SNC 1D0 Identifying Physical and Chemical Changes In this activity, you will observe a number of chemical changes. As you classify these changes, you will identify specific evidence of chemical change. Purpose To collect and use evidence to identify chemical changes Equipment and materials 1. Eye protection 2. 2 test tubes / group 3. Test-tube rack 4. Test-tube stoppers 5. Candle 6. Scoopula 7. Pipette or eye dropper 8. 50 mL beaker of solutions: a. Dilute hydrochloric acid (0.1 M HCl) b. Distilled water c. Dilute sodium hydroxide (0.1M NaOH) d. Potassium iodide solution (saturated) e. Lead nitrate solution (saturated) 9. Magnesium ribbon (Mg) 10. Wooden splint 11. Copper(II) sulphate (CuSO4) 12. Steel wool Procedure 1. Use the data tables provided. You will be required to make your own for the lab report. 2. Put on your eye protection and keep it on for the duration of lab. Part A Change 1 3. Add hydrochloric acid to a test tube to a depth of about 2cm (finger width) 4. Before you add the magnesium ribbon observe and record the properties of both reactants (acid and magnesium). 5. Add two 1cm strips of magnesium ribbon to the test tube. Place stopper on the tube. Check for evidence of change occurring inside test tube. Check the bottom of the test tube with your hand for temperature changes. Record your observations. 6. Place the test tube in a test tube rack and wait 15sec. Change 2 7. Light a wood splint from the candle flame (lit by your teacher) 8. Bring the splint close to the mouth of the test tube. 9. Remove the stopper and hold the burning splint near the mouth of the “acid + magnesium” test tube. Record your observations 10. Dispose of the contents of the test tube into the beaker labelled “waste” on teacher’s desk 11. Rinse the test tube well with tap water Part B Change 3 12. Pour distilled water into a test tube to a depth of about 3cm 13. Before you add copper (II) sulphate observe and record its properties. 14. Add about 2 g of copper (II) sulphate (1 cm of the end of the scoopula) to the test tube. 15. Stopper and invert the test tube several times to mix its contents well. Record your observations Change 4 16. Before you add the steel wool to the above test tube observe and record its properties. 17. Remove the stopper. Add a small ball of steel wool (about the size of an aspirin tablet) to the test tube with the copper (II) sulphate solution.. 18. Stopper the test tube again and mix well 19. Wait 2 minutes and observe. Record your observations Change 5 20. Before you start adding sodium hydroxide to the above test tube observe and record its properties. 21. Remove the stopper. Add about 5 drops of sodium hydroxide to the test tube using the pipette. Observe and record observations. 22. Slowly add drops of hydrochloric acid to the test tube using a pipette. Gently swirl the test tube after every couple of drops. Continue adding drop wise until the solid disappears. Record your observations 23. Before you start adding sodium hydroxide again predict what will happen. Add a few drops of sodium hydroxide again and observe what happens. Record your observations 24. Dispose the contents into the waste beaker 25. Rinse the test tubes well with water. Part C Change 6 26. Obtain 5 ml of potassium iodide and 5 mL of lead nitrate solutions in separate test tubes 27. Examine the potassium iodide and lead nitrate solutions and record your observations 28. Pour 5 mL of potassium iodide into 5 mL of lead nitrate solution 29. Observe what happens 30. Record your observations Discussion questions: (Analysis of Data) 1. List the 5 indicators to watch for as evidence that a chemical reaction has occurred. 2. Define precipitate. In which step(s) did you observe the formation of a precipitate? 3. Define Endothermic and Exothermic. In which step(s) did you observe a change in temperature? Tell if the changes were endothermic or exothermic. 4. In which step(s) did you observe a color change? 5. In which step(s) did you observe the formation of a gas? Name the gas? 6. In which step(s) did you observe formation of light? 7. Where there any physical changes in this lab? If so where did they occur? Lab Report format: 12 font, Times new roman You are to write a lab report with the following sections: Cover page: (Your name, Partners name(s), my name, title, date submitted) 2 marks [C] Introduction: 5 marks [C] Maximum 200 words on physical and chemical changes. Evidence for each. In-text referencing using MLA format. Cite at least 2 references. Purpose: 2 marks [C] 1-2 sentence to explain the purpose of this lab Observation Charts: 10 marks [C] Insert your typed up observation table(s), detailing observations for every change. Discussion Questions. Q #1 3 marks [T/I] Q#2 3 marks [MC] Q#3 3 marks [MC] Q#4 1 mark [MC] Q#5 2 marks [MC] Q#6 1 mark [MC] Q#7 3 marks [MC] Total Lab /35 (refer to rubric for more detail on each section) Identifying Chemical Changes PART A: Change 1 Reactants Possible Observation Tables Properties Reaction Observations Change 2 Hypothesis: ___________________________________________________________ Hydrochloric acid + magnesium Products + flame PART B: Change 3 Reactants Properties Reaction Observations Copper sulphate + water Copper sulphate + iron + sodium hydroxide + hydrochloric acid + sodium hydroxide PART C: Observations Before mixing After mixing potassium iodide + lead nitrate