January 2016 School of Chemistry Structured PhD Programme (GYR05) In addition to the research thesis (CH650) some extra courses (modules) will be taken by students registered for their PhD in the School of Chemistry over a 4 year period. Students in the School in the four year structured programme will normally take 30 credits through these courses. Students with 3 years of funding where a structured component is not required (e.g. MSc graduates) may request from Dean of Science permission to carry out the PhD through the traditional 3 year PhD progamme (GYT13-1PS1) where the student is not required to take extra courses. The pass level in Chemistry modules will generally be a 40% in line with University marks and standards. A grade may not specifically be awarded (if student completes the module at PhD level then they pass). It is now possible for students registered through the 1 year MSc programme to formally apply for transfer to the PhD programme. Such students would normally have passed 30 credits of modules (CH5102 (15 credits) and CH5103 (10 credits) + 5 other credit module) and these modules should be recognised as part of the PhD programme and can also be taken by PhD students entering the Structured PhD programme. Core Modules The following are three core modules which all students in the PhD programme will be required to complete University Modules 1. Seminar programme ECTS Code Coordinator 5 GS501 PK 10 5 CH5103 GS506 FA PF 5 CH506 or CH5102 NG or 2. Chemical Research and Problem Solving* Teaching & Learning School of Chemistry Modules 3. Core Skills for Chemistry Research or Techniques and Skills for Chemistry Research* 15 NG * module given in semester one only 1 Elective Modules The following Graduate Studies Approved Modules may be taken as electives by PhD students in the School of Chemistry. Students can take one or more master classes. University Modules 4. Statistical Methods for Research 5. Masterclass in Carbohydrate Chemistry or Masterclass in Carbohydrate Chemistry with Practical Work 6. Masterclass in Radical Chemistry 7. Research placement 8. Industrial placement 9. Masterclass: Quantitiative analysis of solid-state pharmaceuticals 10 Combustion Chemistry and Kinetics 11. Advanced Biomaterials 12. Problem Solving in Chemistry 13. Process Development and Scale-Up in the Pharmaceutical Industry 14. Graduate Research Information & Skills 15. Oral / poster communications 16. Communication & Outreach ECTS Code 5 5 10 5 5 10 15 5 10 15 5 GS507 CH503 CH*** CH504 GS511 GS513 GS514 GS516 GS517 GS518 CH505 SD PM PM FA 5 5 5 5 CH507 BME500 CH509 CH510 HC YR POL DS 5 5 5 GS530 GS526 GS536 RD Supervisor Supervisor PM PM AE The module descriptor for BME500 can be found at: http://www.nuigalway.ie/engineeringinformatics/prospectivestudents/postgraduatestudents/structuredphdprogramme/ Coordinator: Dr Yury Rochev, Chemistry The module descriptor for GS507 can be found at: http://www.nuigalway.ie/graduate-studies/currentstudents/gsmodules/gs507/ Coordinator: Sandra Donohue, Graduate Studies The module descriptor for GS530 can be found at: http://www.library.nuigalway.ie/researchsupport/gs530graduateresearchinformationskillsm odule/ Coordinator: Rosie Dunne, Research Support, Library The module descriptor for GS526 can be found at: http://www.nuigalway.ie/graduate-studies/currentstudents/gsmodules/gs526/ The module descriptor for GS536 can be found at: http://www.nuigalway.ie/graduate-studies/currentstudents/gsmodules/gs536/ Modules GS526 and GS536 are assessed by the PhD Supervisor and GRC 2 Other Module Descriptors Title Seminar programme Credits (ECTS) 5 Module Coordinator Dr Paul Kavanagh Module Code: GS501 Elective Places Indicative Module Descriptor: In this module the students will attend a series of seminars. Students will attend a minimum of 16 seminars (E.g. Conference presentations, Seminar series). The School of Chemistry requirement will be 24 seminars during the course of the PhD with at least 18 selected from the official School of Chemistry Seminar Programme The module aims to give students the opportunity to; Further their knowledge in diverse research areas Develop critical analysis skills *Develop abstract writing skills and/or develop presentation skills Indicative Learning Outcomes: On successful completion of this module, students should; Have learnt about current topics having attended a series of seminars covering diverse range of subject matter Gained experience in critical analysis of speakers at seminar Become experienced in writing abstracts relating to seminars attended (optional) *Improved presentation skills (optional) Workload: (specify or delete as appropriate) 