.. .. .. .. .. KETEK GmbH Hofer Str. 3 81737 München Phone +49-89-673467-70 Fax +49-89-673467-77 KETEK GmbH VITUS Silicon Drift Detectors . . . . User’s Manual . . . . . . Steffen Pahlke Rev. 3 Information furnished by KETEK is believed to be accurate and reliable. However, no responsibility is assumed by KETEK for its use, nor for any infringements of patents or other rights of third parties that may result from its use. Specifications given in this document subject to change without notice. No license is granted by implication or otherwise under any patent or patent rights of KETEK. Trademarks and registered trademarks are the property of their respective owners. KETEK GmbH, Hofer Str. 3, D-81737 München, Germany Tel: +49-(0)89-67346770 Fax: +49-(0)89-67346777 www.ketek.net ©2012 KETEK GmbH. All rights reserved. KETEK VITUS SDD Manual 1. Table of Contents 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. Table of Contents............................................................................................................................ 3 Revision History .............................................................................................................................. 3 Features .......................................................................................................................................... 5 Applications ..................................................................................................................................... 5 Functional Block Diagram ............................................................................................................... 5 General Description ........................................................................................................................ 5 Safety .............................................................................................................................................. 6 General Restrictions ....................................................................................................................... 7 Specifications .................................................................................................................................. 8 Absolute Maximum Ratings ........................................................................................................ 9 Ambient Conditions .................................................................................................................. 10 ESD Caution ............................................................................................................................. 10 Pin Configuration and Functional Descriptions ........................................................................ 10 Typical Performance Characteristics ........................................................................................ 11 Theory of Operation .................................................................................................................. 17 Applications and Operations Information ................................................................................. 19 16.1. Wiring ................................................................................................................................... 19 16.2. Mechanical Connection ........................................................................................................ 19 16.3. Readout Circuit for Temperature Sensor ............................................................................. 20 16.4. Operating Voltages .............................................................................................................. 21 16.5. Preamplifier Design .............................................................................................................. 22 16.6. Peltier Characteristics .......................................................................................................... 23 Collimator ................................................................................................................................. 25 Outline Dimensions .................................................................................................................. 26 Footprint ................................................................................................................................... 27 Ordering Guide ......................................................................................................................... 