AB SCIEX 5500 Series of Instruments
Site Planning Guide
Document Number: D5034384 A
Release Date: August 2012
This document is provided to customers who have purchased
AB Sciex equipment to use in the operation of such AB Sciex
equipment. This document is copyright protected and any reproduction
of this document or any part of this document is strictly prohibited,
except as AB Sciex may authorize in writing.
Software that may be described in this document is furnished under a
license agreement. It is against the law to copy, modify, or distribute
the software on any medium, except as specifically allowed in the
license agreement. Furthermore, the license agreement may prohibit
the software from being disassembled, reverse engineered, or
decompiled for any purpose.
Portions of this document may make reference to other manufacturers
and/or their products, which may contain parts whose names are
registered as trademarks and/or function as trademarks of their
respective owners. Any such use is intended only to designate those
manufacturers' products as supplied by AB Sciex for incorporation into
its equipment and does not imply any right and/or license to use or
permit others to use such manufacturers' and/or their product names
as trademarks.
AB Sciex makes no warranties or representations as to the fitness of
this equipment for any particular purpose and assumes no
responsibility or contingent liability, including indirect or consequential
damages, for any use to which the purchaser may put the equipment
described herein, or for any adverse circumstances arising therefrom.
For research use only. Not for use in diagnostic procedures.
The trademarks mentioned herein are the property of
AB Sciex Pte. Ltd. or their respective owners.
AB SCIEX™ is being used under license.
AB SCIEX
71 Four Valley Dr., Concord, Ontario, Canada. L4K 4V8.
AB Sciex LP is ISO 9001 registered.
© 2012 AB SCIEX.
Printed in Canada.
Contents
Chapter 1 Customer and FSE Responsibilities. . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Customer Site Planner Responsibilities . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
FSE Responsibilities . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
During Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Operator Familiarization . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Technical Support . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Chapter 2 Site Planning Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Customer Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Comments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Exceptions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Signoff . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Appendix A Site Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Site Layout Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Weights and Dimensions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Layout Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Installation Site Clearances . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Electrical Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
International Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
North American Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Mains Supply Fluctuations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
Protective Earth Conductor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
UPS (Uninterruptible Power Supply) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
System Electrical Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Gas Supply Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
Optional Generators . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
Ventilation and Waste-Collection Requirements . . . . . . . . . . . . . . . . . . . . . . . . .21
General Guidelines for the Laboratory Ventilation System . . . . . . . . . . . . . . .22
Network and Computer Equipment Requirements . . . . . . . . . . . . . . . . . . . . . . .23
Customer Printer Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
LAN Connection (Optional) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
Environmental Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Standard Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Optional Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Sound Pressure Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Vibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Customer Supplied Solutions and Equipment . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Appendix B Health and Safety Precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Appendix C Equipment Safety Categories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
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Contents
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1
Customer and FSE Responsibilities
This guide is for the site planner, the individual responsible for preparing the facility for the
installation of the AB SCIEX QTRAP® 5500 system or AB SCIEX Triple Quad™ 5500 system.
Note: If the site preparation tasks are not complete when the AB SCIEX Field Service
Employee (FSE) arrives, the scheduled installation will be postponed.
Customer Site Planner Responsibilities
Caution: Potential Instrument Damage: Do not unpack the mass spectrometer crate or
computer boxes. The FSE will unpack and move the mass spectrometer at the time of the
installation.
•
Verify that adequate space and the required shipping facilities are available. Refer to
Site Layout Requirements on page 13.
•
Provide all required electrical receptacles. Refer to Electrical Requirements on
page 16.
•
Provide all required regulators, shut off valves, and gases, as detailed in this guide.
Refer to Gas Supply Requirements on page 20.
•
Provide and install all required vents and ventilation devices. Refer to Ventilation and
Waste-Collection Requirements on page 21.
•
Provide a printer and (optional) active, tested LAN connection. Refer to Network and
Computer Equipment Requirements on page 23.
•
Verify that the requirements for the operating environment are met. Refer to
Environmental Requirements on page 24.
