1 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Americium -241 Alpha foils and sources for smoke detectors Related Products Americium-241 (Am-241) alpha particle emitting foil, made by Detector Technology, is widely used in ionization chamber smoke detectors (ICSD). The foil combines high integrity of containment with high emission efficiency. Detector Technology has a wide-ranging expertise in the design and construction of ionization chambers, built up over 30 years of experience in smoke detection. A consultancy service is offered for the design and/or manufacture of ionization chambers intended for use both in smoke detection and other applications. Detector Technology has over 30 years experience of foil technology and offers a well established standard product range of foil mounted in holders. Regulatory Compliance Construction Detector Technology foil meets the regulatory requirements of most national authorities worldwide. Detector Technology Am-241 foil has been evaluated and registered by the US Nuclear Regulatory Commission (NRC). These registrations are now under the jurisdiction of the Massachusetts Radiation Control Program. Registrations tabulated below, are recognized in the US as equivalent to NRC registrations and so has nationwide validity. The radioactive material Am-241 emits alpha and low energy Xand γ-radiation. It is incorporated within a gold matrix and sandwiched between a silver backing and a palladium laminate face, as illustrated schematically below. The face layer is thick enough to retain completely the Am-241 but thin enough to allow efficient emission of the α-radiation. The shaped foil pieces are then mounted into various holders by staking, securing between spot welded metal plates or rolling over the holder edges. Foil for use in smoke detectors Detector Technology has developed techniques for producing foil pieces cleanly, reproducibly and safely, and also for mounting them into holders. Specialized equipment and appropriately licensed facilities are essential to both processes. It is strongly advised that these operations be carried out at our facilities. US-Model number Detector Technology offers a standard product range. Certain foil pieces are also available as indicated. We welcome early discussions on new customer requirements. Cross Section Foil emitting one side only AMM.1001 Foil emitting from both sides AMM.1001D Foil mounted in holder AMM.1001H Palladium facing (-2mm) Active matrix (~1mm) Silver backing (0.15-0.25mm) 2 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Sources In Holders X.0868 Holder It is strongly recommended that customers purchase sources that are already staked directly into holders by Detector Technology. This avoids the need for customers to maintain radioactive facilities for foil handling. Sources in holders pass the statutory leak tests that are required for sealed sources and they meet the requirements of regulatory authorities worldwide. Six standard product examples are illustrated below. Alternative designs are also available, for which enquiries are welcomed. Detector Technology has extensive experience of holder design and manufacture and is pleased to advise on any aspects of technical performance, safety, quality and service. Ø 4.9 1.3 0.4 Ø 8.9 Dimensions in mm Several staking and sealing patterns are available. These comprise 5 or 6-point staking patterns or holders that are continuously crimped around the circumference of the source and holder. Activity A continuous crimp design provides added strength and integrity by continuously sealing the foil around the cut active edge. Activity tolerance Product code 18.5kBq (0.5mCi) ±20% AMMK7648 29.6kBq (0.8mCi) ±20% AMMK1235 Closure: 6-point stake or extended width crimp pattern Quality control: Wipe test I Safety performance rating: ANSI/ISO C64444 Recommended working life: 10 years X.0849 Holder X.0869 Holder Ø 6.4 1.5 1.6 Ø 4.9 1.3 Ø 3.2 0.4 Dimensions in mm Ø 6.3 Activity Activity tolerance Dimensions in mm Product code 18.5kBq (0.5mCi) ±20% AMMK7540 29.6kBq (0.8mCi) ±20% AMMK5597 Activity Closure: 6-point stake or extended width crimp pattern Quality control: Wipe test I Safety performance rating: ANSI/ISO C64444 Recommended working life: 10 years Activity tolerance Product code 18.5kBq (0.5mCi) ±20% AMMK7649 29.6kBq (0.8mCi) ±20% AMMK7650 Closure: 6-point stake or extended width crimp pattern Quality control: Wipe test I Safety performance rating: ANSI/ISO C64444 Recommended working life: 10 years 3 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Foil Pieces Users of un-mounted foil pieces must have specialized radioactive handling and testing facilities, which need to be licensed by an appropriate national regulatory authority. Measurement To control the content of individual foil pieces, the radioactive content of all rolled foil, and hence the final activity per unit area, is accurately measured. Five standard foil piece types are presently available. Nonstandard designs can be provided on request. Activity Activity tolerance Product code Size(mm) 18.5kBq (0.5mCi) ±20% AMMK7169 f 2.38 29.6kBq (0.8mCi) ±20% AMMK6045 f 2.38 18.5kBq (0.5mCi) ±20% AMMK5588 f 5.00 29.6kBq (0.8mCi) ±20% AMMK3457 f 5.00 18.5kBq (0.5mCi) ±20% AMMK7620 3.5 x 3.5 Depending on user requirements and quantities involved, it is possible to offer the following additional measurements: · activity content of individual sealed sources or foil pieces · spectrometry showing typical emitted energy distribution · full-width half-maximum values determined from spectrometry, i.e. the energy width at half the maximum intensity value · spatial distribution - the measured intensity along the 2p arc above the emitting surfaces from a given batch. · ion current as measured in an