28 Optional .................................................................................................................................... 28 Contact ..................................................................................................................................... 29 2. Revision History 11/07 – Revision 0: Initial Version 12/03 – Revision 1: Minor textual changes, accommodation of Specifications 12/08 – Revision 2: Minor textual changes, accommodation of Specifications 12/11 – Revision 3: Update Gain of SDD, update Typical Performance Characteristics due to new FET, update spectral definitions Rev. 3 Page 3 of 29 KETEK GmbH KETEK VITUS SDD Manual Rev. 3 Page 4 of 29 KETEK GmbH KETEK VITUS SDD Manual 3. Features Silicon Drift Detector energy resolution down to 123eV FWHM at Mn-Kα excellent peak-to-background operable at an ambient temperature of up to +80°C with excellent performance high count rate capability up to 1,000,000 cps efficient integrated Peltier element no liquid nitrogen cooling required radiation hardness during more than 10 years standard count rate exposure easy to use active areas from 7 to 100mm² available 4. Applications XRF µ-XRF EDX EDS TXRF XRD Handheld 5. Functional Block Diagram Fig. 1: KETEK VITUS SDD Functional Block Diagram 6. General Description KETEK VITUS Silicon Drift Detectors (SDD) are the state-of-the-art X-ray detectors based on silicon substrates. Their typical X-ray energy range is between 0.2keV and 30keV. They are used in applications such as EDX, EDS, XRF, TXRF in bench top as well as in handheld based systems. Due to their wide operating temperature range they are especially suited for industrial and automotive applications. Rev. 3 Page 5 of 29 KETEK GmbH KETEK VITUS SDD Manual 7. Safety It is strongly recommended to read this user manual carefully and completely before installing or activating the SDD. Please keep this user manual always with the system for that any operator can get this important information. In case of resale – even when second hand – or in case of scrapping at the end of lifetime this manual has to be given along with the system. Please handle the attached documents “Beryllium Material Data Sheet” and “Statement of contamination…” the same way. WARNING! The detector contains a thin, fragile Be window. If this window is damaged, the detector will be destroyed and cannot be repaired. Be windows damaged due to improper handling are not covered under warranty. This product uses – a very small amount - of toxic beryllium material at the inner side of the detector foil. Beryllium is preferred as an entrance window coating because it provides a light-tight seal and, further, does not introduce spurious peaks in the measured spectrum. In normal operation there is no danger to get in contact with any toxic materials. If the SDD window was destroyed by accident, follow our safety instructions. Scrapping at end of lifetime has to be done according to the (local) legal requirements. Make the “Beryllium Material Data Sheet” available to your waste disposal contractor. Do not scrap the SDD to your domestic waste. Due to the very thin window foil you should take care neither to touch it with fingers nor to bring other things or materials under test too near to it. Keep away excessive dust particle streams from the SDD window. Excessive electrostatic discharge might destroy the window. Take care ESD is well bled off in your application. Some of the SDD types are evacuated. A damaged entrance window may implode scattering small beryllium particles in the immediate vicinity of the SDD. In this case, rigorously clean the SDD and its surrounding area following all the precautions mentioned in the “Beryllium Material Safety Data Sheet”. Always keep the SDD protection cap with the system, even if fixed mounted. It’s necessary for cleaning, service and shipping to be able to protect the beryllium window. CAUTION! High voltages need to be applied to the detector for use. To prevent electrical shock, do not touch the detector. Do not drop or cause mechanical shock to the detector. Components inside the detector are mechanically fragile and may be damaged if the unit is dropped. Avoid temperature shocks. If the detector is out of allowed temperature range, make sure to acclimate slowly. Avoid air pressure shocks. Especially in evacuated applications take care to ventilate slowly. Let the