•
Provide the required solutions and laboratory equipment, including all equipment,
fittings, and sample tubing required for the liquid chromatography (LC) equipment,
unless purchased from AB SCIEX. Refer to Customer Supplied Solutions and
Equipment on page 25.
•
Complete the checklist in Site Planning Checklist on page 7 and return it to the FSE.
Note: The FSE will follow up if the checklist is not received prior to the
scheduled installation date.
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Customer and FSE Responsibilities
FSE Responsibilities
•
Supply all fittings, plugs, and cables required to connect the mass spectrometer to
the electrical receptacles, and regulators, provided they are within the maximum
distances described herein.
•
Assemble and set up any AB SCIEX benches ordered with the mass spectrometer.
•
Test and qualify the system to the specifications in the Installation Guide.
•
Set up LC equipment sold and supported by AB SCIEX. Integrate other supported
LC equipment.
•
Set up optional gas generator equipment sold by AB SCIEX only.
During Installation
After an FSE unpacks the system (with assistance from people at your site), it takes several
hours for the FSE to set up the system and check its operation. When the system reaches proper
vacuum, the FSE will perform installation qualification tests.
Operator Familiarization
During installation, the FSE provides a system and software overview, reviews data, and
provides some basic operator familiarization. Training for auxiliary equipment supplied by other
manufacturers is not provided by the FSE.
Note: Online training is available at www.absciex.com/training.
Technical Support
AB SCIEX and its representatives maintain a staff of fully-trained service and technical
specialists located throughout the world. They can answer questions about the system or any
technical issues that may arise. For more information, visit the web site at www.absciex.com.
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Site Planning Checklist
Customer Information
Organization
Address
City
Country
ZIP/Postal Code
Telephone #
Fax #
Site planner
contact name
E-mail address
Requirements
Caution: Potential Instrument Damage: Do not unpack or connect any components. The
FSE will unpack, connect, and configure the system for the proper operating voltage.
Table 2-1 Site Planning Checklist
Requirements
Complete
Site Layout Requirements
Refer to Site Layout Requirements on page 13.
The measured building clearances can accommodate the equipment and crate
dimensions.
.
.
If the requirements cannot be met, contact the FSE.
Electrical Requirements
Refer to Electrical Requirements on page 16.
One branch circuit (200 VAC to 240 VAC) is provided for the mass spectrometer.
The mains supply outlet is less than 1.6 m (69 inches) from the mass
spectrometer.
.
.
The optional bench can be connected to the mass spectrometer branch circuit.
One branch circuit (200 VAC to 240 VAC) is provided for the roughing pump. The
mains supply outlet for the roughing pump is less than 1.6 m (69 inches) from the
roughing pump.
.
.
Record the following values. The measured mains voltage over 24 hrs was:.
• High value +%:
• Low value –%:
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Site Planning Checklist
Table 2-1 Site Planning Checklist (Continued)
Requirements
Complete
The mains voltage source does not fluctuate more than ±10% from the nominal
voltage.
.
.
Note: Peripheral devices may have different mains supply fluctuation limits.
Check the mains supply fluctuation limit with the vendor of each peripheral
device that will be used with the mass spectrometer.
The mains supply includes a correctly installed protective earth conductor.
.
.
(Optional) A customer-supplied UPS is provided for the system. The UPS must
deliver 230 VAC, 50/60 Hz, 4000 VA (min). Refer to UPS (Uninterruptible Power
Supply) on page 18.
.
.
(Optional) A customer-supplied power conditioner is provided for the system. It
must deliver 230 VAC, 50/60 Hz, 4000 VA (min). Refer to UPS (Uninterruptible
Power Supply) on page 18.
.
.
A qualified electrician has determined the appropriate mains supply configuration
based on the system electrical specifications found in Table A-4 on page 19.
.
.
Electrical Requirements (North America)
Refer to Electrical Requirements on page 16.
The branch circuits referred to above:
• Have duplex receptacles, nominal 15A 208/240 VAC (voltage fluctuations
between 180 VAC and 264 VAC), 50/60 Hz.
.
.
• Are terminated with CSA/NEMA 6-15R receptacles.
Electrical Requirements (Accessories)
A minimum of two mains supply outlets is provided for computer equipment
(computer, monitor, printer):
.
