MITTATEKNIIKAN KESKUS CENTRE FOR METROLOGY AND ACCREDITATION Julkaisu J5/1998 FINNISH NATIONAL STANDARDS LABORATORIES FINMET ANNUAL REPORT 1997 Helsinki 1998 Contents page 1. INTRODUCTION 5 2. NATIONAL MEASUREMENT SERVICE 6 2.1 DEFINITION 6 2.2 NATIONAL MEASUREMENT STANDARDS AND TRACEABILITY OF MEASUREMENTS 6 2.3 ORGANISATION OF THE MEASUREMENT SERVICE 7 2.4 INTERNATIONAL CO-OPERATION 10 3. ACTIVITIES OF THE NATIONAL STANDARDS LABORATORIES IN 1997 11 3.1 CALIBRATIONS 11 3.2 INTERNATIONAL INTERCOMPARISONS 12 3.3 PARTICIPATION IN THE EUROMET-PROJECTS 13 3.4 DEVELOPMENT PROJECTS 15 3.5 CENTRE FOR METROLOGY AND ACCREDITATION 17 3.6 VTT AUTOMATION 34 3.7 VTT MANUFACTURING TECHNOLOGY 41 3.8 FINNISH GEODETIC INSTITUTE 45 3.9 TELECOM FINLAND LTD, TELECOM ENGINEERING 52 3.10 HELSINKI UNIVERSITY OF TECHNOLOGY 58 3.11 FINNISH CENTRE FOR RADIATION AND NUCLEAR SAFETY 76 APPENDIX 1. List of FINAS accredited calibration laboratories 5 1. INTRODUCTION The aim in maintaining and developing the National Measurement System is to support the competitiveness of the Finnish industry and the economy, to fulfil the needs of consumers and the society, and to integrate the Finnish metrological infrastructure with the European and international infrastructures. Organisation of the National Measurement Standards System was launched by a Government Decree in 1978, considering especially the growing needs of industrial metrology. National standards were established for most of the basic units and some derived units by the Council of State which appointed a number of public research institutions as National Measurement Centres. In 1994, according to a new Law on Units of Measurement and the National Measurement Standards, the Ministry of Trade and Industry was authorised to decide for which basic and derived SI units National Measurement Standards are realised and maintained. The authority to designate the National Standards Laboratories was delegated to the Centre of Metrology and Accreditation (MIKES). The Finnish Organisation of National Standards Laboratories is called FINMET. This publication contains general information on the Finnish metrological system and a summary of the activities of FINMET in 1997. MIKES Julkaisu J5/1998 Annual Report 1997 6 2. NATIONAL MEASUREMENT SERVICE 2.1 DEFINITION The Finnish National Measurement Service consists of National Standards Laboratories (FINMET) and the calibration laboratories accredited by MIKES. FINMET is responsible for realisation of the SI system units, maintenance and development of the National Standards and the dissemination of the units determined within the National Measurement Standards to standards of lower accuracy. The services provided by the Accredited Calibration Laboratories are normally traceable to the National Measurement Standards maintained by FINMET. 2.2 NATIONAL MEASUREMENT STANDARDS AND TRACEABILITY OF MEASUREMENTS The principal task of the National Measurement Service is to create prerequisites for the traceability of physical measurements. Traceable measurements are generally required in applications for which regulations, standards or agreements specify certain requirements for the verification of measurements. These requirements include verification of measurements in accordance with industrial quality system standards, laboratory standards or the ISO standards. Traceability means a link between the measurement results and the International or National Measurement Standards, obtained through an unbroken chain of comparisons (Fig.1). Measurement standards can be instruments, devices or reference materials that are used to define, realise or maintain the measurement unit of a quantity or its multiples. Primary standards represent the best metrological quality of standards. In practice, they are standards by which the units of measurement are realised according to their internationally accepted definitions. These primary standards are used to disseminate the unit of the measurement to a lower level of accuracy i.e. to the secondary, reference and working standards. SI unit definition National Measurement Standard Measurement standard of an Accredited Calibration Laboratory Reference standard of a laboratory Fig. 1. Traceability chain In practice, the unbroken chain of comparisons is obtained by calibrating the measuring instruments. Calibration means a comparison in which the uncertainty of the instrument to be calibrated is determined using a more precise instrument of known uncertainty. The measurement standards of the basic and derived units of the SI-unit system are the cornerstones of the traceable physical measurements. The traceability chains of the measurement standards of derived units are based, either directly or indirectly, on the MIKES Julkaisu J5/1998 Annual Report 1997 7 measurement standards of the basic units (metre, kilogram, second, ampere, kelvin, candela and mole). All measurement results have a degree of uncertainty, which is an essential factor describing the quality of measurements as well as the quality of a measurement standard. National and international standards belong to the highest degree of accuracy. Accuracy requirements in various routine measurements are totally dependent on the particular measurement applications. 2.3 ORGANISATION OF THE MEASUREMENT SERVICE The Finnish Measurement Service is from its organisational principle similar to the metrological systems in most European industrialised countries (Fig. 2). Its most essential duty is to arrange the traceability chains from the measuring instruments of the end users to the SI unit system. International System of Units (SI) BIPM International Collaboration National Metrology Institutes EUROMET EAL NORMET SMT PTB NPL etc. National Standards Laboratories FINMET Centre for Metrology and Accreditation Accredited Calibration Laboratories Calibration Laboratories of Industry Tracebility Collaboration Fig. 2. Traceability to SI-units and collaboration concerning calibration activities The Centre for Metrology and Accreditation (MIKES), subordinated to the Ministry of Trade and Industry, is the co-ordinating national body of the Measurement Service (Fig. 3). The Finnish National Measurement Standards System, FINMET, is a so called decentralised system, in which a number of research institutes act as National Standards Laboratories. The laboratories are responsible for the maintenance and development of the National Measurement Standards. MIKES designates the National Standards Laboratories included in FINMET and supervises their operations. Financing and international co-operation are also channelled through MIKES. MIKES Julkaisu J5/1998 Annual Report 1997 8 Ministry of Trade and Industry Advisory Commission for Metrology (expert groups) Centre for Metrology and Accreditation FINMET National Standard Laboratories Safety Technology Authority (Legal Metrology) Centre for Metrology and Accreditation (MIKES) Technical Research Centre of Finland (VTT) Finnish Geodetic Institute (FGI) Telecom Finland Oy Tele-Engineering (TELE) Helsinki University of Technology (HUT) Accredited Calibration Laboratories Fig. 3. Organisation of metrology in Finland Finland currently has five National Standards Laboratories: the Technical Research Centre of Finland (VTT), the Finnish Geodetic Institute (FGI), Telecom Finland Ltd (TELE), Helsinki University of Technology (HUT), and MIKES. In accordance with a separate Decree, the Finnish Centre for Radiation and Nuclear Safety (STUK) is responsible for maintaining measurement standards for ionising radiation. The National Standards Laboratories are presented in Fig. 4. A National Standards Laboratory is responsible for the National Measurement Standards of one or more quantities, and they represent the highest level of the traceability chain. The measurement standards may be either primary or secondary standards. In the latter case the traceability is achieved from the foreign (or international) standards laboratories. The National Standards Laboratories are also responsible for the traceability of measurement standards of the Accredited Calibration Laboratories within their range of measurement quantities. In addition, they offer calibration services directly to other clients. The Advisory Committee for Metrology, appointed by the Council of State, acts as an expert body in an advisory capacity. The Committee is divided into three sections: Measurement Service, Verification and Chemical Metrology. In addition, a number of expert working groups operate under these sections. Regarding the Measurement Service Section there are working groups corresponding to various quantity groups i.e. mass, electricity/time, length, temperature, radiometry and photometry, flow and acoustics. MIKES Julkaisu J5/1998 Annual Report 1997 9 FINMET NATIONAL STANDARDS LABORATORIES 1.1.1998 NATIONAL STANDARDS LABORATORY QUANTITIES HEAD OF CALIBRATION LABORATORY e-mail Centre for Metrology and Accreditation POB 239, FIN-00181 Helsinki tel. 358 9 616 761* fax 358 9 6167 467 mass pressure length1 temperature humidity Kari Riski Markku Rantanen Kari Riski Thua Weckström Martti Heinonen kari.riski@mikes.fi markku.rantanen@mikes.fi kari.riski@mikes.fi thua.weckstrom@mikes.fi martti.heinonen@mikes.fi VTT Automation Measurement Technology Metrology Section POB 1304, FIN-02044 VTT tel. 358 9 4561* fax 358 9 456 7029 electric voltage (dc and ac) electric current (dc and ac) electric power (dc and ac) resistance, capacitance time interval, frequency instant of time Aarne Oja aarne.oja@vtt.fi VTT Manufacturing Technology, Production Engineering POB 1702, FIN-02044 VTT tel. 358 9 4561* fax 358 9 460 627 length, angle flatness, straightness roundness, roughness Heikki Lehto heikki.lehto@vtt.fi Finnish Geodetic Institute Geodeetinrinne 2 FIN-02430 Masala tel. 358 9 295 550* fax 358 9 2955 5200 acceleration of free fall geodetic length Jussi Kääriäinen jussi.kaariainen@fgi.fi Telecom Finland Oy Tele-Engineering POB 65, FIN-00211 Helsinki tel. 02040 4475 fax 02040 474 voltage (hf) power (hf) attenuation sound pressure Tuomo Valkeapää tuomo.valkeapaa@tele.fi Helsinki University of Technology High Voltage Institute POB 3000, FIN-02015 HUT tel. 358 9 4511* fax 358 9 451 2395 dc voltage, ac voltage (50 Hz) capacitance (50 Hz), loss factor, inductance (high voltage reactors), lightning impulse voltage, switching impulse voltage other impulse voltages impulse current, impulse energy Martti Aro martti.aro@hut.fi Helsinki University of Technology Metrology Research Institute POB 3000, FIN-02015 HUT tel. 358 9 4511* fax 358 9 460 224 luminous intensity illuminance optical power transmittance, reflectance spectral responsivity optical wavelength Erkki Ikonen erkki.ikonen@hut.fi 1) Lasers, long gauge blocks and line scales Position of Finnish Centre for Radiation and Nuclear Safety is based on the relevant legislation. Finnish Centre for Radiation and Nuclear Safety POB 14, FIN-00881 Helsinki tel. 358 9 759 881* fax 358 9 7598 8450 MIKES Julkaisu J5/1998 exposure (in the air) Hannu Järvinen hannu.jarvinen@stuk.fi air kerma rate absorbed dose (water, soft tissue, on the surface of tissue) dose equivalent (photon-, beta- and neutron radiation) Annual Report 1997 10 Fig. 4. The National Standards Laboratories of Finland The Accredited Calibration Laboratories offer calibration services directly to the end users. The calibration certificates given by them belong to the scope of the multilateral agreement of the co-operation organisation for the Accreditation Bodies of European Laboratories (EAL). The Finnish Accredited Calibration Laboratories are presented in appendix 1. Legal metrology or verification is also closely connected with the field of the National Measurement Service. The primary scope of verification in Finland is focused on the measures and measuring instruments used in commercial transactions. The Safety Technology Authority (TUKES) is the national authority that supervises and controls the field of legal metrology and contributes to the drafting of relevant legislation. 2.4 INTERNATIONAL CO-OPERATION MIKES is responsible of the general international co-operation concerning the Measurement Service and metrology. In addition, the National Standards Laboratories take care of the international connections in their special areas. Intercomparisons of National Measurement Standards of different countries are an essential means of co-operation, through which the international competency and consistence can be shown. The principal forums of co-operation are: CGPM/CIPM/BIPM based on the Metre Convention, EUROMET collaboration between the European National Metrology Institutes, EAL and NORMET co-operation among the Nordic countries. In legal metrology the main organisations are WELMEC, for western European co-operation and OIML, for international co-operation. The EC's Standards, Measurements and Testing Programme (SMT) is also a significant form of collaboration. MIKES Julkaisu J5/1998 Annual Report 1997 11 3. ACTIVITIES OF THE NATIONAL STANDARDS LABORATORIES IN 1997 3.1 CALIBRATIONS Table 1. The number of Accredited Calibration Laboratories and the number of calibration certificates issued by National Standards (NSL) and Accredited Calibration Laboratories (ACL). Certificates (NSL) ACL Certificates -93 -94 -95 -96 -97 Number -95 -96 -97 MIKES (temp.) 213 332 331 250 210 5 MIKES (mass) 225 172 178 174 180 3 1 160 2 276 2 887 63 60 95 126 116 6 31 49 48 1 8 7 5 MIKES (pressure) MIKES (humidity) MIKES (length) VTT MT (dimensional quant.) VTT Automation (electrical quant., time) TELE (sound press., hf electrical quant.) FGI (g and geodetic length) HUT quantities) SUM 773 657 963 788 1 043 10 18 380 500 382 383 452 6 1 035 3 314 3 135 72 76 71 82 52 13 1 213 1 644 1 654 15 36 30 33 32 1 3 51 1 4 1 32 2 (optical HUT (high voltage) STUK (ionising radiation) 519 94 17 34 17 21 76 72 969 1 230 1 220 1 214 1 224 26* 4 700 8 689 9 736 *Some Accredited Calibration Laboratories are operating in several different fields. MIKES Julkaisu J5/1998 Annual Report 1997 12 3.2 INTERNATIONAL INTERCOMPARISONS Table 2. The number of international intercomparisons participated by National Standards Laboratories. The year refers to the publishing date of the final report. Year Year Year Year Year Year Year Year -90 -91 -92 -93 -94 -95 -96 -97 SUM MIKES (temp.) MIKES (mass) 1 MIKES (pressure) 2 3 1 1 1 MIKES (humidity) 1 1 3 6 TELE (sound press., (hf electrical quant.) 