ionization chamber with an agreed specific geometry. · acceptable quality level (AQL) Safety performance testing: ANSI/ISO C64444; IAEA Special Form is applicable to foil pieces greater than 5mm diameter. When used as part of single station smoke detectors, Detector Technology sources are also fully compatible with the requirements of: · · · Safety Performance ISO 2919 classification Underwriters Laboratories Standard UL 217(2) European Norm EN 54(3) UK National Radiological Protection Board (NRPB) criteria of acceptability(4) upon which intended UK legislation relating to smoke detectors is based Source performance under working conditions is tested in accordance with internationally defined (ISO) standards. Please refer to the Detector Technology document 'Safety and Packaging'(7) for details of the test data and system of classification. Quality Assurance The ISO rating recommended for ionization chamber smoke detector sources is C32222. By use of optimum design parameters, the performance of Detector Technology's sources significantly exceeds this in all cases, as indicated above. ISO 9001 conformity The design, manufacture and testing of Detector Technology Americium-241 foils is managed within the scope of the Quality Management System which is approved by Lloyds Register Quality Assurance for compliance with BS EN ISO 9001:2000.(5) Other tests Many other tests designed to simulate severe industrial environments have been performed on samples of alpha foil, including exposure to sulphur dioxide gas, to salt spray and to ozone. Details of such tests can be supplied on request. Quality Control Surface contamination National radiation regulations(9), in common with other national regulations, require that radioactive sources should not be handled with bare fingers. They must be handled using forceps, vacuum pick-up or protective gloves, taking care not to damage the emitting face. For alpha foil sources these simple procedures are generally adequate, though other mechanical systems may be used if required. Sources in Holders: Sources in holders are batch tested in conformity with BS 5288(6). External surfaces, including the alpha-emitting faces, are wiped with a swab of tissue or cotton wool moistened with alcohol or water. Any activity removed is measured by a liquid scintillation counting technique. The acceptance criterion is <185Bq (<5nCi). Considerable additional safety precautions are required for the processing of un-mounted foil pieces. Users may contact Detector Technology or the competent national authority for advice on particular operations but it is recommended that such operations be entrusted to Detector Technology which has extensive experience of all aspects of foil handling. Foil pieces:. The tests used to check for surface contamination depend on the size, shape and quantity of the pieces. The tests may vary to suit user requirements. Further details are available on request. 4 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 References External radiation attributable to the Am-241 source in an ICSD is normally extremely low. The following approximate dose rate calculations based on thermo luminescent dosimetry data derived in respect of a typical Detector Technology ICSD are given for guidance. These data will enable users to comply with the US Code of Federal Regulations [10 CFR.32.26.(6).] Directions Distance (cm) Normal to surface of outer cap electrode 5 Normal to surface of outer cap electrode 25 Normal to source electrode 5 Normal to source electrode 25 1. 'Smoke Detector Ionization Chambers: DSCA2 and DSCA3.' Data Sheet No 11247, Detector Technology, 1979. 2. 'Standard for Single and Multiple Station Smoke Detectors.' UL 217, Fourth Edition, Underwrites Laboratories Inc., Northbrook, Illinois, 10th May 1993. Dose rate Sv/year rem/year 0.1 0.01 0.005 0.0005 0.6 0.06 0.003 0.0003 3. 'Components of Automatic Fire Detection Systems.' EN 54, European Commission for Standardization (CEN), Brussels, July 1982. 4. 'Board Statement on Approval of Consumer Goods Containing Radioactive Substances.' Documents of the NRPB, Volume 3, No. 2, National Radiological Protection Board, Didcot, 1992. 5. 'Quality systems: Model for quality assurance in design, development, production, installation and servicing.' BS EN ISO 9001, British Standards Institution, London, 1994. By comparison, the background dose rate can typically be 2mSv/year (0.2rem/year) in the UK and 3.7mSv (0.37rem/year) in the USA. 6. 'Specification - sealed radioactive sources.' BS 5288, British Standards Institution, London 1976. Reference may also be made to the Detector Technology ‘Safety and Packaging' document(7). For any other safety advice please enquire as above. 7. 'Safety and Packaging.' Data sheet reference HI045. SOU/120/95/KI, Detector Technology, 1995. Nuclear Data for Am-241 used in Detector Technology Foil 8. 'IAEA Safety Standards: Regulations for the Safe Transport of Radioactive Materials, 1985 Edition. As Amended 1990.' International Atomic Energy Authority, Vienna, 1990. Half-life 9. 'The Ionising Radiations Regulations 1985.' Statutory Instrument 1985 No. 1333: Health and Safety, Her Majesty's Stationery Office, London, 1990. 433 years Principal alpha particle energies Principal photon particle energies Radionuclidic purity 5.338MeV 14% 59.5kV (36%) <0.5% Am-241 5.445MeV 12.8% Np LX-rays <0.0001% other 5.486MeV 85.2 12-22keV (~40%) gamma impurities Others Low Chemical purity > 99% 5 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Smoke detector ionization chambers DSCA2C and DSCA3C DSCA2C and DSCA3C General description Both the DSCA2C and DSCA3C products incorporate a dual ionization chamber of advanced design containing a single radioisotope source producing ionization in both chambers. The design was developed using a computer model to optimize performance characteristics. A performance test electrode is incorporated in the DSCA3C. The design, manufacture and testing of the DSCA2C and DSCA3C ion chambers are managed within the scope of the Detector Technology Quality System which is certified by Lloyds Register Quality Assurance for compliance with BS EN ISO 9001:2000.