Engineering Manual Multicore® LF318 Solder Paste Introduction About the electronics group of Henkel Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details Henkel is the world’s leading and most progressive provider of qualified, compatible material sets for semiconductor packaging, board level assembly and advanced soldering solutions. Through its Hysol®, Loctite® and Multicore® brands, and its global customer support infrastructure, Henkel delivers world-class materials products, process expertise and total solutions across the board to preempt industry changes. By partnering with key industry leaders to pioneer added-value materials and processes, and by prioritizing environmental responsibility and training, Henkel is formulating the materials to enable tomorrow’s electronic industry. Slide 2 Across the Board. Around the Globe. <Prev Next> Print About the electronics group of Henkel Product description Features & benefits Introduction Product description Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details Henkel’s Multicore LF318 solder paste is a halide-free, no-clean, pin-testable solder paste. It was previously supplied to selected customers and independent test houses for evaluation purposes as development product XP48. <Prev Next> About the electronics group of Henkel Product description Features & benefits Slide 3 Across the Board. Around the Globe. Print Introduction Features & benefits Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Print Product attribute Process benefit About the electronics group of Henkel Outstanding humidity resistance – exhibits high coalescence even after 72 hrs @ 27°C/80%RH Reduces process variation due to environmental factors, a particular advantage in high temperature/humidity conditions Product description Colorless residues Improves speed and ease of post-reflow inspection Soft, non-stick pin-testable residues Improves ease and reliability of in-circuit testing and reduces frequency with which test probes require cleaning Fine alloy particle size and optimized paste viscosity Suitable for fine pitch, high speed printing up to 150 mm/s (6 in./s) Extended open time & tack-life Reduces solder paste wastage Halide-free flux classification: ROL0 to ANSI/J-STD-004 High reliability of finished assembly without cleaning High tack force Resists component movement during high speed placement, reducing the need for rework Long printer abandon times Reduces solder paste wastage Excellent solderability Suitable for use on a wide range of surface finishes including HASL, Ni/Au, immersion Sn, immersion Ag and OSP Cu Wide printing and reflow process windows Accommodates a wide range of printer settings and reflow profiles. Suitable for use in air and nitrogen Low voiding Reduced risk of bridging on small pitch BGAs or CSPs. Reduced risk of decreased joint reliability and/or outgassing. Low slump Reduced bridging Slide 4 Across the Board. Around the Globe. Features & benefits Physical properties Technical data Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Technical data Datasheet LF318 Click icon Slide 5 Across the Board. Around the Globe. Print Operating parameters Printing: Process window Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details LF318 solder paste was subjected to testing in Henkel laboratories to establish the print process window, using the following equipment: <Prev Next> Printing Process window Printer DEK 260 Squeege Metal blade, 230 mm (approx. 9"), 60º Stencil Laser cut, stainless steel, 125 µm (approx. 0.005") thickness Boards Bare copper, no resist Abandon time Deposits examined 0.64 mm (approx. 0.025") QFP100 (0.38 mm (approx. 0.015") pads), 0.5 mm (approx. 0.020") TQFP100 (0.25 mm (approx. 0.010") pads), 0.4 mm (approx. 0.016") TQFP (0.2 mm (approx. 0.008") pads) and BGA225 (1.27 mm (approx. 0.050") pitch) Volume consistency Stereomicroscope (X10-X30) Reflow Inspection Print Slump testing Ambient conditions during testing were 24ºC/28%RH. Process window & thermal profiles A solder paste bead of approximately 250 g was placed on the stencil and printed onto the boards at speeds ranging from 20 to 200 mm/s and squeege pressures ranging from 2–8 kg (approx. 