rh Rst uDe To Our Readers: A s y o u r e a dt h r o u g ht h i s f i f t h e d i t i o no f o u r d e p a r t m e n t anl e w s l e t t e rl,' m c e r t a i n y o u ' l l a g r e et h a t f o r u s , 1 9 8 3w a s a n e x c i t i n gy e a r .I h o p e t h a t t h e p a s ty e a r E d i t o r i aAl s s i s t a n tJ:a n e B r a d l e y w a s a l s o a g o o d o n e f o r y o u . I n A u g u s t ,t h r e e n e w f a c u l t ym e m b e r s j o i n e dt h e d e p a r t m e n tD : anArmstrong, R u s sL a r s e n ,a n d B o b W a l k u p .E a c ho f t h e s en e w m e m b e r sh a s a l r e a d ym a d e i m p o r t a n tc o n t r i b u t i o n st o o u r t e a c h i n g a n d r e s e a r c hp r o g r a m s . S e a r c h e sa r e c u r r e n t l yi n p r o g r e s sf o r f a c u l t ya d d i t i o n st o t h e B i o c h e m i s t r ya n d P h y s i c aC l h e m i s t r yD i v i s i o n sT. h e f o r m e r w i l l h a v er e s e a r c he x p e r t i s ei n m o l e c u l a r b i o l o g ya n d t h e l a t t e ri n p i c o s e c o n d s p e c t r o s c o p ya n d t h e d y n a m i c so f e x t r e m e l yr a p i d r e a c t i o n sT. h e s e o p e n i n g sa r e c r e a t e db y t h e r e t i r e m e not f " M a c "M c P h e r s o n a n dt h e c o m i n g r e t i r e m e not f B a r n e yG u e r r a n td u r i n g t h e c u r r e n ta c a d e m i cy e a r .T h e e f f o r t so f t h i s d y n a m i cd u o i n t h e g e n e r a cl h e m i s t r y p r o g r a mw i l l b e d i f fi c u l t t o r e p l a c e . I n o t h e rf a c u l t yn e w s ,d e p a r t m e n t a l m e m b e r sr e c e i v e dt w o o f t h e n i n e T e x a s T e c h U n i v e r s i t yd e v e l o p m e nlte a v e sf o r 1 9 8 3 - 8 4D . a v i dK n a l f s p e n t t h e f a l l s e m e s t e ri n t h e B i o p h y s i c sD e p a r t m e n ot f t h e U n i v e r s i t oy f L e i d e ni n T h e N e t h e r l a n d sw,h i l eD i c k R e d i n g t o ni s s p e n d i n gh i s l e a v ea t t h e N S F C e n t e rf o r L a s e rS p e c t r o s c o p yo f M l T . N e w b a c h e l o r ' sd e g r e ep r o g r a m sf o r t h e D e p a r t m e not f C h e m i s t r yh a v eb e e n s u b m i t t e df o r a p p r o v a lB. e g i n n i n gi n t h e f a l l o f 1 9 8 5 .w e h o p e t o o f f e r b o t h t h e B a c h e l o ro f S c i e n c ea n d B a c h e l o ro f A r t s D e g r e e si n B i o c h e m i s t r yS. t r o n gs t u d e n t i n t e r e s ti n b i o c h e m i s t r ya n d m o l e c u l a r b i o l o g yl e d t o t h e p r o p o s e dn e w c u r r i c ul a . I n t h e a r e ao f s c i e n t i fc i n s t r u m e n t a t i o n , e made f o r i n s t r u c t i o na n d r e s e a r c hw . H e w l e t tP a c k a r d i m p o r t a n tp r o g r e s sA 5 9 9 5G C / M S h a s b e e n p u r c h a s e da n d i s i n o p e r a t i o nD. o n a t i o n so f g a s c h r o m a t o g r a p h yi n s t r u m e n t a t i o fnr o m V a r i a nl n s t r u m e n t sa n d H e w l e t tP a c k a r d a r e g r a t e f u l l ya c k n o w l e d g e d . A l t h o u g hp r o b l e m sw i l l a l w a y sr e m a i n , l ' m v e r y o p t i m i s t i cf o r t h e c o n t i n u e d d e v e l o p m e not f b o t h t h e u n d e r g r a d u a t e a n d g r a d u a t ep r o g r a m si n t h e D e p a r t m e n t of Chemistry. T H E C H E M I S T R YD E P A R T M E N TN E W S L E T T E R1 9 8 4 T e x a sT e c hU n i v e r s i t y E d i t o r :H e n r yJ . S h i n e L u b b o c kT, e x a s M6#4 R i c h a r dB a r t s c h C h a i r m a n ,D e p a r t m e not f C h e m i s t r y Prof. William Moore Craig T h i s i s s u eo f o u r N e w s l e t t e irs d e d i c a t e dt o P r o f .W . M . C r a i g w h o d i e d o n M a y 2 4 , 1 9 8 3 ,i n a n u r s i n gh o m e i n H e r e f o r d .l t i s a n a t u r a l .i f s a d . p h e n o m e n o nt h a t t h o s e o f u s w h o s t r u g g l ei n t h e p r e s e n t e n d t o l o s es i g h t o f t h o s ew h o s t r u g g l e di n t h e p a s t ,a n d o n w h o s es h o u l d e r sw e s t a n d .W . M . C r a i g l o l l e g ei n c a m e t o T e x a sT e c h n o l o g i c aC 1 9 2 6w h e n v i r t u a l l yl i t t l ee x i s t e di n t h e w a y o f h i g h e re d u c a t i o nb u t t h e s p i r i tt o b u i l d .H e r e m a i n e dw i t h t h e d e o a r t m e n t for 32years, retiring in 1958as professor e m e r i t u s .H e k e p t i n t o u c h w i t h t h e d e p a r t m e na t n d w a s a f a m i l i a rf i g u r e o n the campus for many years thereafter. W e b r i n g P r o f .C r a i g b a c k i n t c o u r m e m o r i e sf i r s t b y f e a t u r i n go n o u r c o v e r a n o f t - u n n o t i c e dp a r t o f o u r o l d , o r i g i n a l b u i l d i n gT. h e s y m b o l so f t h e p e r i o d i c t a b l ea n d o f t h e a l c h e m i c a o l a s tw e r e c u t i n t o t h e f a c e o f t h a t b u i l d i n gf r o m C r a i g ' s d e s i g n s .T h e b u i l d i n gw a s c o n s t r u c t e d d u r i n g C r a i g ' se a r l yy e a r so n t h e f a c u l t y , i n a t i m e w h e n c h e m i s t r yw a s t a u g h t ,l i k e a l l o t h e r s u b j e c t s ,i n w h a t i s n o w c a l l e d t h e A d m i n i s t r a t i obnu i l d i n g C . hemistry w a s i n i t s b a s e m e n tO . f lesser-known h i s t o r y ,t h e s a m es y m b o l sw e r e c u t f i r s t i n t o t h e f a c a d eo f a n o t h e rc h e m i s t r y b u i l d i n g ,a l s o c o n s t r u c t e dd u r i n g C r a i g ' s t e n u r eo n t h e f a c u l t y ,n a m e l yt h a t o f t h e t h e n R i c e I n s t i t u t e n, o w R i c e U n i v e r s i t y . T h e s a m ea r c h i t e c td e s i g n e db o t h b u i l d i n g sa , n d C r a i g ,t e a c h i n ga t R i c e during 1922-1925,was the consultantfor t h e f a c a d e ' sd e c o r a t i o n H . i s i n t e r e s ti n a l c h e m i c asl y m b o l sw a s d e v e l o p e dw h i l e a s t u d e n ta t H a r v a r d d , o i n g r e s e a r c hi n a t o mi c - w e i g h td e t e r mi n a t i o n s . W . M . C r a i gw a s b o r n i n t h e s m a l l c o m m u n i t yo f W e s t ( n e a rW a c o ) i n M c O l e n n a nC o u n t y ,T x . A t t h e a g e o f e i g h t h i s f a m i l y m o v e dt o G e o r g e t o w n , t h e h o m b o f a , t h e n , l e a d i n gs c h o o l i n t h e state,SouthwesternUniversity,from w h i c h C r a i g o b t a i n e dt h e B . A . ( 1 9 0 6 )a n d M . A . ( 1 9 0 7 ) .H e w a s a t t h a t t i m e t h e y o u n g e s tp e r s o nt o g r a d u a t ef r o m S o u t h w e s t e r nA. f t e r g r a d u a t i o nC r a i g t a u g h ta t H e n d r i xC o l l e g e( A r k . )f o r o n e y e a r a n d i n t h e W i c h i t aF a l l sa n d W a c o h i g h s c h o o l sf o r s i x y e a r s .I n 1 9 1 4 , w i s h i n gt o u p - d a t eh i s k n o w l e d g eo f c h e m i s t r yh e e n t e r e dU T ( A u s t i n )a n d o b t a i n e da n M . S .d e g r e ei n 1 9 1 6 .H e r e m a i n e da s a t u t o r a t U T u n t i l t h e f a l l o f 1 9 1 7e , n l i s t e di n t h e U S a r m y i n t h