100 Class Contact: Seminar attendance Workshop at least 16 Specified Assignment(s) Seminar abstract preparation/critique 48 Autonomous Student Learning Seminar reflectance 16 Reading research papers 20 Assessment(s) (choose from below or add your own) Evidence of attendance (attendance signing sheet or book) *and one of the following: Completion of reflective journal comprised of a one abstract per seminar attended (e.g. 250 words) and critique of each seminar attended. *A student in the School of Chemistry may alternatively prepare and give at least two presentations on selected topics related to the seminar programme/recent research as agreed with their supervisor. This will usually be based on recent published research. Type Year 1: Seminar attendance Assessment of reflective journal/*abstracts or assessments of the presentations Result % of marks Timing Mandatory 100% Pass 3 Title Chemical Research & Problem Solving Credits (ECTS) 10 Module Coordinator Dr Fawaz Aldabbagh Module Code: CH5103 Elective Places Indicative Module Descriptor: In this module the students will be required to attend a series of advanced chemical research lectures given by academic staff of the School of Chemistry and by a series of visiting invited speakers from outside the School of Chemistry. The module aims to give students the opportunity to; Further their knowledge in areas at the frontiers of Chemistry Develop critical analysis skills Develop problem solving skills in chemistry Develop writing skills Develop presentation skills Indicative Learning Outcomes: On successful completion of this module, students should; Demonstrate breadth and depth of knowledge of topics at the frontiers of Chemical research Have gained experience in critical analysis Demonstrate increased knowledge in breadth and depth of chemistry and in problem solving Become experienced in writing abstracts relating to seminars attended Gain experience in giving a presentation Workload: (specify or delete as appropriate) 200 Class Contact: Lecture & seminar attendance Workshop Specified Assignment(s) Abstract preparation, preparation of presentation Autonomous Student Learning Reading research papers & autonomous study 16 4 80 100 Assessment(s) (choose from below or add your own) 1. Evidence of attendance (attendance signing sheet or book) 2. Submission of five one page abstracts based on research seminars given by staff of the School of Chemistry 3. Giving a presentation on a research topic related to the presentation given by a visiting speaker in the School of Chemistry and answering questions as part of a journal club 4. Written examination paper where students will solve problems related to the research topics covered. These will be set by the School of Chemistry staff giving the research seminars. Type % of marks Timing Year 1: Seminar attendance Abstracts Presentation Examination Result Mandatory 20% 30% 50% Mark out of 100 4 Title Teaching & Learning Credits (ECTS) 5 Supervisor Approval Supervisor approval is not a pre-requisite for this module due to teaching contribution of 120 hours per year (section 5.7 Duties) Module Places Module Coordinator Dr Pau Farràs Module Code: Please indicate if generic (GS) or specialised Elective Places GS506 Indicative Module Descriptor: This module will provide a comprehensive introduction to aspects of teaching and learning in higher education, offering an overview of basic ideas such as learning outcomes, teaching methods, assessment and approaches to learning. It will build experience of self-reflection through teaching practice, the identification of critical incidents and the use of a range of approaches to evaluation. All participants must undertake appropriate teaching practice, whether through tutoring, leading seminars or laboratory demonstration. st In the School of Chemistry this will normally be laboratory demonstration to the 1 year Undergraduate Chemistry class. Indicative Learning Outcomes: On successful completion of this module, students should; demonstrate awareness of the range of possible approaches to teaching and the promotion of active student learning available in higher education contexts; demonstrate awareness of the contextual factors and challenges which impact on an effective teaching and learning experience and identify some strategies for dealing with some common difficulties that may arise demonstrate appreciation of the particular role and responsibilities of the tutor or demonstrator; acquire significant experience in teaching and supporting learning in undergraduate (or postgraduate, if appropriate) programmes; have utilised appropriate approaches (including peer/mentor