.
• North America:120 VAC, 60 Hz
• Europe:230 VAC, 50 Hz
• Japan: 100 VAC, 50/60 Hz
For optional devices: electrical outlets are provided as necessary for the LC
pump, autosampler, diode array detector, and gas generator depending on
equipment requirements and installation location. Refer to the documentation
that comes with the device.
.
.
Gas Supply Requirements
Refer to Gas Supply Requirements on page 20.
Gas 1/Gas 2 supply is available:
• Zero grade air
• Delivery pressure of 100 psi (max.) with flows up to 22 L/min
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.
.
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Site Planning Checklist
Table 2-1 Site Planning Checklist (Continued)
Requirements
Complete
Curtain Gas™ supply and CAD gas supply are available:
• UHP nitrogen (99.999%)*
• Delivery pressure up to 60 psi (max.) with flows up to 10 L/min
.
.
* or approved AB SCIEX gas generator
Source exhaust gas supply is available:
• Clean, dry, and oil-free air or nitrogen
• Maximum delivery pressure of 55 psi (3.8 bar) with flows up to 8 L/min
.
.
If an optional wall-mounted gas generator or the optional mass spectrometer
bench is used, a supply of compressed oil-free air is provided, with a delivery
pressure of 120 psi (8.3 bar).
.
.
Liquid nitrogen generators, if used, are secured to meet local safety standards
and regulations. Use only regulators and connectors that comply with local
regulations.
.
.
Gas delivery lines are installed as required by local safety standards and
regulations.
.
.
Ventilation and Waste Collection Requirements
Refer to Ventilation and Waste-Collection Requirements on page 21.
Installation of plumbing and ventilation fixtures complies with local bylaws and
biohazard regulations.
.
.
A negative flow vent is provided with a total flow rate capacity of 283 L/min
(10 cfm).
.
.
A smooth fitting is provided for the roughing pump, with an outside diameter
(o.d.) of 3.2 cm (1.25 inch). The vent is within 1.5 m (5 ft) of the exhaust port on
the roughing pump, and at least 1 m (3 ft) above the floor.
.
.
A fitting is provided for the source exhaust drain bottle with an o.d. of 1.3 cm
(0.5 inch). The vent is within 1.5 m (5 ft) of the source exhaust drain bottle.
.
.
Ventilation of the laboratory environment in which the mass spectrometer will be
used complies with local regulations, and the air exchange rate is appropriate for
the work performed.
.
.
The length and number of bends in the ducting system is minimized.
.
.
The ventilation system uses smooth stainless steel tubing, with 45 degree
elbows to turn corners.
.
.
(Recommended) The blower for the source exhaust system is equipped with an
indicator light.
.
.
The length of the duct entering the blower is a straight length of at least ten times
the duct diameter.
.
.
The outlet end of the ventilation system is equipped with a backdraft damper and
exhaust stack, and is away from open windows or inlet vents.
.
.
The quantity of makeup air supplied matches the quantity of air exhausted by the
system.
.
.
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Site Planning Checklist
Table 2-1 Site Planning Checklist (Continued)
Requirements
Complete
Computer Requirements
Refer to Network and Computer Equipment Requirements on page 23.
A network or IT specialist is available to connect the computer to the company
LAN while the AB SCIEX FSE is present.
.
.
A network computer name and domain password are available.
.
.
An active, tested LAN connection is available.
.
.
A network printer or a dedicated printer and necessary print drivers are available.
.
.
Environmental Requirements
Refer to Environmental Requirements on page 24.
An ambient temperature of 15°C to 30°C (59°F to 86°F). The ambient
temperature cannot change more than 2°C (3.6°F) per hour.
.
.
Note: Peripheral devices may have different operating environment
requirements. Check the operating environment requirements with the vendor of
each peripheral device that will be used with the system.
The relative humidity level is 20% to 80%, non-condensing.
.
.
Air conditioning provides a minimum of 6500 Btu/hr (mass spectrometer and
roughing pump only).
.
.
(Optional) A customer-supplied soft wall is installed behind the mass
spectrometer to reduce noise.