e s u m m e r ,1 9 1 8 ,a n d s e r v e di n a n e w l y f o u n d e dO T C c h e m i c a lw a r f a r eg r o u p u n t i l t h e s p r i n g ,1 9 1 9 .T h e f e w y e a r sa t U T w e r et o p r o v ed e c i s i v ei n C r a i g ' sa n d T T U ' s l i f e .A m o n g t h e g r o u p o f M S s t u d e n t sw i t h C r a i g a t U T w e r eW i l l i a mT . R e a da n d W i l l i a mL . R a y ,w h o w e r e t o b e c o m et h e f i r s t h e a da n d f u l l p r o f e s s o r , r e s p e c t i v e l yo,f c h e m i s t r yi n t h e i n f a n t T e x a sT e " c h n o l o g i c a Clo l l e g e .C r a i g w a s b r o u g h tt o T T C i n 1 9 2 6b y R e a d . DESIGNED, BLOWN,MANIPULATED AND DRAWNBY PROEWILLIAMM. CRAIG T E X A S T E C HU N I V E R S I T Y F R O M :T H E A T O M I CW E I G H TO F G A L L I U M T . W .R I C H A R D S A N D W .M . C R A I G ,J . A m . C h e mS , oc.,45,lt55(1923) Reproduction of figure from the 1923 JACS paper. The photograph and tettering used for this cut were made by Prof- M. Kasha, Florida State University,in 1970and presented by him to Prof. Craig. C r a i g e n t e r e dH a r v a r di n 1 9 1 9a n d b e g a nr e s e a r c hw i t h T . W . R i c h a r d so n t h e a t o m i cw e i g h to f g a l l i u m ,t h e w o r k w h i c h , i n p a r t ,w a s t o b r i n g R i c h a r d st h e N o b e l P r i z ef o r a t o m i cw e i g h t d e t e r m i n a t i o n sG. a l l i u m ,a l i t t l e - k n o w n e l e m e n tw a s o b t a i n e df r o m t h e r e s i d u e s o f l e a d r e m a i n i n gf r o m t h e d i s t i l l a t i o no f z i n c o r e n e a r B a r t l e s v i l l eO, k l a .T h e d e f i n i t i v ep a p e ro n T h e A t o m i c W e i g h to f G a l l i u mb y R i c h a r d sa n d C r a i g U A C S 4 5 , 1 1 5 5 - 1 6 7( 1 9 2 3 ) 1d,e s c r i b e sC r a i g ' s w o r k - u p o f 6 0 K g o f l e a dt o o b t a i n6 0 g o f g a l l i u m .T h e p a p e rs a y s" d u r i n gt h e e l e c t r o l y s i s( o f c r u d e g a l l i u ms a l t s )t r a c e s o f a r s i n ew e r e e v o l v e da n d m u c h o f t h e a r s e n i cr e m a i n i n gi n t h e p r e p a r a t i o nw a s e l i m i n a t e di n t h i s d i s a g r e e a b l a en d u n w h o l e s o m ef a s h i o n . "l t w a s t h i s d i s a g r e e a b l fea s h i o nw h i c h k e p t C r a i g i n a n d o u t o f h o s p i t a lf o r o n e y e a r w i t h a r s e n i cp o i s o n i n gd u r i n g h i s g r a d u a t e w o r k . C r a i g o b t a i n e dt h e P h . D .d e g r e ei n 1927 atter returningto Harvardduring 1 9 2 5 - 1 9 2a 6 n d a f t e r h i s s t u d i e sw e r e i n t e r r u p t e db y i l l n e s sa n d b y h i s t e a c h i n g , first at Rice and next at TTC. We r e p r o d u c eh e r et h e d r a w i n go f C r a i g ' s g a l l i u m - p u r i f i c a t i olni n e ,a l l o f w h i c h w a s b u i l tf r o m h i s o w n g l a s s b l o w i n g . R e s e a r c hd i d n o t c o m e e a s i l y ,a p p a r e n t l y , e v e na t H a r v a r di n t h o s e y e a r s .N o r , i n f a c t ,w a s i t a l w a y sf u n d e d ,f o r C r a i g j o u r n e y e dt o B a r t l e s v i l l teo b u y l e a d r e s i d u e sf o r h i s w o r k o u t o f h i s o w n oocket. lf researchwas difficult at Harvardhow d i f f i c u l tw a s i t t h e n o n t h e S o u t h P l a i n s ? D r . J o e D e n n i sh a s d e s c r i b e dh o w C r a i g was devotedto researchas a personal p u r s u i t ,p a y i n gf o r i t a g a i nf r o m h i s o w n f u n d s .R e s e a r c hw a s c a r r i e do u t i n a d d i t i o nt o h e a v yt e a c h i n gl o a d si n a n a l y t i c a lg, e n e r a l ,a n d p h y s i c a l chemistryb , o t h o n t h e g r a d u a t ea n d undergraudate l e v e l .C r a i g ' sp r i n c i p a l i n t e r e s tw a s i n e m i s s i o ns p e c t r o g r a p h y . A m o n g h i s M . S .d e g r e es t u d e n t sw e r e J o h n R . B r a d f o r d( 1 9 4 8 ) l, o n g - t i m eD e a n o f E n g i n e e r i n ga n d n o w V . P .f o r D e v e l o p m e nat t T T U ; G e o r g eW . D r a k e ( 1 9 3 2 ) l,a t e r ,P r o f e s s o o r f Chemistry, U n i v e r s i t yo f H o u s t o n ;H o w a r dH . ; l a r e n c eE . R a n n e f i e l d H u r m e n c e( 1 9 3 8 ) C (1940)R ; e c t o rP . R o b e r t s( 1 9 3 5 ) a; n d J o h n W . S h e e h a n( 1 9 4 0 ) . It was Prof. Craig's practiceto make a p h o t o g r a p ho f e a c h o f h i s c l a s s e s M . any o f t h e s ep h o t o g r a p h sa r e n o w o n f i l e i n t h e a r c h i v e so f T T U ' s S o u t h w e s t C o l l e c t i o nS . o m eo f t h e p h o t o g r a p h s h a n g ,s t i l l ,i n t h e s e c o n d - f l o o rh a l l w a yo f o u r o l d b u i l d i n g l.t i s o p p o r t u n et o r e p r o d u c ef r o m o n e o f t h e s et h e p h o t o g r a p ho f C . M . M c P h e r s o ni n t h i s issue. C r a i g h a s b e e nd e s c r i b e da s a p r e c i s e p e r s o nw h o f o s t e r e da n d r e q u i r e d o r e c i s i o ni n a n d f r o m h i s s t u d e n t s .H e w a s a s t a u n c ha n d l o y a lf r i e n d ,i m p a t i e n t o f s l a c k b e h a v i o ra n d i n t o l e r a n o tf d i s h o n e s t yO . u t s i d eo f h i s p r o f e s s i o n a l l i f e h e w a s ,a s a y o u n g m a n ,a p o l e v a u l t e ro f c o n s i d e r a b l es k i l l .H e l o v e dt o s i n g a n d w a s r e g u l a r l ya m e m b e ro f h i s c h u r c hc h o i r . P r o f .C r a i g r e t i r e df r o m T T C i n 1 9 5 8 , f o u r y e a r sa f t e r h e i n t e r v i e w e di n N Y C a n d a t t r a c t e dt o T e x a sT e c h y o u r h o n . e d . ,w h o h a v i n ga c c e p t e dt h e j o b , h a d t o g o t o t h e N Y C 4 2 n d S t r e e tL i b r a r yt o f i n d o u t t h e l o c a t i o no f L u b b o c k .A l l o f u s o w e t o h i m ( a n d h i s e a r l yc o - w o r k e r s )t h e u n r e p a y a b l ed e b t f o r p l a n t i n gt h e s e e d so f o u r d e p a r t m e n tT. o J o e D e n n i sw e l e a v e t h e s u m m i n gu p : " l n n o s m a l lm e a s u r eW . M . C r a i g w a s r e s p o n s i b l ef o r k e e p i n gt h e f lame of researchalive at Texas Tech in t h o s e d a y s w h e n i t f a c e dt r e m e n d o u s o d d s a n d w a s o f t e n f l i c k e r i n ga t b e s t . " ) r a i gb u i l t a P r o f .a n d M r s . ( E l i z a b e t hC h o m e o n l B t h S t . i n 1 9 2 9 ,w h e r e M r s . C r a i gl i v e ss t i l l ,a c o n t i n u i n gm e m b e ro f o u r d e p a r t m e n t af al m i l y . D r . J o h n L . K i c e h a s c o m o l e t e dh i s 3 y e a r t e r m o n t h e E x e c u t i v eC o m m i t t e e a n d G o v e r n i n gB o a r do f t h e C o u n c i lf o r C h e m i c a lR e s e a r c hI.n J a n u a r y - F e b r u a r y , 1 9 8 3 ,D r . a n d M r s . K i c e s p e n tt h r e ew e e k s i n J a p a n ,w h e r e D r . K i c e w a s a F e l l o wo f t h e J a p a nS o c i e t yf o r t h e P r o m o t i o no f S c i e n c e .I n J a p a nh e g a v ea p l e n a r y l e c t u r ea t 1 1 t hS y m p