4.4 – 17.6 lbs). Stroke was set at 230 mm (approx. 9"), separation speed at 10% and the print gap at zero (contact print). Humidity resistance & solder balling performance During printing, paste roll, stencil wipe, aperture release and drop-off were assessed with the naked eye. After printing, the solder paste deposits were examined using a stereomicroscope to assess the general appearance and to note the incidence of any defects: Topography Ideally the shape and volume of the paste deposit should reflect the stencil aperture geometry Skipping Little or no evidence of printed paste on the pad due to non-filling of stencil apertures or nonrelease of paste from apertures Incomplete or insufficient fill Poor paste coverage on the pads due to paste not being released from the stencil or not filling some of the printed area Spikes Central area of the printed deposit raised, usually attributable to excessively low print pressure Dog-ears Extremities of the paste deposit raised Slide 6 Across the Board. Around the Globe. Wetting Voiding Tack Tack performance Operating parameters Printing: Process window Introduction Physical Properties Operating Parameters Test Data Troubleshooting LF318 Print Process Window Print speed plotted against squeegee pressure (kg/cm squeegee blade length). Contact Details <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Test board includes 0.6 mm (approx. 0.025"), 0.5 mm (approx. 0.020") and 0.4 mm (approx. 0.016") pitch components. Slide 7 Across the Board. Around the Globe. Tack performance Operating parameters Printing: Slump testing Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details In-house testing LF318 solder paste was subjected to slump testing in the Henkel laboratories in accordance with IPC™-650-2.4.35, using a 0.2 mm (approx. 0.008") thick stencil, IPC slump pattern A-21. Results are below. <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance Slide 8 Across the Board. Around the Globe. Operating parameters Printing: Slump testing Introduction Physical Properties Operating Parameters Test Data Troubleshooting Details IPC ANSI/J-STD-005 Slump Test Contact Details <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance 1 min 150ºC 15 min 150ºC Slide 9 Across the Board. Around the Globe. 15 min RT Operating parameters Printing: Slump testing Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Print Printing Details JIS-Z-3284 Slump Test Summary of slump data Process window 96SCLF318AGS88.5V Batch No. CP4I0623 Room Temperature, 60 minutes 150°C for 1 minute 3.0 x 1.5 mm apertures 0.2 mm 0.3 mm 3.0 x 0.7 mm apertures 0.2 mm 0.2 mm Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance 1 min 150ºC 15 min 150ºC Slide 10 Across the Board. Around the Globe. 15 min RT Operating parameters Printing: Abandon time Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details Response to 1 hour Pause/Procedure <Prev Next> Print Printing Process window 4 knead prints 5 prints 5 prints 1 print Volume Measurement Slump testing Abandon time Understencil clean Understencil clean 1 hour abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance Slide 11 Across the Board. Around the Globe. Operating parameters Printing: Abandon time Introduction Physical Properties Operating Parameters Abandon time/Results AGS: 20-45 µm powder ADP: 15-38 µm powder Test Data Troubleshooting Contact Details <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance Slide 12 Across the Board. Around the Globe. Operating parameters Printing: Volume consistency Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Equipment used: DEK Infinity Cyberoptics SE300; deposits examined 0.4 mm QFP, 0.4 mm & 0.5 mm CSP Solder paste: 96SCLF318AGS88.5V, batch no. CP5A008 Settings: 50 mm/s, 6 kg, 250 mm/60° squeegee, 100 mm thick stencil Printing Deposits examined: Abandon time Aperture Shape Dimensions No. of deposits examined per board 0.4 mm CSP Round Ø245 µm 964 0.5 mm CSP Square 270 µm x 270 µm 337 0.4 mm QFP Rectangular 830 µm x 220 µm 97 Print Process window Slump testing Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Procedure 4 