.
.
Mass Spectrometer Bench
A bench is provided for the mass spectrometer, either a moveable bench or a
fixed bench with 1 m (3 ft, 4 inches) of clearance on three sides for service
access.
.
.
A bench is provided for the data acquisition workstation, located within 4 m
(13 ft) of the mass spectrometer.
.
.
Make sure that there is 1 m of clearance from the front, back, and left sides.
Materials Required for Routine Operation
Refer to Customer Supplied Solutions and Equipment on page 25.
All required solutions are available.
.
.
All required LC equipment and supplies are available.
.
.
Tubing and fittings required to connect the supported LC equipment to the mass
spectrometer are available.
.
.
Additional Site Planning
Complete site planning for peripheral devices and software, as required.
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.
.
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Site Planning Checklist
Table 2-1 Site Planning Checklist (Continued)
Requirements
Complete
Training
Complete the online training. Go to www.absciex.com/training.
.
.
Obtain and review system documentation. Go to www.absciex.com. Navigate to
Downloads > Mass Spectrometry User Guides.
.
.
Comments
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Site Planning Checklist
Exceptions
Signoff
Complete the checklist and return it to the FSE email specified below on or before the Return
Date.
Site Planner
contact name
I acknowledge that all installation requirements, as specified in this
document, have been met.
FSE name
Site Planning Review
Completion Date
.
.
Return date
FSE e-mail
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A
Site Requirements
Note: The site must not be designated BioSafety Level 3 (BSL-3) or BSL-4. AB SCIEX
does not install, service, or repair AB SCIEX mass spectrometers in areas designated
BSL-3 or BSL-4.
Site Layout Requirements
Return to checklist.
Weights and Dimensions
Check the weight and dimensions in Table A-1 and make sure that you can move the system to
the installation site. Make sure that the installation site can accommodate the equipment
dimensions, weight, and associated clearance.
The mass spectrometer has been designed to support 77 kg (170 lbs). The mass spectrometer
bench is designed to support the weight of the mass spectrometer plus its associated load,
roughing pump, and an additional 77 kg (170 lbs).
Table A-1 Weights and Dimensions
Equipment
Height
Crate
Length
Weight
84.5 cm; 33.3 in. 99.3 cm; 39 in.
112 cm; 44 in.
70 kg; 154 lbs.
Mass spectrometer
59 cm; 24 in.
79 cm; 32 in.
79 cm; 32 in.
130 kg; 285 lbs.
Roughing pump
22 cm; 9 in.
30 cm; 12 in.
42 cm; 17 in.
34 kg; 75 lbs.
Bench
78 cm; 31 in.
100 cm 40 in.
84 cm; 34 in.
120 kg; 265 lbs.
Accessories crate
129.5 cm; 51 in.
104 cm; 41 in.
132 cm; 52 in.
178 kg; 391 lbs.
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Site Requirements
Layout Requirements
Return to checklist.
Figure A-1 to Figure A-4 show examples of typical configurations.
Figure A-1 Layout configuration (not to scale)
Figure A-2 Layout configuration (not to scale)
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Site Requirements
Figure A-3 Layout configuration (not to scale)
Figure A-4 Layout configuration (not to scale)
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Site Requirements
Installation Site Clearances
Return to checklist.
Make sure the installation site meets the required building clearances. Refer to Table A-2.
Table A-2 Site Clearances
Clearance
Measurement
Front, back, and left sides
Mass spectrometer clearance requirement is 1 m for service
access.
Electrical Requirements
Return to checklist.
WARNING! Electrical Shock Hazard: Use only qualified personnel for the
installation of all electrical supplies and fixtures, and make sure that all
installations adhere to local bylaws.
The total combined system (mass spectrometer and roughing pump) power consumption is 2200
VA (50 Hz or 60 Hz) at 230 VAC.
You do not need an external line transformer for the mass spectrometer, optional mass
spectrometer bench, or roughing pump.
International Requirements
Return to checklist.
•
For installations outside North America, use locally approved standard connections
and cables. If the voltage changes more than 10% in 24 hours, use a power
conditioner.