observation) to evaluate teaching; be able to reflect on critical incidents and learning events and evaluate the success or otherwise of particular approaches to teaching in the courses which they are supporting; have completed a reflective journal detailing their experiences and making suggestions and recommendations for subsequent improvement of their own performance and that of the students in their classes. Structure: This module will be delivered following a blended learning model which consists of three primary components: Online materials (in the Blackboard site for the module) and guided reading; Two three-hour workshops (one per semester) with associated activities and discussion; Reflection and peer discussion based on teaching practice as a tutor, laboratory demonstrator or in a similar capacity. In the School of Chemistry guidance will be provided to graduate students taking this module on grading. The graduate student will act as an instructor/demonstrator to ~16 first year students in Chemistry during their laboratory course and grade their work. Assessment(s): The module will be assessed on a pass/incomplete basis following completion, to an appropriate standard, of the following: A reflective journal providing evidence of reflection, improved practice and evaluation of student learning; Completion of an acceptable level of teaching hours, evidenced by a detailed log over the appropriate period; 5 Active participation in, and completion of associated tasks, the workshops and online course materials/exercises (which will include some short written contributions). A peer-assessment review of teaching Teaching Portfolio for Chemistry Postgradudates undertaking the module on Teaching & Learning For the award of the academic credit pertaining to this module, students are required to submit a portfolio, structured as follows. 1. Teaching responsibilities and experience Describe the courses/modules you are teaching on, the level of the modules (ie first year, final year, etc), the numbers of students in the class and the number that you are responsible for, the type of class (laboratory, tutorial, etc) and the duties required of you (eg demonstrating, providing lab briefings, marking and giving feedback, etc), and the overall aims or stated learning outcomes for that module. Briefly describe your past experience as a student in similar classes and to what extent you feel that it was an effective learning experience and what might have worked better. Provide a summary of the number of hours taught and have it signed by the person in charge of the lab/module you supported. 2. Practical aspects of teaching in class Readings relevant to Laboratory Demonstrating and Problem-solving classes are available on the Blackboard site for this module (Facilitating Learning: Key Skills & Techniques). Summarise the main points you have taken from these readings and indicate how they might affect the way you carry out your duties as a demonstrator or tutor. The peer observation exercise, whereby you get feedback from a fellow demonstrator/tutor (or from your academic mentor) can be a very effective means of thinking about and improving your teaching skills. The act of observing another also sheds light on issues that you might not have previously considered. Either complete the Peer Observation/Review exercise as described on the Blackboard site or get together with a fellow demonstrator/tutor and share with each other your respective approaches to and experiences of teaching this year. Then reflection in writing on what you have learned about the practice of teaching from this sharing. 3. Marking and Giving Feedback Read the section on marking and giving feedback. This is likely to be very relevant to your role as a demonstrator (or tutor) and addresses key issues such as consistency of grading, providing effective feedback to students to improve their performance and means of improving the quality and efficiency of the marking process as you build experience. In the portfolio, provide a brief summary of the key points of learning from this reading; describe the type of marking and grading in which you are involved, outlining the extent to which you have freedom over determining the grades and the forms of feedback and how this is managed and grades from different markers combined or compared. Comment on your experience this year in such marking and identify any challenges/difficulties you may have faced, how you worked with other demonstrators in ensuring consistency and how the students seem to respond to the feedback you provide to them. If you have any information regarding the distribution of marks across