S C IP P Charge Collection in p-type Si Tracking Detectors 1) LHC Upgrade environment 2) C-V and CCE after Proton/Pion Irradiation 3) Annealing after neutron irradiation 4) Bias Dependence of collected charge 5) Efficiency M.K. Petterson, R.F. Hurley, K. Arya, C. Betancourt, B. Colby, M. Gerling, C. Meyer, J. Pixley, T. Rice, H. F.-W. Sadrozinski SCIPP UC Santa Cruz ,1156 SCIPP, 1156 High St St., Santa Cruz Cruz, CA 95060 Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 1 Fluence in Proposed sATLAS Tracker Long Strips sATLAS Fluences for 3000fb-1 1.E+17 All: RTF Formula n ((5cm poly) p y) pion proton 2 1.E+16 Fluence e neq/cm Radial Distribution of Sensors determined by Occupancy < 2% S C IP P 5 - 10 x LHC Fl ence Fluence Mix of n, p, π depending on radius R 1.E+15 1.E+14 1.E+13 Short Strips 1.E+12 0 Pixels 20 40 60 80 100 120 Radius R [cm] Strips damage largely due to neutrons ATLAS Radiation Taskforce http://atlas.web.cern.ch/Atlas/GROUPS/PHYSICS/RADIATION/RadiationTF p _document.html Design fluences for sensors (includes 2x safety factor) : Innermost Pixel Layer: O t t Pixel Outert Pi l Layers: L Short strips: Long strips: 1*1016 neq/cm2 3*1015 neq/cm / 2 1*1015 neq/cm2 4*1014 neq/cm2 Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 Pixels Damage due to neutrons+pions: need high fluence proton irradiations 2 RD50 Test Sensors 4” : Micron CNM S C IP P IRST RD50 Common Micron (6”) ATLAS Upgrade HPK (6”) Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 3 RD50 MICRON 6” project S C IP P •36 36 processed , 20 received •Fz (Topsil) and MCz (Okmetic) wafers of p&n type material •n-on-n, n-on-p, p-on-n structures (pixels, strips, diodes) Strips: St i ATLAS strips i geometry 80 μm μ pitch i h ((w/p~1/3) / 1/3) Pads: 5 x 5 mm2 , multiple guard rings MCz (n-p) V(FD) [V] MCz(n-n), (p-n) 520 Fz (n-p) 220 Fz (n-n), (p-n) 75 95 Resitivity 1.9 kΩcm 1.4 kΩcm 13 kΩcm 3.3 kΩcm Orientation <100> <100> <100> <100> Neutron and Proton and Pion (Aug. ’07 ) irradiation of SSD and Diodes Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 4 Charge collection CCE in p-type MCz after a te Proton oto Irradiation ad at o S C IP P MedQ vs. Bias 3.5 3 Med Q [fC] M 2.5 2 1.5 1 2552-6-9-1 n-on-p Mcz 1.3e14 05 0.5 2552-7-13 N-on-P MCz (Micron) Pre-rad 0 0 200 400 600 800 1000 Bi Bias Voltage V lt Curious: large loss of charge at small fluence Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 5 Bias Dependence of Efficiency, CCE, Singles S C IP P Proton Irradiation 1.3e14 M edQ 3 2 .5 eff @ 1fC 2 1.2 1 .5 Median Charge 1 1 0.8 0 .5 0.6 0 0 100 200 300 400 500 Efficiency y @ 1 fC 0.4 0.2 0 0 100 200 300 400 500 Count Rate @ 1 fC Saturation: Efficiency before Median pulse height Median pulse height = Single rate Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 6 C-V and CCE in MCz (Protons 1.3e14) S C IP P CV comparison C-V taken at -20oC and 450Hz 0.014 0.012 1/C overestimates the depletion voltage 0.008 0.006 0.004 C/1 MedQ norm 0.002 0 0 50 100 150 200 250 300 350 400 SMART p-on-n FZ 187 Bias Voltage [V] Agreement between low T– Low f 1/C-V and CCE less perfect than seen before in n-type FZ M K Petterson M.K. P tt ett al., l NIMA 583, 583 189 (2007) 3.5 Collected Cha arge [fC] 1/C [1/pF] 1 0.01 3.0 2.5 20 2.0 1.5 1/C 10kHz;+ 22°C 1/C 10kHz; -11°C 1/C 400Hz; -11°C Charge median value 1.0 0.5 00 0.0 0 Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 200 400 600 Voltage [V] 800 7 Protons & P-type: Compare FZ and MCz S C IP P p FZ: proton p irradiation 8.E-04 1/C^2 [1/pF F^2] 6.E-04 p-type FZ: Monotonic Increase in Full Depletion Voltage: Monotonic Introduction of Acceptors Material becomes more p-type Introduction rate not constant? Donor removal? 