North American Requirements
Return to checklist.
•
Two separate15A branch circuits are required to supply the mass spectrometer,
roughing pump, and mass spectrometer bench. These branch circuits must
•
Have duplex receptacles: nominal 15A 208/240 VAC. Total of four outlets.
•
Be equipped with CSA/NEMA 6-15R straight blade receptacles as shown in
Figure A-5.
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Site Requirements
Figure A-5 CSA/NEMA 6-15 duplex receptacle and plug
•
The optional gas generator requires an additional separate branch circuit equipped
with a CSA/NEMA 6-15R straight blade receptacle (208/240 VAC).
•
Additional outlets (120 VAC) are required for the computer, monitor, printer, and LC
equipment.
1
2
3
4
Figure A-6 System mains supply configuration
Item Description
1
One 15 A branch circuit is required for the mass spectrometer.The optional
mass spectrometer bench can be plugged into the mass spectrometer
branch circuit.
2
One 15 A branch circuit is required for the roughing pump.
3
One branch circuit is required for the optional gas generator.
4
Additional 120 VAC outlets for computer, monitor, printer, and LC
equipment as required.
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Site Requirements
Mains Supply Fluctuations
Return to checklist.
In areas where the mains supply is subject to voltage fluctuations exceeding ±10% of the nominal
value (200 VAC to 240 VAC), a power conditioner may be required. High or low voltages can
adversely affect the electronic components of the mass spectrometer. Refer to Table A-3.
Note: Peripheral devices may have different mains supply fluctuation limits. Check the
mains supply fluctuation limit with the manufacturer of each peripheral device that will
be used with the mass spectrometer.
Protective Earth Conductor
Return to checklist.
The mains supply must include a correctly installed protective earth conductor that must be
installed or checked by a qualified electrician before connecting the mass spectrometer.
WARNING! Electrical Shock Hazard: Do not intentionally interrupt the protective
conductor. Any interruption of the protective conductor is likely to make the
installation dangerous.
UPS (Uninterruptible Power Supply)
Return to checklist.
Use a pure sine-wave UPS or power conditioner to maintain the system supply (mass
spectrometer, computer, monitor, and roughing pump) during power outages.
If you power the system from a UPS or power conditioner, it must meet the following
specifications.
Table A-3 UPS and Power Conditioner Requirements
Condition
Requirements
Output voltage
200–240 VAC True on line (double conversion)
Frequency
50/60 Hz
Waveform
Pure sine wave
Minimum peak current
3 × nominal current
Output voltage distortion
<3%
Output protection
Circuit breaker
Minimum power requirement
4000 VA
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Site Requirements
System Electrical Specifications
Return to checklist.
The following tables contain the electrical specifications for the mass spectrometer, roughing
pump, mass spectrometer bench, computer, and monitor.
Note: Specifications are subject to change without notice.
Table A-4 Mass Spectrometer Electrical Specifications
Mass spectrometer
Value
Nominal input voltage
200 VAC to 240 VAC
Input voltage fluctuation
±10% of nominal
Frequency
50/60 Hz
Max input current
10 A
Max input power
1000 VA
Table A-5 Roughing Pump Electrical Specifications
Varian 849-9240 roughing pump
Value
Nominal input voltage
200 VAC to 240 VAC
Input voltage fluctuation
±10% of nominal
Frequency
50/60 Hz
Max input current
—
Max input power
1200 VA
Table A-6 Optional Mass Spectrometer Bench Electrical Specifications
Optional mass spectrometer bench
Value
Nominal input voltage
100 VAC to 240 VAC
Input voltage fluctuation
±10% of nominal
Frequency
50/60 Hz
Max input current
1A
Max input power
240 VA
Table A-7 Computer Electrical Specifications
Computer (P-390)
Value
Nominal input voltage
115/230 VAC
Input voltage fluctuation
±10% of nominal
Frequency
50/60 Hz
Max input current
6/3 A
Max input power
690 VA
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Site Requirements
Table A-8 Monitor Electrical Specifications
Monitor (1907FP)
Value
Nominal input voltage
100 VAC to 240 VAC
Input voltage fluctuation
+6/–10% of nominal
Frequency
50/60 Hz
Max input current
1.5 A
Max input power
360 VA
Gas Supply Requirements
Return to checklist.
