3.155J/6.152J Lecture 13: MEMS Lab Testing Prof. Martin A. Schmidt Massachusetts Institute of Technology 10/31/2005 Outline Review of the Process and Testing Mechanics Cantilever Fixed-Fixed Beam Second-order effects Residual stress Support compliance References Senturia, Microsystems Design, Kluwer Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 2 The Process – Lab 1 Grow 1.0µm of Si-Rich Silicon Nitride (SiNx) LPCVD Process (details to follow) Characterize (UV1280) Thickness Refractive index Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 3 The Process – Lab 1 Pattern Transfer Deposit photoresist Expose on contact aligner Plasma etch using SF6 chemistry Strip resist Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 4 The Process – Lab 2 KOH Undercut Etch 20%, 80C Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 5 The Process – Lab 3 Break the wafer into die Mount the die on a metal plate Test using the Hysitron Nanoindenter F w Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 6 Testing Cantilever Young’s Modulus Fixed-Fixed Beams Young’s Modulus Residual Stress Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 7 The Mask Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 8 The Mask - Cantilevers Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 9 The Mask – Fixed-Fixed Beams Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 10 Cantilever Data Force (m icroN ewtons) F=kx 12 10 8 6 4 2 0 0 100 200 300 400 500 600 Displacement (nanometers) Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 11 Force on a Beam Fall 2005 – M.A. Schmidt C.V. Thompson – 6.778J 3.155J/6.152J – Lecture 13 – Slide 12 Uniaxial Stress C.V. Thompson – 6.778J Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 13 Material Properties: Elastic/Plastic Figure removed for copyright reasons. C.V. Thompson – 6.778J Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 14 Material Properties: Brittle Figure removed for copyright reasons. C.V. Thompson – 6.778J Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 15 Differential Equation of Bending w(x) x dx ds z x d2w = M EI dx2 θ(x) dθ Figure by MIT OCW. H = thickness W = width I= ( ( 1 WH3 12 Reference: Senturia, S.D. Microsystems Design. Norwell, MA: Kluwer Academic Publisher, 2001. C.V. Thompson – 6.778J Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 16 POINT LOAD F MR 0 FR x L Figure by MIT OCW. Deflection of a Cantilever - 2 3L Ref: Senturia (Kluwer) C.V. Thompson – 6.778J Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 18 Deflection of a Cantilever - 3 W = width H = thickness L = length Ref: Senturia (Kluwer) C.V. Thompson – 6.778J Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 19 Deflection of a Plate - 1 ANTICLASTIC CURVATURE Given axial strain εx = z ρ ( ρ/ν ( Poission effect leads to transverse strain εy given by εy=-νεx where ν is Poisson's ratio (unitless and about 1/3 for most materials) ρ So εy = ν z ρ ( ( More important as W L (beams approach plates) Original cross-section Figure by MIT OCW. Fall 2005 – M.A. Schmidt Ref: Senturia (Kluwer) C.V. Thompson – 6.778J 3.155J/6.152J – Lecture 13 – Slide 20 Deflection of a Plate - 2 εx = σ x − νσ y E But ε y is constrained to be zero ⇒ 0 = εy = σ y − νσ x E ⇓ ⎛ E ⎞ σx = ⎜ ε 2 ⎟ x 1 −2ν4 ⎝1 4 3⎠ Replace Modulus(E) with Plate Modulus Plate Modulus Ref: Senturia (Kluwer) Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 21 Fixed-Fixed Beam Load (m icroN ewtons) 1800 1600 1400 1200 1000 800 600 400 200 0 0 500 1000 1500 2000 2500 3000 3500 Displacement (nanometers) Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 22 Fixed-Fixed Beam: Large Displacement Beam stretches under large displacement Becomes ‘stiffer’ Solved by Energy Methods c=w Ref: Senturia (Kluwer) Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 23 Residual Axial Stress in Beams Residual axial stress in a beam contributes to it bending stiffness 2ρWP0 = 2σ0WH σ0 H ⇒ P0 = Leads to the Euler beam equation ρ which is equivalent to a distributed load d 2w q0 = P0W = σ0WH 2 dx Insert as added load into beam equation : d 4w EI 4 = q + q0 dx d 4w d 2w EI 4 − σ0WH 2 = q dx dx Ref: Senturia (6.777) Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 24 Effect of stress on stiffness Figure removed for copyright reasons. Graph found in Senturia, S.D. Microsystems Design. Norwell, MA: Kluwer Academic Publisher, 2001. Ref: Senturia (6.777) Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 25 Effect of Residual Stress Not an issue in cantilevers For a point load, F, in the center of a bridge Important when Ref: Senturia (Kluwer) Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 26 Compliant Supports C.V. Thompson – 6.778J Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 27 MEMS Lab Report Report Young’s Modulus extracted from Cantilevers Fixed-Fixed Beams Explain differences from ideal theory Compare to literature values for mechanical properties Assess the effects of: Residual stress Estimate from measurements Experimental error Compliant supports Beam versus Plate Others…. Fall 2005 – M.A. Schmidt 3.155J/6.152J – Lecture 13 – Slide 28