www.CTLGroup.com Leading Solutions in Materials Science Laboratories overview CTLGroup’s world-class laboratories are designed and staffed to provide the most demanding Quality Management System for routine and complex analysis testing of materials and structural components. Our scientists and engineers regularly help solve a wide range of problems in cementitious materials, aggregates, building systems, and metals, and develop specialized testing programs for unique challenges. testing services ww Analytical Chemical Testing ww Fatigue Testing (Stay Cable,AREMA, AAR) ww Mechanical Behavior Testing ww Mortar | Cement | Concrete Testing ww Nondestructive Testing ww Petrography ww Physical Testing ww Specialized Testing quality management system (QMS) CTLGroup has one of the most demanding QMS for laboratory testing of materials and structural components. Through our QMS, our firm has achieved various accreditations and certifications: ww IAS ISO 17025 accredited ww AASHTO accredited ww 10 CFR 50, Appendix B/NQA-1 Compliant ww ISO 9001:2008 Bureau Veritas ww ACI certified technicians ww Association of American Railroads ww Laboratories are validated by US Army Corps of Engineers ww Stadium® certified user CORPORATE OFFICE | LABORATORIES 5400 Old Orchard Road Skokie, IL 60077 800.522.2285 For decades, our experts have been involved in the development of nationally recognized tests and standards, giving them unique insight and ability to create solutions. With 60,000 square feet of laboratory facilities on campus, it enables the firm to provide a combination of testing, research and engineering services rarely matched in the industry. We have an unparalleled capability to not only perform tests and evaluations, but to also interpret the data and translate them into meaningful results and action plans. Laboratory Facilities & Resources CTLGroup’s laboratory facilities are internationally respected as one of the most comprehensive testing and research facilities in cementitious materials, chemical admixtures, mortars, construction products and structural systems. The firm’s 60,000 square feet of facilities consist of industry-leading: Materials Laboratories (Analytical Chemical, Mortar, Cement, Concrete, Physical Testing) Petrography Laboratory Creep & Shrinkage Laboratory Structural & Transportation Laboratory (One of the largest private structural labs in the U.S., conducting static or dynamic testing of full-scale engineered systems and components. CTLGroup’s laboratory staff comprises several PhDs, registered professional engineers and accredited technicians. Our team includes chemists, process engineers, chemical engineers, a metallurgist, pavement engineers, civil engineers and materials engineers, many of whom are world-recognized authorities in their fields. We are multi-disciplinary professionals accustomed to working together to meet our clients’ needs. Testing Areas of Scope: Materials analysis & characterization Materials performance assessment Research & product development Failure Analysis Construction materials optimization Service life prediction and modeling Specialized Testing Materials Consulting www.CTLGroup.com S E R V I C E | at-a-glance CTLGroup’s scientists and engineers help solve a range of materials-related problems in cementitious materials. Our cement chemists and process engineers can address any problem in cement manufacturing, while our materials, pavement and structural engineers help clients create structures that are strong, stable and durable. Working together, our experts address problems by applying in-depth knowledge of how cementitious materials work, while drawing on extensive experience to ensure that the solutions offered are practical and cost effective. A Matter of Scale Please visit our world-class laboratories that provide the most demanding Quality Management Systems for the testing of materials and structural components. CORPORATE OFFICE | LABORATORIES 5400 Old Orchard Road Skokie, IL 60077 800.522.2285 AUSTIN OFFICE 3737 Executive Center Drive, Suite 255 Austin, TX 78731 512.219.4075 NAPERVILLE OFFICE 40 Shuman Boulevard, Suite 218 Naperville, IL 60563 630.995.3949 Engineers normally work in large dimensions without always needing to consider what is happening at a very small scale. On the other hand, scientists often deal with interactions at a molecular scale. CTLGroup’s unique synergy means that our engineers and scientists straddle this dimensional divide, thus enhancing our approach to those seemingly impossible problems in your concrete. Some Problems We’ve Solved Identify causes and suggest solutions for blockages in a cement plant kiln system Analyze a bridge’s environment and design a suitable high-performance concrete mixture design for the bridge deck Determine materials, workmanship or design-related causes for concrete cracking Evaluate cement and concrete for potential uses as silica-based waste product Design a very low-density, structural concrete mixture for a roof application