Use high-pressure liquid nitrogen dewars or AB SCIEX approved gas generators.
Caution: Potential Instrument Damage: Each supply must be separately regulated at the
mass spectrometer otherwise over pressure can damage gas controllers.
It
1
1
2
2
3
3
Figure A-7 Gas connection configuration
Item Gas
Description
Requirements
Tubing
1/4 inch
1
Gas 1/Gas 2
Zero air
Zero grade air at 100 psi
(max.); flow rate of 22 L/min.
2
Curtain Gas™
supply; CAD gas
UHP (ultra high purity)
nitrogen (N2)
UHP N2 at 60 psi (max.); flow 1/4 inch
rate of 10 L/min.
3
Source exhaust
House air, zero air, or
UHP N2
House air, zero air, or UHP
N2 at 55 psi; flow rate of
8 L/min. Do not operate
below 55 psi.
1/4 inch
Note: All regulator output fittings must be 1/4 inch NPT to 1/4 inch Swagelok
(Swagelok PN SS-400-11-4).
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Figure A-8 Swagelok connection and tubing
Optional Generators
Return to checklist.
Gas generator are available from AB SCIEX. Refer to the manufacturer’s documentation that
comes with the generator for system specifications.
Ventilation and Waste-Collection Requirements
Return to checklist.
WARNING! Radiation Hazard, Biohazard, or Toxic Chemical Hazard: Make sure
that the laboratory is equipped with an appropriate ventilation system. Adequate
laboratory ventilation is required for safe operation of the mass spectrometer.
WARNING! Radiation Hazard, Biohazard, or Toxic Chemical Hazard: Use only
qualified personnel for the installation of plumbing and ventilation fixtures, and
make sure that all installations follow local bylaws and biohazard regulations.
Caution: Potential Instrument Damage: Do not connect the source exhaust hose to the
vent. The connection must be made by a qualified AB SCIEX FSE.
•
Provide a ventilation system with a total negative flow rate capacity of 283 L/min
(10 cfm) at item 1 in Figure A-9.
•
Provide a smooth fitting for the roughing pump, with an o.d. of 3.2 cm (1.25 inch).
The vent must be within 1.5 m (5 ft) of the exhaust port on the roughing pump, and at
least 1 m (3 ft) above the floor. Refer to Figure A-9.
•
Provide a fitting for the source exhaust drain bottle with an o.d. of 1.3 cm (0.5 inch).
The vent must be within 1.5 m (5 ft) of the source exhaust drain bottle. Refer to
Figure A-9.
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1
2
5
4
3
Figure A-9 Vent connections
Item Description
1
Vent
2
Source exhaust hose: 1.3 cm (0.5 inch) i.d. (inside diameter)
3
Source exhaust drain bottle. In this drawing, the capped drain bottle is shown at the
back of the mass spectrometer, to make connection points visible. The drain bottle is
located at the side of the mass spectrometer when installed.
4
Source exhaust drain tubing
5
Roughing pump exhaust hose: 3.2 cm (1.25 inch) i.d.
General Guidelines for the Laboratory Ventilation System
Return to checklist.
•
Make sure that the ventilation of the laboratory environment in which the mass
spectrometer will be used complies with local regulations, and that the air exchange
rate is appropriate for the work performed.
Note: In the United States, OSHA 29 CFR Part 1910-1450 requires 4 to 12
air changes per hour in laboratories.
•
Minimize the length and number of bends in the ducting system.
•
Use smooth stainless steel tubing instead of flexible tubing to reduce friction loss or
drag in the ventilation system. Use 45 degree elbows to turn corners.
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•
(Recommended) Equip the blower used for the source exhaust with an indicator light
located near the mass spectrometer, so that the operator can easily see whether the
blower is on.
•
Make sure that the length of the duct that enters the blower is a straight length of at
least ten times the diameter of the duct.
•
Equip the outlet end of the system with a backdraft damper and an exhaust stack.