o s i u mo n O r g a n i c S u l f u ra n d P h o s p h o r u sC h e m i s t r y , T s u k u b a .H e g a v es e m i n a r sa l s o a t O s a k a C i t y , K y o t o ,T s u k u b a ,H o k k a i d o ,T o k y o M e t r o p o l i t a nT, o k y o ,a n d K e i o U n i v e r s i t i e sa,n d t h e G i f u C o l l e g eo f P h a r m a c yA . s e l f - t r a i n e dc o m p u t e r p r o g r a m m e rD , r . K i c e i s a l s oa s s i s t i n g l e s s e rm o r t a l s( n a m e l y y, o u r h o n . e d . ) i n i n t e r f a c i n go u r n e w m a s ss p e c t r o m e t e r Dr. RobertD. Feltham(facingcamerc)and f o r h i g h - s p e e dd i s c d r i v ed a t a h a n d l i n g DeanLawrenceGraves(nowrctired)at the capability. receptionfor Dr. Feltham,March7, 1983. D r . D a v i dK n a f f s p e n t p a r t o f t h e s u m m e ra n d a l l o f t h e f a l l s e m e s t e ri n n e t w o r kp r o m o t i o n so f s c i e n c e .H e H o l l a n da s a V i s i t i n gP r o f e s s o o rf a p p e a r e di n a 3 0 - m i n u t eT V m o v i ef o r t h e B i o p h y s i c sa t t h e S t a t eU n i v e r s i t yo f A C S " C h e m i s t r yt,h e E n d l e s sF r o n t i e r " , L e i d e n .D r . K n a f fw a s o n s a b b a t i c al e a v e , w h i c h w a s r e l e a s e di n O c t o b e r1 9 8 3 .T h e A C S r a d i os h o w " T h e C h e m i s t r yo f C l e a n c a l l e dh e r ed e v e l o p m e nlte a v e ,f r o m T T U . W h i l eo n l e a v eD r . K n a f f p r e s e n t e dp a p e r s C l o t h e s "f e a t u r i n gD r . A r m s t r o n gw a s a t t h e 6 t h I n t e r n a t i o n aPl h o t o s y n t h e s i s r e l e a s e dn a t i o n w i d eo n a r e g u l a rs e r i e s C o n g r e s si n B r u s s e l s( A u g u s t1 ) , a n d a t c a l l e d" D i m e n s i o n si n S c i e n c e " A . oart s eeting f r o m t h e s ea c t i v i t i e sa n d h i s t e a c h i n ga n d t h e a n n u a lD u t c h B i o e n e r g e t i c M i n L u n t e r e n( N o v e m b e r1 7 ) .H e g a v e r e s e a r c hs u p e r v i s i o nD r . A r m s t r o n gk e p t r e s e a r c hs e m i n a r si n H o l l a n d( L e i d e n , h i m s e l fo c c u p i e db y c o n s u l t i n gf o r G r o n i n g e na, n d W a g e n i n g e n G ),ermany W h a t m a nC o r p . ,N . J . ,A d v a n c e d ( M a r b u r gK , o n s t a n za, n d B o c h u m ) , S e p a r a t i o nT e c h n o l o g i e sN , . J . ,a n d T h e Faculty News B r u n s w i c kC o r p o r a t i o n D , e f e n s eD i v i s i o n , S w i t z e r l a n d( Z r i r i c h a n d N e u c h d t e l ) ,l t a l y ( B o l o g n a )a , n d F r a n c e( P a r i s ) a , ll of Marian, VA. Frq4_lheqe inqlqslrial_ D r . J o e A . A d a m c i kh a s b e e ne l e c t e dt o w h i c h r e p r e s e n t a m i g h t y i n t e r e s t i n gi o t c o m p a n i e s h e h a s r e c e i v e d unrestricted a n o t h e r3 - y e a rt e r m o n t h e B o a r do f of develooment. f u n d i n g ( $ 3 0 0 0 f) o r r e s e a r c hi n D i r e c t o r so f t h e A m e r i c a nC h e m i c a l D r . R i c h a r dL . R e d i n g t o nw a s a l s o chromatography. S o c i e t y .D r . A d a m c i ks e r v e sa s a w a r d e da d e v e l o m e n t al le a v ea n d s p e n t C h a i r m a no f t h e B o a r dC o m m i t t e eo n D r . R i c h a r dA . B a r t s c hp r e s e n t e da i t d o i n g r e s e a r c hw i t h P r o f .R o b e r tF i e l d P r o f e s s i o n aal n d M e m b e rR e l a t i o n sa, n d p a p e r" S o l v e n tE x t r a c t i o no f M e t a ll o n s a t M l T . T h e r e ,D r . R e d i n g t o ns t u d i e dl a s e r a s a m e m b e ro f t h e S o c i e t yC o m m i t t e eo n b y l o n i z a b l eC r o w n E t h e r s "a t t h e 1 9 8 3 s p e c t r o s c o p yo f h i g h - e n e r g yv i b r a t i o n C h e m i c a lA b s t r a c t sS e r v i c e B . o a r dd u t i e s I n t e r n a t i o n aSl o l v e n tE x t r a c t i o n r o t a t i o nt r a n s i t i o n si n t h e g r o u n d t o o k h i m t o W a s h i n g t o nD, . C . ,i n C o n f e r e n c eD , e n v e r ,C o l o . ( A u g u s t ) .H e p r e s e n t e da l s o a n i n v i t e dp l e n a r yl e c t u r e S e p t e m b e ra n d D e c e m b e r 1 , 9 8 3 .I n " C o m p l e x a t i o no f A l k a l i M e t a la n d D e c e m b e rh e w a s e l e c t e dt o t h e E x e c u t i v eC o m m i t t e eo f t h e B o a r d .D r . Alkaline-Earth C a t i o n sb y L i p o p h i l i c A d a m c i ki s a l s o h a r d a t w o r k d e v i s i n g l o n i z a b l eP o l y e t h e r sa" t t h e 7 t h c o m p u t e ra s s i s t e di n s t r u c t i o nf o r h i s S y m p o s i u mo n M a c r o c y c l i cC o m p o u n d s , crasses. P r o v o ,U t a h ( A u g u s t ,1 9 8 3 ) . D r . J o h n A . A n d e r s o np r e s e n t e da D r . " S a n d y "D a s g u p t ah a s r e c e n t l y p a p e r" C o n v e r s i o no f E l y m o c l a v i n e to demonstratedthe superior mass-transfer P a s p a l i cA c i d b y a P a r t i c u l a t eF r a c t i o n e f fi c i e n c yo f a n n u l a rf l o w s y s t e m s , f r o m a n E r g o t a m i n e - p r o d u c i nSgt r a i no f e s p e c i a l l yw h e n t h e f l o w i s h e l i c a l .T h i s i s Clavicepssp." at the FABS meeting,San r e g a r d e da s o f f u n d a m e n t ailm p o r t a n c e F r a n c i s c oJ. u n e . 1 9 8 3 . b y c o l l e a g u e si n t h e f i e l d .T h e a p p l i c a t i o n o f t h i s c o n c e p tt o w a r d a c o n t i n u o u s l y D r . D a n i e lW . A r m s t r o n gp r e s e n t e d g e n e r a t e di o n - e x c h a n g e rc,o m p r i s e do f p a p e r so n h i s r e s e a r c ha t t h e P i t t s b u r g h a n a n n u l a rh e l i x m a d ef r o m a n i o n C o n f e r e n c eo n A n a l y t i c a C l hemistry, e x c h a n g e rm e m b r a n et u b e w i l l b e A t l a n t i cC i t y , N . J . ( M a r c h1 9 8 3 ) ,t h e publishedin Analytical Chemistryin 1984. N a t i o n a lA C S m e e t i n g ,S e a t t l e W , ash. ( M a r c h1 9 8 3 ) ,t h e E a s t e r nA n a l y t i c a l Dr. Robert A. Holwerda presenteda SymposiumN , e w Y o r k , N . Y .