the group or the whole class, then you should refer to this here also. 4. Reflections and recommendations Look over the section on the principles of course design and briefly comment on the extent to which the module(s) that you support as a demonstrator (or tutor) appear to follow the model outlined there. If you can see ways in which the module or course might be improved with regards to the learning outcomes, learning and assessment methods or more general aspects of the organization of practical and taught 6 components, please note these here. You have experience of working closely with a number of students over several weeks, your own past experience as a student, as well as access to the basic module/course documentation – all of which might help inform such recommendations. Workload: (specify or delete as appropriate) Class Contact Workshop 6 hours Specified Assignment(s) Portfolio to include ( as appropriate to the Teaching responsibilities) elements such as: Reflective Journal Teaching Log Peer-Assessment/Observation or critical review of a Laboratory Teaching session Series of specific teaching experience exercises/tasks based on online materials Extensive online materials and lessons Teaching Practice Series of readings from text, papers, reports and websites. Autonomous Student Learning (please specify) Assessment(s) (choose from below or add your own) Type Assignments Reports Oral or Written Presentations as appropriate Result Successful completion of assignments from workshops and literature assignment % of marks Timing 100% Pass 7 Title Core Skills for Chemistry Research Credits (ECTS) 5 Module Coordinator Dr Niall Geraghty Course Instance Module Code: CH506 Please indicate if generic (GS) or Specialised specialised module Indicative Module Descriptor: (about 150 words) The course aims to provide a platform of training in key skills relevant to carrying out effective research in Chemistry. A series of lectures/demonstrations and training will be given in 12 areas. The areas covered will include Health and safety in Chemistry, Fire training, 2D NMR techniques, High performance liquid chromatography (HPLC), Gas chromatography (GC), Characterization and purity assessment of organic compounds, Text and structure based searching of online resources (Reaxys, SciFinder), Simulation software (ACD Labs), Molecular modelling of small molecules (Spartan), Gel permeation chromatography (GPC), Scanning electron microscopy, Mass spectrometry (MS), Electrochemical Methods, and X-ray crystallography. Indicative Learning Outcomes: On successful completion of this module, students should: have an awareness of the variety of techniques available in the School of Chemistry which are relevant to their research; understand and demonstrate that they have the potential to apply these techniques, as appropriate, to a research project. Workload: (specify or delete as appropriate) Class Contact Seminars (18-24 h) relating to 12 of the areas listed above (Health and safety and Fire training are mandatory). Supporting information will be provided on Blackboard Workshop (other forms of educational activity) Specified Assignment(s) Carry out assignments in 6 of the 12 areas listed above (Health and safety is mandatory; there is no Fire training assignment) (72 h). Autonomous Student Learning The background reading, autonomous (please specify) learning, experimental work and report writing associated with each assignment will not involve more than 12 h work Assessment(s) (choose from below or add your own Type Result % of marks Timing Students must satisfy the Unit Coordinator that adequate competency has been acquired in the particular skill. Pass 8 Title Credits (ECTS) Techniques and Skills for Chemistry Research 15 Module Coordinator Dr Niall Geraghty Course Instance Module Code: CH5102 Please indicate if generic (GS) or Specialised specialised module Indicative Module Descriptor: (about 150 words) The course aims to provide a platform of training in key skills relevant to carrying out effective modern research in Chemistry. A series of lectures/demonstrations and training will be given in 12 areas. The areas covered will include Health and Safety in Chemistry,A series of modern analytical techniques such as Microscopy, Electrochemistry, Structure based searching of online resources (Reaxys, SciFinder), Modern 1D & 2D NMR techniques, MS, X-ray crystallography, Computational Chemistry for small molecule modelling, drug design and reaction modelling, using the Cambridge Crystallographic database etc. Indicative Learning Outcomes: On successful completion of this module, students should: Gain a theoretical knowledge of