protection cap be mounted at the SDD as long as the system isn’t mounted in its end application. Your end application has to be designed that way to make unexpected, damaging contact with the SDD window impossible. Make sure your samples under test might never touch the SDD window. Do not remove the protective cap from the detector until data is to be taken. The detector window is made from thin beryllium which is extremely brittle and can shatter very easily. Do not have any object come in contact with the window. Do not touch the detector because the oil from the fingers will cause it to oxidize. Use gloves. The window cannot be repaired. If the window is damaged the detector assembly must be replaced. Be windows damaged due to improper handling will not be covered under warranty. Keep the protective cover nearby at all times and cover the detector when the instrument is not in use. Rev. 3 Page 6 of 29 KETEK GmbH KETEK VITUS SDD Manual Radiation damage to the detector will occur if it is exposed to a high flux environment. Synchrotron Radiation Beams should be modified with attenuators before they are allowed to strike the detector or the fluorescence target. Damage to the detector will be permanent if the flux from an X-Ray Tube, a strong nuclear radiation source, or an accelerator is not attenuated. No user serviceable parts inside the units. Refer servicing to KETEK GmbH. To prevent electrical shock, do not remove covers. Keep the device dry and clean! Warranty KETEK GmbH warrants to the original purchaser this instrument to be free from defects in materials and workmanship for a period of one year from shipment. KETEK GmbH will, without charge, repair or replace (at its option) a defective instrument upon return to the factory. This warranty does not apply in the event of misuse or abuse of the instrument or unauthorized alterations or repair. KETEK GmbH shall not be liable for any consequential damages, including without limitation, damages resulting from the loss of use due to failure of this instrument. All products returned under the warranty must be shipped prepaid to the factory with documentation describing the problem and the circumstances under which it was observed. Additionally the statement of contamination must be filled out completely and returned with the product. KETEK must be notified prior to return shipment. The instrument will be evaluated, repaired or replaced, and promptly returned if the warranty claims are substantiated. A nominal fee will be charged for unsubstantiated claims. Please include the model and serial number in all correspondence with KETEK. Care Instructions Do not clean the SDD under any circumstances. Do not use any alcoholic, acid or rubbing cleaning agents. 8. General Restrictions and Recommendations Rev. 3 - do not use detector without heat sink connection. Overheating will destroy the module - do not solder the pins or any other part of the detector module - avoid touching the detector module - use gloves to avoid corrosion - avoid touching the entrance window of the detector module. It contains hazardous materials Page 7 of 29 KETEK GmbH KETEK VITUS SDD Manual 9. Specifications Parameter VOLTAGES R1 RX BACK FET-Substrate/Bulk Drain CURRENTS R1 = RX BACK* Drain Temp.-Sensor PELTIER (TEC) Voltage Current Voltage Current Gain Conditions/Comments measured before filtering Min Typ Max Tolerance -25 -160 -100 -7 1 -20 -130 -65 -4 3 -5 -80 -35 -2 4 ±1 ±5 ±2 ±1 ±0.1 V V V V V 10 20 at maximum cooling 1 2 2 3 4 0.1 1 5 -35°C operating temp @ 20°C heat sink temp. H7 / H20 / H30 / H50 1.6 1.7 1.8 H7 / H20 / H30 / H50 250 300 350 maximum cooling @ 20°C heat sink temp. H7 / H20 / H30 / H50 3.0 3.3 3.6 H7 / H20 / H30 / H50 600 650 700 0.9 ±5 ±0.1 ±0.1 ±0.1 µA nA mA µA ±0.1 ±10 V mA 5 ±0.1 ±10 ±30% Unit V mA mV/keV * Back voltage absolute value should not exceed one half of the RX voltage absolute value by more than 10V These specifications refer to the whole VITUS SDD class. Please refer to the individual SDD datasheet for detailed information. Rev. 3 Page 8 of 29 KETEK GmbH KETEK VITUS SDD Manual 10. Absolute Maximum Ratings Parameter VOLTAGES R1 RX BACK* FET-Substrate/Bulk Peltier H7/H20/H30/H50 Peltier H80 Peltier H7LE/H15LE/H20LE CURRENTS RX Drain Temp.