knead prints 5 prints 5 prints Volume Measurement Voiding Tack Understencil clean Understencil clean Slide 13 Across the Board. Around the Globe. Tack performance Operating parameters Printing: Volume consistency Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance Slide 14 Across the Board. Around the Globe. Operating parameters Reflow: Process window & thermal profiles Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details LF318 solder paste was subjected to testing in Henkel laboratories to establish the reflow process window, using the following equipment and settings: Printer DEK 260 Print settings Print speed 75 mm/s (approx. 2"/s); pressure 8 kg (approx. 17.5 lbs) Stencil Stainless steel laser-cut stencil, 125 µm (approx. 0.005") thickness Boards Bare copper, no resist Reflow oven Seho FDS6440 PCB areas examined 0.6 mm (approx. 0.025") QFP pads, 0.4 mm (approx. 0.016") TQFP pads, 0.3 mm (approx. 0.012") TQFP pads and 0.2 mm (approx. 0.008") BGA225 pads Inspection Stereomicroscope (X10-X30) Boards were printed and reflowed at varying times to peak process temperature, from 2–12 minutes. Both linear and soak-type reflow profiles were used, and the reflowed boards examined using a stereomicroscope. Reflow quality was assessed according to the appearance of the solder fillet and post-reflow residue, paying particular attention to coalescence during reflow, solder surface appearance, solder balling, residue surface quality and residue color. <Prev Next> Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance Slide 15 Across the Board. Around the Globe. Print Operating parameters Reflow: Process window & thermal profiles Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details Linear Reflow Profile The convection oven’s zone settings were maintained at the settings shown below; the peak temperature & time to peak temperature were adjusted by varying the belt speed from 30 cm/min (12”/min) to 130 cm/min (51”/min). <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance Range of acceptable reflow conditions: T>217°C: 11.5 – 171 s Peak temperature: 223 – 266°C Belt speed: 30 – 120 cm/min (These should not be taken as guidelines for profiling – they merely indicate that LF318 has a large process window when assessed under laboratory conditions.) Slide 16 Across the Board. Around the Globe. Operating parameters Reflow: Process window & thermal profiles Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details Soak Reflow Profile The convection oven’s zone settings were maintained at the settings shown below; the peak temperature & time to peak temperature were adjusted by varying the belt speed from 30 cm/min (12”/min) to 130 cm/min (51”/min). <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Range of acceptable reflow conditions: T>217°C: 11.5 – 171 s Peak temperature: 223 – 266°C Belt speed: 30 – 120 cm/min (These should not be taken as guidelines for profiling – they merely indicate that LF318 has a large process window when assessed under laboratory conditions.) Slide 17 Across the Board. Around the Globe. Tack performance Operating parameters Reflow: Humidity resistance & solder balling performance Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details LF318 was tested to establish humidity resistance and solder balling performance. After printing, coupons were stored in a temperature/humidity controlled chamber. After the appropriate storage period they were removed from the chamber and reflowed, in air, using a convection reflow oven. Profile peak temperature was 242°C, time to peak 5 min 15 s, time above liquidus (217°C) was 80 s. <Prev Next> Print Printing Process window Slump testing LF318: Humidity resistance Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Initial Reflow after 4 hrs, 27°C/80%RH Wetting Voiding Tack Tack performance Reflow after 24 hrs, 27°C/80%RH Reflow after 72 hrs, 27°C/80%RH Note: J-STD condition 25ºC, 50%RH initial and after 4 h Slide 18 Across the Board. Around the Globe. Operating parameters Reflow: Wetting Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details Wetting behaviour of LF318 according to J-STD-005. <Prev