2 6 1 3 11 1 1 1 1 4 3 7 1 2 2 2 1 7 5 2 1 1 18 2 GL (g and geodetic length) 1 2 3 VTT MT (dimensional quant.) 6 3 MIKES (length) VTT Automation (electr. quant., time) 1 1 2 1 2 2 6 1 1 7 HUT (optical quantities) 1 1 2 HUT (high voltage) 2 1 3 STUK (ionising radiation) SUM MIKES Julkaisu J5/1998 2 6 14 17 2 2 3 1 1 11 10 9 12 8 12 88 Annual Report 1997 13 3.3 PARTICIPATION IN THE EUROMET-PROJECTS 30 25 20 15 10 All projects AMOS Acoustics Flow Photometry Radiation Thermometry Time Length Electricity 0 Mass 5 Finland's participation Fig. 5. Agreed and proposed projects January/98 12 10 8 6 4 All projects AMOS Acoustics Flow Photometry Radiation Time Length Electricity Mass 0 Thermometry 2 Finland´s participation Fig. 6. Completed projects January/98, Ref. No. >300 MIKES Julkaisu J5/1998 Annual Report 1997 14 Projects LU TR GR IS IE CZ SK PL HU AT PT BE NO ES CH FI SE DK NL IT FR GB DE 120 110 100 90 80 70 60 50 40 30 20 10 0 Projects/GNP Fig. 7. Agreed and proposed projects January/98 30 25 20 15 10 Projects LU TR GR IS IE CZ SK PL HU AT PT BE NO ES CH FI SE DK NL FR GB DE 0 IT 5 Projects/GNP Fig. 8. Completed projects January/98, Ref. No. >300 List of country abbreviations: AT BE CH CZ DE DK Austria Belgium Switzerland Czech Republic Germany Denmark MIKES Julkaisu J5/1998 ES FI FR GB GR HU Spain Finland France United Kingdom Greece Hungary IE IS IT LU NL NO Ireland Iceland Italy Luxembourg Netherlands Norway PL PT SE SK TR Poland Portugal Sweden Slovakia Turkey Annual Report 1997 15 3.4 DEVELOPMENT PROJECTS Table 3. Development and maintenance projects in 1997. The table does not include the projects of the Finnish Geodetic Institute and the Finnish Centre for Radiation and Nuclear Safety and the maintenance costs of MIKES’ own national standards. ELECTRICITY VTT Aut: Development of Electricity Quantities VTT Aut: Measurement System for Common View Time Comparison According to the BIPM Protocol VTT Aut: Development of a 10 V Josephson Standard for the Maintenance of DC Voltage VTT Aut: Automatisation of Maintenance Measurements of Resistance of DC Voltage VTT Aut: Development of a Micromechanical Sensor for Measuring the RMS Voltage of a 50 Hz High-Voltage Power Line VTT Aut: Maintenance Project VTT Aut Total: 32,0 % HUT HVI: HUT HVI: Tele Eng: Tele Eng: Tele Eng: Research and Development of National Standard and Calibration Systems for High Voltage Measurements Maintenance Project (high voltage) HUT HVI Total: 8,1 % MT: MT: MT: MT: OPTICS HUT MRI: HUT MRI: HUT MRI: HUT MRI: HUT MRI: HUT MRI: HUT MRI: 90 1258 3350 180 1258 4440 238 850 315 1285 7,6 % 47,7 % 115 400 275 790 4990 165 620 480 1265 6990 5,3 % 350 200 550 635 425 1060 1,6 % 54 110 164 54 245 299 11,5 % 18,3 % 300 200 300 400 1200 1914 385 309 372 448 1514 2873 Development of a Detector Based Standards for Optical Quantities Dev. of Measurement Systems for Linearity and Spatial Responsivity of Detectors Dev. of Standards for Optical Wavelength and Laser Sources as Nordic Co-operation Development of a Calibration System for Low-Level-Light Measurements Development of Aperture Area Measurement Purchase of a Specroradiometer Maintenance Project (optical quantities) Optics Total: 15,2 % 320 230 175 125 225 115 400 1590 595 328 309 181 240 169 905 2727 Development of Attenuation Reference Standard Device Investments of High Frequency Maintenance Project (high frequency) Development of the Stabilised Lasers *) Development of a Refractometer *) Maintenance Project (coordinate measuring machines) Comparison of Finnish Coordinate Measuring Machines TUT Total: VTT VTT VTT VTT 84 300 469 970 MIKES Total: TUT (ACL): TUT (ACL): 73 262 455 612 Tele Eng. Total: Electricity Total: LENGTH MIKES: MIKES: FIM 1000 MIKES’ Total funding costs 1212 2149 Development of the Instrumentation for Calibr. of Expansion Coefficients Development of a Calibr. of 3-Point Mikrometers Development of a Calibr. Device for Perpendicularity Maintenance Project (dimensional quantities) VTT MT Total: Length Total: MIKES Julkaisu J5/1998 Annual Report 1997 16 MASS MIKES: MIKES: MIKES: Development of the National Standard Lab. for Mass *) Investigation of Mass Comparators Development of the National Standard Lab. for Pressure *) 5,6 % 280 110 200 590 644 240 500 1384 4,3 % 9,9 % 370 80 450 1040 853 161 1014 2398 6,5 % 230 80 370 680 335 80 425 840 Acoustics Total: 1,3 % 30 110 140 30 130 160 Flow Total: 0,7 % 76 76 126 126 Total: 0,3 % 29 29 10459 16143 MIKES Total: Raute (ACL): Raute (ACL): Maintenance Project (force measurements) Intercomparison of Torque Measurements with PTB Raute Total: Mass Total: TEMPERATURE MIKES: New ITS-90 fixed point cells *) MIKES: New Equipment for Thermocouple Calibration MIKES: Improvement of the Calibr. of Infrared Thermometers *) Temperature Total: ACOUSTICS Tele Eng: Organising of EUROMET meeting Tele Eng: Maintenance Project (sound pressure) FLOW IVO (ACL): Intercomparison with NEL SUPPORT TO ACLS WHICH OPERATE WITHOUT SERVICES OF NSL TOTAL: *) Financed from MIKES' operating costs budget MIKES Julkaisu J5/1998 Annual Report 1997 17 MIKES MASS 3.5 CENTRE FOR METROLOGY AND ACCREDITATION, MASS LABORATORY 1. NAME OF THE NATIONAL STANDARDS LABORATORY Centre for Metrology and Accreditation, Mass laboratory 2. QUANTITIES Mass 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 180 3.2 Number of accredited calibration laboratories 3 3.3 Number of official calibration certificates given by accredited calibration laboratories 2887 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) Pt-Ir prototype kilogram No 23. The mass scale in the range 1 mg - 10 kg has been established. 4.2 Maintenance The secondary kilogram standards of MIKES have been calibrated against the Pt-Ir prototype (National standard). No significant changes in the masses of the secondary kilograms were observed. 4.3 Development projects Development of a weight handler for weights up to 5 g. The design of the handler has been completed. The handler has 10 positions for weights. Weights of different shapes (cylindrical weights, plate weights, wire weights) can be measured. MIKES Julkaisu J5/1998 Annual Report 1997 18 MIKES MASS Investigation of mass comparators. Tests of the linearity of mass scales and the temperature gradients inside the weighing chambers of mass comparators at MIKES have been started. Preliminary results show that the nonlinearity of the mass scale is usually insignificant. Weight handler for the 1 kg mass comparator. A new weight handler for the 1 kg mass comparator have been installed and tested. The temperature rise due to the handler is less than 0,1 K. The standard deviation of the comparator with the new handler is less than 2 µg. Mass comparator for 20 kg and 10 kg weights. A new 20 kg mass comparator with a weight handler for four weights has been installed and tested. The standard deviation of the comparator is usually less than 0,2 mg. Test procedures for weights. Development of test methods and procedures for weights has been completed. The result will be published as a supplement to OIML R111. SP, DFM, JV, OIML. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories There has been two intercomparisons organised by EAL: Ma1 comparisons of mass standards (one accredited laboratory from Finland) and Ma3 calibration of two balances based on circulated data (three laboratories from Finland). 4.4.3 International comparisons Euromet project 324: Intercomparison of the volume magnetic susceptibility and magnetisation of two cylindrical weights (DE, NO, FI, FR, IT, BIPM, ES, GB, CH). There was a relatively good agreement between the results from different laboratories including MIKES. EAL comparison Ma1: Comparison of mass and density of weights (100 g, 50 g, 1 g, 500 mg, 10 mg and 1 mg). The reference laboratory was PTB. All En values were less than 1. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES MIKES Julkaisu J5/1998 Annual Report 1997 19 MIKES MASS 5.1 Publications 5.2 Conferences H. Kajastie, K. Riski and H. Rossi, ”A weight handler for a 2 kg mass comparator”, Proceedings of the XIV IMEKO World Congress, IMEKO, vol. 3, 53-58 (1997). H. Kajastie and K. Riski, ”Automatic weight handlers for mass comparators”, Proceedings of Weighing and Measurement in the Year 2000 Conference, 16 - 17 September 1997. Sheffield, UK, 67-74 (1997). 5.3 Reports 5.4 Lectures K. Riski: Laboratoriolaitteiden kalibrointi ja kunnossapito: Punnukset, vaa’at ja dimensiomittaukset AEL-INSKO, 7 April and 8 December 1997, (in Finnish). H. Kajastie: A weight handler for a 2 kg mass comparator, The XIV IMEKO World Congress, 1 - 6 June 1997, Tampere, Finland. H. Kajastie: Automatic weight handlers for mass comparators, International Conference of Weighing and Measurement in the Year 2000, 16 - 17 September 1997, Sheffield, UK. 5.5 Other activities K. Riski has participated to the EUROMET Contact Person Meeting February 6 - 7 1997, NMi VSL, Delft, The Netherlands. H. Kajastie participated International Conference of Weighing and Measurement in the Year 2000, 16 - 17 September 1997, Sheffield, UK. H. Kajastie and K. Riski participated The XIV IMEKO World Congress, 1 - 6 June 1997, Tampere, Finland. K. Riski has participated to the meetings of EAL Task Force for measurement uncertainty (Revision of WECC Doc. 19-1990). The following persons have visited the laboratory: Markus Beeler, Mettler-Toledo AG, 4 June 1997, Leslie Pendrill, SP, Sweden, 20 November 1997. The following visits by the laboratory personal have been made: K. Riski has visited VSL NMi, Delft, 6 - 7 February 1997, H. Kajastie has visited South Yorkshire Trading Standards Units, Sheffield, 18 September 1997. MIKES Julkaisu J5/1998 Annual Report 1997 20 MIKES LENGTH CENTRE FOR METROLOGY AND ACCREDITATION, LENGTH LABORATORY 1. NAME OF THE NATIONAL STANDARDS LABORATORY Centre for Metrology and Accreditation, Length laboratory 2. QUANTITIES Length 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 5 3.2 Number of accredited calibration laboratories 3.3 Number of official calibration certificates given by accredited calibration laboratories 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) The Finnish primary standard for length is realised according to the recommendations given by CGPM and CIPM, by three iodine stabilised 633 nm helium-neon lasers. The expanded uncertainty of the realisation is 5·10-11. These lasers form the basis for traceable length measurements in Finland. 4.2 Maintenance Three iodine stabilised lasers at 633 nm have been maintained in the qualified conditions. The correct operation of the lasers is ensured by regular participation in international comparisons. Interferometers for calibration of long gauge blocks and line scales have been maintained in operation condition. MIKES Julkaisu J5/1998 Annual Report 1997 21 MIKES LENGTH 4.3 Development projects Development of iodine stabilised lasers. An iodine stabilised 543 nm He-Ne laser has been successfully constructed. The frequency of the laser has been stabilised on the hyperfine absorption components of iodine molecular transitions 26-0, R(12) and 28-0, R(106) at 543 nm. This project is a co-operation between MIKES and Helsinki University of Technology (HUT). Development of an air refractometer. An interferometric variable vacuum length refractometer has been constructed. The testing and finishing of the software of the device is still in progress. This project is a co-operation between MIKES and HUT. Development of an iodine stabilised diode laser at 633 nm. A compact diode laser system has been stabilised to the Doppler-free spectrum of molecular iodine at the He-Ne laser wavelength of 633 nm. Single frequency operation and wavelength control of the diode laser in a compact form is obtained by employing weak optical feedback from an integrated microlens. This project is a co-operation between MIKES and HUT. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories 4.4.3 International comparisons Intercomparison of non-metallic gauge blocks (100 mm) and line scales (50 mm and 200 mm) between MIKES and VNIIM was concluded. The results of two gauge blocks and two line scales agreed within standard uncertainties of comparison. Poor graduation line quality was found to be a limiting factor of good agreement of results of two other line scales. The frequency of the iodine stabilised 633 nm He-Ne laser no: 3 was compared with the BIPM reference standard laser in January 1997. The measured relative difference was 1,4·10-13 at the noise floor. It was one of the best results reported in the international comparisons. Euromet project 299: Intercomparison of iodine stabilised He-Ne lasers at 633 nm was concluded, (participants BIPM, MIKES, SP, DFM). This comparison showed the continuos progress made by the laboratories in their realisation of the metre. MIKES Julkaisu J5/1998 Annual Report 1997 22 MIKES LENGTH Euromet project 450: Interferometric measurement of long gauge blocks was carried out, (participants SP, MIKES). The results of two gauge blocks (400 mm and 800 mm) agreed within standard uncertainties of the comparison. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications J. Hu, T. Ahola, E. Ikonen and K. Riski, Frequency shifts of iodine stabilized He-Ne lasers at higher harmonic order stabilization, IEEE trans. Instrum. Meas. 46 (1997) 186-190. A. Lassila, National standards for dimensional and optical quantities, Thesis for the degree of Doctor of Technology, HUT 1997. A. Lassila, P. Toivanen and E. Ikonen, An optical method for direct determination of the radiometric aperture area at high accuracy, Measurement Science and Technology 8 (1997) 973-977. B. Ståhlberg, E. Ikonen, J. Haldin, J. Hu, T. Ahola, K. Riski, l. Pendrill, U. Kärn, J. Henningsen, H. Simonsen, A. Chartier and J.-M. Chartier, International comparison of HeNe lasers stabilized with 127I2 at λ=633 nm, Metrologia, 34 (1997) 301-307. 