Perform tests to determine causes for lowering strengths of concrete made from a particular cement Help with process planning, materials characterization, equipment selection and ancillary materials, and commissioning a new cement plant Assess distress in a troubled structure, investigate reasons for occurrence and provide technical support in subsequent litigation The materials consulting staff at CTLGroup comprises several PhDs and registered Professional Engineers. Our team includes chemists, process engineers, chemical engineers, pavement engineers, civil engineers and materials engineers, many of whom are world-recognized authorities in their fields. We are multi-disciplinary professionals accustomed to working together to meet your needs. We are regularly involved in training and writing publications aimed at educating the makers and users of cement and concrete. www.CTLGroup.com S E R V I C E | at-a-glance Petrographic Examination One of the most effective methods used to evaluate concrete quality, diagnose causes of deterioration and determine extent of damage is petrographic examination. It is applicable to aggregates, concrete, mortar, grout, plaster, stucco, terrazzo and similar portland cement mixtures. Petrographic methods combine unaided visual inspection and examination using stereo, petrographic and metallographic microscopes. CTLGroup’s expert interpretation of findings helps us develop practical solutions to our clients’ problems. Using guidelines given in ASTM C856, Standard Practice for Petrographic Examination of Hardened Concrete, CTLGroup’s staff of internationallyrecognized professional petrographers derive information that includes: Condition of material of inferior quality, distress or deterioration Probable future performance Compliance with project specifications Description of concrete Causes Petrographic examination can provide descriptive information that includes: Degree of cement hydration of water-cement ratio Extent of paste carbonation Presence and amount of fly ash Extent of corrosion of reinforcing steel Evidence of alkali-aggregate reaction, sulfate attack or other chemical attack Presence of potentially reactive aggregates Evidence of improper finishing Estimation of air content Evidence of early freezing Causes of cracking Estimation Petrographic examination is often supplemented with chemical analysis, X-ray diffraction analysis and scanning electron microscopy. Physical tests develop data on compressive strength, volume change, air content of hardened concrete, freeze-thaw durability and rapid chloride permeability. CTLGroup provides all of these services. Our expert petrographers and concrete technologists are available for on-site investigations. CORPORATE OFFICE | LABORATORIES 5400 Old Orchard Road Skokie, IL 60077 800.522.2285 Analytical Services www.CTLGroup.com S E R V I C E | at-a-glance CTLGroup’s chemical services team uses several instrumental methods, as well as traditional wet chemical techniques, to provide a wide range of services. Instrumental analytical tools include Inductively Coupled Plasma Spectroscopy, Direct Mercury Analysis, Ion Specific Electrode Analysis, Ultraviolet-Visible Light Spectroscopy, Fourier Transform Infrared Spectroscopy, Gas Chromatography, X-ray Fluorescence Spectroscopy, X-ray Diffraction Spectroscopy and Atomic Absorption Flame - Graphite Furnace Spectroscopy. Inductively Coupled Plasma Spectroscopy (ICP) ICP analysis is best suited for determining low concentrations of metals. We use a dual-view optical emission spectrometer with detection limit ranges of 1-10 ppb or less for 71 of the 74 elements we can analyze by ICP. Atomic absorption spectroscopy, by flame and graphite furnace, are complementary instrumental methods to ICP and are also available at our laboratory. Direct Mercury Analysis (DMA) CTLGroup uses a direct mercury analyzer that can detect less than one part per billion of mercury. The analyzer, which is calibrated in nanograms, can analyze samples ranging from a few milligrams to several grams. Sample preparation involves reducing a solid specimen to a uniform fine powder, which ensures virtually no loss of mercury. Fourier Transform Infrared Spectroscopy (FTIR) FTIR spectroscopy is used primarily for qualitative and quantitative analysis of organic compounds, and also for determining the chemical structure of inorganic compounds. FTIR applications include materials evaluation, identification, failure analysis and quality control screening. The plot of a compound’s IR transmission versus frequency is its “fingerprint,” which when compared to reference spectra identifies material. We can also use gas chromatography in the determination of organic compounds. Ultraviolet and Visible Light Spectroscopy (UV-Vis) Ultraviolet and visible absorption spectroscopy measures the attenuation of a beam of light after it passes through a sample or after reflection from a sample surface. With a spectral range from 190 to 900 nm, the UV-Vis spectra