variety of techniques available in the School of Chemistry which are relevant to their research Understand and demonstrate that they have can apply a subset of the techniques to Chemical problem solving in a laboratory setting Workload: (specify or delete as appropriate) Class Contact Workshop (other forms of educational activity) Specified Assignment(s) Lectures & seminars 30 h. Supporting information will be provided on Blackboard Demonstrate competence in 8 of the core skills, which must include health and safety. Each skill will have a specified assignment (120 h) 100 Autonomous Student Learning (please specify) Assessment(s) (choose from below or add your own Type Class contact Assignment Written Examination Paper Result % of marks Timing Mandatory 50% 50% Mark out of 100 9 Title Masterclass in Carbohydrate Chemistry Credits (ECTS) 5 Module Coordinator Prof Paul Murphy Course Instance Module Code: CH503 Please indicate if generic (GS) or specialised module Specialised. 3 Years of Chemistry at BSc level would be a minimum prerequisite. Indicative Module Descriptor: (about 150 words) The course focuses on core aspects of carbohydrate chemistry, including introduction to basic structures and concepts; carbohydrates in biological systems. Glycoside synthesis, glycopeptide, glycoprotein and glycolipid structure, properties and synthesis. Protecting groups in carbohydrate chemistry. Strategies for oligosaccharide synthesis. Analysis of carbohydrates and oligosaccharide structures, glycosensors and applications. Computation of carbohydrates. Indicative Learning Outcomes: On successful completion of this module, students should: Be able to devise and plan stereoselective syntheses of target oligosaccharides, glycopeptides, glycoproteins & glycolipids. Understand key concepts in carbohydrate chemistry and be able to apply these in solving assigned problems Understand and discuss publications in the carbohydrate chemistry area Be able to write an abstract of a specialised research lecture given during the course Workload: (specify or delete as appropriate) Class Contact Workshop (other forms of educational activity) Lectures 20 h. Supporting information provided (e.g. Blackboard) 4 h workshop & Seminars Specified Assignment(s) Autonomous Student Learning (please specify) Assessment(s) (choose from below or add your own Complete assignments which tests basic knowledge and understanding of essential concepts and involves problem solving (16 h) Present and discuss a recent publication (8 h) 60 h Type Result % of marks Timing Students must pass each task within the assignment Pass 10 Title Masterclass in Carbohydrate Chemistry with Practical Work Credits (ECTS) 10 Module Coordinator Prof Paul Murphy Course Instance Module Code: New modules Please indicate if generic (GS) or specialised module Specialised. 3 Years of Chemistry at BSc level would be a minimum prerequisite. Indicative Module Descriptor: (about 150 words) The course focuses on core aspects of carbohydrate chemistry, including introduction to basic structures and concepts; carbohydrates in biological systems. Glycoside synthesis, glycopeptide, glycoprotein and glycolipid structure, properties and synthesis. Protecting groups in carbohydrate chemistry. Strategies for oligosaccharide synthesis. Analysis of carbohydrates and oligosaccharide structures, glycosensors and applications. Computation of carbohydrates. Indicative Learning Outcomes: On successful completion of this module, students should: Be able to devise and plan stereoselective syntheses of target oligosaccharides, glycopeptides, glycoproteins & glycolipids. Understand key concepts in carbohydrate chemistry and be able to apply these in solving assigned problems Understand and discuss publications in the carbohydrate chemistry area Be able to write an abstract of a specialised research lecture given during the course Carry out preparative carbohydrate chemistry work and contribute to drafting a manuscript to the level of Carbohydrate Chemistry Proven Synthetic Methods or check carbohydrate synthetic work described in the literature to the level required for Carbohydrate Chemistry Proven Synthetic Methods Workload: (specify or delete as appropriate) Class Contact Workshop (other forms of educational activity) Lectures 20 h. Supporting information provided (e.g. Blackboard) 8 h workshop & Seminars Specified Assignment(s) Autonomous Student Learning (please specify) Assessment(s) (choose from below or add your own Complete a relevant assignment which tests understanding of essential concepts and involves problem solving (12 h) Present and discuss a recent publication (8 h) Practical work, including drafting of experimental to the level of Carbohydrate Proven Methods (100 h) 60 h Type Result % of marks Timing Students must pass each task within the assignment Pass 11 Title Masterclass in Advanced Radical Chemistry Credits (ECTS) 5 Module Coordinator Dr Fawaz Aldabbagh Course Instance Module Code: CH504 Please indicate if generic (GS) or specialised module Specialised. 