Keep the exhaust outlet away from open windows or inlet vents.
•
Supply a quantity of makeup air that matches the quantity of the air exhausted by the
system. An airtight lab causes an efficiency loss in the exhaust system.
Network and Computer Equipment Requirements
Return to checklist.
•
Make sure that an IT specialist is available to install the security software while the
FSE is present.
Caution: Potential Instrument Damage: Other than security software, do not install
additional software on the computer. Changes to the configured software could void the
instrument warranty and cause the system to stop operating.
Customer Printer Requirements
Return to checklist.
The system can be connected to a network or dedicated printer.
•
Make sure that the printer and any necessary print drivers are available before the
scheduled installation.
LAN Connection (Optional)
Return to checklist.
•
Make sure that an active, tested LAN connection is in place before the scheduled
installation date.
•
Make sure that a network specialist is available to connect the computers to your
LAN while the FSE is present.
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Environmental Requirements
Return to checklist.
Standard Requirements
•
An ambient temperature of 15°C to 30°C (59°F to 86°F)
The rate of the change in temperature should not be more than 2°C (3.6°F) per hour.
Ambient temperature fluctuations may result in mass shifts in spectra.
•
Relative humidity from 20 to 80%, non-condensing
•
The cooling and venting requirement for the mass spectrometer and roughing pump
is 6500 Btu/hr
Caution: Potential Instrument Damage: Do not place the roughing pump in an
enclosed unventilated area. Otherwise, it will fail prematurely or shut down
from overheating and may cause severe damage to the mass spectrometer.
Note: Operation of the mass spectrometer at altitudes higher than
2000 m (6400 ft.) above sea level may impact mass spectrometer
performance.
Optional Requirements
We recommend that you install a soft wall behind the mass spectrometer to reduce the reflection
of sound generated by the equipment.
Note: Peripheral devices may have different operating environment requirements.
Check the operating environment requirements with the manufacturer of each
peripheral device that will be used with the mass spectrometer.
Sound Pressure Specifications
Table A-9 Sound Pressure Levels
Sound pressure
Level
Average sound pressure level
65 dBA
Maximum sound pressure level
68 dbA (at ion source)
Vibration
•
The packaged instrument was tested to confirm the effects of transportation do not
impact instrument performance upon arrival at the customer destination.
•
AB SCIEX has no specific data that relates to instrument performance under the
effects of vibration.
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Customer Supplied Solutions and Equipment
Return to checklist.
WARNING! Toxic Chemical Hazard: Follow all safety guidelines when handling,
storing, and disposing of chemicals. For health and safety guidelines, see Health
and Safety Precautions on page 27.
•
HPLC-grade ammonium acetate (100 mg)
•
MS-grade acetonitrile (2 L)
•
MS-grade methanol (2 L)
•
HPLC-grade deionized water (2 L)
•
Formic acid, 99% or higher (50 mL)
•
LC system, including waste bottles unless ordered through AB SCIEX
•
Pipettors (20 µL, 100 or 200 µL, 1 mL)
•
Printers
•
Table for the computer and monitor. Refer to Layout Requirements on page 14.
•
Mass spectrometer bench, unless ordered through AB SCIEX
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Health and Safety Precautions
•
Determine what chemicals may have been used in the instrument. Refer to Safety
Data Sheets if you are not familiar with the chemicals and the health and safety
precautions that should be followed.
•
Work in a well-ventilated area.
•
Always wear assigned personal protective equipment, including powder-free nitrile
gloves, safety glasses and a laboratory coat.
•
Follow required electrical safe work practices.
•
Avoid ignition sources when working with flammable materials, such as isopropanol,
methanol, and other flammable solvents.
•
Take care in the use and disposal of any chemicals. Potential risk of personal injury
if proper handling and disposing of chemicals are not followed.
•
Avoid skin contact with chemicals during cleaning, and wash hands after use.
•
Comply with all local regulations for the handling of radioactive materials.
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Equipment Safety Categories
C
Table C-1 Equipment Safety Categories
Description
Category
Equipment pollution degree
Pollution Degree 2
Mains supply transient overvoltage Overvoltage Category II
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