are very useful for quantitative measurements. X-ray Analysis X-ray Fluorescence (XRF) and X-ray Diffraction (XRD) spectroscopy are complementary analytical techniques. XRF is used to determine the elemental composition of substances and XRD to determine actual crystalline forms. CORPORATE OFFICE | LABORATORIES 5400 Old Orchard Road Skokie, IL 60077 800.522.2285 www.CTLGroup.com S E R V I C E | at-a-glance ASR Evaluation, Mitigation and Monitoring Alkali-silica reactivity (ASR) is a physico-chemial reaction that sometimes occurs in concrete and can lead to the premature deterioration and shortened service life of concrete structures. CTLGroup is at the forefront of the management of concrete structures subjected to ASR. We offer clients in a broad range of industries, including nuclear, a full in-house approach, from initial diagnosis and evaluation of the structure all the way through the repair and long-term monitoring of the repair. Since the discovery of ASR in the early 1940s, CTLGroup scientists and engineers have been industry leaders in its detection, identification, mitigation and testing. Decades of experience in ASR-related issues have been instrumental in developing our approach, and our portfolio includes work on many projects, specifications, test methods, rehabilitation techniques and handbooks noted throughout the industry. CTLGroup is an AASHTO Accredited Laboratory for aggregates, cement, and concrete and is an ASR approved laboratory by MassDOT. This demonstrates our commitment to delivering laboratory and consulting services that meet the rigorous quality demands required by many industries, such as DOTs. Materials consulting & testing evaluation Chemical analysis Specialized concrete mixture formulations for power applications Nondestructive testing & evaluation Instrumentation & structural heath monitoring Assessment of concrete Structural condition assessment for nuclear containments & other structures Creep & shrinkage testing Mass concrete planning & thermal stress analysis Cooling tower evaluation & repair Petrographic Quality Management System & Accreditations ISO 9001 ISO 17025 AASHTO 10CFR50 Appendix B/NQA-1 compliant U.S. Army Corps of Engineers IAS CORPORATE OFFICE | LABORATORIES 5400 Old Orchard Road Skokie, IL 60077 800.522.2285 AUSTIN OFFICE 3737 Executive Center Drive, Suite 255 Austin, TX 78731 512.219.4075 NAPERVILLE OFFICE 40 Shuman Boulevard, Suite 218 Naperville, IL 60563 630.995.3949 Chemical Testing www.CTLGroup.com S E R V I C E | at-a-glance CTLGroup’s chemical services team draws on more than 100 years of collective laboratory experience to answer our clients’ complex questions. With support from CTLGroup’s full range of testing and consulting services, including physical testing, we can offer clients a single source for complete materials characterization. Our materials analysis capabilities include: Environmental Concrete, — trace metals analyses including TCLP extractions cement, fly ash, slag and aggregate percentages in hardened concrete cement testing Aggregate composition and alkali aggregate reactivity Admixtures Forensics/failure analyses Coatings, paints and sealers Lead in paint (qualitative and quantitative analysis) Water — solids, alkalinity, direct mercury analysis, metals and corrosivity Hexavalent chromium Concrete mix-water suitability Chloride content and depth profiling Cement heat of hydration Crystalline silica Thermal analysis, thermogravimetric analysis and differential scanning calorimetry X-ray fluorescence (XRF) spectrometry Infrared spectroscopy and chromatography Soil XRF spectrometry is used in the cement and minerals industries for formulations and process control. XRF can analyze the elemental composition of virtually any substance. XRF complements x-ray diffraction (XRD), in that XRF determines the presence and quantity of each element in a specimen, and XRD determines the actual crystalline forms. The technique is used extensively in the cement industry to analyze cement, gypsum, limestone, clay, iron ore and other materials. Concrete and concrete aggregates, ceramics, coal and fly ash also are routinely characterized using these techniques. CTLGroup chemical services staff are recognized for expertise in XRF spectrometry. CTLGroup also uses fourier transform infrared spectroscopy (FTIR), gas chromatography (GC) and UV-Vis spectrometry to identify and quantify organic compounds such as polymers, chemical admixtures, chemical additives, oils, paints and coatings. Infrared spectroscopy also has applications for inorganic materials such as clays, gypsum, silicates and carbonates. FTIR can be used to study cement hydration and to identify rocks and minerals. CORPORATE OFFICE | LABORATORIES 5400 Old Orchard Road Skokie, IL 60077 800.522.2285 www.CTLGroup.com S E R V I C E | at-a-glance Construction Materials Testing CTLGroup provides a full range of materials testing services. We offer both standard and specialized tests of aggregates, admixtures, concrete, curing