3 Years of Chemistry at BSc level would be a minimum prerequisite. Indicative Module Descriptor: (about 150 words) The course focuses on modern applications of radical chemistry in four broad areas (students will choose 3 out of the 4 areas below)– 1. Mechanisms (Incl. Designing and Investigating Radical Reactions): choosing the appropriate radical initiator, detecting radicals, chain versus non-chain, the persistent radical effect, regio- and stereoselectivity 2. Organic Synthesis using Radicals: cascade, organometallic, metal free, photochemical and trapping reactions with applications to natural product, heterocyclic and carbohydrate synthesis. 3. Polymer Chemistry: kinetics and mechanisms, copolymerizations, living/controlled polymerizations, (computer) simulations, molecular weight distribution, heterogeneous polymerizations, green chemistry. 4. Medicinal Chemistry: oxidative stress, cancer, (computational) drug-design, DNA-damage and response, enzymes, case studies in biomolecular and biomacromolecular design. Indicative Learning Outcomes: On successful completion of this module, students should: Be able to devise and plan complex reactions, and devise mechanisms using radical intermediates. Understand key concepts in radical chemistry and be able to apply these to solving assigned problems Understand and discuss publications in the radical chemistry area Be able to write an abstract of a specialised research lecture given during the course This course will be based at NUI Galway with additional lectures from experts in the field. Workload: (specify or delete as appropriate) Class Contact Workshop (other forms of educational activity) Seminars & Lectures 20 h. Supporting information provided (e.g. Blackboard) And / or 10 h workshop or Symposium Specified Assignment(s) – 30 h divided as shown: 1. 2. 3. Autonomous Student Learning (please specify) Assessment(s) (choose from below or add your own Write two summary/abstracts of lectures identified from the course (4 h). Complete two assignments, which tests understanding of essential concepts and involves problem-solving (18 h) Present and discuss two recent publications identified by the module coordinator or supervisor (8 h) 40 h Type % of marks Pass 12 Timing Title Research placement Credits (ECTS) Module Coordinator 5-15 (depends on length of training; 1-3 months) This is an elective module and placement must be organised by supervisor and agreed with a host. To be assigned Course Instance Occasional Module Code: GS511 Module Places Please indicate if generic (GS) or Specialized specialised module Indicative Module Descriptor: (about 150 words) A graduate student may need to visit an academic or research laboratory outside NUI Galway to obtain training in a technique (e.g. access to and using an 800 MHz NMR facility, solid phase synthesis, Maldi-TOF MS, biophysical measurement technique, specialised polymer chemistry technicques etc). The student may spend up to three months in this training placement. Indicative Learning Outcomes: On successful completion of this module, students should: Have developed and demonstrated competency in the technique Understand the benefits of this training to a research project Workload: (specify or delete as appropriate) Class Contact Workshop (other forms of educational activity) Specified Assignment(s) The student will normally spend 1 (5 credits) to 3 months(15 credits) being trained in an external laboratory The graduate student will prepare a detailed report which includes: (i) a statement about the training (ii) evidence of the training obtained and a letter from the host laboratory confirming the time spent on the training and that they have become competent (iii) evidence that they applied the training in research Autonomous Student Learning (please specify) Assessment(s) (choose from below or add your own Type Result % of marks Timing Students must pass each task within the assignment Pass 13 Title Industrial Placement Credits (ECTS) 5-15 Module Places This is an elective module and placement must be organised by supervisor and agreed with an Industrial host Prof Murphy Module Coordinator Course Instance Module Code: GS516 (5 credits); GS517 (10 credits); GS518 (15 credits) Specialized Please indicate if generic (GS) or