Laboratory Practice | Cert 3 | 2012 This subject does not provide a final mark to your course. It is linked to some of the units of competence that comprise the certificate 3 qualification. These are listed as part of your enrolment / timetable package. ASSESSMENT DETAILS LABORATORY WORK HEALTH AND SAFETY (WHS) Laboratory WHS is a compulsory unit incorporated within Laboratory Practice focusing on WHS issues within the context of a science laboratory. Event 1 – Major Assignment Consists of a take home assignment covering topics relevant to safety in the laboratory. This will be due for submission on 19 June 2012. Event 2 – Laboratory WHS Quiz Closed book assessment of laboratory WHS issues covered throughout semester 1. LABORATORY PRACTICE Event 1 – Exams There will be TWO (2) practical exams and TWO (2) theory exams throughout the year, assessing important aspects of this subject. These are scheduled in the 2012 program below. Event 2 – Task Completion Students are encouraged to undertake and complete ALL programmed laboratory tasks. Your progress during each entire laboratory task will be closely monitored and recorded as competent, upon satisfactory completion of all task aspects, including: written record of prework, observations, results, calculations and task questions as they are applicable to the task. A 5 min Risk Assessment must also be completed prior to undertaking every task. Event 3 – Full Laboratory Reports A full report structure is required for completion and submission during THREE (3) compulsory laboratory tasks, as indicated on the practical timetable. See handout: Logbook / Full Report Structure for further details. 1 Assessment will be ongoing throughout the entire year. Formal assessment events are described above. Further observations of your performance in the laboratory, or supporting information will comprise aspects of your informal assessment. These will also be recorded as part of your teacher’s markbook. Informal assessment details may include, but not be limited to: Preparedness for the task (you will receive a practical timetable). Ability to follow procedures within a laboratory context with efficiency and competence. Safety awareness in the laboratory. General tidiness of your work area, during and at the end of the class. Completion and / or submission of supplementary worksheets and assignments as they are issued. NECESSARY PURCHASES Texts: 1. PRACTICAL LABORATORY SKILLS (Krajniak, Barker, Fullick) Personal Protective Equipment: 1. Safety Glasses (prescription glasses are acceptable) 2. Laboratory Coat 3. Enclosed Footwear 2 2012 PROGRAM: Laboratory Practice Certificate 3 - Ourimbah Date 7 Feb Practical Task *Library tour – 2PM (Julie Mundy-Taylor) *Admin / Intro Lab Ref. 1.1, Worksheet *Emergency procedures *Lab familiarisation / Lab map *Safety task 14 Feb 21 Feb 28 Feb 6 Mar *Meat / chems *Spills demo *Lab signs / labels 1.5, 1.2 *Techniques for separating mixtures TPC pp31-32 *Meat / chems conclude *Simulated lab hazards / Risk assessment 1.5, Worksheet *Properties and structure (investigating elements) TPC pp44-49 *Lab apparatus ID 4.1 *Physical versus chemical change TPC p29 *MSDS written exercise, 2.2 6.1, 6.2, 6.3, *Sampling and particle sizing (sieving) *Gas cylinders 5.8, DVD 13 Mar *Reading scales (i) *Balance rules *Glassware cleaning Worksheet, 5.2A, 5.10 20 Mar *Error / precision *Balance calibration 3.4, 5.2B *Properties and structure (physical properties of compounds) TPC p71 *Reading scales (ii) *Material handling intro Worksheet, 5.1 *Solubility, precipitation reactions and ionic equations TPC pp90-91 *Density (irregular solids and liquids) 7.7 *Yield experiment 1: magnesium oxide TPC p102 27 Mar 3 Apr HOLIDAY 24 Apr *Fieldwork Worksheet 1 May *pH 7.1, 7.2 8 May *Quantitative volumetric techniques 4.2, 4.3, 5.3A, 5.3B *Written task: volumetric equipment Worksheet 15 May *Sampling (coning / quartering & immiscible liquids) 6.1, 6.2, 6.3 22 May *Simple filtration techniques 5.5A 29 May *Advanced filtration techniques 5.5B 5 Jun 12 Jun *Investigation – Separation of a mixture: sand, salt & sawdust (Report) Worksheet *Solution preparation 5.4A 19 Jun *Solution preparation and quantitative serial dilution 5.4B HOLIDAY 3 17 Jul *Calibrating volumetric glassware 5.3C 24 Jul *Density & calibration (granular solids and sugar solutions) 7.7 31 Jul PRACTICAL EXAM 1 (open book) 7 Aug THEORY EXAM 1 (closed book) 14 Aug *Gravimetric analysis: Moisture content (Report) 8.1, 8.2 21 Aug *Gravimetric analysis: Ash content and TDS 8.4, 8.5 28 Aug 4 Sep *Yield experiments 2 & 3: Zinc Iodide synthesis and Gas Volumes TPC pp105-106 / pp112-113 *Gravimetric analysis: Sulfate in bore water 8.6 11 Sep 18 Sep *Gravimetric Analysis: Nickel-DMG Worksheet *Heating & cooling systems *Temp calibration 4.4, 5.7A HOLIDAY 9 Oct *Volumetric analysis: Introduction & HCl analysis Worksheet, 9.1 16 Oct 23 Oct 30 Oct 6 Nov 13 Nov * Finish 9.1 *Volumetric analysis: HCl standardisation (Report) 9.2 *Volumetric analysis: NaOH standardisation 9.3 *Volumetric analysis: Vinegar analysis 9.4 *Volumetric analysis: Washing soda / Cloudy Ammonia 9.5, Worksheet 20 Nov PRACTICAL EXAM 2 (open book) THEORY EXAM 2 (closed book) 27 Nov *Catchup HOLIDAY 4