( N o v . ,1 9 8 3 ) , p a p e r" S p e c t r o s c o p i cE, l e c t r o c h e m i c a l , a n d t h e U S A / B r a z iS l y m p o s i u mo n a n d R e a c t i v i t yS t u d i e so f T y p e 2 C o p p e r M i c e l l e sV , e s i c l e sa, n d M i c r o e m u l s i o n s , DepletedLaccase"at the NationalACS C a m p i n a s ,B r a z i l( A u g u s t ,1 9 8 3 ) .I n 1 9 8 3 M e e t i n g ,W a s h i n g t o nD , . C . ,S e p t e m b e r , h e g a v es e m i n a r sa l s o a t B o s t o n ,R u t g e r s , 1 9 8 3 .D r . H o l w e r d aa n d g r a d u a t es t u d e n t , V i r g i n i aC o m m o n w e a l t ha, n d E a s tT e x a s R a n d yJ o h n s o n ,h a v er e c e n t l yc o m p l e t e d S t a t eU n i v e r s i t i e sa,n d t h e F o o d a n d D r u g t h e i n t e r f a c i n go f t h e i r s t o p p e d -lfo w a n d Mr. Michael Campbell, Banquet awards, April A d m i n i s t r a t i o nW , a s h i n g t o nD , . C .D r . Lambda-5UV-VlSspectrometerswith 28.1983. A r m s t r o n gh a s a l s o b e e n i n v o l v e di n Applell Computers. e l e c t r o n i cs t a t eo f m o l e c u l e su, s i n gt h e s t i m u l a t e de m i s s i o np u m p i n g( S E P ) m e t h o d .T h e m e t h o di s b a s e do n t h e u s e o f t w o t u n a b l ed i e l a s e r s . Dr. Robert W. Shaw has been electedto a s s o c i a t em e m b e r s h i pi n t h e A m e r i c a n l hemists. S o c i e t yo f B i o l o g i c a C D r . H e n r y J . S h i n ea n d M r s .S h i n ew e r e i n P o l a n da n d E n g l a n d( w h e r ee l s e ? ) d u r i n g S e p t e m b e r1, 9 8 3 .I n P o l a n dS h i n e , roclaw, v i s i t e dt h e T e c h n i c a lU n i v e r s i t yW and the Universityof Katowice,from w h i c h c a m e t h e l a r g ep r o p o r t i o no f P o l i s h post-doctoralfellows in our department, I n E n g l a n dS h i n ea t t e n d e dt h e 3 r d E u r o p e a nS y m p o s i u mo n O r g a n i c C h e m i s t r y( E S O C - I l l )h e l d i n t h e Universityof Canterbury,and presenteda paper on "Electron Transfer Reactions betweenAzoalkanesand Th ianthrene C a t i o nR a d i c a l . "D r . S h i n ew a s e l e c t e dt o m e m b e r s h i pi n t h e F a c u l t yS e n a t e t, h e w i s d o mo f w h i c h ( h i s e l e c t i o n ,n o t t h e . hine S e n a t e )h e s o m e t i m e sq u e s t i o n sS w a s a l s o a p p o i n t e dt o m e m b e r s h i po n t h e College of Arts and SciencesResearch Council. D r . P i l lS o o n S o n g h a sb e e n reappointedfor his fourth term (1984-87) as editor-in-chiefof Photochemistryand Photobiology.He was an invitedspeaker a t t h e I n t e r n a t i o n aCl o n f e r e n c eo n P h o t o c h e m i s t r ay n d P h o t o b i o l o g y , A l e x a n d r i aE , g y p t ,i n J a n u a r y ,1 9 8 3 ,a n d a t t h e I n t e r n a t i o n aSl y m p o s i u mo n B l u e Light Effects,Marburg,Germany in July, 'l 1 9 8 3 .D u r i n g 9 8 3 h e a l s o g a v es e m i n a r s o n p h y t o c h r o m ea t J o h n s H o p k i n s U n i v e r s i t ya n d f o u r " C h e v r o nL e c t u r e s " y t t h e U n i v e r s i t yo f on photochemistra Nevada. D r . W a y n eS m i t h l e f t t h e d e p a r t m e n at t t h e e n d o f t h e s u m m e r ,1 9 8 3 ,a n d i s n o w on the researchstaff at Los Alamos N a t i o n a lL a b . Dr. Roy E Mitchell, Banquet speaker,APril 28, 1983. Energy-ConservationRenovalions The extensiverenovations(one m e g a b u c kp l u s )d e s c r i b e di n Newsletter4 are just about complete. Some bugs are yet to be worked out, such as the need to wear sweaters and scarves(no gloves)in the b u i l d i n gw h e n o u t s i d et e m p e r a t u r e s plummetedjust beforeChristmas. Come to think of it, that u/asenergy conservation.lf we do not reporton the renovationsin Newsletter6 you may regardthat as (a) a sign of a d e l i c a t es i t u a t i o n (, b ) t h e b a n i s h m e n t of hon. ed. or, maybe (c) that all is well. With bated,if frigid, breathwe wait to see. News of Faculty Emeritus The two "senior" membersof emeritusprofessorscontinuein their wonderfullyproductivehabit.Welch ProfessoremeritusCharlesShoppee works at the bench in his lab at LaTrobeUniversity,Melbourne, Australiawhere,taking uP the c h a l l e n g eo f a p r o b l e mb e g u nm a n Y yearsago he has finally synthesized the lactoneof gammaacid, and hydroxyperbromofumaric shown that it is also formed by photochemicaloxidationof tetrabromofuran.By the time this newsletterreachesits lucky public ProfessorShoppee's80th birthday (February24, 1984)will havearrived. We tip our hats in fond salute. Shoppeehas not retiredcompletely to the laboratory,though. In the early F a l l 1 9 8 3h e t o o k o f f f o r m a i n l a n d China and has written of his gustatoryexperiencestherein,during a three-weektour. From closerto home in AlbuquerqueProf. Morris Stubbs writesof his giving his 88th talk on s c i e n c ea n d e n e r g ys i n c eh i s retirement.But, the retirementhe meansis from the Universityof Albuquerqueto which he went after retiringfrom TTU to which he came after retiringfrom the School of Minesof Socorro.Vivat Morris!Vivat Charles! Here,at home, ProfessorsJoe Dennisand MargretStuart rejointhe departmentalfamily occasionally, most recentlyat the farewellbash for Mac McPherson. Mass Spectrometer(At Last) We are happy to report that after long and painfulyearsof gestation the departmentwas deliveredof a new massspectrometerin December, 1983.Fundsapproximating$100,000 were providedby TTU for the purchaseof a Hewlett-Packard quadrupoleinstrument,model 59958, with an HP computer upgradedby a Winchesterhard-discdrive.The departmentexpressesits gratitudeto DeanWilliamConroy,Vice President for ResearchJ. Knox Jones,and AcademicVice PresidentJohn R. D a r l i n gf o r t h i s h a n d s o m ef i n a n c i a l backing.The HP 59958 is a routine massspectrometerbut is capableof G C / M S ,C h e m i c a l o n i z a t i o n( C l l M S ) , S e l e c t e dl o n M o n i t o r i n g( S l M )a n d Direct InsertionProbe Mass Spectrometry(DlP/El).The new i n s t r u m e nbt r i n g sm u c h r e l i e ft o t h e strainon the department.Yet, it is o n l y a b e g i n n i n ga, n d d o e s n o t b e a r comparisonwith facilitiesavailablein our sisterinstitutionsin Texas.In that regardwe have many a long mile yet to go. Welch Foundation News Two Welch Foundationlectures w e r eg i v e ni n 1 9 8 3 .O n M a r c h7 , P r o f. RobertD. Feltham,UniversitYof Arizona(seecut) sPokeon "Structure,Bonding,ReactivitY Relationshipsin Metal NitrosYl Compfexes".On October2O,Prol. Colin Eaborn,UniversitYof Sussex, Englandspoke on "Novel O r g a n o s i lc o n C o m p o u n d sa n d Reactions." Scholarshipsand Awards to UndergraduateStudents,1983 T h e S a m u e lH u n t L e e M e m o r i a l Award (to an outstandingfreshman c h e m i s t r ym a j o r ) ,V i c t o rA k i n . T h e C R C P r e s s ,l n c . 3 5 t hA n n u a l FreshmanChemistryAchievement Award, (to an outstandingstudentin freshmanchemistry),RobertColla. A m e r i c a nC h e m i c a S l o c i e t yS t u d e n t A f f i l i a t eS c h o l a r s h i p( t o a n o u t s t a n d i n gs o p h o m o r ec h e m i s t r y s t u d e n t )S , t e p h e nH a l l . The Analytical Chemisfry Award (to t h e b e s tj u n i o r c h e m i s t r ym a j o ri n analyticalchemistry),Tracey Price. The Texas Instituteof the American Instituteof Chemists,StudentAward ( f o r o u t s t a n d i n ga c c o m p l i s h m e ni n t a program in chemistry baccalaureate or chemicae l n g i n e e r i n ga, n d potentialas a professionalchemist), StephenStults. The Merck lndex Award (for o u t s t a n d i n ga c h i e v e m e nbt y a g r a d u a t i n gs e n i o r ) ,L y n d r aB i l l s . TheWeymouth-Campbell S c h o l a r s h i p sf o: r s u p e r i o r performance(as a freshman c h e m i s t r ym a j o r ) ,V i c t o rA k i n ,J e r r y M c L a u g h l i nJ, o n a t h a nM e t z l e r( a sa s o p h o m o r ec h e m i s t r