(1) Side View The general construction was designed to meet the requirements of Underwriters Laboratories Inc. Standard UL 217(2) and EN 54:part 7.(3) and both designs have been recognized by UL for many years. For maximum corrosion resistance the electrodes and source holder are made of AISI 316 stainless steel, the support molding of polypropylene and the insulators of polytetrafluoroethylene Teflon™. Details of the source are given in the data sheets 'Americium-241 alpha foil and sources'(4) and 'Safety and Packaging'(5), both available on request. In accordance with OECD requirements(6) the source activity is less than 37kBq (lmCi) Am-241. The Recommended Working Life of the source is 10 years. The ANSI/ISO classification of the ionization chamber is C64646. View from underneath The units as supplied are assembled ready to mount on a suitable printed circuit board using the pre-tinned tags provided. No source adjustment is required. B A The DSCA3C's test electrode permits the checking not only of the operational functioning of the ion chamber but of all associated electronic circuitry. When actuated, the electrode disturbs the balance conditions to simulate the presence of smoke by an obscuration of 4.0%/Ft. A. Outer Cap Electrode B. Source Plate Electrode C. Test Electrode D. Collector Electrode C The design is compatible with commercially available integrated circuits. Detector Technology expertise in the design and construction of ion chambers is long established and wide-ranging. A consultancy service is available to assist in the design of systems using ion chambers. A 6 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Regulatory Compliance To improve corrosion resistance, the associated circuitry should be sealed in a container, using a suitable sealant where the chamber terminals enter the chamber (avoiding sealant on the collector electrode insulator). Detector Technology sources used in the detectors meet the regulatory requirements of most national authorities worldwide. Chambers intended for use at high altitudes may require adjustment of the tripping level of the detector circuit for optimum sensitivity. Specifically Detector Technology sources comply with: · · · European Norm EN 54(3) UK National Radiological Protection Board (NRPB) criteria of acceptability(7) upon which UK legislation relating to smoke detectors is based. Sources have been recognized by Underwriters Laboratories Inc in compliance with Standard UL 217(2) as a component of smoke alarms and detectors. Within reasonable limits, the balance potential remains relatively unaffected by temperature, pressure, humidity and wind velocity. Specification The general specification is tabulated below. Conditions, except where specified, are: Principle of Operation · · · The collector electrode is charged by an imbalance in the ionization currents flowing in the inner and outer chambers, until these currents come into balance. In the absence of smoke or combustion products, the balance potential remains constant, apart from small variations due to statistical fluctuation of the ionization current. Minimum Collector electrode balance potential When smoke enters the chambers the ionization currents change, that in the outer chamber more so than in the inner camber. The collector electrode is then charged to a new balance potential. The change in potential is used to trigger an alarm circuit. · Typical Maximum Units 5.0 - 6.0 V at 0.2% obscuration foot * at 0.4% obscuration foot * - 0.7 0.3 - V V Insulator leakage - - 0.5 pA Capacitance (collector to outer + source electrode) - 6 - pF - 20 0.5 26 0.7 kBq mCi Change in collector balance potential with smoke: The performance of the DSCA3C has been independently assessed in the following two studies: · Outer electrode to source electrode potential: 9V Temperature: 20°C ± 3°C Ambient pressure: atmospheric, near sea level, clean air in smoldering smoke and fire tests by Underwriters Laboratories Inc.(8) in accordance with a 'Testing Program for Automatic Fire Alarm Equipment for Residential Use' by the Danish Research Centre for Applied Electronics(9) Am-241 activity * Obscuration limits specified by UL 217(2) Copies of both reports are available on request. Precautions and Recommendations The ionization current is approximately 20pA. Precautions to preserve the insulation of the input connection path to the electronics are critical for correct operation of the device. In particular the collector electrode and its connections must remain free from contamination, e.g. from solder flux or manual contact. The lead from the collector electrode to the detector circuit should preferably be short and clear of the circuit board and other components. The chamber is shielded from external electric fields by its outer cover. Suitable shielding should be provided for the associated circuitry, because of the necessarily high impedance of the circuit connected to the chamber collector electrode. 