4.E-04 2.E-04 pre-rad 1e14 proton 3 14 proton 3e14 t 0.E+00 0 100 200 300 400 Bias Voltage [V] 500 600 700 p MCz proton irradiation 2 0E-04 2.0E-04 p-type MCz 1/C^2 [1/pF F^2] 1.5E-04 Non-Monotonic Increase in depletion p voltage: g Introduction of Donors Material becomes initially more n-type: Type inversion? Large initial donor introduction rate 1.0E-04 5.0E-05 pre-rad 1e14 proton 4e14 proton 0.0E+00 0 100 200 300 400 Bias Voltage [V] 500 600 700 Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 8 Pions & P-type: Compare FZ and MCz S C IP P Micron: 1e14 Pion Irradiated SSD 0.0008 0 0007 0.0007 0.0006 1/C [1/pF F] 0.0005 0.0004 0.0003 0.0002 pre rad 3-1 pre-rad 3 1 2551-2 2551 2 0.0001 p FZ 1e14 3-1 2551-2 p MCz pre-rad 2552-6 n-p MCz 1e14 3-4 2552-6 0 0 100 200 300 400 500 600 700 Bias Voltage [V] Same as for Protons: MCz and FZ different! CCE should h ld be b interesting! i t ti ! Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 9 New Wafer Scorecard? S C IP P • Materials: Neff = Neff0+g*Φeq • • For p-type: need Neff0 low: high resistivity For n-type, need Neff0 high: low resistivity 2.50 24 GeV Protons reactor neutrons 2.00 NEG. SPACE CHARGE Acceptors gc [[10-2 cm-1] 1.50 1.00 0 50 0.50 0.00 FZ-p,n -0.50 -1.00 DOFZ-p,n MCz - n? MCz - p EpiSi-p,n POS. SPACE S CE CHARGE Donors We are analyzing g more proton and pion data to verify that donors are produced in p MCz FZ and Mcz data verified for neutron irradiation: Radiation damage in MCz different for protons and neutron irradiation? Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 10 Annealing of p-type FZ and DOFZ sensors S C IP P (n irradiated) Annealing of Micron Detectors (neutrons, 500V Bias) 16000 14000 Med Q @500V (e-) 12000 10000 8000 6000 4000 N-on-P N on P FZ (Micron) Φ=5e14 Φ 5e14 neutron 2551-7-9 2551 7 9 N-on-N MCz (Micron) Φ=1e15 neutron 2553-11-11 N-on-P FZ (Micron) Φ=1e15 neutron 2551-7-11 N-on-P MCz (Micron) 1e15 neutron 2552-7-11 N-on-P MCz (Micron) Φ=5e14 neutron 2552-7-9 2000 0 1 10 100 1000 10000 Anneal time (min) Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 11 CCE vs. Annealing (n irradiated) S C IP P Annealing of Micron Detectors: 800V 18000 16000 Med Q @800V V (e-) 14000 12000 10000 8000 6000 N-on-P FZ (Micron) F =5e14 neutron 2551-7-9 N-on-N MCz (Micron) F =1e15 neutron 2553-11-11 N-on-P FZ (Micron) F =1e15 neutron 2551-7-11 N-on-P MCz (Micron) 1e15 neutron 2552-7-11 ) )p-on-n MC 1.7e15 MCz 1 7 15 neutron t (SMART 176-7 176 7 4000 2000 0 1 10 100 1000 10000 Anneal time (min) At sLHC fluences for p-type sensors, the entire annealing process is much less pronounced. than for n type FZ. It opens the possibility that sensors need to be cooled only during operations to control the leakage current, but not during beam-off time to prevent anti-annealing Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 12 CCE in neutron Irradiated SSD n-on-p n on p FZ 2551-7 2551 7 n-on-p FZ 1000 min ann n-on-n MCz 2553-11 n-on-n MCz 1000min ann p-on-n MCz 176-7 p-on-n MCz MC 1000 min i ann n-on-p Mcz 2552-7 n-on-p Mcz 1000min p-on-n Epi SMART p-on-n MCz SMART n-on-p Fz SMART 25000 Bias Voltage 800V 20000 Median Q [e-] S C IP P 15000 10000 5000 0 0.0E+00 5.0E+14 1.0E+15 1.5E+15 2.0E+15 2.5E+15 3.0E+15 2 Fluence [neq/cm ] SMART data from A. Messineo (Pisa), Epi(150um) at ~ 300V Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 13 Charge Collection in Irradiated SSD n on p FZ 2551 n-on-p 2551-7 7 n-on-p FZ 1000 min ann n-on-n MCz 2553-11 n-on-n MCz 1000min ann p-on-n MCz 176-7 p-on-n MCz 1000 min ann n-on-p Mcz 2552-7 n-on-p n on p Mcz 1000min p-on-n Epi SMART p-on-n MCz SMART n-on-p Fz SMART Casse casse casse protons 25000 Bias Voltage 800V 20000 Median Q [e-] S C IP P 15000 10000 5000 0 0.0E+00 5.0E+14 1.0E+15 1.5E+15 2.0E+15 2.5E+15 3.0E+15 Fluence [neq/cm2] P-on-n MCz