-Sensor Peltier H7/H20/H30/H50 Peltier H80 Peltier H7LE/H15LE/H20LE Radiation Hardness @17keV Torque Stresses beyond those listed under Absolute Rating Maximum Ratings may cause permanent ≥ -30V ≥ -180V ≥ -100V ≥ -15V ≤ 3.6V ≤ 4.5V ≤ 4V damage to the device. This is a stress rating only; functional operation of the device at these or any other conditions above those indicated in the applications and operations section of this specification is not implied. Exposure to absolute ≤ 1mA ≤ 10mA ≤ 50µA ≤ 700mA ≤ 1000mA ≤ 900mA 12 ≤ 10 Photons ≤ 0.8Nm maximum rating conditions for extended periods may affect device reliability. * Back voltage absolute value should not exceed one half of the RX voltage absolute value by more than 10V Rev. 3 Page 9 of 29 KETEK GmbH KETEK VITUS SDD Manual 11. Ambient Conditions Parameter OPERATING Temperature Humidity Pressure Pressure Change STORAGE Temperature Humidity Min Max Unit 0 10 0 60 80 1.1 100 °C % RH atm mbar/s 0 10 60 90 °C % RH Conditions non condensing non condensing 12. ESD Caution ESD (Electrostatic Discharge) sensitive device. Charged devices and circuit boards can discharge without detection. Although this product features patented or proprietary protection circuitry, damage may occur on devices subjected to high energy ESD. Therefore, proper ESD precautions should be taken to avoid performance degradation or loss of functionality. 13. Pin Configuration and Functional Descriptions VITUS H7, H20, H30, H50 Pin No. 1 2 3 4 5 6 7 8 9 10 11 12 Rev. 3 Description Temp Sensor - /GND Temp Sensor + Ring 1 Back Reset FET-Substrate / Bulk Source Drain Feedback Peltier + Ring X Peltier - VITUS H80, R100 Mnemonic TD- /GND TD+ R1 BK RES SUB / BULK FFS FFD FB P+ RX P- Pin No. 1 2 3 4 5 6 7 8 9 10 11 12 Page 10 of 29 Description Peltier Ring X Feedback Peltier + Drain Source Reset FET-Substrate / Bulk Back Ring 1 Temp Sensor + Temp Sensor - /GND Mnemonic PRX FB P+ FFD FFS RES SUB / BULK BK R1 TD+ TD- /GND KETEK GmbH KETEK VITUS SDD Manual 14. Typical Performance Characteristics Fig. 2: Typical KETEK VITUS Silicon Drift Detector Spectrum of H7 active area type SDD with an Fe-55 source, taken with a KETEK preamplifier and a digital pulse processor. Fig. 3: Definition of Peak-to-Background (P/B) and Peak-to-Tail (P/T) of a typical spectrum taken with a KETEK preamplifier and a digital pulse processor. Rev. 3 Page 11 of 29 KETEK GmbH KETEK VITUS SDD Manual 1.0 0.9 0.8 Transmission 0.7 0.6 8 µm 12.5 µm 25 µm 0.5 0.4 0.3 0.2 0.1 0.0 500 1000 1500 2000 2500 3000 Photon energy (eV) Fig. 4: Typical transmission of KETEK Silicon Drift Detectors with different Beryllium entrance window thickness Fig. 5: Typical transmission of KETEK Silicon Drift Detectors with low energy AP3.3 entrance window Fig. 6: Typical absorption efficiency of KETEK Silicon Drift Detectors with a thickness of 450µm and 8µm Beryllium window Rev. 3 Page 12 of 29 KETEK GmbH KETEK VITUS SDD Manual Fig. 7: Typical control range of Silicon Drift Detector chip temperature at different ambient temperatures Fig. 8: Typical calculated energy resolutions of Silicon Drift Detectors for low energies Fig. 9: Typical Input to Output Count Rate Ratio (Throughput) for different Peaking Times taken with a KETEK VITUS H30 SDD and an XIA Mercury Digital Pulse Processor Rev. 3 Page 13 of 29 KETEK GmbH KETEK VITUS SDD Manual H7 H20 H30 H50 H80 H7-LE H15-LE Fig. 10: Typical KETEK VITUS Silicon Drift Detector Spectrum with an Fe-55 source, taken with an KETEK preamplifier and an XIA Mercury digital pulse processor for the different VITUS active areas. Rev. 3 Page 14 of 29 KETEK GmbH KETEK VITUS SDD Manual H7 H15 / H20 H30 H50 H80 Fig. 11: Typical energy resolution for different chip operating temperatures dependent on the Peaking Time for different SDD sizes. Rev. 3 Page 15 of 29 KETEK GmbH KETEK VITUS SDD Manual H7 H15 / H20 H30 H50 H80 Fig. 12: Typical energy resolution for different input count rates dependent on the Peaking Time for different SDD sizes. Rev. 3 Page 16 of 29 KETEK GmbH KETEK VITUS SDD Manual 15. Theory of Operation The silicon bulk of the Silicon Drift Detector (SDD) has to be depleted completely to make the sensor sensitive for incoming photons. By applying a negative voltage to the back contact of the SDD, the detector bulk is completely depleted. An incoming photon will generate a number of electrons and holes dependent on its energy. The holes drift to the back side of the detector formed by the large area back contact whereas the electrons drift to the anode where the accumulated charge can be measured or read out. The drift field for the electrons is applied by a ring structure on one side of the SDD with a negative voltage at the outer ring (Ring X) and a voltage close to 0V at the innermost ring (Ring 1). Fig. 13: Silicon Drift Detector potential diagram The anode is connected to: a) the gate of the first field effect transistor (FET), b) the feedback capacitance (CFB) and c) the cathode of the reset diode (D RES). The combination of a) and b), the FET and the feedback capacitance, respectively, forms the first part of a charge sensitive amplifier, used to read out the accumulated electrical charge. The combination forms a transimpedance (current to voltage) and an integrator when connected to the subsequent stages of the pre-amplifier. Therefore the source of the FET has to be connected to ground and the drain voltage and current need to be set appropriately (typically 3V and 3mA). The operating point of the FET is optimized by setting its bulk or substrate voltage. GND UOR Driftfield UIR Anode -V UBACK Homogeneous thin entrance window Fig. 14: Silicon Drift Detector schematic Rev. 3 Page 17 of 29 KETEK GmbH KETEK VITUS SDD Manual The FET is operated in a common source configuration. The leakage current sensed at the FET gate causes a ramp signal at the output of the pre-amplifier. The slope of the ramp signal, and thus its frequency, is dependant on the operating temperature. The incoming photons generate short current pulses, with a certain rise time (dependant on the location of interaction of the x-ray with the SDD chip), and a certain duration and amplitude (dependent on the energy of the incoming photon). In turn, these short pulses generate steps superimposed on the pre-amplifier’s ramped output signal. The height of a step contains the information necessary to determine the energy of the interacting photon. 1,5 Preamp Out Reset Out 1 Amplitude [V] 0,5 0 -0,5 -1 -1,5 0 5 10 15 20 Time [ms] Fig. 15: Typical KETEK Preamplifier Output Signal including Preamplifier Reset Pulse Output using a KETEK VITUS SDD irradiated with an Fe-55 Source at -35°C Operating Temperature 0,04 Amplitude [V] 0 -0,04 -0,08 Preamp Out -0,12 -0,16 0 20 40 60 80 100 120 Time [µs] Fig. 16: Zoom of Figure 15, typical KETEK Preamplifier Output Signal including Preamplifier Reset Pulse Output using a KETEK VITUS SDD irradiated with an Fe-55 Source at -35°C Operating Temperature showing step like pulses Rev. 3 Page 18 of 29 KETEK GmbH KETEK VITUS SDD Manual 16. Application and Operation Information For (optimal) operation, SDDs require the application of several voltages and integration with a charge sensitive amplifier and other pulse forming electronics (either analog or digital). Typically, a high voltage DC power supply feeds the drift ring voltages; a high current, linearly regulated, low voltage power supply feeds the Peltier element; and a bipolar, linearly regulated power supply feeds the charge sensitive amplifier and pulse forming electronics. The drift ring voltages can be generated from a filtered high voltage rail, by using several voltage dividers. Each detector may have individual ring currents. Thus potentiometers should be used for voltage adjustments as the voltage drop at the voltage dividers depends on the ring currents. Fig. 17: KETEK Silicon Drift Detector connected to typical preamplifier board – block diagram The Peltier power supply should be regulated with a PI/PID loop to keep the operating temperature of the SDD chip stable. Therefore it is necessary to read out the temperature sensor of the SDD. 16.1. Wiring The SDD should be placed as close as possible to the preamplifier. It is recommended to shield at least the preamplifier connections. It is strongly recommended using a single point ground. Please note that also the housing of the SDD should be connected to ground. 16.2. Mechanical Connection WARNING: Do not operate the detector without proper heat sink connection. Overheating of the detector will destroy the module. It is strongly recommended to install the detector connected to a proper heat sink. Dimensioning the heat sink is dependant on ambient temperature, air ventilation, operating temperature of the SDD, surface area and its condition. The guaranteed operating temperature is always related to the heat sink temperature. Therefore the minimum operating temperature can vary and is directly dependant on the quality of the heat sink interconnection. Rev. 3 Page 19 of 29 KETEK GmbH KETEK VITUS SDD Manual 16.3. Read out Circuit for Temperature Sensor a) Temperature Diode: Using a diode as temperature sensor leads to a linear relationship