7 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Radiological data Performance Users of these units in all countries should ensure that they comply with all relevant regulations on the control of radioactive materials. Collector potential change with B.S. smoke Whatman #2 filter paper heated on electric element The DSCA3C unit has been independently assessed and found satisfactory in the following respects: · · a general Radiological Assessment by the NRPB(10) an NEA 1200°C incineration test by the NRPB(11) Copies of the NRPB reports are available on request. In both devices, external radiation attributable to the Am-241 sealed source is normally extremely low. The following approximate dose rate calculations based on thermo luminescent dosimetry data derived in respect of a typical Detector Technology unit are given guidance. These data will enable users to comply with the US Code of Federal Regulations [10 CFR.32.26(6).] Directions Distance (cm) Normal to surface of outer cap electrode 5 Normal to surface of outer cap electrode 25 Normal to source electrode 5 Normal to source electrode 25 % obscuration per Foot Ratio of collector potential at balance to supply potential Dose rate Sv/year rem/year 0.1 0.01 0.005 0.0005 0.6 0.06 0.003 0.0003 Supply (V) Balance voltage change with time after activation of the test electrode By comparison, the background dose rate can typically be 2mSv/year (0.2rem/year) in the UK, or 3.7mSv (0.37rem/year) in the USA. Reference may also be made to the Detector Technology 'Safety and Packaging' document(5). For any other safety advice please enquire as above. Seconds Collector potential change With altitude Pressure (mmHg) Altitude (feet) 8 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Smoke detector ionization chambers DSCB1C & DSCB2C Fig 1 -DSCB1C General Description The DSCB1C (fig 1) is a small, compact and robust dual ionization chamber of advanced design containing a single radioisotope source producing ionization in both chambers. The chamber has a unique internal geometry, which allows the detector chip to be positioned beneath the chamber within a recess in the moulded plastic base. Pin-15 of the chip can be connected directly to the collector electrode inside the protective RF shield of the cover. This isolates the highly sensitive connection between the collector electrode and pin-15 from other parts of the detection circuitry and it provides a high degree of immunity from external electrical interference. Fig 2 - Side view The external design features and dimensions of the DSCB1C are shown in figures 2 and 3. The design was optimised for smoke sensitivity with the assistance of proprietary computational modelling software, developed by Detector Technology. Smoke detection performance is optimised, whilst minimising sensitivity to climatic variations and to design tolerances. The electrodes and source holder are made of AISI 304 stainless steel. The plastic insulator material is specially chosen for its exceptional mechanical stability and resistance to moisture and oxidising chemicals in the air. The units are supplied assembled and ready to mount on a suitable printed circuit board using the pre-tinned tags provided. Dimensions in mm Fig 3 - Bottom view Details of the sealed source design can be found in the data sheets 'Americium-241 alpha foil and sources' (4) and 'Safety and Packaging'(5). Both of these are available on request. In accordance with OECD requirements (6) the source activity is less than 37kBq (1mCi) Am-241. The Recommended Working Life of the source is 10 years. The BS/ISO/ANSI rating of the ionisation chamber is C64646. The design manufacture and testing of the DSCB1C is managed within the scope of Detector Technology's Quality System which is certified by Lloyds Register Quality Assurance for compliance with BS EN ISO9001:2000 (1) Detector Technology expertise in the design and construction of ion chambers is well established and wide-ranging. A consultancy service is available to assist in the design of systems using ion chambers and in the provision of testing and computational modelling services to measure and model the performance of customers' own designs. Dimensions in mm 1 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Fig 4, DSCB1C – internal design schematic Fig 6a DSCB1C smouldering paper sensitivity computer modelled ion distribution C han ge in Balance voltage vs Light O b scuratio n S moulder ing Paper Te st 2.5 2 dV (volts) source chip recess 1.5 1 0.5 0 0 source electrode cover electrode Fig 5 1 2 3 4 Light O b scuratio n % collector electrode Fig 6b DSCB1C sensitivity smoky paraffin Recommended circuit design for use with the MC1446 detector chip C hange in B alanc e voltag e vs Lig ht Ob scurati on S m o ky P araffin Test 3 dV (volts) 2 1 0 0 1 2 3 Lig ht Ob scura tion % Fig 6c DSCB1C smouldering wick sensitivity Cha ng e in Ba la nce vo lta ge vs L ig ht Ob scu ration Smou ld erin g Wick T e st Performance and Sensitivity 4 The smoke detection performance of the DSCB1C chamber has been measured using a variety of different types of smoke. Sensitivity to smouldering paper, smoky paraffin and smouldering wick are shown in figures 6a, 6b and 6c. dV (volts) 3 2 1 Performance and sensitivity to humidity, temperature, pressure and air velocity are shown in figures 7, 8, 9 and 10. The air velocity response may vary depending on the design and configuration of components adjacent the ion chamber in the smoke alarm. 0 0 1 2 3 4 Lig ht Obscu ration % Fig 7 DSCB1C humidity response at 230C DSCB2C Ion Chamber 7 Balance Voltage (V) The DSCB2C is a modified version of the DSCB1C in which the bent-in louvers in the cover shown in fig.1 have been removed. It provides the DSCB2C with the benefit of having a fast response to smouldering fires by allowing air to flow more easily through the chamber. This design also limits the stability of the unit when operating under conditions of high air velocity. Customers may select either the DSCB1C or DSCB2C designs to optimise whichever performance characteristics are preferred. 