and FZ strip sensors not sufficiently radiation-hard for the sLHC P-on-n Epi (150 μm) is better alternative Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 14 Charge Collection in Irradiated SSD Peak and Median Q @ 800V 25000 S C IP P SCIPP n-on-p FZ 2551-7 n irr (prel SCIPP n-on-p FZ n irr 1000 min ann (prel Casse NIM A n-on-p FZ p irr SCIPP n-on-n MCz 2553-11 n irr (prel SCIPP n-on-n MCz n irr 1000min ann (prel SCIPP p-on-n MCz 176-7 n irr (prel Collected Charg ge Q [e-] 20000 SCIPP p-on-n MCz n irr 1000 min ann. (prel Long Strips S/N > 10 .Casse IEEE07 n-on-p FZ n irr 15000 Short Strips S/N > 10 n-on-p FZ 10000 5000 SCIPP: Binary, Median, Strips Casse: Analog, Peak, Strips p on n Mcz p-on-n 0 1.E+14 1.E+15 1.E+16 Fluence [neq/cm2] N-on-p strip sensors are sufficiently radiation-hard for the sLHC Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 15 Charge Collection in Upgrade Strips S C IP P ATLAS bias bi voltage lt is i constraint t i t to t < 500V (cables!). ( bl !) Peak and Median Q @ 500V SCIPP n-on-p FZ 2551-7 n irr (prel SCIPP n-on-p FZ n irr annealed (prel 25000 C Casse n-on-p FZ n-irr. i IEEE07 Ljubljana n-on-p FZ pad 2551-7 n irr (prel Ljubljana n-on-p Mcz pad 2552-7 n irr(prel Collected d Charge Q [e-] Casse NIM A n-on-p FZ p irr 20000 SCIPP n-on-n MCz 2553-11 n irr (prel SCIPP n-on-n MCz n irr ann. 80 min (prel SCIPP n-on-n MCz MC n irr i ann. 1000 min i (prel ( l Long Strips S/N = 10 .Casse IEEE07 n-onp nirr 15000 Short Strips S/N = 10 10000 5000 SCIPP: Binary Binary, Median, Median Strips Casse: Analog, Peak, Strips Ljubljana: Analog, Peak, Pads 0 1.E+14 1.E+15 1.E+16 2 Fluence [neq/cm ] N-on-p strip sensors are sufficiently radiation-hard for the sLHC ? Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 16 Efficiency vs. Collected Charge • For tracking sensors with binary readout, the figure of merit is not the collected charge, h bbutt the th efficiency. ffi i • 100% efficiency is reached at a signal-to-noise ratio of S/N ≈ 10, S/Thr > 2 • For long strips (5e14 cm-2) with a signal of about 14ke, the usual threshold of 1fC = 6400 e can be used. Median Pulse Height vs. Efficiency (n-on-p FZ, 5e14 n) S C IP P Efficiency Median Q Fluence 25000 B D Pre-rad E G 5e14 n 1.2 1 20000 08 0.8 15000 0.6 10000 04 0.4 5000 0.2 0 0 200 400 600 800 0 1000 Bias Voltage [V] Long strips efficient at 1fC threshold Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 17 Efficiency vs. Collected Charge Median Pulse Height vs. Efficiency (n-on-p FZ, 1e15 n) S C IP P Efficiency Median Q Fluence • The threshold needs to be reduced to about 4500 e, i.e. electronics must be designed for a noise of ~700e. D Pre-rad H J 1e15 n 1.2 1 20000 08 0.8 15000 0.6 10000 04 0.4 5000 0.2 0 0 200 400 600 800 Efficien ncy at 1 fC T Threshold • For short strips (1e15 cm2) with a signal of about 8ke, the efficiency at 500V is only 70%. Media an Charge Co ollected [e-] 25000 B 0 1000 Bias Voltage [V] Short strips efficient if threshold can be lowered Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 18 Conclusions S C IP P Much progress with p-type sensors, both in production and understanding Difference between proton/pion and neutron radiation damage in MCz. P-type: FZ seems to be more predictable than MCz. G d annealing Good li behavior b h i for f CCE in i p-type t N-on-n has good CCE. Long strips will work with 1 fC threshold at 500V (ATLAS). (ATLAS) Short strips need lowered threshold at 500V (ATLAS). Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 19 Acknowledgments S C IP P Thanks to RD50 collaborators in Ljubljana, Louvain, CERN, Karlsruhe, PSI, UCSC for carrying out the irradiations. irradiations Collaboration with SMART, Liverpool, Ljubljana. Hartmut F.-W. Sadrozinski, Barcelona April 14, 2008 20