specialised module Indicative Module Descriptor: (about 150 words) Occasionally a graduate student may have funding from IRCSET-Enterprise partnership or from another industrial source. It may be to the student’s educational benefit to go on a placement with the industrial sponsor where they will gain experience of working in industry. During the course of their placement they will develop new skills and techniques and carry out research there, although the research may not form part of the PhD thesis. Indicative Learning Outcomes: On successful completion of this module, students should: Have demonstrated ability to solve problems and carry out research in an Industrial environment Gained new knowledge and skills and perspectives from the industrial placement Workload: (specify or delete as appropriate) Class Contact Workshop (other forms of educational activity) Specified Assignment(s) The student will normally spend up to 1-3 months being trained in the industrial laboratory Various The graduate student will prepare a report which includes: (i) a statement about their industrial placement (ii) Evidence of training and skills obtained (iii) Evidence that they applied the training in research (iv) An industrial supervisor will be nominated and they will provide a short report on the students activities Autonomous Student Learning (please specify) Assessment(s) (choose from below or add your own Type Result % of marks Timing Students must pass each task within the assignment. Pass 14 Title Credits (ECTS) Masterclass: Quantitative analysis of solidstate pharmaceuticals 5 Module Coordinator Dr Andrea Erxleben Course Instance to be announced Module Code: CH505 Please indicate if generic (GS) or specialised module Specialised. 3 Years of Chemistry at BSc level would be a minimum prerequisite. Indicative Module Descriptor: (about 150 words) The course focuses on the quantitative analysis of solid-state pharmaceuticals. The techniques covered will include IR and NIR spectroscopy, DSC and X-ray powder diffraction. Data analysis will cover the construction and use of multivariate calibration models. The analysis will focus on the determination of APIs in API excipient combinations and the quantification of polymorphic mixtures of APIs. Indicative Learning Outcomes: On successful completion of this module, students should: be able to select an appropriate analytical method be able to construct multivariate calibration models be able to assess the quality of analytical results be able to assess analytical data from published papers Workload: (specify or delete as appropriate) Class Contact Workshop (other forms of educational activity) Seminars 20 h. Supporting information supplied on-line provided (e.g. Blackboard) 10 h workshop Specified Assignment(s) 1. 2. 3. Autonomous Student Learning (please specify) write a comparative summary of the analytical techniques used build and apply a multivariate model present and discuss the results of the multivariate analysis 60 h Assessment(s) (choose from below or add your own Type Result %of marks Timi ng Students must pass each task within the assignment Pass 15 Title Problem Solving in Chemistry Credits (ECTS) 5 Module Coordinator Dr Patrick O’Leary Module Places Module Code: CH509 Elective Places Indicative Module Descriptor: In this module the students will work on preparing problems, solving problems independently and discussing solutions in problem solving seminars. . The module aims to give students the opportunity to; Broaden their knowledge to areas outside their specific research area. Gain a deeper understanding of Chemistry related to their research and outside their research area Develop problem solving skills Indicative Learning Outcomes: On successful completion of this module, students should; Have attended a series of problem solving seminars in Chemistry related topics Gained experience in Chemistry based problem solving Workload: (specify or delete as appropriate) 100 Class Contact: Attending seminars where solutions to problems are discussed. Specified Assignment(s): Setting and independently working on assigned problems in Chemistry Preparing solutions to problem sets Autonomous Student Learning 30 h (over 3 years) 60 30 Assessment(s) (choose from below or add your own) Students performance will be assessed by the supervisor (or another academic) during problem solving seminars where student will be expected to discuss/present solutions to problems in seminars where other PhD students are present. Students are expected to provide and keep records of the problems they work on during the course of their PhD study for auditing by the module coordinator.. Type % of marks Timing Year 1-3: Result Pass 16 Title Combustion Chemistry and Kinetics Credits (ECTS) 5 Module Coordinator Prof Henry Curran Course Instance To be announced Module Code: CH507 Please indicate if generic (GS) or Specialised. 