compounds, all cementitious materials, packaged repair materials and grouts, dimensional stone, cast stone, masonry, sealers or coatings for concrete and reinforcing steel. Our website provides specifics on more than 350 tests performed in our labs. Our Materials Engineering Group can help resolve issues of durability, incompatibility or contamination. In addition to developing specialized concrete mixture designs, we also consult for product development, certification, on-site troubleshooting and calibration services. Known and respected for the dependability of our results, CTLGroup regularly provides third-party or referee services to other labs and product manufacturers, as well as litigation support. CTLGroup staff members are active in ASTM and ACI technical committees. CTLGroup laboratories are also: AASHTO Accredited Inspected by Cement and Concrete Reference laboratory (CCRL) Participant in Cement and Concrete Proficiency Sample Program QMS meets requirements of the U.S. Army Corps of Engineers. Validated to perform a variety of material test methods. ISO 17025 Accredited CTLGroup operates a state-of-the-art facility, fully equipped for X-ray Fluorescence (XRF), X-ray Diffraction (XRD), Conduction Calorimetry, Atomic Absorption (AA), Chloride Titration, Particle Size Distribution (PSD), and Thermal Gravimetric Analysis (TGA). We run a variety of wet chemistry tests and are one of only a handful of U.S. labs able to perform heat-of-hydration testing. Wide-ranging facilities and multidisciplinary staff allow us to solve all sorts of construction industry problems, from design failures and repair specifications to materials issues, to product development and cable-stay bridge design and testing. CTLGroup offers a single source to meet all your material testing needs. CORPORATE OFFICE | LABORATORIES 5400 Old Orchard Road Skokie, IL 60077 800.522.2285 www.CTLGroup.com S E C T O R | at-a- glance services highlights •Materials • analysis & characterization •Chemical • analysis •Elemental • analysis: XRD, XRF, TGA •Petrography • •Clinker • characterization and microscopy •Quarry • mapping •Environmental • & waste stream materials consulting key facts •60,000 • square feet of lab space - one of the world’s most comprehensive facilities serving the cement industry •World • class creep & shrinkage room •Lab • facilities, equipment and expertise to characterize materials from nanoscale to full scale •Materials • characterization labs (XRD, XRF, TGA, SEM), concrete and mortar labs, physical testing capabilities and loading frames in excess of 10 million pounds •Expertise • in cement pure compounds •Interpreting • the full life cycle of cement from materials characterization in the lab to evaluation of effectiveness in the field Global Cement CTLGroup provides materials science and building system solutions for clients such as manufacturers, architects, engineering firms and contractors through materials characterization testing and analysis, addressing issues relevant to the cement industry. We tackle a diverse set of challenges for our cement clients, including: Production Process Product Performance Raw Setting Productivity Strength feed/clinker grindability enhancement Nodulization Burnability Combustion Kiln system deposits Environmental and Sustainability Consulting Energy consumption emissions Life cycle inventories Low carbon cement production Stack Workability Water demand/bleeding reflectance Mineral admixtures Cement/admixture compatibility Supplementary cementing materials (SCM) Color/solar ACCREDITATIONS IAS ISO 17025 accredited accredited 10 CFR 50, Appendix B/NQA-1 Complaint Laboratories are validated by US Army Corps of Engineers Stadium® certified user AASHTO REPRESENTATIVE ENGAGEMENTS Burj Khalifa creep & shrinkage tests National Institute of Standards and Technology (NIST) developed standard reference materials Life Cycle Inventory of Portland Cement Manufacture life cycle assessment including CO2 emissions Composition Analysis for several manufacturers composition of powdered activated carbon influence on air content in fresh concrete Panama Canal Expansion Project chemical and physical evaluation of materials for Grupo Unidos por el Canal CONTACTS Timothy Tonyan, Ph.D. 847.972.3146 TTonyan@CTLGroup.com Don Broton 847.972.3292 DBroton@CTLGroup.com www.CTLGroup.com S E C T O R | at-a-glance Ready Mix Concrete CTLGroup provides the ready mixed concrete industry with much more than just standard testing services. Our expertise includes developing specialized concrete mixture proportions to meet challenging placement requirements or modern performance specifications. We help improve overall concrete production quality, plant performance and environmental compliance, and we assist with on-site plant set up and qualification. Additionally, CTLGroup experts optimize proportions to help clients gain a competitive edge, meet performance based specifications and determine difficult mixture interactions in the field. We tackle