Next> Print Printing This test is carried out to determine the ability of a solder paste to wet an oxidised copper surface & to qualitatively examine the amount of solder spatter of the paste during reflow. LF318 was printed onto 4 copper test pieces (each 76x25x0.8 mm) using a 0.2 mm thick stencil with round apertures 6.5mm in diameter. Two test pieces were reflowed immediately after printing on a solder bath at 242°C. The reflowed solder was then examined at 10X magnification to establish if the copper was uniformly wetted with no evidence of non-wetting, de-wetting or spatter around the deposit.The test was repeated on the remaining test coupons after 4 hours exposure to 25°C/50%RH. LF318 passes this test. Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Reflowed within 15 minutes of printing Reflowed after 4 hours exposure to 25ºC/50%RH Slide 19 Across the Board. Around the Globe. Tack Tack performance Operating parameters Reflow: Wetting Introduction Physical Properties Operating Parameters Test Data Troubleshooting SOT23 Pads: Offset print Contact Details <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Bare Copper After print Immersion Tin After print Immersion Silver After print Gold over nickel After print Process window & thermal profiles Humidity resistance & solder balling performance Wetting Voiding Tack Tack performance Bare Copper After reflow Immersion Tin After reflow Immersion Silver After reflow Slide 20 Across the Board. Around the Globe. Gold over nickel After reflow Operating parameters Reflow: Voiding Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Print Printing Process window Slump testing Void % area = 0.49% over 132 balls Void % area in balls containing voids = 3.38% Total of 16 Voids 1 Void > 10% ball area 2 Voids 10% - 5% 13 Voids < 5% Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Linear Profile (Worst case scenario) Device: TBGA132 SnPb balls PCB: Cu pads @ 0.5 mm pitch Stencil thickness = 120 µm Wetting Voiding Tack Tack performance Slide 21 Across the Board. Around the Globe. Operating parameters Tack perfomance Introduction Physical Properties Operating Parameters Test Data Troubleshooting Tack testing according to J-STD-005 Contact Details <Prev Next> Print Printing Process window Slump testing Abandon time Volume consistency Reflow Process window & thermal profiles Humidity resistance & solder balling performance Wetting Tack testing should be continued until tack reaches 80% of the initial tack force is reached. However, as can be seen, even after 72 hours LF318 tack remained high. Testing was not continued after this time. Voiding Tack Tack performance Slide 22 Across the Board. Around the Globe. Test data Pin testability assessment Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details Pin testability in Air/N2 Pin test done on copper laminate; electrical continuity during testing monitored using an electronic counter Boards were reflowed using profile below, 3 in air & 3 in N2 environment Test done using 4-pin crown point probe (Croda PA4QPS-040) 840 test points per PCB <Prev Next> Pin testability assessment J-STD-004 reliability test results JIS standards testing GR-CORE-78 Slide 23 Across the Board. Around the Globe. Print Test data Pin testability assessment Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Print Pin testability assessment Pin-testability: Air reflow Board No. (Reflowed in air) % contacts using crown probe on 840 test pads Result 1 100% Pass 2 100% Pass 3 100% Pass Probe appearance after 840 hits Slide 24 Across the Board. Around the Globe. J-STD-004 reliability test results JIS standards testing GR-CORE-78 Test data Pin testability assessment Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Print Pin testability assessment Pin-testability: N2 reflow Board No. (Reflowed in N2) % contacts using crown probe on 840 test pads Result 1 100% Pass 2 100% Pass 3 100% Pass Probe appearance after 840 hits; one reflow cycle Slide 25 Across the Board. Around the Globe. J-STD-004 reliability test results JIS standards testing GR-CORE-78 Test data Pin testability assessment Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details