Laboratory TEMPERATURE PORTUGUESE INSTITUTE FOR QUALITY FIELD OF ACTIVITY LNM Cell for realization of the Triple point of the water Realization of the triple point of argon Furnace with Freezing Point of copper The Temperature Laboratory is responsible for the development of the national standards of temperature and relative humidity and has the following duties: SI UNIT The realization of the International Temperature Scale of 1990 (ITS90) on the fixed points between the triple point of argon (-189,3442 °C) and the freezing point of silver (961,78 °C); The realization too the ITS90 based on Planck radiation, with the freezing point of copper (1084,62 °C); To assure the traceability on Temperature measurements on the measuring interval from – 190 °C to 2500 °C; Calibrate reference standards of secondary laboratories, accredited laboratories and industry; Participate and coordinate interlaboratorial comparisons; Technical support to the legal metrology. International System Base Unit of Temperature (T ) kelvin (K) defined as: The fraction 1 / 273,16 of thermodynamic temperature of the triple point of water Derived unit of the International System of the temperature quantity (t ): degree Celsius (ºC) defined by the equation: t = T - T0 , where T0 = 273,15 K is the ice point. The unit of Celsius temperature unity is by definition equal in magnitude to the kelvin. The unit of Relative Humidity quantity (UW ) with respect to water: Symbol (%) defined as follows: The ratio of the actual vapour pressure (e) to the saturation vapour pressure (eW) over a plane liquid water surface at the same temperature t (ºC), expressed as percentage. This is commonly understood when the term “X percent relative humidity” is used. TRACEABILITY UW e 100 eW The traceability to SI units is achieved through the realization of the Fixed Point of EIT90 and appropriate resistance standards. AVAILABLE SERVICES Calibration EQUIPMENT Contact Thermometry Thermometers Temperature Sensors Standard Platinum Resistance Thermometers Comparison at stirred liquid bath Contact Thermometry Thermometers Temperature Sensors Noble -metal thermocouples Type S and R Comparison at heat pipe Contact Thermometry Liquid-in-glass thermometers Comparison at stirred liquid bath Non-contact Temperature Radiation thermometers Optical pyrometers Measuring instruments of relative humidity Platinum Resistance Thermometers Noble metal thermocouples Optical pyrometers RANGE -75 ºC a 0 ºC 0ºC a 20 ºC 20 ºC a 50 ºC 50 ºC a 100 ºC 100 ºC a 200 ºC 300 º C a 450 ºC 0 º a 300 ºC 300 ºC a 600 ºC 600 º C a 900 ºC UNCERTAINTY 0,01 ºC 0,005 ºC 0,007 ºC 0,010 ºC 0,020 ºC 0,035 ºC 0,4 ºC 0,5 ºC 0,7 ºC 900 ºC a 1050 ºC 1,0 ºC -40 ºC a 0 ºC 0ºC a 50 ºC 50 ºC a 100 ºC 100 ºC a 200 ºC 200 ºC a 300 º C 300 º C a 450 ºC Ponto de Gelo 30 °C a 500 °C 500 ºC a 1600 ºC 1600 ºC a 2500 ºC 0,01 ºC 0,005 ºC 0,01 ºC 0,01 ºC 0,1 ºC 0,2 ºC 0,5 ºC 0,5 ºC 0,1 % 0,2 % 10 % a 90 % 2% Liquid nitrogen boiling point 77 K (-196 ºC) (by comparison) 83,8058 K (argon triple point) to 273,16 K (water triple point) -38,8344 ºC (mercury triple point) to 29,7646 ºC (gallium melting point) 0 ºC to 29,7646 ºC (gallium melting point) 0 ºC a 156,5985 ºC (indium freeze point) 0 ºC a 231,929 ºC (tin freeze point): 0 ºC a 419,527 ºC (zinc freeze point): 0 ºC a 660,323 °C (aluminium freeze point) 0 ºC a 961,78 ºC (silver freeze point): 231,929 ºC (tin freeze point): 419,527 ºC (zinc freeze point): 660,323 ºC (aluminium freeze point) 961,78 ºC (silver freeze point) Copper freeze point (1084,62 ºC) 5 · 10-3 ºC 2 · 10-3 ºC 1 · 10-3 ºC 1 · 10-3 ºC 3 · 10-3 ºC 3 · 10-3 ºC 5 · 10-3 ºC 1 · 10-2 ºC 5 · 10-2 ºC 0,4 ºC 0,4 ºC 0,4 ºC 0,4 ºC 0,5 ºC Metrological Control CONTACT EQUIPMENT TESTS Measuring Instruments and Pattern Approval Temperature recorders used for the control of ultra-frozen food in transport and store houses. LEGISLATION Portaria n.º 1129/2009 de 1 de outubro INSTITUTO PORTUGUÊS DA QUALIDADE (Portuguese Institute for Quality) Rua António Gião, 2 PT-2829-513 Caparica TEMPERATURE LABORATORY THERMOMETRY Head: Engª. Isabel Lóio Tel: +351 212 948 163 E-mail: iloio@ipq.pt ITS90 Head: Engª. Liliana Eusébio Tel +351 212 948 156 E-mail lilianae@ipq.pt Manuela Oliveira Tel: +351 212 948 196 E-mail: moliveira@ipq.pt