a diverse set of challenges for our cement clients, including: Products & Services Materials testing & new product development & training Plant services & optimization xx On-site batch plant configuration & troubleshooting xx Quality control evaluations, equipment performance inspection & plant audits xx Energy use audits & environmental compliance testing Mixture proportion consulting & optimization xx Review of concrete mixture proportions & specifications xx Low heat mass concrete mixture optimization xx Aggregate optimization & void space/particle packing analysis xx Mixture development for creep & shrinkage performance xx Sustainable concrete mixture development to reduce carbon footprint xx Fiber reinforced concrete (FRC) xx Flowable, tremie & self-consolidating concrete (SCC) xx Rapid setting or high early strength concrete xx Mixture development for durability/service life requirements or performance based specification assistance xx Mixture cost optimization Engineering & problem solving xx Concrete precooling & thermal analysis xx Extended slump life/pumpability troubleshooting xx Setting time/early strength troubleshooting & maturity for early formwork removal xx Formwork pressure assessment xx Admixture - cementitious material interaction & fly ash troubleshooting Education accreditations •ISO • 9001: 2008 Bureau Veritas certified •IAS • ISO 17025 accredited •AASHTO • accredited •Inspected • by Cement and Concrete Reference Laboratory (CCRL) •Laboratories • are validated by US Army Corps of Engineers •Participates • in Cement and Concrete Proficiency Sample Program •10 • CFR 50, Appendix B/NQA-1 Complaint •NIAC • audited key facts •60,000 • SF of lab space – one of the world’s most comprehensive facilities •World • class creep & shrinkage room •Lab • facilities, equipment & expertise to characterize materials from nano-scale to full scale •Materials • characterization labs (XRD, XRF, TGA, SEM), concrete & mortar labs, physical testing capabilities & loading frames in excess of 10 million pounds CONTACTS Timothy Tonyan, Ph.D. 847.972.3146 TTonyan@CTLGroup.com Boyd Clark, Ph.D. 847.972.3348 BClark@CTLGroup.com REPRESENTATIVE ENGAGEMENTS Illinois Tollway development of high-early strength concrete for pavement & bridge deck repair Kiewit concrete mixture development of South River Tunnel & Pumping Station Prairie, Inc. creep testing for Trump Tower Walsh Construction batch plant consulting & development of selfconsolidating mass concrete for the Holtwood hydroelectric project www.CTLGroup.com S E R V I C E | at-a-glance Structural Investigation, Testing & Research Since 1958, CTLGroup has studied structural component behavior resulting in noteworthy contributions to structural engineering and engineered construction including: Today’s design code provisions for reinforced and prestressed concrete on seismic behavior of reinforced concrete structures Design methodology to minimize progressive collapse of precast structures Experimental data to support analytical design assumptions and concepts for nuclear plant containments Innovations in bridge design, testing and evaluation Data The Facilities and Equipment The CTLGroup structural testing facility has a 56x120 ft test floor adaptable for three-dimensional loading in static, dynamic and pseudodynamic testing. Conventional and digital servohydraulic ram and actuator systems are configured for multiple power units ranging in individual capacity from 1,000 to 10,000,000 lb force and stroke up to 36 in. Also included are: Twin 20-ton radio-controlled overhead cranes 300-, 400-, and 1,000-kip universal testing machines 1,000-kip compression testing machine Carpentry, machining and welding shops Concrete casting equipment 55-, Control, measurement, storage and analysis of applied loads and structural response for on-site and laboratory testing are accomplished using transducers to measure force, strain, pressure, displacement, fluid flow, temperature, humidity, acceleration and rotation. Test control and data acquisition/analysis are accomplished using continually upgraded digital hardware and software designed, configured and applied by professionals who provide clients with structural measurements and diagnostics expertise. CTLGroup uses state-of-the-art nondestructive testing and diagnostic technology for structural health monitoring and performance evaluation. These include impact echo, impulse response, parallel seismic, ultrasonic pulse velocity, corrosion assessment, covermeter surveys, rebound hammer, ultrasonic thickness measurement of metal, cable wire break detection system and vibration and modal analysis. CTLGroup’s laser-based vibration and cable-force measurement techniques offer fast, economic alternatives. The Service Range Structural integrity and reliability assessments testing Instrumentation/data acquisition Failure analysis Research Commercial product testing Calibration Load CORPORATE OFFICE | LABORATORIES 5400 Old Orchard Road Skokie, IL 60077 800.522.2285