feed side of the
filter or embedded in the filter media and some small solid particulates find their way
through the filter. As a chemistry and engineering technique, there is always some lost
product, whether it's the liquid or solid being collected.
Examples of Filtration
While filtration is an important separation technique in a laboratory, it's also common in
everyday life.
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Brewing coffee involves passing hot water through ground coffee and a filter. The
liquid coffee is the filtrate. Steeping tea is much the same, whether you use a tea
bag (paper filter) or tea ball (usually a metal filter).
The kidneys are an example of a biological filter. Blood is filtered by the
glomerulus. Essential molecules are reabsorbed back into the blood.
Air conditioners and many vacuum cleaners use HEPA filters to remove dust and
pollen from the air.
Many aquariums use filters that contain fibers that capture particulates.
Belt filters recover precious metals during mining.
Water in an aquifer is relatively pure because it has been filtered through sand and
permeable rock in the ground.
Basic priniciple of filtration:
Filtration is a simple technique used to separate solid particles from suspension in a liquid
solution. There are many filtration methods available, but all are based on the same
general principle:
 A heterogenous mixture is poured over a filter membrane.
 The filter membrane has pores of a particular size.
 Particles larger than the pores will be unable to pass through the membrane, so
liquid will easily pass through it.
 The final result of a filtration process is a collection of residue on the filtration
membrane. This residue is therefore effectively separated from the rest of the
mixture that passed through the membrane.
Filtration Methods
There are many different methods of filtration; all aim to attain the separation of
substances. Separation is achieved by some form of interaction between the substance or
objects to be removed and the filter. Which method is used depends largely on whether
the solid is a particulate (suspended) or dissolved in the fluid.
General Filtration: The most basic form of filtration is using gravity to filter a mixture.
The mixture is poured from above onto a filter medium (e.g., filter paper) and gravity
pulls the liquid down. The solid is left on the filter, while the liquid flows below it.
Vacuum Filtration: A Büchner flask and hose are used to pull a vacuum to suck the
fluid through the filter (usually with the aid of gravity). This greatly speeds the separation
and can be used to dry the solid. A related technique uses a pump to form a pressure
difference on both sides of the filter. Pump filters do not need to be vertical because
gravity is not the source of the pressure difference on the sides of the filter.
Cold Filtration: Cold filtration is used to quickly cool a solution, prompting
the formation of small crystals. This is a method used when the solid is
initially dissolved. A common method is to place the container with the solution in an ice
bath prior to filtration.
Hot Filtration: In hot filtration, the solution, filter, and funnel are heated to minimize
crystal formation during filtration. Stemless funnels are useful because there is less
surface area for crystal growth. This method is used when crystals would clog the funnel
or to prevent crystallization of a second component in a mixture.
Sometimes filter aids are used to improve flow through a filter. Examples of filter
aids are silica, diatomaceous earth, perlite, and cellulose. Filter aids may be placed on the
filter prior to filtration or mixed with the liquid. The aids can help prevent clogging of the
filter and can increase porosity of the "cake" or feed into the filter.
Filtration Versus Sieving
A related separation technique is sieving. Sieving refers to use of a single mesh or
perforated layer to retain large particles, while allowing the passage of smaller ones. In
filtration, in contrast, the filter is a lattice or has multiple layers. Fluids follow channels in
the medium to pass through a filter.
Alternatives to Filtration
In some situations, there are better separation methods than filtration. For example, for
very small samples where it's important to collect the filtrate, the filter medium may soak
up too much of the fluid.
Figure : Vacuum filtration by Büchner funnel and flask
Filtration occurs both in nature and in engineered systems; there are biological, geological,
and industrial forms. For example, in animals (including humans), renal
filtration removes wastes from the blood, and in water treatment and sewage treatment,
undesirable constituents are removed by absorption into a biological film grown on or in the
filter medium, as in slow sand filtration.
Filter media
Two main types of filter media are employed in laboratories: a surface filter, a solid
sieve which traps the solid particles, with or without the aid of filter paper (e.g. Büchner
funnel, Belt filter, Rotary vacuum-drum filter, Cross-flow filters, Screen filter); and
a depth filter, a bed of granular material which retains the solid particles as it passes
(e.g. sand filter). The first type allows the solid particles, i.e. the residue, to be collected
intact; the second type does not permit this. However, the second type is less prone to
clogging due to the greater surface area where the particles can be trapped. Also, when
the solid particles are very fine, it is often cheaper and easier to discard the contaminated
granules than to clean the solid sieve.
Filter media can be cleaned by rinsing with solvents or detergents. Alternatively, in
engineering applications, such as swimming pool water treatment plants, they may be
cleaned by backwashing. Self-cleaning screen filters utilize point-of-suction backwashing
to clean the screen without interrupting system flow.
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