ym a j o r ) ,Q u i n n B l i g h ,S t e p h e nH a l l ,S u s a nJ a c k ( a sa j u n i o r c h e m i s t r ym a j o r ) ,G e n e McDonaldK , a r e nM i k k e l s o n . Teaching AssistantAwards lo GraduateStudents TexasTech UniversityOutstanding GraduateStudentTeacherAward: JesseYeh. Departmentof ChemistryAward for SuperiorPerformanceas a Teaching Assistant: David Babb C l i n t o nA n d e r s o n W David Babb and Clinton Anderson receive outstanding TA awards f rom Dr. Bartsch,April 28, 1983. Scholarship and Prize Awardees,April 28, 1983.Front: Lyndra Bills, StephenStu/ts, Jesse Yeh,' Middle: StephenHally, David Babb, Clinton Anderson; Top: Victor Akin, Robert Golla. ScholarshipAwards to Graduate Students The Weymouth-Campbell Scholarships: J a m e sS m i t h Weymouth-CampbellScho/ars 1983-1984with Mike Campbell. L to R: Karen Mikkelson, Jerry McLaughlin, Victor Aikin, Stephen Hall, SusanJack, Quinn Bligh, and Gene McDonald. Weymouth-Campbell scholars 1982-1983with Mike Campbell L to F.'Stephen Stults, David Womack, Lyndra Bills, Floyd Barry and Ricky Matos. Graduate Degrees1983 J o h n D . C l e m m e rl,l l , M . S .( D r . Holwerda). Alan P. Croft, Ph.D.(Dr. Bartsch),"A MechanisticStudy of Complex BaseReactions.': Promoted1,2-Elimination , h . D .( D r . M a r x ) , R o n a l dl - 1E . r i c k s o nP "Approachesto the Synthesisof Gnididone." T a e - R y o n gH a h n ,P h . D .( D r .S o n g ) , "MolecularDifferencesBetweenthe PhysiologicallyActive (Pfr) and Inactive(Pr) Formsof Phytochrome." G w i - S u kH e o ,P h . D .( D r . B a r t s c h ) , "Synthesisof FunctionalizedCrown Ethersand Cation ComplexationbY Crown Ethers." H o o n H w a n g ,M . S .( D r . D a s g u P t a ) , "Microdetermination of Sulfatein EnvironmentalSamples." S a n l h n K a n g ,P h . D .( D r . B a r t s c h ) , "lonizableCrown Ethersfor the S e p a r a t i o no f A l k a l ia n d A l k a l i n e Earth Cations.Synthesisand Applications." Y o u n g H e e K i m K a n g ,M . S .( D r . Kice),"Studiesof the Chemistryof Selenosulfonates." l l - K y u nK i m , M . S .( D r . S o n g ) , "FurtherCharacterization of PhotosensoryTransductionin Stentorcoeruleus." S o u - U nK i m , P h . D .( D r .A n d e r s o n ) , "ln vivo Metabolismof Agroclavine and Elymoclavinein ClavicepsSp." Y u n g L i u , P h . D .( D r . B a r t s c h ) , " s y n t h e s i sa n d A p p l i c a t i o n so f Functionalized Crown Ethers." T h o m a sH . L y s t e r ,M . S .( D e c .1 9 8 2 ) ( D r . S m i t h ) ," T h e E l e c t r o c h e m i c a l S y n t h e s i so f O r g a n o m e t a l l iN c ickel C o m p o u n d sw i t h C h e m i c a l Applications." K o o n H a P a r k ,P h . D .( D r .S h i n e ) , "Heavy-atomKinetic-lsotopeEffects i n S o l v i n gM e c h a n i s m o sf Benzidine Rearrangements.Hydrazobenzene and 2,2'-Dimethoxyhydrazobenzene." H e r m a n t aK . S a r k a r ,P h . D .( D r . Song),"HydrodynamicProperties and MolecularTopographyof Phytochrome." R i c h a r dM . W y n n ,M . S .( D r . K n a f f ) , " B i o c h e m i c aM l o d i fi c a t i o na n d ReactivityStudiesof the MetalloenzymeLaccase." Chemistry Department/American Chemical Society Annual Awards Banquet The Departmentand the South P l a i n sS e c t i o no f t h e A C S j o i n e di n , p r i l 2 8 ,1 9 8 3 . t h e i ra n n u a lb a n q u e t A The banquetspeaker,Dr. RoYE. Mitchell(seecut) regaledthe crowd with a descriptionof his researchin n iththe w i n e m a k i n gi n c o l l a b o r a t i o w experimentalvineyardsof the Universityof Texaswhich are now d o t t i n gt h e o i l l a n d so f t h e P e r m i a n B a s i n .U T i s p l a n n i n gf o r t h e d a Y w h e n o i l r u n sd r y , i t s e e m s . The banquetservedfor awardsof prizesand scholarshipsand also to introducethe faculty and studentsto , h o c a m et o M r . M i c h a e lC a m p b e l lw year's the to award Lubbock W e y m o u t h - C a m p bIeslc h o l a r s h i p s . UndergraduateDegrees1983 R o b e r tH . B e h a l ,B . A . L y n d r aJ . B i l l s ,B . S . C a r o l lA . B u r k e ,B . A . L i s aL . B u r n s ,B . S . RobertD. Chan_ce, B.A. E r i cJ . C o l l , B . A . R o b i nL . C o o p e r ,B . S . StevenS. Gates,B.A. L e eA n n e H a l t o m .B . A . , .A. M i c h a e lP . H a n n u s c h B Jose R. Matos.B.S. M a r i t aA . M e r c u r i o B , .S. D a v i dM . M o r r i s ,B . A . J a m e sL . M y e r s ,B . S . Jon L. Pearce,B.A. SherylA. Presnal,B.A. DavidC. Riojas,B.A. James F. Ryder,B.A. LeonardB. Sommitz,B.A. S t e p h e nD . S t u l t s ,B . S . R o b M . T s c h a u n e rB , .S. D a v i dS . W o m a c k ,B . S . Moreon NewFaculty Dr. Robert D. Walkup,organic chemistry. Dr. Daniel W. Armstrong, analytical chemistry, works the balance while grad student, Larry Spino,watches. In our last Newsletterwe reported t h a t t h r e en e w a p p o i n t m e n t h sad been made to our faculty.Drs. Dan A r m s t r o n gR , u s s e l Ll a r s e n a, n d R o b e r tW a l k u pj o i n e du s i n t h e F a l l , 1 9 8 3 .W e c a n n o w s h o w y o u t h e i r p l e a s a n pt h y s i o g n o m i easn d t e l l y o u a l i t t l em o r ea b o u tt h e m . D a n A r m s t r o n gw a s b o r n i n F o r t W a y n e ,I n d i a n ai n 1 9 4 9 .H e r e c e i v e d t h e B . S .d e g r e ei n I n t e r d e p a r t m e n t a l S c i e n c ea n d M a t hf r o m W a s h i n g t o n a n d L e e U n i v e r s i t yi n 1 9 7 2 t, h e M . S . i n C h e m i c aO l c e a n o g r a p h y1,9 7 4 , a n d P h . D .i n C h e m i s t r y , 1 9 7 t7r ,o m TexasA&M. He stayedat TAMU for postdoctoralresearchu ntil S e p t e m b e1 r 9 7 8 ,a n d t h e n h e l d assistantprofessorsh i ps at Bowdoin (1978-79)and Georgetown U n i v e r s i t i e(s1 9 8 0 - 8 3 )w, h e n h e j o i n e do u r d e p a r t m e nat s A s s o c i a t e Professorof AnalyticalChemistry. His researchinterestsare in chromatographic separations,phase transfercatalysis,surfactants,and p s e u d o p h a s lei q u i dc h r o m a t o g r a p h y . D a n h a s a b o u t4 0 o u b l i c a t i o n isn thesefieldsand has given over 50 l e c t u r e sa n d s e m i n a r so n t h e s et o p i c s i n u n i v e r s i t i easn d i n d u s t r i a l l a b o r a t o r i eisn t h e U S A a n d a b r o a d . Dan and Linda Armstronghavetwo s o n s ,L i n c o l nT h o m a s( 8 ) a n d R o s s Alexander(6). Dr. RussellD. Larsen,coordinator of genetal chemistrv. B o b W a l k u pw a s b o r n i n A s h e v i l l e , RussellLarsenwas born in N . C .i n 1 9 5 2 .H e r e c e i v e dt h e B . S . M u s k e g o nM , i c h i g a ni n 1 9 3 6 .H e d e g r e ew i t h h o n o r si n c h e m i s t r yf r o m receivedthe B.A. degreefrom the Universityof Delawarein 1974, KalamazooCollegein 1956,and the a n d t h e P h . D .f r o m S t a n f o r di n 1 9 8 1 . P h . D .f r o m K e n t S t a t eU n i v e r s i t yi n After a postdoctoralfellowshipwith 1964.Russellwas a postdoctoral Al Meyersat ColoradoState fellow at Princeton(1964-65)and U n i v e r s i t y( 1 9 8 1 - 8 3h) e j o i n e do u r