5.2 Conferences A. Lassila, K. Riski, L. Abramova, E. Latysheva and V. Bolonin, Intercomparison of line scale and gauge block calibrations with ceramic and glass standards, in: J. Halttunen (ed.), Proceedings of the XIV IMEKO World Congress, Tampere, Finland 1997 Vol. 8, 123-128. A. Lassila, J. Hu and K. Riski, The facilities for calibration of gauge blocks and line scales at MIKES, In: Proceedings of Måleteknik & Kalibrering, Nyborg, Denmark 1997. E. Ikonen, A. Lassila and P. Toivanen, A new optical method for high-accuracy determination of aperture area, poster in Newrad’97, Tucson, Arizona 1997. 5.3 Reports Pituuden mittauslaitteiden kalibrointitoiminnan järjestäminen, Mittatekniikan keskus, julkaisu J3/1997. Pituusmittauksen mittausepävarmuuden laskentaohje, Mittatekniikan keskus, julkaisu J12/1997. P. Tallgren, Interferometrinen ilman taitekertoimen mittauslaite, thesis for the degree of Master of Science, HUT 1997. 5.4 Lectures MIKES Julkaisu J5/1998 Annual Report 1997 23 MIKES LENGTH 5.5 Other activities K. Riski is a member of the program committee of ”Technical Conference on Recent Developments in Optical Gauge Block Metrology” at SPIE annual meeting 1998. Advisory Commission for Metrology, length expert group, K. Riski and A. Lassila (members). K. Riski and J. Hu visited BIPM, Paris, France, January 13 - 17, 1997. J. Hu visited National Institute of Metrology, Beijing , China, July 10, 1997. Antti Lassila attended to Euromet contact persons’ meeting (Length), IPQ, Portugal, November 3 - 4, 1997. Director T. Quinn, BIPM, visited length laboratory March 10, 1997. Dr. Xu Yi, National Institute of Metrology, China, visited length laboratory June 10, 1997. Dr. L. Pendrill, SP, visited length laboratory November 20, 1997. Prof. M. Downs, NPL, visited length laboratory December 4, 1997. MIKES Julkaisu J5/1998 Annual Report 1997 24 MIKES PRESSURE CENTRE FOR METROLOGY AND ACCREDITATION, PRESSURE LABORATORY 1. NAME OF THE NATIONAL STANDARDS LABORATORY Centre for Metrology and Accreditation, Pressure laboratory 2. QUANTITIES Pressure 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 116 3.2 Number of accredited calibration laboratories 6 3.3 Number of official calibration certificates given by accredited calibration laboratories 1043 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) In the range 1 kPa … 500 MPa the unit of pressure is realised using a set of pressure balances. The effective areas are traceable to LNE, France, completed with dimensional measurements of VTT Manufacturing Technology for one piston/cylinder unit in the range 20 kPa … 1 MPa. In the low absolute pressure range 0,2 Pa to 1 kPa capacitive transducers are used. They are traceable to FFA, Sweden. 4.2 Maintenance In 1997, three piston/cylinder units were calibrated at LNE, the units for ranges 0,5 … 50 MPa and 2 … 200 MPa, oil pressure, and the unit for the range 20 kPa … 1 MPa, gas pressure. Capacitive absolute pressure transducers for ranges 0 … 130 Pa and 0 … 1300 Pa were calibrated at FFA in June 1997. 4.3 Development projects MIKES Julkaisu J5/1998 Annual Report 1997 25 MIKES PRESSURE Improvement of calibration facilities for low absolute and differential pressures. In 1997, a second pressure balance with a 35 mm diameter piston cylinder unit was taken in operation. It is now possible to calibrate differential pressure transducers between the two pressure balances, and differential pressure transducers can be used for absolute pressure by using very low vacuum as reference pressure. For measurements in the low vacuum range a spinning rotor-type instrument was purchased. The data logging programs, however, are still under development. Determination of the pressure balance effective area based on dimensional measurements. The effective area of the new ceramic 35 mm diameter piston/cylinder unit was determined based on dimensional measurements made by VTT Manufacturing technology. This result was completed with the results of our own pressure measurements and with the results of pressure measurements at NMi, the Netherlands. In 1998, both pressure and dimensional measurements on this unit will be performed at CMI, the Czech Republic. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories An intercomparison in the gauge pressure range 0,5 … 12 MPa was arranged. There were five participants in this intercomparison. The same transfer standard and similar measurement instructions were used even in an intercomparison in Sweden, and a joint meeting on the results was arranged in October for the Finnish and Swedish participants. 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories There was one EAL-pressure intercomparison going on in 1997, EAL Pr-6 for differential pressure range 0 … 1,25 kPa. One Finnish laboratory is participating, but it made its measurements already in 1996. 4.4.3 International comparisons In 1997 three final reports were published on earlier intercomparisons, participated by MIKES: EUROMET Project No. 45. Final Report. EUROMET intercomparison in the pressure range 50 - 500 MPa. BNM-LNE, May 1997. The other participants in EUROMET No. 45 were BEV/AT, FI/DK, CEM/ES, LNE/FR, NMi/NL and FFA/SE. EUROMET Project No. 305. Final Report. EUROMET intercomparison in the gas pressure range 0,5 to 5 MPa. PTB 1997. In EUROMET No. 305 the following MIKES Julkaisu J5/1998 Annual Report 1997 26 MIKES PRESSURE laboratories were participating: BEV/AT, MIKES/FI, PTB/DE, CEM/ES, LNE/FR and FFA/SE. Perkin, M. P.: A comparison of low differential pressure standards in the range 3 Pa to 1000 Pa. NPL Report CMAM 3, August 1997. In the low differential pressure intercomparison there were eleven participants from 8 countries. The results of MIKES were within the claimed uncertainty limits in all these three intercomparisons. As to the on-going intercomparisons, the measurements in EUROMET No. 389 (oil pressures up to 100 MPa) were made in July 1997, and an intercomparison in the gas pressure range 0,05 MPa to 0,35 MPa between CMI/CZ, MIKES/FI and NMi/NL was started during Summer 1997. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications 5.2 Conferences 5.3 Reports M. Rantanen: Paineen vertailumittaus P11. Ylipainealue 0,5 … 12 MPa. Mittatekniikan keskus. Julkaisu J16/1997. M. P. Perkin: A comparison of low differential pressure standards in the range 3 Pa to 1000 Pa. NPL Report CMAM 3 1997. 5.4 Lectures M. Rantanen: Painemittareiden kalibrointi. AEL-INSKOn kurssi Kalibrointi - tarve ja suoritus käytännössä. 18 April 1997, Helsinki and 29 October 1997, Vantaa. 5.5 Other activities In addition to EUROMET intercomparisons, MIKES participated in two other EUROMET projects No. 291 on the uncertainty of digital pressure balances and No. 338 on comparison of pressure balance calibration methods. M. Rantanen participated in the EUROMET Mass Contact Persons Meeting in Delft, 6 - 7 February 1997 and in the EAL Pressure Experts Group Meeting at NPL, Teddington, 9 - 10 October 1997. M. Rantanen participated in the EUROMET Vacuum Workshop at NPL, Teddington 8 October 1997. M. Rantanen visited the pressure laboratories of FFA, Stockholm 12 - 13 June 1997, NMi, MIKES Julkaisu J5/1998 Annual Report 1997 27 MIKES PRESSURE Delft 30 June - 4 July 1997 and NPL, Teddington 8 October 1997. Mrs. C. Bergström and her three colleagues from the pressure laboratory of FFA visited MIKES 28 October 1997. M. Rantanen is a secretary in the Expert Group on Mass and Derived Quantities of the Advisory Commission for Metrology in Finland. MIKES Julkaisu J5/1998 Annual Report 1997 28 MIKES TEMPERATURE CENTRE FOR METROLOGY AND ACCREDITATION, THERMOMETRY LABORATORY 1. NAME OF THE NATIONAL STANDARDS LABORATORY Centre for Metrology and Accreditation, Thermometry laboratory 2. QUANTITIES Temperature 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 210 3.2 Number of accredited calibration laboratories 5 3.3 Number of official calibration certificates given by accredited calibration laboratories 963 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) International temperature scale ITS-90. 4.2 Maintenance Nanovoltmeter for thermocouple calibrations. 4.3 Development projects New ITS-90 fixed point cells: In and Ag. The In cell (156,5985 °C) is a new fixed point for the realisation of the ITS-90 at MIKES. Integrating spheres for the measurement of the sizeof-source effect for infrared thermometers. 4.4 Intercomparisons MIKES Julkaisu J5/1998 Annual Report 1997 29 MIKES TEMPERATURE 4.4.1 National intercomparisons for accredited calibration laboratories An intercomparison of calibrating two surface thermometers from 30 °C to 240 °C. The results show that more effort has to be put in, so that the calibration methods for these instruments can be harmonised. 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories The final report of the EAL Th-6 intercomparison (calibration of industrial resistance thermometers) was published. The EAL Th-7 glass thermometers were circulated in Finland. 4.4.3 International comparisons EUROMET 278, an intercomparison of water triple point cells: the results were sent to the CCT meeting. EUROMET 280, an intercomparison of mercury cells: the results were presented at the Beijing conference. The results are also found in the BNM Synthesis report 23.12.1997. The MIKES cell produced a temperature that was 0,00002 °C higher than the value of the circulating cell. The temperature of 7 of the participating cells produced a temperature that was higher than that of the circulating cell, with a maximum deviation of 0,00017 °C, and 7 cells produced a lower temperature, with a maximum deviation of 0,00042 °C. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications 5.2 Conferences T. Weckström and N. Uusipulkamo, Using the LabView Software for Temperature Calibrations, XIV IMEKO World Conference, Tampere, 1 - 6 June, 1997. 5.3 Reports T. Weckström: Lämpötilan vertailumittaus Mittatekniikan keskuksen julkaisu J14/1997. L8, Digitaalilämpömittarin kalibrointi, T. Weckström: Lämpötilan vertailumittaus Mittatekniikan keskuksen julkaisu J15/1997. L9, Pintalämpömittareiden kalibrointi, 5.4 Lectures MIKES Julkaisu J5/1998 Annual Report 1997 30 MIKES TEMPERATURE T. Weckström, Lämpötilojen valvontakurssi, Lappeenrannan kaupungin ympäristövirasto, 13 November 1997. 5.5 Other activities EAL Subgroup Meeting: Temperature indicators, UKAS, Teddington, January 17, 1997. EUROMET Meeting-Thermometry, Forbairt, Dublin, 10 - 12 March 1997. EAL Temperature and Humidity Experts Group Meeting, INTA, Madrid, October 27 and 28, 1997. Pentronic AB, Temperaturmätning på sin spets/2, Västervik 7 - 8 Oktober, 1997. Visitor: Bloembergen, P., NMi, Delft, 5 June 1997. MIKES Julkaisu J5/1998 Annual Report 1997 31 MIKES HUMIDITY CENTRE FOR METROLOGY AND ACCREDITATION, HUMIDITY LABORATORY 1. NAME OF THE NATIONAL STANDARDS LABORATORY Centre for Metrology and Accreditation, Humidity laboratory 2. QUANTITIES Dew-point temperature Relative humidity 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 48 3.2 Number of accredited calibration laboratories 1 3.3 Number of official calibration certificates given by accredited calibration laboratories 18 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) The dew-point temperature scale and the relative humidity scale are realised by using a twotemperature generator system. 4.2 Maintenance The dew-point temperature scale has been investigated by comparing the dew-point generator with a chilled mirror system and with a cooling coil system. 4.3 Development projects Development of a dew-point temperature comparator. A prototype was constructed and initial tests were carried out. Equipment for an improved system were ordered. MIKES Julkaisu J5/1998 Annual Report 1997 32 MIKES HUMIDITY Development of a two-pressure generator for low humidity range. A prototype was constructed and initial tests were carried out. Equipment for an improved system were ordered. Improvement of the dew-point generator and the transfer standard. A new saturator bath was bought and the dew-point hygrometer was transported to the manufacturer. EU/SMT project: The use of a humid air generator as a reference method for measuring humidity. The project was completed. The different methods to generate humid air were found consistent to each other and it was not possible to name any method to be most suitable for realisation of the dew-point temperature scale. The results obtained by eight laboratories agreed very well in the dew-point temperature range above 0°C and below -50°C. The agreement in the range from -50°C to -10°C was not as good as in the high range but a reliable explanation was not found. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories EAL-TH8: Relative humidity, Nordic intercomparison for relative humidity (pilot laboratory). 4.4.3 International comparisons Comparison of the dew-point generators within the European project (see 4.3). The range for the MIKES was from -40°C to +75°C. In the range above 0°C, the results obtained by most of the laboratories were within the uncertainty limits reported by the MIKES (±0.07°C … ±0.09°C). In the low range, the MIKES results agreed well with the results obtained by the CETIAT (France) and the IMGC (Italy). MIKES Julkaisu J5/1998 Annual Report 1997 33 MIKES HUMIDITY 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications 5.2 Conferences M. Heinonen; National basis of traceability in relative humidity measurements, XIV IMEKO World Congress, Tampere 1 - 6 June 1997, vol. XA, pp. 210-215. M. Heinonen; Calibration of a hydrometer by means of hydrostatic weighing, 19th Nordic Conference "Måleteknikk og kalibrering", 23 - 26 November 1997, Nyborg, Denmark. M. Heinonen; Nordic humidity intercomparison, 19th Nordic Conference "Måleteknikk og kalibrering", 23 - 26 November 1997, Nyborg, Denmark. 5.3 Reports M. Heinonen; Validation of The MIKES Primary Dew-point Generator, Julkaisu J1/1997, Centre for Metrology and Accreditation, Helsinki 1997. M. Heinonen; Nordic intercomparison for relative humidity, Julkaisu J8/1997, Centre for Metrology and Accreditation, Helsinki 1997. 5.4 Lectures M. Heinonen; Kosteusmittarien kalibrointi, Kosteuskalibrointikurssi, MIKES 17 - 18 March 1997. M. Heinonen; National basis of traceability in relative humidity measurements, XIV IMEKO World Congress, Tampere, 1 - 6 June 1997. M. Heinonen; EU Project MAT 1 CT 9400 17: Measurements at the MIKES, Final Meeting of the project, INTA, 30 - 31 October 1997, Madrid, Spain. 