between the measured voltage and sensor temperature. The line’s slope depends on the diode bias current. For the recommended 1µA, the slope is 2.35mV/K. It is recommended to apply a constant current. b) Thermistor (NTC resistor): In case of the thermistor the temperature function is given by the following equation: 1 3 1.129241 103 2.341077 10 4 ln( R) 8.775468 108 ln( R) T The function is shown in the following plot. At 25°C the resistance is 10kΩ. 1E7 Resistance [Ohm] 1000000 100000 10000 1000 100 -100 -50 0 50 100 150 Temperature (°C) Fig. 18: Temperature function of a thermistor as SDD temperature sensor To read out the temperature sensor, the following schematic is recommended. Although a diode (D1) is shown in the schematic, it may be replaced with a thermistor (say, Rt); the equations given below apply, if D1 is replaced with Rt. R4 limits the maximum current through the temperature sensor and should be set as follows: R4 U V1 I I ( D1) For example: The voltage V1 is +5V and the current I(D1) should be 1µA. This leads to R4=5MΩ. R1 and R2 form a voltage divider representing the offset voltage. They can be used to set the circuit’s signal swing, given the operational demands on the SDD, e.g. if an ADC is used to digitize the voltage, tuning R1 and R2 would ensure the desired temperature range corresponds to voltage values in the ADC’s range. R1, R2 and R3 determine the gain of the circuit. The gain can be calculated as follows: A 1 Rev. 3 R3 ( R1 R 2) Page 20 of 29 KETEK GmbH KETEK VITUS SDD Manual Fig. 19: Typical Read out Circuit for temperature sensors with linearization, offset correction and gain. 16.4. Operating Voltages Several voltages are needed for operating the detector (exact values are given in each detector data sheet), for example: 1. Ring 1 = approx. -20V 2. Ring X = approx. -130V 3. Back = approx. -65V The detector voltages should be filtered using the following combinations of resistors and capacitors providing low pass filters: 1. Ring 1: RR1 = 15kΩ, CR1 = 220nF 2. Ring X: RRX = 500kΩ, CRX = 47nF/250V 3. Back: RBack = 1MΩ, CBack = 47nF/250V Fig. 20: Operating voltages filtering block diagram Rev. 3 Page 21 of 29 KETEK GmbH KETEK VITUS SDD Manual Before switching on the system, the output-signal of the preamplifier and the shaped signal should be connected to an oscilloscope. The preamplifier operating voltage must be switched on first. The detector voltages should be switched on in the following order: R1 – RX – Back The voltages to be applied must be set according to the detector datasheet. Typical currents flowing are several μA through Ring 1 and Ring X (voltage divider) and approx. 1nA for the back contact if the back voltage is applied. R1 and RX currents should be equal! After switching on the detector voltages the signal of the preamplifier should show a ramp. The ramp period depends on the chip temperature. At -35°C the ramp period should be in the range of several microseconds. 16.5. Preamplifier Design For the design of the preamplifier it is recommended to use the FET in the common source configuration. Therefore the source of the FET can be connected directly to signal ground. The drain drives the signal. The substrate or bulk should be adjusted to the value given in the datasheet of each single SDD. Also a low pass filter should be used to suppress any noise. Typical values are: Substrate/Bulk: RSUB = 10kΩ, CSUB = 4.7µF/16V Tantalum, low ESR The drain can be driven by a simple current source formed by a resistor. Additional low pass filtering is mandatory. Tantalum capacitor with low ESR of at least 100µF should be chosen. The Drain and Feedback lines should be well separated to avoid any ringing or crosstalk. It is recommended to shield at least one of the above lines. The Reset circuit should include a current limiter. This will protect the sensitive reset diode mechanism inside the SDD. It is recommended to use an in-line resistor of at least 2kΩ. Fig. 21: Preamplifier connection block diagram Rev. 3 Page 22 of 29 KETEK GmbH KETEK VITUS SDD Manual 16.6. Peltier Characteristics The KETEK Silicon Drift Detectors are provided in three different performance grades, based on the package’s internal atmosphere and size: evacuated TO-8 packages (H7, H20, H30, and H50); evacuated non-TO-8 packages for larger devices (H80, R100); and, low-energy, nitrogen filled TO-8 packages (H7-LE, H15-LE). The three types have different cooling capabilities because of the different internal atmosphere (vacuum or nitrogen) and different sizes. 