Pin testability after multiple reflow cycles Some copper laminate test boards with 840 pads made with 96SCLF318AGS88.5V were reflowed in air a number of times to simulated double-sided boards with selective soldering. The profile used can be seen below. Pin testability was then assessed after reflow using a 4-pin crown point probe (Croda PA4QPS-040); electrical continuity during testing was monitored using an electronic counter <Prev Next> Pin testability assessment J-STD-004 reliability test results JIS standards testing GR-CORE-78 Slide 26 Across the Board. Around the Globe. Print Test data Pin testability assessment Introduction Physical Properties Operating Parameters Pin-testability: Air reflow 3 test boards per condition Probe appearance after 840 hits; two reflow cycles Test Data Troubleshooting Contact Details Pin-testability: Air reflow 3 test boards per condition Probe appearance after 840 hits; three reflow cycles Reflowed twice % contacts using crown probe on 840 test pads Result Reflowed three times % contacts using crown probe on 840 test pads Result 1 100% Pass 1 100% Pass 2 100% Pass 2 100% Pass 3 100% Pass 3 100% Pass Probe appearance after 840 hits Slide 27 Across the Board. Around the Globe. Probe appearance after 840 hits <Prev Next> Print Pin testability assessment J-STD-004 reliability test results JIS standards testing GR-CORE-78 Test data J-STD-004 Reliability test results Introduction Physical Properties Operating Parameters Test Data Troubleshooting J-STD004: copper mirror IPC-TM-650, 2.3.32 Flux induced corrosion (copper mirror) No breakthrough of copper = flux classification ‘L’ Contact Details <Prev Next> Pin testability assessment J-STD-004 reliability test results JIS standards testing GR-CORE-78 LF318 Copper Mirror- no breakthrough Print Control Copper Mirror – no breakthrough Slide 28 Across the Board. Around the Globe. Test data J-STD-004 Introduction Physical Properties Operating Parameters J-STD004: halide test IPC-TM-650, 2.3.33 Silver chromate paper method No discoloration of silver chromate paper = flux activity ‘0’ Test Data Troubleshooting Contact Details <Prev Next> Pin testability assessment J-STD-004 reliability test results JIS standards testing GR-CORE-78 LF318 Control Slide 29 Across the Board. Around the Globe. Print Test data J-STD-004 Introduction Physical Properties Operating Parameters Test Data J-STD004: flouride test IPC-TM-650, 2.3.35.1 No change in colour from purple to yellow confirms absence of flourides Flux activity type ‘0’ Troubleshooting Contact Details <Prev Next> Pin testability assessment J-STD-004 reliability test results JIS standards testing GR-CORE-78 Zirconium-alazarin purple lake With LF318 added Slide 30 Across the Board. Around the Globe. Print Test data J-STD-004 Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details J-STD004: chlorides & bromides IPC-TM-650, 2.3.35 Chloride & bromide concentrations Halide content <0.005% Next> Print Pin testability assessment J-STD-004 reliability test results J-STD004: flux solids IPC-TM-650, 2.3.34 Flux solids (non-volatile content) determination Approximately 2 g of flux medium was accurately weighed into a clean metal dish which was then placed into an air circulating oven at 145°C for 2 hours. The dish was allowed to cool and re-weighed. The solids content was calculated using the following equation: Solids content = (final mass of flux medium/initial mass of flux medium) x 100% Solids content was found to be 69% J-STD004: flux corrosion IPC-TM-650, 2.6.15 No evidence of corrosion = type ‘L’ flux classification Test done in duplicate: 240 hrs (10 days) humid storage at 40°C/93±2%RH – no evidence of corrosion products LF318 – coupon 1 <Prev LF318 – coupon 2 Slide 31 Across the Board. Around the Globe. JIS standards testing GR-CORE-78 Test data J-STD-004 Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details J-STD004: SIR IPC-TM-650, 2.6.3.3 Moisture & surface insulation resistance Passmark: 1 x 108 Ω <Prev Next> Print Pin testability assessment J-STD-004 reliability test results 24 hrs at 85°C, 85%RH, 50V bias. 96 hrs at 85°C, 85%RH, 50V bias. 168 