5.5 Other activities Advisory Commission for Metrology; Expert Group on Temperature Measurements. International Steering Committee for the Third International Symposium on Humidity and Moisture ´98. MIKES Julkaisu J5/1998 Annual Report 1997 34 VTT AUT ELECTRICITY 3.6 VTT AUTOMATION, ELECTRICAL QUANTITIES 1. NAME OF THE NATIONAL STANDARDS LABORATORY VTT Automation 2. QUANTITIES DC voltage and current, resistance, AC voltage and current, electric power and energy, capacitance 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 47 3.2 Number of accredited calibration laboratories 10 3.3 Number of official calibration certificates given by accredited calibration laboratories 1425 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) DC voltage: Weston and Zener standards, Josephson voltage standard. Resistance: resistance standards and quantum-Hall standard. AC voltage: multi-junction and Fluke 540B thermal AC/DC converters. AC current: multi-junction and Fluke 540B thermal AC/DC converter and A40 shunt resistors. Power: HEG power comparator. Capacitance: AndeenHagerling and GenRad capacitance standards. 4.2 Maintenance The measuring place for electric power was moved to a new laboratory. The real-time environmental data of various laboratories were made accessible via local computer network. MIKES Julkaisu J5/1998 Annual Report 1997 35 VTT AUT ELECTRICITY 4.3 Development projects DC voltage: An accurate voltage divider based on mercury batteries was constructed and tested. Upgrade of our Josephson standard up to 10 V level has been started. Resistance: A new superconducting 12 T magnet system was installed. It was used together with our home made cryogenic current comparator for tracing standard resistors in the range 1 W - 100 kW to the quantised Hall resistance at 1.5 K. The measuring range for standard resistors was extended up to 1 TW by a step-up measurement. A new Guildline direct current comparator was taken in use for comparing resistance standards. AC voltage: New range resistors were built to trace AC voltages in the range 300 V - 1000 V and 40 Hz - 1 MHz to multijunction thermal converters. AC current: Step-up measurement of AC current in the range 10 mA 20 A and 40 Hz - 5 kHz using multijunction thermal converters, Fluke shunt resistors, and home made amplifiers. Electric power and energy: Digitised sampling technique was developed for power measurements. A new power source was taken in routine use. Capacitance: New capacitance standards were taken in use. Measurements were made for the EUROMET-345 comparison of 10 pF and 100 pF capacitance standards. Electrolytic conductivity: An instrument was constructed for tracing the electric conductivity of liquids to the units of capacitance and resistance. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories DC-voltage intercomparisons during assessment visits to accredited laboratories. The results are given in assessment reports. A summary of the comparisons is in preparation. Intercomparison of AC voltages S-6 (Report J4/1997, Centre for Metrology and Accreditation). Intercomparison of electric power measurements S-7 (Report J6/1997, Centre for Metrology and Accreditation). 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories EAL-EL24 capacitance intercomparison (the VTT results are reported in the calibration certificate VTT97KM070). EAL-EL25 AC voltage intercomparison (the VTT results are reported in the calibration certificate VTT98KM009). 4.4.3 International comparisons Measurements were made for the EUROMET-345 intercomparison of 10 pF and 100 pF capacitances. MIKES Julkaisu J5/1998 Annual Report 1997 36 VTT AUT ELECTRICITY 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications H. Seppä, A. Satrapinski, “AC Resistance Bridge Based on the Cryogenic Current Comparator”, IEEE Trans. Instrum. Meas., Vol. 46(2), p. 463, 1997. 5.2 Conferences K. Kalliomäki, A. Oja, and A. Satrapinski participated to the XXII Convention on Radio Science held in the University of Oulu in November 1997. The following papers were published in the Proceedings. K. Kalliomäki, “Electrical Metrology in Finland”, Proceedings of XXII Convention on Radio Science, University of Oulu, pp. 11 - 12, 1997. A. Satrapinski, A. Oja and H. Seppä, “Quantum Hall Effect Resistance Standard at VTT”, Proceedings of XXII Convention on Radio Science, University of Oulu, pp. 141 - 142, 1997. This poster was represented also at the Finnish Metrology Day in November 1997. 5.3 Reports A. Satrapinski A. Oja and H. Seppä, “Results of the QHR measurements in April - June 1997”, Report 97R0234-1, VTT Automation, September 1997. A. Satrapinski A. Oja and H. Seppä, “Calibration of 10 kΩ standard resistors by CCC resistance bridge”, Report 97R0235-1, VTT Automation (draft). 5.4 Lectures K. Kalliomäki gave the plenary talk “Electrical Metrology in Finland” at the XXII Convention on Radio Science in the University of Oulu in March 1997. 5.5 Other activities A. Oja was a member of a working group in the development of high-voltage metrology. P. Immonen, T. Mansten and A. Oja contributed to the working group on electric metrology assigned by Centre for Metrology and Accreditation. Dr. Terry Quinn of BIPM visited VTT Automation in March 1997. A. Oja participated to the EUROMET experts meeting on quantum-Hall resistance standards and Josephson voltage standards in Lisbon in April 1997. A. Oja participated to the EUROMET Electricity Contact Persons Meeting at CEM in Madrid in October 1997. MIKES Julkaisu J5/1998 Annual Report 1997 37 VTT AUT ELECTRICITY T. Mansten participated to the EAL Electricity Contact Persons Meeting at CEM in Madrid in October 1997. T. Mansten participated to the EUROMET experts meeting on AC/DC voltage transfer at OFMET in Bern in May 1997. K. Kalliomäki was the chairman of the organising committee of the XXII Convention on Radio Science held at the University of Oulu in March 1997. He was also a co-editor of the proceedings. MIKES Julkaisu J5/1998 Annual Report 1997 38 VTT AUT TIME VTT AUTOMATION, TIME AND FREQUENCY 1. NAME OF THE NATIONAL STANDARDS LABORATORY VTT Automation 2. QUANTITIES Time and frequency 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 5 3.2 Number of accredited calibration laboratories 6 3.3 Number of official calibration certificates given by accredited calibration laboratories 229 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) Time: Cs-clock, 2 GPS receivers, 2 Loran-C clocks (NELS, RNS). Frequency: Cs-clock, two rubidium oscillators. 4.2 Maintenance The measuring place for time and frequency was moved to a new laboratory. The real-time environmental data of the laboratory were made accessible via local computer network. The uncertainty at which the national time can be disseminated through TV frequency is increasing now that analogous links are being replaced by digital ones. MIKES Julkaisu J5/1998 Annual Report 1997 39 VTT AUT TIME 4.3 Development projects Monitoring of a Cs atomic clock for the national time base since January 1997. The measurement of Cs-clocks of Telecom Finland was improved by adding a humidity measurement and comparison to the GPS signal. The time and frequency laboratory and the antenna system were moved. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories During annual inspections of all accredited laboratories a comparison measurement is performed and the result is reported in the assessment statement. 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories 4.4.3 International comparisons A time comparison was carried out with SP using a transportable GPS receiver in November 1996. The final report of the comparison will be written in near future now that SP and BIPM have performed a similar comparison. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications K. Kalliomäki and J. Mannermaa: “TV network signal as a temporary source for navigation”, in the Proceedings of EFTF11. 5.2 Conferences K. Kalliomäki attended to the EFTF11 Conference in Neuchatel, Switzerland, in 1997, where he presented the poster mentioned above. K. Kalliomäki, T. Mansten and A. Rautianen participated to the XXII Convention on Radio Science held in the University of Oulu in November 1997. The following paper was published in the Proceedings: K. Kalliomäki, T. Mansten and A. Rautianen, “The modification of a HP105B frequency standard and its use as a portable frequency reference”, Proceedings of XXII Convention on Radio Science, University of Oulu, pp. 155 - 156, 1997. This poster was represented also at the Finnish Metrology Day in November 1997. MIKES Julkaisu J5/1998 Annual Report 1997 40 VTT AUT TIME 5.3 Reports Monthly reports on the line frequency and of the frame synchronisation phase of the Finnish TV broadcasting company (YLE), the average frequency of the Cs-clocks of TELE, and the phase of the Loran-C signals (RNS & Sylt). Kalevi Kalliomäki, Tapio Mansten ja Anssi Rautianen, “Taajuuden vertailumittauslaitteen HP 105B uudistaminen”, loppuraportti 97R0169, VTT Automaatio, helmikuu 1998, February 1998. 5.4 Lectures 5.5 Other activities K. Kalliomäki attended to the EUROMET time-and-frequency contact persons meeting at Neuchatel, Switzerland, in March 1997. Dr. Terry Quinn of BIPM visited VTT Automation in March 1997. MIKES Julkaisu J5/1998 Annual Report 1997 41 VTT MT 3.7 VTT MANUFACTURING TECHNOLOGY, DIMENSIONAL QUANTITIES 1. NAME OF THE NATIONAL STANDARDS LABORATORY VTT Manufacturing technology 2. QUANTITIES Length, angle, flatness, straightness, roundness, cylindricity and surface roughness 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 452 3.2 Number of accredited calibration laboratories 6 3.3 Number of official calibration certificates given by accredited calibration laboratories 3135 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) Length: HP-Laser-Interferometers and frequency-stabilised lasers (red and green) are calibrated with Ion-stabilised laser. Gauge blocks are calibrated interferometrically with the red and green lasers. Angle: Angle polygons are calibrated with two autocollimators. Autocollimators and the angle options of the Laser-interferometers are calibrated with tangential bar and length measuring instruments. Angle tables are calibrated with polygon and autocollimators using the error separation method. Flatness: Optical flats are calibrated by comparing them to each other and rotating them 90° with natrium light. Surface plates are calibrated with HP Laser -interferometer (angle options) by measuring straightness in three directions. Straightness: MIKES Julkaisu J5/1998 Annual Report 1997 42 VTT MT Straightness normal is calibrated like flats. Roundness: Roundness normal (glass ball, flick standards and the oval standards) is calibrated with the roundness measuring machine (rotating 90°), length measuring instruments and form measuring instruments. The roundness measuring machine is calibrated with the roundness standards and using the laser-interferometer as scale for the sensor. Cylindricity: Cylindricity unit is based to the roundness and straightness measurements. The standards are calibrated by using error separation tectonics. Surface roughness: The surface roughness measuring machine is calibrated with gauge blocks, optical flats, laser-interferometer and PTB roughness standards. 4.2 Maintenance All the standards and measuring machines are calibrated. The rotating table of the angle measuring instrument has been relapped. The spindle and the program of the roundness measuring machine has been changed. 4.3 Development projects Interferometric angle measurements The aim of the VTT/MIKES project is to develop and take in use rotation tables in horizontal and vertical plane where the calibration is based on Laser-interferometer and/or error separation with angle polygons and autocollimator (12/97). Thread measurements The aim of the VTT/MIKES project is to improve the thread measurements scale (M3 - ...) and uncertainty (2/98). 3d-surface roughness measurements The aim of the VTT/MIKES project is to take in use the optical instrumentation for 3D surface roughness measurements (2/98). Step gauge calibration The aim of the VTT/MIKES project is to improve the uncertainty of the calibration of step gauges (<0,5 µm) (5/97). Calibration instructions The aim of the VTT/Industry project is to harmonise the measuring procedures which are used for calibrations of different measuring devices. Co-axiality MIKES Julkaisu J5/1998 Annual Report 1997 43 VTT MT The aim of the VTT/MIKES project is to develop instrumentation and procedures for calibration of optical instruments for co-axiality and straightness measurements (1/98). Lasmet The aim of this project is to improve the accuracy of the measurements done by laserinterferometer in industry VTT/SMT (97-99). Cylindricity The aim of this VTT/MIKES project is to improve the accuracy of the cylindricity and roundness measurements by buying new instrument and developing programs for errorseparation (5/98). 3-point mikrometers The aim of this VTT/MIKES project is to develop an instrument witch which the calibration of the 3-point micrometers can be done (4/98). Dilatometer The aim of this VTT/MIKES project is to develop an instrumentation for measurements of the expansion coefficients of different materials (5/98). Perpendicularity The aim of this VTT/MIKES project is to develop instrumentation for calibration of straight edges both in vertical and horizontal positions (4/98). 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories D2 Calibration of ceramic gauge blocks. Final report. D4 Calibration of the capasitive length measuring instrument (25 mm). Final report. D3 Calibration of the extensometer. Measurements and corrective actions. 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories M19 Screw thread metrology. Reporting and corrective actions. M20 Micrometer and dial indicator. Besides of the accredited laboratories some candidates or other industrial laboratories measured the length measuring instruments. 4.4.3 International comparisons Nordic intercomparison of gauge blocks including surface roughness measurements MIKES Julkaisu J5/1998 Annual Report 1997 44 VTT MT (optical and mechanical). Final results will be published 1998 as an EUROMET report. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications 5.2 Conferences Mittaukset konepajassa -seminaari ”suurten kappaleitten mittaus” Kirkkonummi 18 - 19 September 1997. 