6 5 4 3 2 1 0 0 2 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 20 40 60 % Relative Humidity 80 100 Fig 8 DSCB1C Temperature response at 60%RH Precautions and Recommendations The ionisation current is approximately 16pA. Precautions to preserve the insulation of the input connection path to the electronics are critical for correct operation of the device. In particular the collector electrode and its connections must remain free from contamination e.g. from solder flux or manual contact. The lead from the collector electrode to the detector circuit should preferably be short and clear of the circuit board and other components. Direct connection between pin-15 of the detector chip and the collector electrode within the recess of the chamber is highly recommended. Balance Voltage (V) 7 6 5 4 3 2 1 0 The chamber is shielded from external electric fields by its outer cover. Suitable shielding should be provided for the associated circuitry, because of the necessarily high impedance of the circuit connected to the chamber collector electrode. 0 Within reasonable limits, the collector electrode potential remains relatively unaffected by temperature, pressure, humidity and wind velocity as shown in fig, 8, 9 and 10. Chambers intended for use at high altitudes may require adjustment of the tripping level of the detector circuit for optimum sensitivity. 20 40 Temperature (C) 60 Fig 9 DSCB1C Air pressure Response Balance Voltage (V) 7 Specification The general specification and operating performance under ambient environmental conditions are as follows: - Temperature 200C ±30C - Ambient pressure: atmospheric, near sea level, clean air - Outer electrode to source electrode potential: 9V - The CEV is nominally 5.6V ±0.4V. - Change in CEV with smoke 1% obscuration /foot* 0.6V typical 4% obscuration / foot* 2.2V typical - Insulation leakage <0.5pA. - Capacity (collector to outer + source electrode) 6pF - Am-241 activity 30kBq (~0.8mCi) ±15% * obscuration limits specified by UL217 (2) 6 5 4 3 2 1 0 0.8 1 1.2 Air Pressure (bar) 1.4 . Fig 10 DSCB1C Air Velocity Response Regulatory Compliance Detector Technology sources used in the detectors meet the regulatory requirements of most national authorities worldwide. Specifically Detector Technology sources comply with: · European Norm EN 54(3) · UK National Radiological Protection Board (NRPB) criteria of acceptability(7) upon which UK legislation relating to smoke detectors is based. · Sources have been recognized by Underwriters Laboratories Inc in compliance with Standard UL 217(2) as a component of smoke alarms and detectors. Balance Voltage (V) 7 6 5 4 3 2 1 0 0 3 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 2 4 6 Air Velocity (m/s) 8 10 Technical Support and Design Services References Design and development services can be provided to assist customers in the development of new and improved products. 1. 'Quality systems: Model for quality assurance in design, development, production, installation and servicing.' BS EN ISO 9001, British Standards Institution, London, 2000. 2. 'Standard for Single and Multiple Station Smoke Detectors.' UL217, Fourth Edition, Underwriters Laboratories Inc., Northbrook, Illinois, 10th May 1993. 3. 'Components of automatic fire detection systems.' EN 54: Part 7, European Commission for Standardization (CEN), Brussels, July 1982. 4. 'Americium-241 alpha foil and sources.' Data Sheet No. 11262, Detector Technology, 1997. 5. 'Safety and Packaging.' Data sheet reference SOU/120/95/KL, Detector Technology, 1995. 6. 'Recommendations for ionization chamber smoke detectors in implementation of radiation protection standards': Section 6 Nuclear Energy Agency, Organisation for Economic Co-operation and Development, Paris, 1977. 7. 'Board Statement on Approval of Consumer Goods Containing Radioactive Substances.' Documents of the NRPB, Volume 3, No. 2, National Radiological Protection Board, Didcot, 1992. 8. 'Smoldering Smoke And Fire Tests for Model DCS.A3.' S2182 78NK7050, Underwriters Laboratories Inc., Northbrook, Illinois, 22nd August 1978. Further information about computational modelling, design and development services offered by Detector Technology can be provided on request. 9. 'Informative Test of AFAR-Equipment.' Report No. 324323, Elektronikcentralen: Danish Research Centre for Applied Electronics, Copenhagen, 10th April 1979. . 10. 'Measurement Report: Radiological Assessment.' EMR/1 34/79, National Radiological Protection Board, Didcot, 1979. Detector Technology has developed advanced computational modelling software, which is capable of modelling the performance of ion chambers as a function of design geometry. An example is a compact design that had been modelled prior to prototyping. The performance predicted by the model was later verified in prototype tests to be similar to the performance of larger standard designs. Fig 11 – Example: compact ion chamber prototype ~1cm height . ~2cm diameter 11. 11.'Analytical Report: NEA 1200°C incineration test.' NRPB/CP 3/016, National Radiological Protection Board, Leeds, 1985. 