R i c eU n i v e r s i t y( 1 9 6 5 - 6 6 )H. e h e l d departmentas an assistantprofessor assistantshipprofessorshi ps at i n o r g a n i cc h e m i s t r yB . o b ' sr e s e a r c h l l l i n o i sI n s t i t u t eo f T e c h n o l o g y( 1 9 6 6 interestsare in syntheiic72) and TAlviU (1572-76),associate professorships m e t h o d o l o g ya n d t o t a ls y n t h e s e si n at the Universityof o r g a n i cc h e m i s t r ya n d a l s o i n N e v a d aD , a r t m o u t hC o l l e g e a , ndthe b i o c h e m i c aal d a p t a t i o n o sf marine U n i v e r s i t yo f M i c h i g a nu n t i lt h e F a l l , o r g a n i s m sD . u r i n gt h e s u m m e r ,1 9 8 0 , 1 9 8 3 ,w h e n h e j o i n e dT T U a s t h e h e w a s a v i s i t i n gi n s t r u c t o ri n t h e C o o r d i n a t oor f G e n e r a C l hemistry. lattersubjectat the UT Marine His researchinterestsare in signal Laboratory,Port Aransas,TX. Bob p r o c e s s i n ga n d d a t aa n a l y s i sW , alsh and DeborahWalkup havetwo sons: f u n c t i o n s s, p li n e p r e s e n t a t i o n s , C a r l o sK e a t i n g( 3 ) a n d J o s h u aL a m b m a x i m u m - e n t r o payn a l y s i sa, n d (1) c h e m o m e t r i c sa,n d ,o f c o u r s e , chemicae l d u c a t i o nH . e has p u b l i s h e d2 4 p a p e r si n t h e s ef i e l d s . R u s s e l hl a s a l s o c o n s u m i n gi n t e r e s t s i n a i r s h i p sa n d i s a m e m b e ro f t h e Sons of the Desert,an association d e v o t e dt o m e m o r a b i l i a of theoldtime moviegreats,Laureland Hardy. R u s s e lw l o u l d l i k e t o e s t a b l i s ha chapter(calleda "tent") of Sons of t h e D e s e r ti n L u b b o c k .C o u n t m e i n R u s s .H e a n d J u a n i t aL a r s e nh a v e t w o c h i l d r e n :E r i k ( 1 8 )a n d S u s a n (14) News of Alums C l i n t o nA n d e r s o n( M . S . ' 8 3 )h a s accepteda positionwith Safeway Corp. Dr. Dong Hak Bae(Ph.D.'82) returnedto TexasTech in January 1983for post-doctoralresearchwith D r . S h i n e .D u r i n g1 9 8 2D r . B a ew a s a post-doctoralfellow with Dr. E. C. Ashby at GeorgiaTech. At TTU Bae is doing researchin electron-transfer reactionsand assistingin the supervisionof graduatestudentsin the group. The Baesreturnedto L u b b o c kj u s t i n t i m e t o b r i n ga n o t h e r Texas residentinto the world: MarianneBae,to keep brotherLeon company. C a p t .R i c h a r dG . C a r m i c h a e(l M . S . '76) has returnedfrom overseas a s s i g n m e nitn W i e s b a d e nG, e r m a n y , a n d i s n o w a t F i t z s i m m o nA srmy MedicalCenter,Departmentof Pathology,Aurora,Colo. D r . M i c h a e lM . C h a u ( p o s td o c w i t h Dr. Kice '76-'77)has been named ResearchAssociateat the Pittsburgh PlateGlassCoatingsand Resin D i v i s i o nA , l l i s o nP a r k ,P A . D r . C h a u j o i n e dP P G i n 1 9 7 7 .H i s c o n t r i b u t i o n s in their pioneerpolymerresearch department,particularlyin the area of waterbornepolyurethanetechnology, haveled to the promotionto his new p o s i t i o nC . o n g r a t u l a t i o nM s ike! D r . A l a n P . C r o f t ( P h . D . ' 8 3 )i s e m p l o y e db y D o w C h e m i c a C l o., Freeport,TX. D r . T a e R y o n gH a h n ( P h . D . ' 8 3 )i s now a post-doctoralfellow at Yale University. RoseanneWoo Haltresht(8.S. '77) is continuingto do marketresearch w i t h D i a m o n dS h a m r o c k b . ut in a j o i n t v e n t u r ew i t h a S w i s sf i r m , createdin some reorganizationin D i a m o n dS h a m r o c k R . osean e's w o r k n o w e m p h a s i z eas c q u i s i t i o n analysesratherthan R and D p r o g r a m s I. n t h e e v e n i n g ss h e i s a graduatestudentat CaseWestern Reservestudyingoperations research,preparingher for strategic planning.The corporateworld has thus taken Roseannea long way from basicchemistry,but that's not an uncommonexperiencenowadays. HusbandMicahelHaltreshtis a databaseadministratorfor a Cleveland. O H . ,c o n s u l t i n gf i r m . Thanksgivingluncheon, November 21. Graduate sfudents Andrea Cobb (biochemistry) and Maria Garcia (inoryanic). Thanksgivingluncheon. Former editorial asslstantSharon Grant, now secrctary to attorneys Bass and Hobbs, Lubbock, joined us for lunch. Dr. and Mrs. Bartsch and Dr. Dan Armstrong, at the Thanksgivingluncheon. D r . W i i l i a mR . H e i n e m a n( B . S . ' 6 4 ; P h . D . ,U . N . C a r o l i n a ' 6 8 r) e t u r n e dt o the departmenton December7 to v i s i ta n d g i v ea s e m i n a ro n h i s research.Bill is Professorof Chemistryat the Universityof rf C i n c i n n a t iH . i s f a t h e r ,p r o f e s s o o mathematicsemeritusof TTU, and m o t h e rs t i l l m a k et h e i r h o m e i n Lubbock. D r . G w i S u k H e o ( P h . D .' 8 3 ) i s a post-doctoralfellow with Prof.J. Keana,Universityof Oregon. J o h n R . " B o b b y "H u d g i n s( B . A . ' 7 8 ) is a senior medicalstudentat UT Galvestonwith graduationset for M a y , 1 9 8 4 .D u r i n g1 9 7 8 - 8 0h e w o r k e d a s a n e n v i r o n m e n t aclh e m i s tf o r t h e Texas Departmentof Water R e s o u r c e si n A u s t i n . D r . S a n gl h n K a n g( P h . D . ' 8 3 ) remainsat TTU for post-doctoral researchwith Prof. Kice. D r . l l - H y u nK i m ( M . S .' 8 3 ) i s a n assistantprofessorat the Korea MilitaryAcademy,Seoul,Korea. D r . S o o - U nK i m ( P h . D .' 8 3 )i s n o w a postdoctoralfellow with H. G. Floss i n t h e C h e m i s t r yD e p a r t m e n tO, h i o StateUniversity. Cathy WilhiteLester(B.S.'69; M.S. T A M U ' 7 4 i n h o r t i c u l t u r ei)s a T e c h n i c i a nl l ( p a r t - t i m ei)n t h e B i g S p r i n g ,T X , f i e l d s t a t i o n w , o r k i n gi n wind erosion.After leavingTTU and beforeenteringTAMU Cathy worked f o r C o s d e nO i l a n d C h e m i c a C l o. in Big Spring.The TAMU experienceled to work as a grower-propagator of foliageplantsand woody o r n a m e n t a l sC. a t h ym a r r i e di n 1 9 7 6 a n d i s s e t t l e di n B i g S p r i n g . D r . Y u n g L i u ( P h . D .' 8 3 ) i s w o r k i n g with the Water ResourcesCenterat TTU as a researchchemist. H a r v e yM a l l o r y ,l l l , ( 8 . S . ' 6 0 ,M . S . '61) came back to Texasfrom Delawarebeieflyin 1983to help son, H a r v e yl V , e n r o l li n U T A u s t i n ,w h e r e he has been awardedan Engineering FoundationsScholarshipfor studies i n A e r o s p a c eE n g i n e e r i n gH. a r v e yl l l , i s w i t h t h e i n d u s t r i afli b e r sd i v i s i o no f l arketing d u P o n td o i n gt e c h n i c a m w i t h t h e i r K e v l a ra r a m i df i b e r .T h i s work givesample opportunityfor travel,but so far the marketin Lubbockfor Kevlarhasn'tbrought H M l l l , o u r w a y . D o n ' tw a i t u n t i l w e who-where-here-when are retired beforedropping in to see us. C h r i s t o p h eR r . M a n n ( 8 . A . ' 8 2 )i s now in his secondyear at the Texas Collegeof OsteopathicMedicine, Fort Worth. D r . K o o n - H aP a r k ( P h . D .' 