5.3 Reports Heikki Lehto, Interferometrinen kulman mittaus. Final report of the project (12/97). Tero Autio, Porrasmittapalojen kalibroinnin kehitys. Final report of the project (5/97). Heikki Lehto, Mittausepävarmuuden määrittäminen sekä optimoidut kalibrointijaksot. ISO 9000 ja kalibroinnit. Helsinki, (11/97). Mittatekniikan keskus, 8 p. Heikki Lehto, Mittausepävarmuuden määrittäminen ja Puolustusvoimat, Lievestuore (10/97), 12 p. vertailumittaukset, Suomen Heikki Lehto, Kulmamittalaitteiden kalibrointi. Mittaukset konepajassa, Kirkkonummi (9/97), 8 p. 5.4 Lectures 5.5 Other activities Euromet: The meeting of Expert Group ”Dimensional Metrology” in Lissbon (1 - 4 November 1997). EAL: The meeting of Expert Group ”Dimensional Metrology” in Bern (7 - 9 April 1997). Other Groups for co-operation: IMEKO, SLY, SFS, AEL, MIKES. Visitors from industry and metrology laboratories from Finland and different foreign countries (during the IMEKO conference and in several other events). MIKES Julkaisu J5/1998 Annual Report 1997 45 FGI g 3.8 FINNISH GEODETIC INSTITUTE, ACCELERATION OF FREE FALL 1. NAME OF THE NATIONAL STANDARDS LABORATORY Finnish Geodetic Institute 2. QUANTITIES Acceleration of free fall 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 3.2 Number of accredited calibration laboratories 3.3 Number of official calibration certificates given by accredited calibration laboratories 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) Absolute gravimeter The Finnish Geodetic Institute has two absolute gravity meters, JILAg-1 and JILAg-5 based on the free falling corner cube in the vacuum chamber. 4.2 Maintenance 4.2.1 The absolute gravimeter JILAg-5 has been used in Metsähovi laboratory on 27 - 30 January, 20 - 21 February, 5 - 7 March, 24 - 26 March, 7 - 9 April, 24 - 25 April, 8 9 May, 25 - 27 June, 15 - 18 July, 12 - 15 August, 18 - 20 August, 20 - 22 August and 30 October - 1 November. 4.2.2 The frequency of the two mode laser (Laseangle RB-1 no 18) of JILAg-5 was compared with the meter-laser of the Helsinki University in the Kumpula acceleration laboratory on 23 January, 6 May, 2 July and 11 November. The comparison was MIKES Julkaisu J5/1998 Annual Report 1997 46 FGI g made also on 25 November in BIPM when also the distribution of the intensity was found to be a gaussian one. The rubidium frequency standard (Efratom FRK-L no. 8533) of the JILAg-5 was compared with the hydrogen maser oscillator of the Helsinki University of Technology on 27 January, 8 - 9 May, 5 - 26 July, 16 November and with cesium beam in BIPM on 23 November. 4.2.3. JILAg-5 instrument was also used to determine the gravity difference of the new calibration line Masala-Vihti. The observations were made on 8 - 10 September in Vihti and on 23 - 27 September in Masala. The gravity difference was found to be 53.18 mGal. This new calibration line provides the determination and control for the scale of the relative gravimeters in this gravity difference range. 4.2.4 The superconducting gravimeter SG20 has recorded the variations in gravity at the Metsähovi station properly throughout the year. This gravimeter has been calibrated with the JILAg-5 instrument. 4.2.5 Absolute gravity is measured at the following stations abroad: Strassbourg, France Membach, Belgium Clausthal, Germany Sao Miguel, Azorit, Portugal Flores, Azorit, Portugal Faial, Azorit, Portugal Madrid, Spain Valle de los Caidos, Spain Reykjavik, Iceland Höfn, Iceland 5 - 8 February, 11 - 12 February, 15 - 16 February, 22 - 25 May, 31 May - 1 June, 6 - 8 June, 14 - 15 June, 17 - 18 June, 7 - 8 December, 10 - 13 December. The stations in Iceland are new, on the other sites Finnish Geodetic Institute has measured the absolute gravity earlier and the repeated measurements are due to the investigation of gravity variations. Station Clausthal is also the German reference for gravity. 4.2.6 By relative measurements altogether 928 new gravity points are measured and the new Bouguer-anomaly map of the Finland is published. 4.3 Development projects MIKES Julkaisu J5/1998 Annual Report 1997 47 FGI g 4.4 Intercomparisons Finnish Geodetic Institute participated in key comparison ICAG97 for absolute gravimeters in BIPM, Sevres during 16 - 26 November. The participating instrument was the absolute gravimeter JILAg-5. 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories 4.4.3 International comparisons 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications J. Kääriäinen and J. Mäkinen (1997): The 1979-1996 Gravity Survey and Results of the Gravity Survey of Finland 1945 - 1996. Publ. Finn. Geod. Inst. 125. Kirkkonummi. J. Kääriäinen and H. Virtanen (1997a): The Finnish Superconducting Gravimeter: Some Results Related to Earth Deformation. Proceedings of IAG regional Symposium on Deformations and Crustal Movement Investigations using Geodetic Techniques. August 31 September 5, 1996 , Szekesfehervar, Hungary. J. Kääriäinen and H. Virtanen (1997b): Eräistä suprajohtavalla gravimetrillä havaituista ilmiöistä. XVIII Geofysiikan päivät. 13 - 14 May 1997, Helsinki. H. Virtanen and J. Kääriäinen (1997): The GWR T020 Superconducting gravimeter 1994 1996 at the Metsähovi station, Finland. Rep. Finn. Geod. Inst. 97:4. H. Virtanen (1997): Observations of free oscillations of the Earth by superconducting gravimeter GWR T020. Acta Geod. Geoph. Mont. Hung. Vol. 31 p. 423. 5.2 Conferences Jaakko Mäkinen: Workshop ”Techniques in and applications of modern gravimetry” 19 November at the BIPM, France. 5.3 Reports MIKES Julkaisu J5/1998 Annual Report 1997 48 FGI g M. Amalvict, J. Hinderer, O. Francis, J. Mäkinen: Comparisons between absolute (AG) and superconducting (SG) gravimeters. Scientific Assembly of the IAG, September 3 - 9, Rio de Janeiro 1997. J. Hinderer, M. Amalvict, O. Francis, J. Mäkinen: On the Calibration of Superconducting Gravimeters with the Help of Absolute Gravity Measurements. 13th Int. Symp. on Earth Tides. July 22 - 25, Brussels 1997. H. Virtanen and J. Kääriäinen: One Thousand Days of Superconducting Gravimetry in Finland. 13th Int. Symp. on Earth Tides. July 22. - 25, Brussels 1997. H. Virtanen: Observations of long-term gravity variations by superconducting gravimeter GWR T020. Abstract. European Geophysical Society, Annales Geophysicae, Suppl. I to Volume 15. 5.4 Lectures 5.5 Other activities Jussi Kääriäinen is the member of the Advisory Commission for Metrology (ACM). Jaakko Mäkinen is a member of the Expert Group for Mass and Derived Quantities within ACM. MIKES Julkaisu J5/1998 Annual Report 1997 49 FGI GEODETIC LENGTH FINNISH GEODETIC INSTITUTE, GEODETIC LENGTH 1. NAME OF THE NATIONAL STANDARDS LABORATORY Finnish Geodetic Institute 2. QUANTITIES Geodetic length 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 2 3.2 Number of accredited calibration laboratories 3.3 Number of official calibration certificates given by accredited calibration laboratories 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) 4.1.1 Absolute calibrations of quartz gauges using internationally recommended laser wavelength standards (PTB, Braunschweig). 4.1.2 Maintenance of quartz gauge system by comparisons (Tuorla Observatory, Univ. of Turku). 4.1.3 Interference measurements with Väisälä comparator (Nummela Standard Base Line). MIKES Julkaisu J5/1998 Annual Report 1997 50 FGI GEODETIC LENGTH 4.2 Maintenance 4.2.1 Comparison of quartz gauge no VIII was made in Tuorla Observatory. Epoch of comparison was 1997.047. 4.2.2 EDM-measurements at the Nummela Standard Base Line were made on 14 - 20 May, 22 - 26 May and 11 - 12 June using three Kern Mekometers ME5000. Two of the instrument came from the Industrial Technology Research Institute, Hsinchu, Taiwan and one from the Helsinki University of Technology, Institute of Geodesy and Cartography. This calibration serves also the maintenance of the Taoyuan Standard Base Line in Taiwan, measured in 1993 by FGI. During 21 - 25 April the Nummela Standard Base Line was measured with Wild Distomat DI2002 of the Finnish Geodetic Institute. Projection measurements were made at Nummela on 25 April - 12 May, 27 - 28 May and 16 - 18 June. 4.2.3 Kyviskes base line was measured in Lithuania in June in co-operation with the Vilnius Gediminas Technical University to establish and develop national length standards. The baseline was measured using the Mekometer ME5000 of the Helsinki University of Technology. 4.2.4 The automatic comparator to calibrate levelling rods in vertical position using CCDcamera and laser techniques has been completed. 4.3 Development projects 4.3.1 The standard base line is planned to be measured in 1998 in Chengdu, China using the Väisälä comparator. This is a joint project with the Sichuan Bureau of Surveying and Mapping to establish and develop national length standards. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories 4.4.3 International comparisons MIKES Julkaisu J5/1998 Annual Report 1997 51 FGI GEODETIC LENGTH 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications J. Jokela and M. Poutanen (1997): 50 years of interference observations at the Nummela Standard Baseline. Book of abstracts p. 59, Scientific Assembly of the International Association of Geodesy, Rio de Janeiro, Brazil, 3 - 9 September 1997. M. Takalo (1997): Automated Calibration of Precise Levelling Rods. Rep. Finn. Geod. Inst. 97:3. 5.2 Conferences 5.3 Reports M. Poutanen and J. Jokela (1997): Mittakaavojen äiti täyttää 50. Tiede 2000 6/97 pp. 38-42. M. Takalo: News about the calibration of invar staff. Working group of NKG for height determination. 28 April 1997, Hönefoss, Norway. 5.4 Lectures 5.5 Other activities Jorma Jokela is a member of the Expert Group for length within ACM. MIKES Julkaisu J5/1998 Annual Report 1997 52 TELE, SOUND PRESSURE 3.9 TELECOM FINLAND LTD, TELECOM ENGINEERING 1. NAME OF THE NATIONAL STANDARDS LABORATORY Telecom Finland Ltd., Telecom Engineering 2. QUANTITIES Sound pressure 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 14 3.2 Number of accredited calibration laboratories 3.3 Number of official calibration certificates given by accredited calibration laboratories 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) The unit of sound pressure is realised by the closed coupler reciprocity technique using half inch and one inch standard condenser microphones. Between reciprocity calibrations a group of calibrated condenser microphones was maintained as reference standard. 4.2 Maintenance 4.3 Development projects The reciprocity calibration instrumentation was modified to cower also frequencies from 63 Hz down to 31,5 Hz and the software was updated respectively to calculate appropriate corrections. 4.4 Intercomparisons MIKES Julkaisu J5/1998 Annual Report 1997 53 TELE, SOUND PRESSURE 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories 4.4.3 International comparisons The first series of measurements for the inter laboratory comparison EUROMET 399 was performed and the microphones were hand-carried to NPL for their measurements. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications 5.2 Conferences 5.3 Reports 5.4 Lectures 5.5 Other activities EUROMET acoustics contact person: T Valkeapää. Preparatory meeting for EUROMET project 400 was held at Telecom Engineering on 21 May 1997. The annual EUROMET Acoustics contact persons meeting was organised at Telecom Engineering on 22 May 1997 in Helsinki and 23 May at VTT Manufacturing Technology in Tampere. T Valkeapää visited Acoustics Branch, National Physical on 29 September 1997. IEC TC 29 Electroacoustics, Finnish follow up group: T Valkeapää, member. IEC TC 29 WG 5, Calibration of standard condenser microphones: J Urpalainen, member. Advisory Commission for Metrology: T Valkeapää, vice-member. Advisory Commission for Metrology, Expert group for acoustics: T Valkeapää, member. MIKES Julkaisu J5/1998 Annual Report 1997 54 TELE, SOUND PRESSURE FINAS Technical Assessor (ASS 35): T Valkeapää. MIKES Julkaisu J5/1998 Annual Report 1997 55 TELE, HF ELECT. TELECOM FINLAND LTD, TELECOM ENGINEERING 1. NAME OF THE NATIONAL STANDARDS LABORATORY Telecom Finland Ltd., Telecom Engineering 2. QUANTITIES High frequency power, attenuation and voltage 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 18 3.2 Number of accredited calibration laboratories 1 3.3 Number of official calibration certificates given by accredited calibration laboratories 4 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) Power: Power calibration equipment was calibrated with twin-load calorimeter and PTB calibrated bolometerheads. Attenuation: Attenuation calibration equipment was calibrated with SQUID calibrated reference attenuators and reference step attenuators. Voltage: Voltage was calculated from power and impedance supported by RF/DC-transfer standards below 100 MHz. MIKES Julkaisu J5/1998 Annual Report 1997 56 TELE, HF ELECT. 4.2 Maintenance Studies to replace some old instruments were finished and some new instruments were already received. Several faulty instruments were repaired and adjusted. The air-conditioning system of the laboratory failed repetitively, fortunately no severe damage occurred. Under such circumstances the new laboratory environment supervision and alarm system was proven most important. 4.3 Development projects Development of national standards for reflection coefficient and impedance at high frequencies: The intention is to build a traceability system for HP 8510 ANA to utilise its use as a national standard for reflection coefficient and impedance. Network analyser verification kits with type N and PC 3.5 connectors were acquired. Instrument failures were corrected. Inter laboratory comparisons were agreed to be exercised as a EUROMET project. Development of attenuation reference standard: The aim of the project is to develop a heterodyne based attenuation reference standard to replace the out of date SQUID-attenuation measurement system. We intend to cover first frequencies from 30 MHz to 120 MHz. Experiments for selection of the intermediate frequency was conducted and the influence of the local oscillator was studied. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories EAL Inter Laboratory Comparison HF3, attenuation. 4.4.3 International comparisons MIKES Julkaisu J5/1998 Annual Report 1997 57 TELE, HF ELECT. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications 5.2 Conferences T. Valkeapää, ANAMET meeting in Edinburgh, Scotland on 19 and 20 November 1997. 5.3 Reports 5.4 Lectures ”Quality control of EMC measurements” (in Finnish) a lecture given by T. Valkeapää, AELINSKO seminar on EMC measurements and their quality control on 9 April 1997 in Helsinki. 5.5 Other activities MIKES Julkaisu J5/1998 Annual Report 1997 58 HUT OPTICAL QUANTITIES 3.10 HELSINKI UNIVERSITY OF TECHNOLOGY (HUT), METROLOGY RESEARCH INSTITUTE 1. NAME OF THE NATIONAL STANDARDS LABORATORY Helsinki University of Technology (HUT), Metrology Research Institute 2. QUANTITIES The following optical quantities: luminous intensity, illuminance, optical power, transmittance, reflectance, spectral responsivity, optical wavelength 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 34 3.2 Number of accredited calibration laboratories 1 3.3 Number of official calibration certificates given by accredited calibration laboratories 32 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) The primary standard of optical power measurements is a cryogenic absolute radiometer operated with laser sources. Trap detectors and a pyroelectric radiometer are used as transfer standards to other wavelengths and power levels. Luminous intensity and illuminance are realised with a reference photometer constructed from a trap detector, a V(λ)-filter and a precision aperture. Regular spectral transmittance of filters, regular spectral reflectance of optical components, and spectral responsivity of detectors are calibrated using a reference spectrometer. Measurements of regular spectral reflectance are made by using a dedicated apparatus in the reference spectrometer. Spectral responsivity measurements are made with a trap detector as a reference. Optical wavelength is measured with a Fourier transform wavemeter, traceable to the iodine stabilised laser of the Centre for Metrology and Accreditation. 4.2 Maintenance MIKES Julkaisu J5/1998 Annual Report 1997 59 HUT OPTICAL QUANTITIES The transfer standards for optical power were calibrated and the mechanics for positioning of the laser beam have been improved in the cryogenic radiometer. The trap detector, the filters, and the apertures for the reference photometer of the luminous intensity were calibrated and new stands for the optical bench have been constructed. The transmittance and reflectance scales were checked using the reference materials. New reference detectors were constructed and calibrated for spectral responsivity. The voltmeters and ampere-meters used in optical power measurements have been calibrated. 4.3 Development projects Development of detector-based standards for optical power, luminous intensity and irradiance. The standards for luminous intensity and illuminance have been improved and the measurement ranges have been extended. New standards have been developed for luminance and spectral irradiance. Development of measurement systems for linearity and spatial responsivity of detectors. A setup has been developed for linearity measurement of photo detectors at the uncertainty level of 0.03%. Development of a calibration system for low-level-light measurements. A detection system based on photon counting technique has been constructed. Development of standards for optical wavelength and laser sources as Nordic cooperation. A diode laser has been taken in use as a reference laser at 780 nm. A 15 mW diode laser system has been constructed at 634 nm. Development of aperture area measurement. A new optical method has been developed for measurement of the area of radiometric apertures. The relative uncertainty of the method is close to 0.01% for 3-mm apertures. Spectroradiometer. A spectroradiometer has been ordered from the Bentham company. Development of standards for luminous flux. A miniature scanner is under development for characterisation of an integrating sphere. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories MIKES Julkaisu J5/1998 Annual Report 1997 60 HUT OPTICAL QUANTITIES 4.4.3 International comparisons Comparison of optical power measurements An intercomparison of cryogenic radiometers of HUT, PTB (Germany) and SP (Sweden) using silicon trap detectors was carried out as EUROMET project no. 90. The average relative difference between the results of the laboratories, when all known corrections are applied, are +1×10-4 for HUT-PTB, -3,7×10-4 for SP-PTB and -4,3×10-4 for SP-HUT, with standard uncertainties of 4,3×10-4, 3,0×10-4 and 4,4×10-4, respectively. The final report has been published by A. Lassila, H. Hofer, E. Ikonen, L. Liedquist, K. D. Stock and T. Varpula, “Intercomparison of cryogenic radiometers using silicon trap detectors”, Meas. Sci. Technol. 8 (1997), pp.123-127. Transmittance measurements on V(λ) filters Transmittance measurements on a V(λ) filter have been carried out with the participation of BNM-INM, France; HUT, Finland; and SP, Sweden as the coordinating laboratory. This is the EUROMET project no. 353. The HUT provided the V(λ) filter for this intercomparison. Each participant measured the regular spectral transmittance of the filter in the wavelength range 380-780 nm with steps of 10 nm at most. Further measurements such as uniformity and near-IR leakage checks were made where feasible. The filter was measured at the HUT before and after the other laboratories to check for any changes in the transmittance during the circulation. The results of the comparison measurements will be analysed at the SP. Intercomparison of the luminous responsivity of photometers arranged by CCPR The CCPR decided during the 13th session in September 1994 to undertake an international comparison of the luminous responsivity of photometers. There are 15 different laboratories participating in the comparison, BIPM acting as the coordinating laboratory. The comparison was carried out by sending two calibrated photometers together with the calibration results to the BIPM. During 1997 we characterised our photometers twice: once before sending them to the BIPM and once after they arrived back. The preliminary confidential results of the comparison were submitted to participating laboratories in autumn 1997. The final results will be reported at the next CCPR meeting in April 1999. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications P. Kärhä, P. Toivanen, F. Manoochehri, and E. Ikonen, “Development of a detector-based absolute spectral irradiance scale in the 380-900-nm spectral range”, Appl. Opt. 36 (1997) pp. 8909-8918. T. Kübarsepp, P. Kärhä and E. Ikonen, “Characterization of a polarization independent transmission trap detector”, Appl. Opt. 36 (1997), pp. 2807-2812. MIKES Julkaisu J5/1998 Annual Report 1997 61 HUT OPTICAL QUANTITIES A. Lassila, P. Toivanen and E. Ikonen, “An optical method for direct determination of the radiometric aperture area at high accuracy”, Meas. Sci. Technol. 8 (1997), pp. 973-977. J. Hu, T. Ahola, E. Ikonen and K. Riski, “Frequency shift of iodine stabilized He-Ne laser at higher harmonic order stabilization”, IEEE Trans. Instrum. Meas. 46 (1997), pp. 186-190. H. Talvitie, A. Pietiläinen, H. Ludvigsen and E. Ikonen, “Passive frequency and intensity stabilization of extended-cavity diode lasers”, Rev. Sci. Instrum. 68 (1997), pp. 1-7. A. Lassila, H. Hofer, E. Ikonen, L. Liedquist, K. D. Stock and T. Varpula, “Intercomparison of cryogenic radiometers using silicon trap detectors”, Meas. Sci. Technol. 8 (1997), pp.123127. A. Pietiläinen, H. Ludvigsen, H. Talvitie, and E. Ikonen, “Observation of coherent transient effects in a magneto-optical trap”, Quantum Semiclass. Opt. 9 (1997), pp. 615-619. S. Tammela, H. Ludvigsen, T. Kajava and M. Kaivola, “Time-resolved frequency chirp measurement using a silicon-wafer etalon”, IEEE Photonics Technol. Lett. 9 (1997), pp. 475-477. B. Ståhlberg, E. Ikonen, J. Haldin, J. Hu, T. Ahola, K. Riski, L. Pendrill, U. Kärn, J. Henningsen, H. Simonsen, A. Chartier and J.-M. Chartier, “International comparisons of HeNe lasers stabilized with 127I2 at λ ≈ 633 nm (July 1993 to September 1995), Part II: Second comparison of Northern European lasers at λ ≈ 633 nm”, Metrologia 34 (1997), pp. 301-307. E. Ikonen, “Optical science and engineering in Finland”, Part II, O plus E, no 206, pp. 130132 (1997), translated to Japanese by K. Seta. J. Hu, K. Riski, A. Chartier, J.-M. Chartier and S. Picard, “Intercomparison of 127I2 stabilized He-Ne lasers at 633 nm between MIKES and BIPM”, Metrologia (in press). A. Haapalinna, P. Kärhä and E. Ikonen, “Spectral reflectance of silicon photodiodes”, Appl. Opt. (in press). H. Talvitie, A. Seppänen, A. Äijälä, and E. Ikonen, “Continuous-wave light source at 317 nm based on frequency doubling of a diode laser”, Appl. Phys. B (in press). K. Kübarsepp, A. Haapalinna, P. Kärhä and E. Ikonen, “Nonlinearity measurements of silicon photodetectors”, Appl. Opt. (in press). L. Palva, E. Garam, F. Manoochehri, R. Sepponen, P. Hari, K. Rajala, H. Ruotoistenmäki and I. Seppälä, “A novel multipoint measuring system of photosynthetically active radiation”, Agricultural and Forest Meteorology, (in press). 5.2 Conferences MIKES Julkaisu J5/1998 Annual Report 1997 62 HUT OPTICAL QUANTITIES 5.2.1 International conference proceedings H. Talvitie, A. Seppänen, A. Äijälä and E. Ikonen, “Generation of continuous-wave radiation at 317 nm by frequency doubling of a diode laser”, in Conference on Lasers and Electro-Optics (CLEO’97), Technical Digest Series 1997, Baltimore, USA, May 20 - 22, 1997, pp. 88-89. P. Toivanen, H. Nyberg, P. Kärhä, A. Lassila, F. Manoochehri and E. Ikonen, “Detector-based realisation of the candela”, in Proceedings of the XIV IMEKO World Congress, Tampere, Finland, June 1 - 6, 1997, pp. 114-119. F. Manoochehri, A. Haapalinna and E. Ikonen, “High-accuracy measurement of regular spectral transmittance and reflectance in UV-visible-NIR”, in Proceedings of the XIV IMEKO World Congress, Tampere, Finland, June 1 - 6, 1997, pp. 108-113. A. Lassila, K. Riski. L. Abramova, E. Latysheva and V. Bolonin, “Intercomparison of line-scale and gauge block calibrations with ceramic and glass standards”, in Proceedings of the XIV IMEKO World Congress, Tampere, Finland, June 1 - 6, 1997, pp. 123-128. T. Niemi, M. Söderlund, S. Tammela, T. Kajava, M. Kaivola and H. Ludvigsen, “A device for measurements of time-resolved frequency chirp”, in Conference Digest of 4th Optical Fibre Measurement Conference (OFMC’97), Teddington, UK, September 29 - October 1, 1997, pp. 174-177. H. Ludvigsen, S. Tammela, T. Kajava and M. Kaivola, “Compact, temperaturecontrolled silicon etalon for time-resolved measurements of frequency chirp,” in OSA Annual Meeting, Technical Digest 1997 (Optical Society of America), WQ5. E. Ikonen, A. Lassila and P. Toivanen, “A new optical method for high-accuracy determination of aperture area”, in Abstracts of NEWRAD ’97, Arizona, USA, October 27 - 29, 1997, pp. 006. P. Kärhä, P. Toivanen, A. Haapalinna, F. Manoochehri and E. Ikonen, “Filter radiometry based on direct utilization of trap detectors”, in Abstracts of NEWRAD ’97, Arizona, USA, October 27 - 29, 1997, pp. 025. 5.2.2 National conference proceedings M. Tossavainen, J. Kokkonen, M. Kaivola and H. Ludvigsen, “Delayed selfhomodyne linewidth measurements with a short delay fiber”, in Proceedings of Optics Day ‘97, Physics Series Report 3-97, Tampere 1997, paper 43. A. Äijälä, A. Seppänen, H. Talvitie and M-L. Junttila, “Second-harmonic generation of a diode laser in an external ring cavity”, in Proceedings of Optics Day ‘97, Physics Series Report 3-97, Tampere 1997, paper 49. M. Kujala, A. Pietiläinen, H. Talvitie, H. Ludvigsen and E. Ikonen, “Measurements of coherent transients in a magneto-optical trap”, in Proceedings of Optics Day ‘97, Physics Series Report 3-97, Tampere 1997, paper 15. MIKES Julkaisu J5/1998 Annual Report 1997 63 HUT OPTICAL QUANTITIES P. Kärhä, P. Toivanen, F. Manoochehri and E. Ikonen, “A detector-based spectral irradiance scale and its use in determining photometric and colorimetric quantities”, in Proceedings of the XXXI Annual Conference of the Finnish Physical Society, Report Series HU-P-262, Helsinki University Printing House, Helsinki 1997, paper 7:04. T. Kübarsepp, P. Kärhä and E. Ikonen, “A polarization-independent transmission trap detector with predictable optical characteristics”, in Proceedings of the XXXI Annual Conference of the Finnish Physical Society, Report Series HU-P-262, Helsinki University Printing House, Helsinki 1997, paper 7:03. M. Tossavainen, J. Kokkonen, M. Kaivola and H. Ludvigsen, “1/f noise in selfhomodyne/heterodyne laser linewidth measurements”, in Proceedings of the XXXI Annual Conference of the Finnish Physical Society, Report Series HU-P-262, Helsinki 1997, paper 7:36. S. Tammela, T. Kajava, M. Kaivola and H. Ludvigsen, “New technique for timeresolved measurements of frequency chirp in modulated laser diodes”, in Proceedings of the XXXI Annual Conference of the Finnish Physical Society, Report Series on Physics HU-P-262, Helsinki 1997, paper 7:05. A. Seppänen, H. Talvitie, A. Äijälä and E. Ikonen, “Generation of blue and UV radiation by Frequency doubling of diode lasers”, in Proceedings of the XXXI Annual Conference of the Finnish Physical Society, Report Series in Physics HU-P262, Helsinki 1997, paper 7:32. M. Merimaa, H. Talvitie and E. Ikonen, “Frequency stabilized diode laser at 633 nm”, in Proceedings of the URSI/IEEE/Infotech Oulu/Pro Electronica XXII Convention on Radio Science 1997, Oulu, November 20 - 21, 1997, pp. 117-118. 5.3 Reports H. Nyberg and H. Ludvigsen (editors), Annual report 1996, Metrology Research Institute, Helsinki University of Technology, Espoo 1997, Metrology Research Institute Report 9/97, 38 p. E. Häkkinen, K. Fallström and A. Haapalinna, Häiriökysymykset, Häiriöt mittauksissa, 2nd edition, Espoo 1997, 36 p. (in Finnish). P. Wallin, Sähkömittaustekniikan perusteet, 4th edition, Espoo 1997, 145 p. (in Finnish). A. Pietiläinen, Mittaustekniikan perusteiden laboratoriotyöt, 4th edition, Espoo 1997, 106 p. (in Finnish). 