4 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Quality control contents Routine production checks Special safety performance test on prototypes Measurements Test reports ISO.9001 International quality management system standard 5 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Quality control Quality control of radiation can be divided into four main parts: 1. Routine production checks Quality Assurance Radiation sources are manufactured in accordance with a strict quality assurance program, details of which can be obtained on request. Leakage and contamination tests Stringent tests for leakage are an essential feature of radioactive sources production. They are based on ISO 9978. Some standard methods used for testing radiation sources are listed below. Wipe test I The source is wiped with a swab or tissue, moistened with ethanol or water, the activity removed is measured. Limit: 200Bq (Limit USA: 5nCi) Immersion test II The source is immersed in a suitable liquid at 50°C for at least 4 hours and the activity removed is measured. Limit: 200Bq (Limit USA: 5nCi) Bubble test III The source is immersed in water or a suitable liquid and the pressure in the vessel reduced to 13kPa (100mm Hg). No bubbles must be observed. Krypton emanation test V The source is held under reduced pressure for 24 hours. The content of the chamber is analysed for Krypton-85 by scintillation counting. Limit: 370Bq Krypton emanation test VI The source is held under reduced pressure for 24 hours. The content of the chamber is analysed for Krypton-85 by scintillation counting. The test is repeated after at least 7 days. Limit: 1.85kBq 6 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Quality control 4. Test reports 2. Special safety performance tests on prototypes A test report is supplied with each source or batch of sources. Where appropriate the following information is given: Product code Product description Capsule type ISO classification Special form certificate Serial number of source Measurement check Leakage check Contamination check A radiation source must provide highest possible integrity together with minimum attenuation of the required radiation by the encapsulation materials. A compromise must sometimes be made, particularly for alpha, beta and low energy photon sources. Safety must always be the prime consideration. Standards for the testing of sealed radioactive sources have been specified by ISO.2919 and ISO.9978. ISO.2919 'Sealed radioactive sources — Classification' ISO.9978 'Sealed radioactive sources — leak test methods'. ISO.9001 International Quality Management System Standard This classification system is modeled on USA standard US ANSI N43.6-1997 which also gives a number of comparable leak test methods. In addition to our routine quality control procedures, Detector Technology is approved to the International Quality Management System Standard ISO 9001: 2000. 3. Measurements This Quality Management System is a formal system which defines Quality Policy, describes the necessary organization in place to carry out the policy, and describes the procedures in place which are necessary to carry out and maintain the system. Each source of batch of sources is checked to ensure that the strengths of the sources supplied are within the limits specified. Wherever possible the results of these checks are indicated on the test report. The methods of specifying the strengths of sources are discussed under the heading specification on page E1 and details are included in the appropriate section of this catalog. The System involves the thorough training of all staff, documentation of procedures, maintenance of records and the assessment and rectification of non-conformities. Regular surveillance audits are made by Lloyd's Register Quality Assurance Ltd..*, to ensure that the high standards demanded by ISO.9001 are maintained by Detector Technology to all stages of the source production process from establishing the source specifications, through design, manufacture, test and measurement to dispatch and after sales service. * Lloyd's Register Quality Assurance Ltd. (LRQA) is accredited by the National Accreditation Council for Certification Bodies. 7 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Technical information contents Specifications – SI Units Technical information 8 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Technical information Specification - SI Units The International System (SI) units are a consistent set of units for use in all branches of science. The International Commission on Radiation Units and Measurements (ICRU) has published its recommendations on the quantities and units to be used in the measurement of ionizing radiations and activity. Several countries have already adopted the new SI system and legislation now requires that SI units be used in the UK and Europe from 1st January 1986 onwards. Previously, our catalogs have contained both the old and the new units side by side, or appropriate conversion factors, and this will continue until the new system is accepted by the majority of users. The quantity exposure rate is replaced by the quantity air kerma rate. The preferred SI units for air kerma rate are submultiples of Gray per second. A constant factor may be used to convert from exposure rate to air kerma rate. Quite simply, an exposure of 1 Roentgen per hour (1R/h becomes 2.425 microGray per second (mGy/s), or 8.73 milligray per hour (mGy/h). Gamma radiation sources are specified in terms of the exposure rate or air kerma rate at a distance of 1 meter from the source and at this distance the strength of most sources is such that exposure rate will be in units of mR/h and air kerma rate will be in units of (mGy/h. A conversion factor of 8.73 should therefore be used to convert from mR/h to mGy/h Sources previously specified in terms of equivalent activity may be converted to the new quantity and units by first converting to exposure rate using the appropriate exposure rate constant. A list of exposure rate constants used by Detector Technology for these sources is given in the examples. Conversion from exposure rate to air kerma rate is described in the previous paragraph and is also shown in the examples. In this catalog, source strengths are quoted in appropriate SI units with the previously used quantities and units given alongside. The following quick reference guide gives a useful summary of the relevant quantities, units, conversion factors and prefixes. Some useful examples are given. 