hrs at 85°C, 85%RH, 50V bias. Control (Ω) 5.89 x 109 3.60 x 109 2.85 x 109 96SCLF318AGS88.5V (Ω) 3.13 x 109 1.03 x 109 1.06 x 109 Passmark (Ω) 1.00 x 108 1.00 x 108 1.00 x 108 Slide 32 Across the Board. Around the Globe. JIS standards testing GR-CORE-78 Test data JIS standards testing Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details JIS-Z-3284: SIR <Prev Next> Print Pin testability assessment Pass: 1 x 108 Ω 85°C, 85%RH Initial 24 hours 96 hours 168 hours LF318 (Ω) 7.44 x 1011 1.73 x 109 1.75 x 109 1.96 x 109 Unfluxed control (Ω) 8.94 x 1011 1.51 x 109 1.26 x 109 1.27 x 109 J-STD-004 reliability test results JIS standards testing GR-CORE-78 JIS-Z-3284: electromigration 85°C/85%RH, 50V bias, 1000 hours duration No dendrites observed Slide 33 Across the Board. Around the Globe. Test data GR-CORE-78 Introduction Physical Properties Operating Parameters Test Data Troubleshooting GR-CORE-78: SIR Contact Details <Prev Next> Print Pin testability assessment 35°C/85%RH, 50V bias 24 hours 96 hours LF318 (Ω) 1.489 x 1011 1.84 x 1011 J-STD-004 reliability test results Controls (Ω) 1.804 x 1011 1.47 x 1011 JIS standards testing GR-CORE-78 Slide 34 Across the Board. Around the Globe. Test data GR-CORE-78 Introduction Physical Properties Operating Parameters Test Data Troubleshooting GR-CORE-78: electromigration Contact Details <Prev Next> Print Pin testability assessment 65°C/85%RH, 10V bias 96 hours 500 hours Dendrites LF318 (Ω) 3.73 x 1010 3.47 x 1010 None J-STD-004 reliability test results Controls (Ω) 2.59 x 1010 5.24 x 1010 None JIS standards testing GR-CORE-78 Slide 35 Across the Board. Around the Globe. Troubleshooting Printing Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details For the purposes of this solder paste printing troubleshooting guide, it is assumed that the correct thickness of stencil is used and that gasketing, stencil cleaning, component solderability, board support and handling are satisfactory. <Prev Next> Printing Reflow Paste bleeds under stencil, leading to bridging Paste skips – solder paste does not release completely from stencil Paste deposits are irregular Unsatisfactory aperture filling Paste deposit excessive, leading to bridging Print pressure Separation speed Separation speed; increase print speed to lower viscosity Squeegee speed and pressure settings Squeegee pressure may need to be increased; separation speed Poor print definition leads to ‘dog-ears’ Paste scooping Overprinting – paste deposit exceeds pad area Paste bridges or smears; poor edge definition Print is misaligned Separation speed; increase print speed Reduce squeegee pressure Reduce print pressure or adjust print speed Reduce print pressure Stencil registration/printer alignment Description Slide 36 Across the Board. Around the Globe. Check/adjust Print Troubleshooting Reflow Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details For the purposes of this solder paste reflow troubleshooting guide, it is assumed that component and board storage and handling are satisfactory and that the reflow profile is suited to the specification limits of the components and substrate. Solder joint cracks during cooling Tombstoning/Manhattan effect/drawbridging Reflow incomplete Cooling rate Adjust preheat to balance temperature at both component terminations Reflow profile: balance time Above liquidus with excessive heat causing flux exhaustion Reflow profile – may need to reduce preheat Poor solderability Description Mid-chip beading Paste bridging Uncoalesced solder Check paste life and stencil geometry alignment, gasketting and cleanliness Check the under stencil cleanliness, print preassure, gasketting & the board Check reflow profile to ensure sufficient time above reflow is provided for Slide 37 Across the Board. Around the Globe. Check/adjust <Prev Next> Printing Reflow Print Contact details Introduction Physical Properties Operating Parameters Test Data Troubleshooting Contact Details <Prev Next> Contact Henkel Americas Henkel Europe Henkel Asia 15350 Barranca Parkway, Irvine, CA 92618 USA Tel: +1 949 7839 2500 electronics@us.henkel.com Technologies House, Wood Lane End Hemel Hempstead