5.4 Lectures 5.5 Other activities MIKES Julkaisu J5/1998 Annual Report 1997 64 HUT OPTICAL QUANTITIES 5.5.1 Conferences and meetings The personnel participated in the following conferences and meetings: Start-up meeting of the EC-project: “A calibration services brochure for optical radiation measurements,” National Physical Laboratory (NPL), London, United Kingdom, February 5, 1997; Petri Kärhä. Optics Day ‘97, Tampere University of Technology, Tampere, Finland, February 21, 1997; Anu Äijälä, Antti Pietiläinen, Markku Kujala and Mika Tossavainen presented 1 talk and 2 posters. XXXI Annual Conference of the Finnish Physical Society, Helsinki, Finland, March 13 - 15, 1997; Pekka Wallin, Erkki Ikonen, Hanne Ludvigsen, Petri Kärhä, Tapio Niemi, Antti Seppänen, Mika Tossavainen and Toomas Kübarsepp presented 2 talks and 2 posters. EUROMET Radiometry & Photometry Contact Persons Meeting, Gothenburg, Sweden, March 17 - 18, 1997; Erkki Ikonen. Mini-Symposium: Bose-Einstein Condensation, theory and recent experiments, University of Helsinki, Helsinki Institute of Physics, Helsinki, Finland, March 25 - 27, 1997; Erkki Ikonen, Ilkka Tittonen, Markku Kujala, Antti Pietiläinen and Hannu Talvitie. International Workshop on Detector-Based Radiometry, Berlin, Germany, April 13 15, 1997; Erkki Ikonen gave a talk on “Trap-detector-based filter radiometers for calibration of solar UV spectroradiometers”. Ultraviolet Measurement Workshop, National Physical Laboratory (NPL), London, United Kingdom, April 17, 1997; Petri Kärhä. SMT Workshop for project co-ordinators, European Commission, Brussels, Belgium, April 29, 1997; Erkki Ikonen. Conference on Lasers and Electro-Optics, Baltimore, USA, May 18 - 23, 1997; Hannu Talvitie gave a talk on “Generation of continuous-wave radiation at 317 nm by frequency doubling of a diode laser”. Industrial Optics Day, Tampere University of Technology, Tampere, Finland, May 29, 1997; Atte Haapalinna, Petri Kärhä, Antti Pietiläinen and Hannu Talvitie. XIV IMEKO World Congress, New Measurements - Challenges and Visions, Tampere, Finland, June 1 - 5, 1997; Farshid Manoochehri gave a talk on “Highaccuracy measurement of regular spectral transmittance and reflectance in UVvisible-NIR” and acted as a session chairman, Pasi Toivanen gave a talk on “Detector-based realisation of the candela” and acted as a session chairman and Antti Lassila gave a talk on “Intercomparison of line-scale and gauge block calibrations with ceramic and glass standards”. Meeting of the Comite Consultative Photometrie et Radiometrie (CCPR), Paris, France, June 9 - 11, 1997; Erkki Ikonen. MIKES Julkaisu J5/1998 Annual Report 1997 65 HUT OPTICAL QUANTITIES Joensuu Summer School on Optics, University of Joensuu, Joensuu, Finland, June 9 17, 1997; Pasi Toivanen. Nordic Summer School on Non-linear Optics, Munkedal, Sweden, July 30 - August 7, 1997; Hannu Talvitie and Markku Kujala. Meeting of EC-Project: “A calibration services brochure for optical radiation measurements”, National Physical Laboratory (NPL), London, United Kingdom, August 5, 1997; Erkki Ikonen. International Conference on Metrology, National Metrology Laboratory (NML), Pretoria, Republic of South Africa, August 26 - 30, 1997; Atte Haapalinna gave a talk on “Trap-detector-based filter radiometers for realization of spectral irradiance scales”. European Research Conference on Quantum Optics, Castelvecchio Pascoli, Italy, September 13 - 18, 1997; Ilkka Tittonen presented a poster on “Noise measurements of a high-finesse cavity with a moving mirror. The 4th Optical Fibre Measurement Conference (OFMC’97), Teddington, United Kingdom, September 29 - October 1, 1997; Tapio Niemi presented a poster on “A device for measurements of time-resolved frequency chirp”. OSA Annual Meeting in Long Beach, California, USA, October 12 - 17, 1997; Hanne Ludvigsen gave a talk on “Compact, temperature-controlled silicon etalon for timeresolved measurements of frequency chirp”. NEWRAD ’97, Tucson, Arizona, USA, October 25 - 31,1997; Erkki Ikonen and Petri Kärhä presented posters on “A new optical method for high-accuracy determination of aperture area” and “Filter radiometry based on direct utilization of trap detectors”. Metrology Seminar, Helsinki, Finland, November 19, 1997; Erkki Ikonen, Pekka Wallin, and Hannu Talvitie. Erkki Ikonen gave a talk on “International Development of Metrology”. XXII Convention on Radio Science, URSI, University of Oulu, Oulu, Finland, November 20 - 21,1997; Pekka Wallin. Mikko Merimaa gave a talk on “Frequency stabilized diode laser at 633 nm”. Symposium on Current Trends in Laser Cooling, Stockholm, Sweden, December 3 6, 1997; Ilkka Tittonen, Antti Pietiläinen and Markku Kujala. 5.5.2 Visits by the laboratory personnel Markku Kujala, Antti Pietiläinen and Hannu Talvitie to Atomic Physics Group, University of Stockholm, Sweden, January 9, 1997. Jianpei Hu to Bureau International des Poids et Mesures (BIPM), Paris, France, January 13 - 17, 1997. MIKES Julkaisu J5/1998 Annual Report 1997 66 HUT OPTICAL QUANTITIES Petri Kärhä to National Physical Laboratory (NPL), London, United Kingdom, February 4 - 5, 1997. Erkki Ikonen to Swedish National Testing and Research Institute, Borås, Sweden, March 18. Erkki Ikonen to Berliner Elektronenspeicherring-Gesellschaft Synchrotronstrahlung (BESSY), Berlin, Germany, April 15. für Erkki Ikonen to Bureau International des Poids et Mesures (BIPM), Paris, April 28, 1997. Petri Kärhä to National Physical Laboratory (NPL), London, United Kingdom, April 17 - 18, 1997. Hannu Talvitie to National Institute of Standards and Technology (NIST), Gaithersburg, USA, May 15, 1997. Jianpei Hu to National Institute of Metrology (NIM), Beijing, China, July 10, 1997. Atte Haapalinna to National Metrology Laboratory (NML/CSIR), Pretoria, Republic of South Africa, August 28, 1997. Erkki Ikonen and Petri Kärhä to Optical Sciences Center, Tucson, USA, October 30, 1997. Ilkka Tittonen to Umeå University, Umeå, Sweden, November 11, 1997. Markku Kujala to Stockholm University, Department of Physics, Stockholm, Sweden, December 2, 1997. 5.5.3 Research work abroad Ilkka Tittonen, Universität Konstanz, Konstanz, Germany, January - July, 1997. 5.5.4 Guest researchers Toomas Kübarsepp, Department of Physics, Tartu University, Tartu, Estonia, January 1 - April 30, 1997 and December 10 - 19, 1997. Filippo Perazzini, Politecnico di Milano, Milan, Italy, April 1 - September 30, 1997. Goëry Genty, Ecole Supérieure d’Optique, Paris, France, June 3 - August 31, 1997. 5.5.5 Visits to the laboratory Dr. Terry J. Quinn, Director of the Bureau International des Poids et Mesures, Paris, France, March 11, 1997. Dr. Anders Kastberg, Harald Ellmann, Isolde Sieder and Johan Jersblad, Atomic Physics Group of University of Stockholm, March 25, 1997. MIKES Julkaisu J5/1998 Annual Report 1997 67 HUT OPTICAL QUANTITIES Dr. Pieter Bloembergen, Nederlands Meetinstitut, The Netherlands, June 2, 1997. President M. J. Soileau, Vice President J. Roland Jacobsson and Executive Director James E. Pearson, SPIE - The International Society for Optical Engineering, June 10, 1997. Professor Xu Yi, National Institute of Metrology, Beijing, China, June 10, 1997. Dr. Günther Seckmeyer, Fraunhofer Institut für Atmosphärische Umweltforschung, Garmisch-Partenkirchen, Germany, June 16, 1997. Toomas Kübarsepp, Department of Physics, Tartu University, Tartu, Estonia, September 24 - 25, 1997 and November 27 - 28, 1997. Dr. Anders Kastberg, Stockholm University, Stockholm, Sweden, November 20 - 22, 1997. Dr. Leslie Pendrill, SP Swedish National Testing and Research Institute, Borås, Sweden, November 20 - 21, 1997. Dr. Rainer Köhler, Bureau International des Poids et Mesures, Paris, November 26 29, 1997. Prof. Michael Downs, National Physical Laboratory, London, United Kingdom, December 3 - 7, 1997. Dr. Mackillo Kira, University of Marburg, Marburg, Germany, December 15, 1997. Prof. Steven Chu, Stanford University, Stanford, California, USA, December 17, 1997. Dr. William D. Phillips, National Institute of Standards and Technology, Gaithersburg, Maryland, USA, December 17, 1997. Dr. Päivi Törmä, University of Innsbruck, Austria, December 19, 1997. 5.5.6 Memberships The Comite Consultative Photometrie et Radiometrie (CCPR), Erkki Ikonen (Member). EUROMET, Photometry and Radiometry, Erkki Ikonen (Rapporteur and Contact Person). European Co-operation for Accreditation (EA), Task Force: Photometry and Radiometry, Petri Kärhä (Member). Advisory Commission for Metrology, Pekka Wallin (Member). Advisory Commission for Metrology, Optical quantities expert group, Pekka Wallin (Chairman), Erkki Ikonen (Member). MIKES Julkaisu J5/1998 Annual Report 1997 68 HUT OPTICAL QUANTITIES Advisory Commission for Metrology, Expert group in length metrology, Erkki Ikonen (Member). MIKES Julkaisu J5/1998 Annual Report 1997 69 HUT HIGH VOLTAGE HELSINKI UNIVERSITY OF TECHNOLOGY (HUT), HIGH VOLTAGE INSTITUTE 1. NAME OF THE NATIONAL STANDARDS LABORATORY Helsinki University of Technology (HUT), Department of Electrical and Communications Engineering, High Voltage Institute 2. QUANTITIES Direct voltage Alternating voltage Capacitance Loss factor tanδ Inductance of high voltage reactors Lightning impulse voltage Switching impulse voltage Other impulse voltages Impulse current Impulse energy 1 kV – 200 kV 50 Hz, 1 kV – 100 kV (rms), 1 kV – 140 kV (peak) 50 Hz, 1 kV – 100 kV, 10 pF – 100 uF -5 50 Hz, 1 kV – 100 kV, 1· 10 – 2 50 Hz, 1 µH – 10 H 5 V – 600 kV 1 V – 200 kV 1 V – 200 kV 1 A – 50 kA 1 mJ – 500 J 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 21 (including 58 calibration tasks) 3.2 Number of accredited calibration laboratories 3.3 Number of official calibration certificates given by accredited calibration laboratories MIKES Julkaisu J5/1998 Annual Report 1997 70 HUT HIGH VOLTAGE 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) Direct voltage Alternating voltage Capacitance Loss factor tanδ Inductance of high voltage reactors Lightning impulse voltage Switching impulse voltage Other impulse voltages Impulse current Impulse energy voltage divider, precision voltmeter. standard capacitors, current comparator bridge, digitising precision voltmeter with special software, auxiliary divider. standard capacitors, current comparator bridge. standard capacitors, current comparator bridge, auxiliary resistors. standard capacitors, current comparator bridge. impulse calibrator, peak voltmeter, voltage divider, digital recorder with special software. impulse calibrator, voltage divider, digitising precision voltmeter with special software. impulse calibrator, voltage divider, digitising precision voltmeter with special software. shunt resistors, digital recorder with special software. shunt resistors, digital recorder with special software. 4.2 Maintenance Calibrations of all reference systems according to calibration schedule. Performance checks. Additional performance checks of measuring systems e.g. for calibrations onsite and in clients premises as well as after tests in which reference systems had to be applied. Calibrations of auxiliary instruments in regular basis once a year. Monitoring of stability of reference systems. Monitoring of environmental conditions. Condition monitoring and maintenance of reference systems. Reparations, amendments and modifications of equipment. Amendments and modifications of documentation of reference measuring systems. Final reporting and documentation of DWINA intercomparison co-ordinated by M Aro in 1995 and 1996. Final reporting and documentation of intercomparison of HV impulse measuring systems with digital recorder, co-ordinated by M Aro in 1995 and 1996. Studies for mapping the needs for high-voltage metrology and plans for its development. Checks of the air conditioning of calibration rooms and adjusting its control system. Planning and preparations for renovation of the 800 kV impulse generator. Reparations appeared to be more expensive than a new generator. A possibility to buy a relatively new used generator was checked but finally failed. Purchasing a new generator in 1998. MIKES Julkaisu J5/1998 Annual Report 1997 71 HUT HIGH VOLTAGE Improving transportation cases of reference equipment for calibrations in customers laboratory. Work for Advisory Commission for Metrology MNK and in its working group MNK-S and in FINMET and related meetings. Metrology day. Work in CIGRE working group High Voltage Testing and Measuring Technique. International standardisation work (IEC TC 42 and its working group Digital Recorders). Domestic and international co-operation, visits in other laboratories, visitors in the laboratory. Quality work in the laboratory and in the university. Renewing the quality code. Providing the quality system into Internet. Professional studies and learning of high-voltage measuring techniques and systems. Internal studies, learning and training. Studies and learning of computer applications and software. Quality studies and learning. Information activities, new brochure series, information into Internet, home page creating and updating. 