9 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Technical information Prefixes for units Quick reference guide to the use of SI units for gamma radiation sources Sub multiples 10-3 10-6 10-9 10-12 10-15 10-18 Specification of output New quantity: Air kerma rate Old quantity: Exposure rate or equivalent activity + exposure rate constant New unit: Gray (Gy) per second (s) Old unit: Roentgen (R) per hour (h) Conversion of activity Multiply value by 8.73 to convert from mR/hour to mGy/h Multiples milli micro nano pico femto atto m m n p f a 103 106 109 1012 1015 1018 kilo mega giga tera peta exa k M G T P E Examples Specification of activity Quantity: Activity (content) New unit: Becquerel (Bq) Old unit: Curie (Ci) Example of the conversion of outputs for an equivalent activity of 1 Curie Nuclide Exposure rate at 1m* Air kerma rate at 1m Activity conversion Multiply value by 37 to convert from kCi to TBq or Ci to GBq or mCi to MBq Multiply value by 27.03 to convert from MBq to mCi or GBq to mCi or TBq to Ci Cs-137 Co-60 0.33R/h 1.30R/h 2.9mGy/h 11mGy/h * The value given are also the recommended exposure rate constant values in units of R m2 h-1 Ci-1 Radiation Protection Quantity: Absorbed dose New unit: Gray (Gy) Old unit: rad Quantity: Dose equivalent (biological dose) New unit: Sievert (Sv) Old unit: rem Examples of conversion for units of content activity 1 Bq = 2.703 x 10-11 Ci = 27.03pCi 1nCi = 3.7 x 10Bq = 37Bq 1 kBq = 2.703 x 10-8 Ci = 27.03nCi 1mCi = 3.7 x 104Bq = 37kBq -5 1 MBq = 2.703 x 10 Ci = 27.03mCi 1mCi = 3.7 x 107Bq = 37MBq 1 GBq = 2.703 x 10-2 Ci = 27.03mCi 1Ci = 3.7 x 1010Bq = 37GBq 1 TBq = 2.703 x 10 Ci = 27.03 Ci 1kCi = 3.7 x 1013Bq = 37TBq Conversion Multiply value by 10 to convert from rad to mGy or rem to mSv Multiply value by 100 to convert from Gy to rad or Sv to rem 10 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Technical information Calibration Notes Some of the sources listed in this catalog can be calibrated. Certificates of measurement quote the results of air kerma rate at a specified distance. Daughter Nuclides Some daughter nuclides may not be in equilibrium with the parent nuclide when source is supplied. In cases where this may occur the transition probabilities for the daughter nuclides relate to disintegrations of each daughter; this is stated in the tables. Daughter nuclides with half-lives greater than the parent nuclide have not been listed since they would be present only in insignificant amounts. Calibration uncertainty The reported uncertainty is based on standard uncertainty multiplied by a coverage factor k = 2, providing a level of confidence of approximately 95%. (ISO Guide, 1995). Particular energies For ß-emission, the end-point energy is quoted. Transition probabilities These are expressed as percentages of the total number of nuclear transformations of the relevant nuclides. For electromagnetic transitions the probability of photo emission has been listed. Abbreviations Half-lives y - years d - days h - hours min - minutes s - seconds ms - milliseconds ms - microseconds Type of decay e.c. - electron capture i.t. - isomeric transition s.f. - spontaneous fission Photons emitted IC - indicates that photons of the stated energy are ~ 100% internally converted. 11 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Source safety contents ANSI / ISO classification Performance requirements IAEA special form Source working life 12 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Source safety The suitability and safety of a source will depend on the intended application and the environment of use of which there will be a wide range. It is the customer's (users) responsibility to ensure the source and its specification is suitable and safe for his particular application and environment of use. This applies to standard products and especially to non-standard products or custom made designs. The information given here is intended for guidance. It is recommended that the standards should be consulted for detailed definitive information. The standard tests for the classification of sealed source performance (ISO 2919) are given in Table 1. Examples of additional tests which may be required for specific applications are given in the appendix to ISO 2919. 1. Classification of sealed source performance A radiation source must provide the highest possible integrity for its contents together with the minimum attenuation of the emitted radiation by the encapsulation materials which is consistent with safety and the intended use. However, safety must always be the prime consideration. The International Organization for Standardization have issued a standard (ISO 2919:1999) which establishes a system of classification of sealed radioactive sources based on test performance. It also specifies production tests, marking and gives an example of a test report. Similar standards are ANSI/HPS N43.6-1997 published in the USA. These standards, to quote from ISO2919, "...provides a set of tests by which the manufacturer of sealed radioactive sources can evaluate the safety of his products in use and by which the user of such sources can select types which are suitable for the required application, especially where the release of radioactive material with consequent exposure to ionizing radiation is concerned." 