4 H7-LE 3 H80 Power [W] H7 2 1 0 -60 -50 -40 -30 -20 -10 0 10 20 Temperature [°C] Fig. 22: Typical power consumption of the three different KETEK VITUS SDDs It is strongly recommended to limit the current as mentioned in chapter “10. Absolute Maximum Ratings”. Stresses above those listed under “Absolute Maximum Ratings” may cause permanent damage to the device. Functional operation of the device at these or any other conditions above those indicated in the applications and operations section of this specification is not implied. Exposure to absolute maximum rating conditions for extended periods may affect device reliability. Please note that the behaviour of the Peltiers can vary with changed ambient temperatures. The efficiency of the Peltier elements is increasing approximately by 0.5K for each Kelvin of increasing ambient temperature. Additionally the step response factor will change which will influence the parameters of the control loop for the regulation of the operating temperature. Rev. 3 Page 23 of 29 KETEK GmbH KETEK VITUS SDD Manual 20 10 0 100mA Temperature [°C] -10 -20 200mA -30 300mA -40 400mA -50 500mA 700mA -60 0 50 100 150 200 250 300 350 400 Time [s] Fig. 23: Typical H7 step response functions for different Peltier currents using a diode as temperature sensor with 1µA operating current and 10V compliance voltage. 20 10 100mA 0 Temperature [°C] 200mA -10 300mA -20 400mA 500mA -30 600mA 700mA -40 800mA 900mA -50 1000mA -60 0 50 100 150 200 250 300 350 400 Time [s] Fig. 24: Typical H80 step response functions for different Peltier currents using a diode as temperature sensor with 1µA operating current and 10V compliance voltage. 20 100mA Temperature [°C] 0 200mA 300mA 400mA -20 500mA 600mA 700mA 900mA -40 -60 0 50 100 150 200 250 300 350 400 Time [s] Fig. 25: Typical H7-LE step response functions for different Peltier currents using a diode as temperature sensor with 1µA operating current and 10V compliance voltage. Rev. 3 Page 24 of 29 KETEK GmbH KETEK VITUS SDD Manual 17. Collimator The KETEK Multilayer Collimator consists of a Tantalum (Ta) foil covered with stacked layers of Chromium (Cr), Titanium (Ti) and Aluminium (Al). The purity of the layers is ≥99%. All collimators are mounted on-chip. Fig. 26: KETEK multi-layer collimator Optionally, KETEK offers an external outer clip-on collimator VPROTECT. Depending on the application, the geometry of the x-ray beam can differ. To avoid any foreign absorption or fluorescence the additional collimator can optimize the beam geometry. Fig. 27: KETEK additional external clip-on collimator Rev. 3 Page 25 of 29 KETEK GmbH KETEK VITUS SDD Manual 18. Outline Dimensions H7LE H15LE Ø 4.78 H7 H20 H30 H50 H80 R100 Fig. 28: Outline dimensions of the different KETEK VITUS Silicon Drift Detector types Rev. 3 Page 26 of 29 KETEK GmbH KETEK VITUS SDD Manual 19. Footprint For H7, H20, H30, H50 SDDs: (Bottom View), M4x6 Screw Mating connectors: - Type Tyco Electronics/AMP 6-5330808-5 For H80 and R100 SDDs: (Bottom View), M6x8 Screw Mating connectors: Rev. 3 - Type Tyco Electronics/AMP 2-5331272-3 - Type Tyco Electronics/AMP 2-5331272-7 Page 27 of 29 KETEK GmbH KETEK VITUS SDD Manual 20. Ordering Guide Encapsulation Window Cap material Collimator - Active area - window Chip entrance O Temp. Sensor 2 Peltier F FET 5 450µm Chip thickness Product VITUS V Example: V5F2T0-H30-ML8BEV: VITUS 450µm SDD Chip with low capacitance FET and a Thermistor as temperature sensor, active area of 30mm² with high peak-to-background ratio, multilayer collimator in a bevelled cap with a Be window sealed under vacuum. 21. Optional Optional available are different KETEK products in combination with the VITUS Silicon Drift Detector: - KETEK Preamplifier: High performance stand-alone preamplifier for SDD applications - KETEK VICO: VITUS Components, -PA: Preamplifier, -TC: TEC/Peltier Controller, -HV: High Voltage Power Supply, -DP: Digital Pulse Processor, -EV: Evaluation Board - KETEK VIAMP: VITUS SDD in combination with preamplifier - KETEK AXAS: Analytical X-ray Acquisition System - KETEK VPROTECT: external collimator For detailed information please contact KETEK Sales and Marketing Office. Rev. 3 Page 28 of 29 KETEK GmbH KETEK VITUS SDD Manual 22. Contact KETEK Headquarter Sales Office KETEK GmbH Hofer Str. 3 81737 München Email info@ketek.net Phone +49 (0) 89 673467 75 Fax +49 (0) 89 673467 77 www.ketek.net Rev. 3 Page 29 of 29 KETEK GmbH