4.3 Development projects Research and development of national standard and calibration systems for high voltage measurements (includes first 13 projects): Development of reference measuring system for 200 kV DC voltage. This part project was completed in September 1997. A new high voltage area for dc calibrations was equipped. The uncertainty budget could be completed up to 200 kV with a special heating test under load. The overall uncertainty appeared to be circa 300 ppm which is clearly lower than the specified value 500 ppm. Final reporting of the intercomparison of DC/SI Standard DWINA 100 co-ordinated by the laboratory, could be completed. Development of reference measuring system for AC voltage and impedance quantities. This part project was completed in September 1997. A new voltage source for 45 to 5000 Hz, 220 V, 4,5 kVA was purchased and taken into use by mounting a special user interface and the security system. The uncertainty of AC peak voltage measurement could be reduced from 500 ppm to 200 ppm based on comparisons with SP (1996) and the follow-up calibrations. Development of reference measuring system for lightning impulse voltage and switching impulse voltage. This part project was completed in September 1997. The HPVEE based measurement routines for oscilloscope LeCroy 9384TM completed, documentation 1998. The measurement range of switching impulse voltage could be extended from 140 kV to 200 kV by means of re-tests and re-calibrations. The measurement range of lightning impulse voltage could be extended down to 5 V because of better characteristics of the switch of the calibrator. Development of a new reference divider for 50 kV dc. MIKES Julkaisu J5/1998 Annual Report 1997 72 HUT HIGH VOLTAGE The divider is designed and the parts have been ordered and received. Final assembly, measurements and calibrations in 1998. Extension of a voltage range of a gas capacitor from 100 kV to 200 kV for alternating and from 140 kV to 300 kV for switching impulse voltages. The reparations of the inner parts of the compressed gas capacitor M150 could be finished and the inner electrode had to be renewed completely. All parts are available. Final reassembly, refilling by SF6 instead of N2, final measurements and calibrations will be performed in the first quarter of 1998. Development of calibration methods for high voltage instrument transformers. Start in 1998. Reduction of the uncertainty of lightning impulse front time of impulse voltage calibrator. Modification of the calibrator reduced the front time uncertainty, however, not enough. Further research is needed. New modifications 1998. Extension of capacitance calibration range from 10 nF to 100 µF. Measurement method of loss factor of high capacitance (10 µF - 100 µF) capacitors has been improved by means of a special electronic compensator. This compensating circuit has been planned, constructed and taken into use. A polystyrene capacitor (100 nF) has been provided for temporary reference in calibrations of high capacitances. Uncertainty calculations have been defined and updated. The measurement range could be extended to 100 µF with a reasonable uncertainty of 500 ppm. The range of loss factor measurement could be extended to 100 kV. Calibration system for impulse current. Shunt resistors for impulse current have been purchased and received. Preliminary measurements with a provisional step current generator performed. Two Rogowski coils for high-frequency current measurement received. Full calibrations, evaluations and documentation of the shunts and Rogowski coils in 1998. Development of calibration methods and system for high voltage inductors. Alternatives for reference inductors considered and studied. A reference inductor received. Calibration system for apparent charge of partial discharges. The HPVEE based calibration system (1 to 1000 pC) has been developed, and it works. Intercomparison with PTB completed. Further improvement 1998. Measuring system for 400 kV lightning impulse voltage with optically isolated l.v. transmission system. The design of divider HUT 401 with optical link has been completed. The link and divider parts have been ordered and received. The special h.v. arm resistor has been manufactured. Final assembly, tests and calibrations in 1998. Calibration system of digital recorders. Moving to a real-time HPVEE based calibration system started. Completion in 1998. Calibration system for EMC and ESD pulses. Start in 1998. MIKES Julkaisu J5/1998 Annual Report 1997 73 HUT HIGH VOLTAGE 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories Participation in low voltage intercomparison at AC and DC in Nordic Countries (DE, FI, NO, SW) co-ordinated by SP Borås (Nordtest Project 1255-95). The aim was to investigate the transparency of national evaluation methods. HUT/HVI participated this intercomparison although it was outside our measuring range. We participated on only those measuring points, which support our 50 Hz high voltage measurements: 2 mV 20 Hz, 1 V 10 Hz, 10 V 20 Hz, 200 V 45 Hz and 10 V DC. Our uncertainties were among the lowest, and the En values clearly below one (0,01 - 0,34) in AC and just over one (1,04) in 10 V DC. Co-ordination of international intercomparison HV impulse measuring systems with digital recorder. Final report completed in 1996 and summarising results published in conference ISH 97. See 5.3 Report 1. Co-ordination of international intercomparison of direct and switching impulse voltage measurement systems with Zener diode based reference system DWINA. Final report completed in 1996. Results presented in CIGRE Working Group 33.03. Summarising results to be published in Electra. See 5.1. Participation in intercomparison of apparent charge of partial discharges. Coordinator PTB, project SMT4-CT95-7501. Measurements completed. 4.4.3 International comparisons 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications MIKES Julkaisu J5/1998 Annual Report 1997 74 HUT HIGH VOLTAGE J. Hällström, M. Aro, A. Bergman, V. Jaroslawski: International intercomparison of direct and switching impulse voltage measurement systems with Zener diode based reference system DWINA. Accepted for publication in ELECTRA (April 1998). 5.2 Conferences 10th International Symposium on High Voltage Engineering ISH’97, Montréal 25 - 29 August 1997: M. Aro, J. Hällström, E-P. Suomalainen, one paper. CIGRE 33 Colloquium, Toronto 2 - 3 September 1997: M Aro, J Hällström, E-P. Suomalainen, three papers. CIGRE Working Group 33.03 (High Voltage Testing and Measuring Techniques), Lake George USA 3 - 6 September 1997, M. Aro, J. Hällström, three papers. 5.3 Reports J. Hällström, M. Aro, S. Benda-Berljin, I. Blanc, F. Garnacho, R. Gobbo, L-O. Gunnarsson, H-J. Köster, W. Lucas, M. Muhr, F. Neves Gomes, G. Pesavento, J. Piiroinen, H. Renger, G. Rizzi, B. Sacepe, L. Scheltinga, K. Schon, K-O. Tangen, P. Valve, K-H. Weck and M. Wedberg: European intercomparison of H.V. impulse measuring systems with digital recorder. 10th International Symposium on High Voltage Engineering ISH’97, Montréal 25 29 August 1997. Volume 4, High Voltage Testing and Monitoring, pp. 7 - 13. J. Piiroinen and H. Karlsson: Impulse Calibration of Digital Recorder. CIGRE 33 Colloquium, Toronto 2 - 3 September 1997, paper 5.8, 2 pages. E-P. Suomalainen and J. Hällström: New Type of AC Calibration System. CIGRE 33 Colloquium, Toronto 2 - 3 September 1997, paper 5.9, 2 pages. E-P. Suomalainen and J. Hällström: High Voltage Calibration at Helsinki University of Technology. CIGRE 33 Colloquium, Toronto 2 - 3 September 1997, paper 5.3, 2 pages. M. Aro: Quality of tests depend on quality of measurements, (in Finnish). Sähkö-Tele 70(1997)2, pp. 23 - 26. M. Aro, J. Hällström and S. Nevalainen: Working group for development of high-voltage metrology: Mapping the needs for high-voltage metrology and plans for its development, (in Finnish). Publication J9/97, MIKES 1997. M. Aro (ed.): Measurements of high voltages and diagnostics of high-voltage insulations, (in Finnish/English). Post graduate seminar, Sjökulla 28 - 30 April and 2 - 5 June1997. HUT High Voltage Institute, part 1: 136 p., part 2: 121 p. Brochure series on high-voltage calibrations in English and in Finnish. High Voltage Quantities. DC Voltage. AC Voltage. Impedance Quantities. Impulse Quantities. 5.4 Lectures MIKES Julkaisu J5/1998 Annual Report 1997 75 HUT HIGH VOLTAGE Measurements of high voltages and diagnostics of high-voltage insulations, (in Finnish/English). Post graduate seminar, Sjökulla 28 - 30 April and 2 - 5 June1997. 5.5 Other activities M. Aro is member of CIGRE Study Committee 33 (Power systems insulation co-ordination), CIGRE Working Group 33.03 (High voltage testing and measuring techniques) and Finnish delegate in IEC TC 42 (High voltage testing techniques). J. Hällström is member of IEC TC 42 Working Group 8 (Digital recorders for measurements in high-voltage impulse tests). Meeting in Montreal 29 August 1997. M. Aro is chairman of Finnish National Committee of IEC TC 42 (High voltage testing techniques). Visit by Prof. Eberhard Lemke from Lemke Diagnostics GMBH on 2 - 6 June1997. Invited lecture “PD - History and Future” on 6 June1997. M. Aro, E-P. Suomalainen and J. Hällström visited Prof. Eddy So in NRC Electrical Power Measurements Group, Ottawa, Canada on 29 August 1997. Visit by Dr Hideo Fujinami, Central Research Institute of Electric Power Industry CRIEPI Tokyo Japan 1 September 1997. MIKES Julkaisu J5/1998 Annual Report 1997 76 STUK 3.11 FINNISH CENTRE FOR RADIATION AND NUCLEAR SAFETY (STUK) 1. NAME OF THE NATIONAL STANDARDS LABORATORY Radiation and Nuclear Safety Authority (STUK) Radiation Practices Regulation Radiation Metrology Laboratory 2. QUANTITIES Exposure, air kerma, absorbed dose to soft tissue, dose equivalent 3. CALIBRATION CERTIFICATES 3.1 Number of official calibration certificates given 72 3.2 Number of accredited calibration laboratories 3.3 Number of official calibration certificates given by accredited calibration laboratories 4. MAINTENANCE AND DEVELOPMENT OF NATIONAL STANDARDS AND DISSEMINATION OF UNITS 4.1 Realisation of unit(s) Exposure, air kerma and dose equivalent: Secondary standard ionisation chambers with 60Co and 137Cs gamma sources and X-ray sources (10-320 kV). Secondary standard neutron sources (dose equivalent for fast neutrons). Absorbed dose to soft tissue: Secondary standard beta ray sources, extrapolation ionisation chamber (primary standard). 4.2 Maintenance The quality of all equipment used for calibration and testing were controlled regularly according to the documented quality control programme. The stability of secondary standards remained good and the results of stability tests did not exceed the established action levels. MIKES Julkaisu J5/1998 Annual Report 1997 77 STUK The commissioning procedures for the new X-ray units were completed. The re-construction of the equipment for calibration set-up were continued. 4.3 Development projects The Quality System of the laboratory was developed in accordance with the general guidelines given by the International Atomic Energy Agency (IAEA) for the Secondary Standard Dosimetry Laboratories (SSDLs) of the IAEA/WHO international network of SSDLs (WHO: World Health Organisation). The laboratory participates in a Coordinated Research Program of the IAEA (for 1997-1999), which aims at improving the quality of SSDLs through development of specific guidelines for the Quality Systems. About 80 % of the QS documentation has been finished. The methods of measurement and calibration for boron neutron capture therapy (BNCT) were developed. The laboratory participates in an EU Shared Cost Action under the Standards, Measurement and Testing Program, which was accepted 1997. The aim of the project is to develop European Code of Practice for the BNCT dosimetry. 4.4 Intercomparisons 4.4.1 National intercomparisons for accredited calibration laboratories 4.4.2 International (EAL or other) intercomparisons for accredited calibration laboratories 4.4.3 International comparisons The laboratory participated in annual intercomparisons carried out by the IAEA, using both mailed thermoluminescence dosimeters and therapy level ionisation chambers, for the accuracy of absorbed dose measurement among the 72 SSDL laboratories of the IAEA/WHO network of SSDLs. The deviation of the value given by the laboratory from the reference value of the IAEA was -0.5 % for TLD measurements and -0.7 % and + 0.1 % for ionisation chamber measurements. The results are well within the action level of 3.5 % used by the IAEA. 5. PUBLICATIONS, CONFERENCES, REPORTS, LECTURES AND OTHER ACTIVITIES 5.1 Publications MIKES Julkaisu J5/1998 Annual Report 1997 78 STUK 5.2 Conferences P. Aaltonen-Brahme, A method to determine and to characterize the cumulative dose distribution to the patient. Paper presented at the World Congress on Medical Physics and Biomedical Engineering, Nice 14 - 19 September 1997, (Abstract). H. Järvinen, Reporting of abnormal incidences in radiotherapy. Paper presented at the World Congress on Medical Physics and Biomedical Engineering, Nice 14 - 19 September 1997, (Abstract). 5.3 Reports P. Aaltonen, A. Brahme, I. Lax, S. Levernes, I. Näslund, J.B. Reitan, I. Turesson. Specification of dose delivery in radiation therapy. Recommendations by the Nordic Association of Clinical Physics (NACP). Acta Oncologica 36, Supplementum 10, 1997. 5.4 Lectures A. Kosunen, Säteilymittausten peruskäsitteet, annossuureet Sädeturvapäivät, 22 - 23 October 1997, Tampere-talo. ja mittaussuureet. 5.5 Other activities Standardisation P. Aaltonen-Brahme acted as the chairman of the working group of the Nordic Association of Clinical Physics (NACP): ”Specification of Dose Delivery in Radiotherapy”. H. Järvinen acted as the chairman of Report Committee: ”Beta Rays for Therapeutic Applications” and as a member of Report Committee: ”Dosimetry in Diagnostic Radiology for the patient”, of the International Commission on Radiation Units and Measurements (ICRU). A. Kosunen acted as a member in WG 3: ”Performance of Dosemeters” of Sub-Committee (SC) 62C of the International Electrotechnical Commission (IEC). P. Sipilä acted as a member in WG 2: ”Beam teletherapy and particle accelerators” of SC62C of the IEC. H. Järvinen acted as the chairman of the national working group: ”Terminology of Radiotherapy Physics”. H. Järvinen acted as a member of ESTRO (European Society for Therapeutic Radiology and Oncology) Physics Committee. Training An annual meeting on Dosimetry and Quality Assurance in Radiotherapy was organised 23 24 May for the radiotherapy physicists of Finland. MIKES Julkaisu J5/1998 Annual Report 1997 79 STUK One IAEA fellow from Belarus visited the laboratory for two weeks. Other The laboratory continued as the member in the IAEA/WHO Network of SSDL laboratories (from 1977). The laboratory was a member of EUROLAB-Finland. H. Järvinen acted as the Contact Person for EUROMET in the field of Ionising Radiations and Radioactivity. H. Järvinen acted as a member of the National Advisory Board of Metrology and as the representative of STUK in the Advisory Board for Testing and Certification. H. Järvinen and P. Aaltonen-Brahme participated in the World Congress for Medical Physics and Biomedical Engineering, Nice, 14 - 19 September. H. Järvinen participated as a consultant in two meetings organised by the IAEA (dealing with problems of brachytherapy metrology and quality systems of SSDLs). P. Sipilä participated in Varian User’s Meeting in Algavre. A. Kosunen participated as a member in two national working groups, one concerning normal tissue tolerance study of dog brain with BNCT, and the other concerning the development of dose calculations for BNCT. MIKES Julkaisu J5/1998 Annual Report 1997 80 MIKES Julkaisu J5/1998 STUK Annual Report 1997