Hertfordshire, HP2 4RQ UK Tel: +44 1442 278000 No. 90 Zhujiang Road Yantai Development Zone Shandong China 264006 Tel: +86 535 6399820 electronics.henkel.com Slide 38 Across the Board. Around the Globe. Print Technical Data Sheet LF318 Solder Paste July 2005 PIN-TESTABLE LEAD-FREE SOLDER PASTE PRODUCT DESCRIPTION Multicore™ LF318 solder paste is a halide-free, no clean, pin testable Pb-free solder paste, which has excellent humidity resistance and a broad process window, both for reflow and printing. LF318 solder paste offers a high tack force to resist component movement during high speed placement, long printer abandon times and excellent solderability over a wide range of reflow profiles in air and nitrogen and across a wide range of surface finishes including Ni/Au, Immersion Sn, Immersion Ag and OSP Copper. FEATURES AND BENEFITS • Outstanding humidity resistance – gives excellent coalescence even after 72 hours exposure to 27ºC/80% RH, thus reducing process variation due to environmental factors • Colourless residues for easy post-reflow inspection • Soft non-stick pin testable residues allow easy in-circuit testing • Suitable for fine pitch, high speed printing up to 150mm/s (6”/s) • Extended open time & tack-life leading to low wastage. • Halide free flux classification: ROL0 to ANSI/J-STD-004 TYPICAL PROPERTIES Based upon type 3 powder; other sizes also available DIRECTIONS FOR USE Printing: Multicore LF318 solder paste is available for stencil printing down to 0.4mm (0.016”) pitch devices, with type 3 (AGS) powder. Printing at speeds between 25mm/s (1.0”/s) & 150mm/s (6”/s) can be achieved using laser cut, electropolished, or electroformed stencils and metal squeegees (preferably 600). Acceptable first prints have been achieved at 0.4mm (0.016”) pitch after printer down times of 4 hours without requiring a knead cycle. Reflow: Any of the available methods of heating to cause reflow may be used including IR, convection, hot belt, vapour phase and laser soldering. LF318 is not particularly sensitive to reflow profile type. There is no single reflow profile which is suitable for all processes & applications, but the following graph shows example profiles that have given good results in practice. LF318 96SC, 97SC 20-45 Example Reflow Profiles AGS 88.5 IPC A21 Pattern 0.06 0.33 0.25 0.41 300 Temperature °C Properties Alloys Powder Particle Size, µm Multicore Powder Size Coding Metal Loading (% weight) Slump, J-STD-005, mm(4) RT (15 minutes) 0.33 x 2.03 mm pads 0.63 x 2.03 mm pads 150oC (15 minutes) 0.33 x 2.03 mm pads 0.63 x 2.03 mm pads Solder powder: Careful control of the atomisation process for production of solder powders for LF318 solder pastes ensures that the solder powder is produced to a quality level that exceeds IPC/J-STD006 & EN29453 requirements for sphericity, size distribution, impurities and oxide levels. Minimum order requirements may apply to certain alloys and powder particle sizes. For availability with other alloys and powder sizes, contact your local technical service helpdesk. 250 200 150 100 50 0 0 2 4 6 Time Minutes Viscosity measured at 25°C (Typical) Brookfield, cP(1) Malcom 10rpm, P(2) Thixotropic Index (Ti)(3) Tack(5) Initial tack force, gmm-2 Useful open time, hours (1) 765,000 1961 0.54 2.0 >24 Measured at 25°C, TF spindle at 5rpm after 2 minutes Measured at 25°C, and a shear rate of 6s-1 TI = log (viscosity at 1.8s-1/Viscosity at18s-1) (4) Slump data are expressed as the minimum spacing between pads of the size shown that does not allow bridging (5) Tack data are derived from comparative laboratory tests and do not necessarily relate directly to a particular user’s conditions (2) (3) Cleaning: Multicore LF318 solder pastes are no-clean & are designed to be left on the PCB in many applications since they do not pose a hazard to long term reliability. However, should there be a specific requirement for residue removal, this may be achieved using conventional cleaning processes based on solvents such as Multicore MCF800, or suitable saponifying agents. For stencil cleaning and cleaning board misprints, Multicore SC-01 Solvent Cleaner is recommended. NOT