13 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Source safety Table 1. Classification of sealed source performance Test Class 1 Temperature No test 2 -40°C (20min) +80°C (1 h) 3 4 -40°C (20min) + 180°C (1h) -40°C (20min) + 400°C (1 h) and thermal shock to 20°C 5 -40°C (20min) +600°C (1h) and thermal shock to 20°C 6 X -40°C (20min) Special test +800°C (1 h) and thermal shock to 20°C External pressure No test 25kPa absolute to 25kPa absolute to 25kPa absolute to 25kPa absolute to 25kPa absolute to Special test atmospheric 2MPa absolute 7MPa absolute 70MPa absolute 170MPa absolute Impact No test 50g from 1 m or equivalent imparted energy Vibration No test 3 times 10min 25 3 times 10min 25 to 500Hz at to 50Hz at 49m/s2 (5gn)1) 49m/s2 (5gn)1) and 50 to 90Hz at 0.635mm amplitude peak to peak and 90 to 500Hz at 96m/s2 (5gn)1) 3 times 30min Not used 25 to 80Hz at 1.5mm amplitude peak to peak and 80 to 2000Hz at 196m/s2 20gn)1) Puncture No test 1 g from 1 m or equivalent imparted energy 50g from 1 m or equivalent imparted energy 200g from 1 m or 2kg from 1 m or equivalent equivalent imparted energy imparted energy 10g from 1m or equivalent imparted energy 5 kg from 1 m or equivalent imparted energy 20kg from 1 m or Special test equivalent imparted energy Not used 300g from 1 m or 1 kg from 1 m or equivalent equivalent imparted energy imparted energy Special test Special test 1) Acceleration maximum amplitude Each test can be applied in several degrees of severity which is expressed as a five digit code representing the class numbers which describe the performance for each of the tests. The digits are preceded by the letter C or E indication respectively whether the activity of the source is greater or lesser than a prescribed amount. The limits depend on the toxicity etc of the active components (See ISO 2919) Compliance with the tests is determined by the ability of sealed source to maintain its leak tightness. The leakage tests are defined in ISO 9978. Notes to table 1. 1. Details of the testing procedures are given in ISO.2919 and ANSI N43.6-1997. A further class X can be used where a special test procedure has been adopted. 2. External pressure 100kPa=1 atmosphere (approximate) 3. Impact test The source, positioned on a steel anvil, is struck by a steel hammer of the required weight; the hammer has a flat stricking surface, 25mm diameter, with the edges rounded. 4. Puncture test The source, positioned on a hardened steel anvil, is struck by a hardened pin, 6mm long, 3mm diameter, with hemispherical end, fixed to a hammer of the required weight. 14 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Source safety 2.- Performance requirements for typical uses Typical uses and minimum performance requirements (ISO 2919) are given in Table 2. Table 2 Sealed source classification (performance) requirements for typical usage Sealed source class, depending on test Temperature Pressure Impact Vibration Puncture Radiography-Industrial Sealed source Source to be used in device 4 4 3 3 5 5 1 1 1 1 Medical Radiography Gamma teletherapy Brachytherapy (6)1) Surface applicators2) 3 5 5 4 2 3 3 3 3 5 2 3 1 2 1 1 2 4 1 2 4 4 3 3 3 2 3 3 3 2 Beta gauges and sources for low-energy gamma gauges or x-ray fluorescence analysis2) 3 3 2 2 2 Oil-well logging 5 6 5 2 2 Portable moisture and density gauge (including hand-held or dolly-transported) 4 3 3 3 3 General neutron source application (excluding reactor startup) 4 3 3 2 3 Calibration source activity >1 MBq 2 2 2 1 2 4 5 3 3 3 4 2 2 3 4 3 2 3 2 2 2 2 2 2 1 2 2 1 2 2 Gamma gauges (medium and high energy) Gamma irradiation sources Ion generators3) Unprotected source Source in device Category 1 2) [3], [5] Categories II,III and IV 3) Chromatography Static eliminators Smoke detectors2) 1) Sources of this nature may be subject to severe deformation in use. Manufactures and users may wish to formulate additional or special test procedures. 2) Excluding gas-filled sources. 3) "Source in device" or a "source assembly" may be tested. The requirements take into account normal usage but do not include exposure to fire, explosion or corrosion. The tests specified do not cover all usage situations and where conditions do not match those specified in Table 2 appropriate tests on an individual basis may be required. 15 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320 Current (10-11 Amps) Source safety RECOMMENDED WORKING LIFE OF SEALED RADIATION SOURCES 3. IAEA special form The Recommended Working Life (RWL) is the maximum period within which Detector Technology expects the source to meet it's design requirements under proper conditions of environment and usage. A Source should be replaced within the Recommended Working Life or a proper assessment should be made to verify its suitability for continued use. Sealed sources which have passed the performance tests described in the regulations for the Safe Transport of Radioactive Material, 1996 Edition (Revised), International Atomic Energy Agency (IAEA), No. TS-R-1 (ST-1, Revised) may be approved as Special Form Material by a National Competent Authority. Designation as Special Form allows an increase in the activity limits for shipment as a Type A package. Detector Technology makes no warranties, expressed or implied, or guarantees as to how long any source can actually be safely used. Adverse environments, conditions, improper usage or materials combination in usage could effect the appearance and integrity of the source and it is the user's responsibility to carry out routine inspection and testing to determine when it should be replaced. This catalogue indicates whether Special Form Certificate (SFC) were issued for approved items in the catalog. Detector Technology will determine the RWL based on the construction of the source, application, test data and operational experience. Issued by the Detector Technology Board June 2003 16 USA: QSA Global Inc. 40 North Avenue, Burlington MA 01803 - Phone No: +1 781 272-2000 Hong Kong: Detector Technology Limited, Suites 1401-02, 14/F., Dah Sing Financial Centre 108, Gloucester Road, Wanchai, Hong Kong, Phone No: + 852 2596-7711 Germany: Nuclitec GmbH, Gieselweg 1, 38110 Braunschweig - Phone No: +49 (0)5307 9320