8 3 )i s a postdoctoralfellow with Dr. Marye AnneFoxat UT Austin. D r . A l a n R . P u l s( 8 . A . ' 7 6 )f i n i s h e d hisinternam l e d i c i n er e s i d e n c yi n O k l a h o m aC i t y i n J u n e 1 9 8 3 a , nd begana cardiologyresidencyin July, 1983. D r . H e m a n t aK . S a r k a r( P h . D . ' 8 3 )i s a post-doctoralfellow at the Roche I n s t i t u t eo f M o l e c u l a rB i o l o g y ,N u t l e y , N.J. Dr. K. Jane Scott (8.S. '77) has establishedmedicalgeneralpractice in DenverCity, Texas. D r . J u a n i t a" N i t a " S i l b e r( P h . D . ' 7 2 ) has writtenfrom the Universidad Nacionalde Rio Cuarto,where she is Professorand Chair of the Chemistry Department.Nita is very activein teachingand research,the latter coveringorganoelectrochemistry of a m i n e si n n o n - a q u e o u s o l v e n t sa, n d complexesbetweenaminesand aromaticacceptors.We, at Texas Tech, rememberthe two somewhat overwhelmedand bewilderedSilbers, Nita and Ernesto,who arrivedin L u b b o c ki n t h e F a l l ,1 9 6 7 ,a n d w e n t on each to earn the doctorate. ErnestoSilberdied in the periodof p o l i t i c a tl u r m o i li n A r g e n t i n aN . i t ai s n o w m a r r i e dt o a c o l l e a g u ea, n electrochemist.Nita askedfor news of former co-workersCharles R i s t a g n oC , a r o l eS c h o e n i n gR , ichard G o o d i n ,a n d C h a r l e sB a l d w i n W . rite to her at F. Q. PorrecaNo. 320, Rio Cuarto,Argentina. D r . J a m e sE . W a t s o n J, r . , ( 8 . A . ' 2 9 ) is a generalsurgeonwith officesin the HermannProfessionalBldg., Houston.TX. D r . B . W . W i l l i a m s( 8 . A .C h e m ' 5 0 ; M.D.,UT-Galveston'56) writesfrom L a s C r u c e s ,N . M . t h a td a u g h t e rK a r e n is a medicalstudentat TTUSM. From Bishop,Tx., comes news of two exes.LeanneMayerleHarvey(B.S. '75) writes returning of to her position as Group Leaderover the Special ProblemsSectionat Celanese C h e m i c a lL . e a n n ea n d h u s b a n dM i k e broughta new Texan into the world o n A u g u s t2 , 1 9 8 3 ,J e n n i f e rD e n i s e . Leanne'sreturnto work followedher maternityand vacationleave.News also of John Clemmer at Celanese, who will soon transferto the vinyl acetate unit as a processsupport chemistafter a three-yearstint in the b u t a n o la n d p r o p a n o lu n i t s .J o h n a n d Grace havetwo children,Mary (4) and Rebekah(3). ResearchGrant News. Grants Active in 1983 Dr. John Anderson "Biosynthesisof FungalPigments," Welch Foundation, 6/83-5/85, $35.000. Dr. Dan Armstrong "Use of FunctionalizedSurfactants in Flameand Luminescence Analysis,"DOE 11/83-12/86,$65,000. "PseudophaseLiquid Ch romatography," NSF 8/83-6/84, $25,416. "Researchin AnalyticalChemistry," Whatman Chemical,8/83-8/84. $2.000. Dr. RichardBartsch "SyntheticMacrocyclic MultidentateCompounds,"Welch ResearchGrant News. Grants Foundation, 6/83-5/84,$17,000. Awarded lor 1984. "ComplexingAgents for Metal Dr. RobertHolwerda lons," SerpentixConveyorCorp., "ReactivityStudiesof Transition 9/83-8/84,$20,000. metal lons," Welch Foundation,6/84"lon-SelectiveCompounds,"Miles 5/87, $60,000. Laboratories,6/83-5/84, $15,750. "Crown Ethersfor Determinationof Dr. David Knaff Sodium and Potassiumin Blood," "Electron-Transfer Mechanismsof metallo-Proteins," Welch Foundation, TechniconlnstrumentsCorp., 4/83-5/84,$52,260. 6/84-5/87,$60,000. "Complex Base Promoled1,2Dr. John Marx EliminationReactions," "Synthetic Routesto PRF,5/83-8/84,$4,000. Sesquiterpenes," Welch Foundation, " M i n o r i t yH i g h S c h o o lS t u d e n t 6/84-5/87,$60,000. ResearchApprenticeProgram,"NlH, D r . H e n r yS h i n e 3/83-2/84,$4,500. "Radicaland Cation Radical "lonic Crown Ethers,"DOE,4/8312/84,$138,500. Reactionsat NitrogenCenters," "BiomedicalResearchSupport Welch Foundation. 6/84-5/87. Grant," PHS,4/83-3/84,$19,209. $81.000. "Energetics,TransitionStates,and Dr. WalterChesnavich Mechanismsof Aromatic "PeriodicTrajectoriesin Atom Rearrangements and Cation Radical Diatom ExchangeReactions,"Welch Reactions,"NSF, 1/84-12/86, Foundation, 6/83-5/84,$18,000. $357,000. "EnergySurfacesand Heavy-Atom Dr. Sandy Dasgupta "ContinuousDeterminationof Kinetic lsotope Effects in Ambient HydrogenPeroxide, Photochemical Reactions." Formaldehyde, and Sulfur (lV) in PRF,4/84-8186,$35,000. Gas-Phase and Cloud Water,"US "MatchingFunds,"CER/TTU, EPA,10/83-9/85,$90,103. $20,000. "MatchihgFunds,"Centerfor Dr. Pill-SoonSong EnergyResearch,TTU, $20,000. "Excited Statesand Dr. RobertHolwerda Photochemistryof Photobiological "ReactivityStudiesof Transition Mofecules,"Welch Foundation,6/84- Metal lons,"Welch Foundation, 6/835/87, $63,000. 5/84,$19,500. "An Ethanol-BasedFuel Cell." Dr. RobertWalkup "SyntheticStudiesDirectedToward cER/TTU, $17,000. (+)Osillatoxin-A and RelatedNatural Products,"Welch Foundation. 6/84-5/87,$60,000. *-*@, ,I "Mac" McPherson as he is now, and surrounded by the tout departmental chairmen with whom he served:RichardBartsch,Joe Dennis,Henry Shine,John Kice.Reception,December1o,1ggs. D r .J o h n K i c e "Mechanismsof Reactionsof Organoselenium C o m p o u n d s ,N " SF, 3/83-8/84,$38,300. "Mechanismsof Reactionof O r g a n i cS u l f u rC o m p o u n d s ,W " elch Foundation,6/83-5/84,$28,000. Dr. David Knaff "ElectronTransferReactionsof Copper-Contain ing Proteins,"Welch Foundation, 6/83-5/84,$18,000. "Protein-Protei n Complexesin PhotosyntheticElectronTransfer Reactions,"USDA,9/83-8/85, $80.000. "Electron-Flowand Metabolite Uptakein Photosynthetic Organisms," NSF, 6/83-11/84, $50,000. D r .J o h n M a r x "SyntheticRoutesto Sesquiterpenes," Welch Foundation, 6/83-5/84,$17,500. D r . J e r r yM i l l s "Stereochemistry and Coordination Chemistryof Some Group Va C o m p o u n d s ,W " e l c hF o u n d a t i o n 6/83-5/84,$19,000. Dr.RoyMitchell " O p t i m u mV i n i f i c a t i o n ,U" T , 9/83-8/84,$65,000. D r . R i c h a r dR e d i n g t o n "VibrationalAnalysisof HydrogenBonded Molecules."Welch Foundation,6/83-5/84,$20,000. D r . W i l s eR o b i n s o n "RobertA. Welch Chair in Chemistry," 6/83-5/84, $80,000. "SubnanosecondPrimaryEventsin Biology,"N I H, 7/83-6/84, $37,412. "ChemicalReactionsin Condensed Phase,"NSF,5/83-11/84,$61,000. Dr. RobertShaw "The Role of Metal lons in the Mechanismsof Enzymatic Reactions,"Welch Foundation,6/835/84,$15,000. D r . H e n r yS h i n e "Studiesof Radicaland Cation RadicalIntermediatesin Organic Reactions,"Welch Foundation,6/835/84, $27,000. "Role of Cation Radicalsin Organic Reactions,"NSF,3/83-1/84, $71,300. "SeedGrant,"CER/TTU,$10,000. Dr. WayneSmith "ElectrochemicalInvestigationof the CatalyticPropertiesof Palladium and PlatinumPolypyridyl Complexes,"Welch Foundation6/835/84,$14,000. D r . P i l l - S o o nS o n g "PrimaryMolecularProcessesof Photomorphogen ic Receptor: Phytochrome,"NSF,6/83-11/84, $50,000. "AneuralPhotosensory Transductionin SfentorCoeruleus NrH, 8/83-7184, $35,879. "ExcitedStatesand Photochemistryof Photobiological Molecules,"Welch Foundation,6/835/84,$21,000. D r . R i c h a r dW i l d e "Solid StateStudies,"Welch Foundation 6/83-5/84,$20,000. Au Revoir "Mac" Dr. C. M. McPherson Retires A l o n g ,l o n g a s s o c i a t i o w n iththe Departmentcame to an end on D e c e m b e r1 7 , 1 9 8 3 ,w i t h t h e e n d o f the Fallsemester.Or, should we say that a long, long associationentered yet anotherphase?That very colorful character,Dr. C. M. McPherson,has retiredfrom our faculty.A farewell party was held at the Bartsch'es h o u s ei n M a c ' sh o n o r o n D e c e m b e r 1 0 .H u n d r e d s( t h o u s a n d s !o)f freshmanchemistrystudentshave encounteredthe man we all know as " M a c , "e i t h e ri n t h e l a b o r a t o r yo r i n the classroom.Hundredsof pren u r s i n g( a s t r a n g en a m e ,t h a t ) s t u d e n t sh a v eg o n e t h r o u g hh i s chemistry-for-nurses classeson their w a y t o n u r s i n gs c h o o l .A l l o f t h e m w i l l r e m e m b e tr h e i n f o r m a l i t yo f t h e teacherwho treatedchemistryas if it were as informalas himselfand deliveredit to his studentsoften in the vernacularof WestTexas. " M a c " c a n c l a i mt h e l o n g e s t associationwith the Departmentof any of the current faculty.He first enteredthe Departmentas a student i n t h e F a l l ,1 9 3 8 ,t o m a j o ra s a chemicae l n g i n e e r I. n t h o s ed a y s ,a s m a n yo f y o u k n o w ,c h e m i c a l e n g i n e e r i n ga n d c h e m i s t r yw e r eo n e department.Mac almost made it, but i n t h e F a l l ,1 9 4 1 t, h e l o n ga r m o f U n c l eS a m c l a i m e dh i m f o r s e r v i c ei n W o r l dW a r l l , a n d p l a c e dh i m i n t h e U . S .A i r F o r c e .B y S e p t e m b e r , 1 9 4 2 , our WestTexascolleaguewas flying m i s s i o n s" o v e rt h e H u m p " ,t a k i n g suppliesf rom basesin Assam, n o r t h e a s It n d i at o t h e U . S .b a s e si n K u n m i n ga n d L u c h o w C , h i n a .T h e " H u m p " w a s t h e H i m a l a y am o u n t a i n s . Mac, like so many modestpeopleof those days rarelyspeaksabout this period of service.A popularWWll Historysays:"Only men of special c a l i b e rc o u l d l i v e u p t o t h e d e m a n d s p l a c e do n t h e m b y t h e H u m p . "M a c was a navigatorin the 24th Combat M a p p i n gU n i t ,a n d s o o n a f t e r1 9 4 2 w a s f l y i n go v e r B u r m a ,C h i n aa n d I n d i a ,f r o m b a s e si n C h i n aa n d I n d i a , mappingfuture battleareas photographically. When the war ended Mac returned t o T T U i n t h e F a l l ,1 9 4 6 ,a n d graduatedin the Spring 1947, making up the semesterhe lost five years e a r l i e rA . f t e r r u n n i n ga s m a l l m a n u f a c t u r i n cgo m p a n yu n t i lt h e F a l l ,1 9 4 9 ,h e j o i n e dt h e S l a t o nH i g h School as an instructorin science, servingalso as the bus driverfor i n s e r v i c et r a i n i n gf o r t h e s c h o o l teachersin Slaton.This broughtthe t e a c h e r st o T T U , s o d u r i n gt h i s t i m e , a l s o ,M a c t o o k s u m m e rc o u r s e si n c h e m i s t r ya n d e d u c a t i o na, n d r e c e i v e dt h e M . E d .i n 1 9 5 3 . I n 1 9 5 6M a c w a s i n v i t e dt o j o i n o u r Departmentas an instructor,with the privilegeof carryingout researchin t h e e f f i c a c yo f u s i n gv i s u a la i d s i n t e a c h i n gf r e s h m a nc h e m i s t r yT. h i s w o r k g a i n e dh i m t h e E d . D .d e g r e ei n 1959.At the sametime he was the supervisorof freshmanchemistry labs,and preparedlecture demonstrationsfor use in the freshmancourses.How many studentsrememberthe hydrogen canon and the thermitevolcanoes? ThereafterMac taught in the nurses chemrstryand fr-eshman chemistry programs,as mentionedearlier.He was made assistantprofessorin 1961 and associateprofessorin 1977. D u r i n gt h e s ey e a r st h e t r a i n i n gi n p h o t o g r a p h yM a c g a i n e di n W W l l came to the aid of our department. Slidesmade by Mac have been used by Chemistry'sfacultyall over the w o r l d i n s y m p o s i aa n d m e e t i n g sW . e w i l l m i s st h a t f r i e n d l ys e r v i c ea, n d h o w .A n d t h a t b r i n g su s t o a n o t h e r s i d eo f M c P h e r s o nI.n 1 9 6 9M a c b o u g h t1 0 a c r e so f l a n d s o u t ho f L u b b o c ko n Q u i r t A v e .H i s c o h o r t , Prof.Reedof the Horticulture Department,bought five acres. T o g e t h e rt h e y b e g a ng r o w i n gg r a p e s f o r w i n e ,e x p e r i m e n t a l l yi m , porting vine stock from many parts of the U S A .A w i n e r y ,c a l l e d ,a p t l y ,L l a n o EstacadoWinery,was constructedin t h e S p r i n g ,1 9 7 6 ,i n a l i m i t e d p a r t n e r s h pw i t h o u t s i d ef i n a n c i a l b a c k e r s I. n t h e F a l l ,1 9 7 6 ,1 6 0 0 g a l l o n so f w i n e w a s p r o d u c e df r o m grapesgrown in and around the Lubbockarea.Wine productionand the winery havegrown eversince.In ."Mac" McPherson as he was then: Physical Chemistry 441, 1940.Photo by the late Prof. W. M- Craig. '1980 son Kim McPhersontook over t h e m a n a g e m e not f t h e w i n e r ya n d , as Mac puts it, becamethe only e n o l o g yc o l l e g e - t r a i n ewdi n e m a k e r in Texas.Llano Estacadowines are n o w b e c o m i n gk n o w n ,n o t o n l y i n Texas but, of all places,in California. Some of the winery'swines have taken gold medalsin State competitions,particularlythe 1980 CabernetSauvignon,of which sad-to. a c h a sh i s s a y n o n e r e m a i n sM retirementplans centeredon the v i n e y a r da n d e n o l o g y .H e p l a n st o uproot his vineyardand replantwith c a b e r n e st a u v i g n o no n l y .A p p a r e n t l y he knows a good thing when he sees it. The grapeswon't be readyfor stompingfor severalyears,but when t h e ya r ew e h o p eM a c w i l l r e m e m b e r us and inviteus out for a grapes t o m p i n gf a n d a n g o M . e a n w h i l et,o Mac, we say thanksfor the memories, a n d ,a s C h a u c e rs a i d :" e u ' a u l l e coome-y-backe. 'ON lil.urad 6L/ sexal'Icoqqnl orvd 'lcoqqnl 60t62 sPxal Arlsruraqg1o luau:yedaq Alrsrentulqcal sexal ooPlsod'S'n '616 gr1or4-uo51 a We would be very pleasedto hear from the Department'sgraduates.Send us your updatedaddressand descriptionof what your are now doing professionallyor otherwise.lf there is a particularinquiryyou may have for news of the Department,let us have it please. Name: Dateof Graduation(or Associationwith Department): Address: C u r r e n tP o s i t i o n : Item of news for us: I n q u i r yo f n e w sf r o m u s : Send Responseto: ProfessorH. J. Shine,Editor Dept.of Chemistry Texas Tech University Lubbock, Texas 794091' , Name-the-Newsletler Competition The name of the Newsletter was chosenwith inspirationand sentimentfor our Double-T heritage.lf you can think of a better one let us know, too, and win $25.Send your repliesta the Editoreither "for" the current name or with suggestion(s)for a new one. All valid suggestions will be voted on by membersof the department.The best suggestionfor replacementwill win $25,whetheror not the sentimentis "for" the "Test Tube." Resultswill be published in Newsletter6.