3 years of at BSc and/or BE level specialised module would be a minimum prerequisite. Indicative Module Descriptor: In this module the students will attend a series of lectures on specialized topics in combustion chemistry and chemical kinetics. Students will attend a minimum of 9 lectures. This module is designed to benefit students who require specialized knowledge of specific subject areas as an adjunct to their research activities. Lectures will be selected by the student in consultation with their supervisor(s), their GRC and with the relevant programme coordinators, and module coordinators where appropriate. Assessment of the unit will be through a written assignment constituting a literature review of a field of relevance to the student’s PhD project. Assignment and assessment of this work will be undertaken by the student’s supervisor(s). The module aims to give students the opportunity to; Further their knowledge of specialized areas of combustion; Develop critical thinking skills Develop abstract writing skills Indicative Learning Outcomes: On successful completion of this module, students should; Have developed an in-depth knowledge of specialized areas of combustion; Developed their knowledge of specialized research literature relevant to their projects; Become proficient at evaluating research literature on specialized subject areas. Workload: (specify or delete as appropriate) 100 Class Contact: Lecture attendance Lectures will be provided on the following topics: 1. Basic kinetic and thermodynamic principles 2. Basic Chemical Principles I 3. Basic Chemical Principles II 4. Experimental contribution to Chemical Understanding 5. Experimental contribution to Chemical Understanding 6. Model Construction Autonomous Student Learning 9 Lectures ~100 by completion of assignments Assessment(s) (choose from below or add your own) Attendance at lectures Completion of a literature-based research project assignment Type Year 1&2: Lecture attendance Assessment of assignment Assignment and assessment of written work will be provided the student’s supervisor(s). Result % of marks Timing Students must pass each task in the assignment Pass / Fail 17 Title Process Development and Scale-Up in the Pharmaceutical Industry Credits (ECTS) 5 Module Coordinator Profs Dennis Smith/Paul Murphy Course Instance Module Code: CH510 Please indicate if generic (GS) or Specialised. 3 Years of Chemistry at BSc specialised module level would be a minimum prerequisite. Indicative Module Descriptor: (about 150 words) An introduction to the steps involved in the development and scale-up of processes for the commercial manufacture of drug substances. The focus will be on synthetic processes for “small molecule” drugs and will cover the organic, physical and analytical chemistry involved. Process selection and development, technology transfer and ongoing optimisation will be addressed with reference to the safety, environmental, engineering, quality and regulatory disciplines required. Real examples will be used to illustrate the subject. Indicative Learning Outcomes: On successful completion of this module, students should: Understand the considerations involved in designing a chemical process suitable for commercial manufacture. Appreciate the scientific disciplines involved in bringing a chemical process from laboratory to industrial scale Be familiar with the organic chemistry involved in the manufacture of some significant current drugs Be able to rationalise and discuss the mechanisms of organic reactions involved in the synthesis of drugs Workload: (specify or delete as appropriate) Class Contact Workshop (other forms of educational activity) Specified Assignment(s) Seminars 10 h. Supporting information (lecture overheads provided) 3 h workshop on assignments 1. Write a summary/abstract of one of three lectures identified from the course (e.g. hazard analysis, process validation, environmental considerations) or complete an assignment in one of these topics 2. Complete an assignment which tests understanding of essential concepts of organic synthesis 3. Present and discuss a recent publication in organic process research and development identified by the module coordinator or supervisor. Total work 30 h Autonomous Student Learning 60 h (please specify) Assessment(s) (choose from below or add your own Type Result % of marks Timing Students must pass each task within the assignment Pass 18