Analytical Report for E-Liquid Samples
Certificate Number
Method: GCMS/FID
Date of receipt
#################
Instrument: 7890B-5977
Date of report
5-Sep-16
Expiry Date
#NAME?
R2544
Batch Number
ZAP8700
Product Name
ZEST APPEAL 0mg ZAP8700
Mode of Detection
GC-MS (SIM)
Compound
Diacetyl
Acetyl Propionyl
Acetoin
Ethylene Glycol
Diethylene Glycol
Nicotine
Concentration Units
ppm
ppm
ppm
ppm
ppm
Result
Not Detected
Not Detected
Not Detected
Not Detected
Not Detected
mg/mL
Not Detected
Propylene Glycol
Glycerin
87
Limit of Detection
1
1
1
10
10
0.001
GC-FID
PG:VG Ratio
13
Figure 1. GC-MS (SIM) chromatogram of sample.
Abundance
Diphenylamine
TIC: ZEST APPEAL 0mg ZAP8700.D\datasim.ms
900000
800000
600000
500000
400000
300000
200000
100000
Glycerin
Propylene Glycol
700000
6.00 7.00 8.00 9.00 10.0011.0012.0013.0014.0015.0016.0017.0018.00
Time-->
Figure 2. GC-FID chromatogram of sample.
Abundance
Signal: ZEST APPEAL 0mg ZAP8700.D\FID1A.ch
3500000
3000000
2500000
-
2000000
1500000
1000000
500000
6.00 7.00 8.00 9.00 10.0011.0012.0013.0014.0015.0016.0017.0018.00
Time-->
Page 1 of 2
C:\GCMS\custrpt\ECIG SIM FID GENERAL.CRT
5/9/2016 10:27 AM
Figure 3: GC-MS Total Scan (Total Ion Chromatogram) of sample
Abundance
TIC: ZEST APPEAL 0mg ZAP8700.D\data.ms
900000
800000
700000
600000
500000
400000
300000
200000
100000
6.00
7.00
8.00
9.00 10.0011.0012.0013.0014.0015.0016.0017.0018.00
Time-->
GENERAL REPORT NOTES:
This report only relates to the Lot/batch number and sample name given above. Each sample has been analysed
as received and so the lab does not bear any responsibility for variations in expected results due to inappropriate
packaging, storage and transportation prior to receipt. All samples, upon receipt, are secured within access controlled
storage.
Samples are analysed within quality controlled batches. Each batch consists of a set of matrix-matched control
standards; independent standards; and internal calibration standard. The target compounds used are sourced from ISO
Guide 34 compliant suppliers where possible; and the dilution/preparing of the calibration solutions were prepared
in accordance to in-house procedures.
The metrological traceability of the gravimetric measurements employed in the analytical technique is assured in
accordance to ISO/IEC 17025. The analytical balance employed was first checked before use with class E2 analytical
weights, traceable to DKD. Cold storage is maintained within set limits (5±3°C) and monitored daily using calibrated
thermometers that are NIST traceable.
The hyphenated analytical technique employed was Gas Chromatography with Mass Spectrometer and Flame
Ionisation Detection (GC-MS-FID).
The quality control measures employed within each batch ensures that each analysis is acceptable to ±10% of the true
value.
COMMON NAME
Diacetyl
Acetyl Propionyl
Acetoin
Ethylene Glycol
Diethylene Glycol
Propylene Glycol
Glycerin
Nicotine
Diphenylamine
CHEMICAL NAME
2,3-Butanedione
2,3-Pentanedione
3-Hydroxybutan-2-one
1,2-Ethanediol
Bis(2-Hydroxyethyl)ether
1,2-Propanediol
1,2,3-Propanetriol
3-[(2S)-1-methylpyrrolidin-2-yl]pyridine
N-Phenylalinine
CAS No.
431-03-8
600-14-6
513-86-0
37221-95-7
111-46-6
190913-75-8
29796-42-7
54-11-5
122-39-4
Definitions:
Not Detected: Target compound is less than the method detection limit or limit of quantification. If limits of detection
are different from that quoted, a caveat will be included in the comment section of the report.
Limit of Detection: The least amount of a target substance that can be clearly differentiated from other components
within the same matrix and distinguished from a blank sample.
Analysed by:
Approved by:
Contact Phone:
Richard Gandon
Kenoye Muzan
01733 562 322
Sequence File Path:
D:\Routine\Routine 249\
This report has been generated by Electronic Cigarettes LTD Unit 3 Fengate Trade Park, Peterborough, PE1 5XA
Page 2 of 2
C:\GCMS\custrpt\ECIG SIM FID GENERAL.CRT
5/9/2016 10:27 AM