FOR PRODUCT SPECIFICATIONS THE TECHNICAL INFORMATION CONTAINED HEREIN IS INTENDED FOR REFERENCE ONLY. PLEASE CONTACT HENKEL TECHNOLOGIES TECHNICAL SERVICE FOR ASSISTANCE AND RECOMMENDATIONS ON SPECIFICATIONS FOR THIS PRODUCT. NEXT LF318, July 2005 RELIABILITY PROPERTIES Solder paste medium: Multicore LF318 medium contains a stable resin system and slow evaporating solvents with minimal odour. The formulation meets the requirements of the Telcordia (formerly known as Bellcore) GR-78-CORE and ANSI/J-STD-004 for a type ROL0 classification. Test Copper Plate Corrosion Copper Mirror Corrosion Chlorides & Bromides Surface Insulation Resistance (without cleaning) Flux Activity Classification (without cleaning) Specification ANSI/J-STD-004 ANSI/J-STD-004 ANSI/J-STD-004 ANSI / J-STD-004 Telcordia GR-78-Core JIS-Z-3284 ANSI/J-STD-004 Results Pass Pass Pass Pass Pass Pass ROL0 PACKAGING Containers: Multicore LF318 solder paste is supplied in: • • 500g plastic jars with an air seal insert. 1kg, 600g or 500g Semco cartridges GENERAL INFORMATION For safe handling information on this product, consult the Material Safety Data Sheet, (MSDS). Note The data contained herein are furnished for information only and are believed to be reliable. We cannot assume responsibility for the results obtained by others over whose methods we have no control. It is the user's responsibility to determine suitability for the user's purpose of any production methods mentioned herein and to adopt such precautions as may be advisable for the protection of property and of persons against any hazards that may be involved in the handling and use thereof. In light of the foregoing, Henkel Corporation specifically disclaims all warranties expressed or implied, including warranties of merchantability or fitness for a particular purpose, arising from sale or use of Henkel Corporation’s products. Henkel Corporation specifically disclaims any liability for consequential or incidental damages of any kind, including lost profits. The discussion herein of various processes or compositions is not to be interpreted as representation that they are free from domination of patents owned by others or as a license under any Henkel Corporation patents that may cover such processes or compositions. We recommend that each prospective user test his proposed application before repetitive use, using this data as a guide. This product may be covered by one or more United States or foreign patents or patent applications. Other packaging types may be available on request; please contact your local technical service helpdesk for assistance. Storage: It is recommended to store LF318 at 0-10°C (NB cartridges should be stored tip down to prevent the formation of air pockets). The paste should be removed from cold storage a minimum of 8 hours prior to use. Do not use forced heating methods to bring solder paste up to temperature. Multicore LF318 solder paste has been formulated to minimize flux separation on storage but should this occur, gentle stirring for 15 seconds will return the product to its correct rheological performance. To prevent contamination of unused product, do not return any material to its original container. For further specific shelf life information, contact your local Technical Service Centre. Shelf Life: Provided Multicore LF318 solder pastes are stored tightly sealed in the original container at 0-10°C, a minimum shelf life of 6 months can be expected. Air shipment is recommended to minimize the time that containers are exposed to higher temperatures. DATA RANGES The data contained herein may be reported as a typical value and/or range. Values are based on actual test data and are verified on a periodic basis. Americas Henkel Corporation 15350 Barranca Parkway Irvine, CA 92618 U.S.A. 949.789.2500 Europe Henkel Loctite Adhesives Ltd Technologies House, Wood Lane End Hemel Hempstead Hertfordshire HP2 4RQ, United Kingdom +44 (0) 1442 278 000 Asia Henkel Loctite (China) Co. Ltd No. 90 Zhujiang Road Yantai Development Zone Shandong, China 264006 +86 535 6399820 All trademarks, except where noted are the property of Henkel Corp. BACK