This article appeared in a journal published by Elsevier. The attached copy is furnished to the author for internal non-commercial research and education use, including for instruction at the authors institution and sharing with colleagues. Other uses, including reproduction and distribution, or selling or licensing copies, or posting to personal, institutional or third party websites are prohibited. In most cases authors are permitted to post their version of the article (e.g. in Word or Tex form) to their personal website or institutional repository. Authors requiring further information regarding Elsevier’s archiving and manuscript policies are encouraged to visit: http://www.elsevier.com/copyright Author's personal copy Quaternary Science Reviews 31 (2012) 67e81 Contents lists available at SciVerse ScienceDirect Quaternary Science Reviews journal homepage: www.elsevier.com/locate/quascirev The sequence and timing of large late Pleistocene floods from glacial Lake Missoula Michelle A. Hanson a, *, Olav B. Lian b, John J. Clague a a b Department of Earth Sciences, Simon Fraser University, 8888 University Drive, Burnaby, British Columbia, Canada V5A 1S6 Department of Geography, University of the Fraser Valley, 33844 King Road, Abbotsford, British Columbia, Canada V2S 7M8 a r t i c l e i n f o a b s t r a c t Article history: Received 24 March 2011 Received in revised form 28 October 2011 Accepted 10 November 2011 Available online 30 November 2011 Glacial Lake Missoula formed when the Purcell Trench lobe of the Cordilleran ice sheet dammed Clark Fork River in Montana during the Fraser Glaciation (marine oxygen isotope stage 2). Over a period of several thousand years, the lake repeatedly filled and drained through its ice dam, and floodwaters coursed across the landscape in eastern Washington. In this paper, we describe the stratigraphy and sedimentology of a significant new section of fine-grained glacial Lake Missoula sediment and compare this section to a similar, previously described sequence of sediments at Ninemile Creek, 26 km to the northwest. The new exposure, which we informally term the rail line section, is located near Missoula, Montana, and exposes 29 units, each of which consists of many silt and clay couplets that we interpret to be varves. The deposits are similar to other fine-grained sediments attributed to glacial Lake Missoula. Similar varved sediments overlie gravelly flood deposits elsewhere in the glacial Lake Missoula basin. Each of the 29 units represents a period when the lake was deepening, and all units show evidence for substantial draining of glacial Lake Missoula that repeatedly exposed the lake floor. The evidence includes erosion and deformation of glaciolacustrine sediment that we interpret happened during draining of the lake, desiccation cracks that formed during exposure of the lake bottom, and fluvial sand deposited as the lake began to refill. The floods date to between approximately 21.4 and 13.4 cal ka ago based on regional chronological data. The total number of varves at the rail line and Ninemile sites are, respectively, 732 and 583. Depending on lake refilling times, each exposure probably records 1350e1500 years of time. We present three new optical ages from the rail line and Ninemile sites that further limit the age of the floods. These ages, in calendar years, are 15.1 0.6 ka at the base of the Ninemile exposure, and 14.8 0.7 and 12.6 0.6 ka midway through the rail line exposure. The sediment at the two sections was deposited during later stages of glacial Lake Missoula, after the largest outburst events. Ó 2011 Elsevier Ltd. All rights reserved. Keywords: Glacial Lake Missoula Outburst floods Stratigraphy Sedimentology Varves Optical dating 1. Introduction The Purcell Trench lobe of the Cordilleran ice sheet filled the basin now occupied by Lake Pend Oreille, Idaho, during the Fraser Glaciation (late Wisconsinan; marine oxygen isotope stage 2). The ice lobe blocked Clark Fork River and impounded glacial Lake Missoula in the intermontane basins of western Montana (Fig. 1; Pardee, 1910, 1942). At its maximum, glacial Lake Missoula had a volume of 2200e2600 km3 and a depth at the ice dam of 610e640 m (Pardee, 1942; Bretz, 1969; Clarke et al., 1984; Craig, 1987; Smith, 2006). When water in glacial Lake Missoula reached * Corresponding author. Present address: Saskatchewan Geological Survey, Saskatchewan Ministry of Energy and Resources, 200-2101 Scarth Street, Regina, Saskatchewan, Canada S4P 2H9. Tel.: þ1 306 798 4211; fax: þ1 306 787 1284. E-mail addresses: mhanson@sfu.ca, Michelle.Hanson@gov.sk.ca (M.A. Hanson), olav.lian@ufv.ca (O.B. Lian), jclague@sfu.ca (J.J. Clague). 0277-3791/$ e see front matter Ó 2011 Elsevier Ltd. All rights reserved. doi:10.1016/j.quascirev.2011.11.009 a critical depth, the east end of the ice dam became buoyant, tunnels opened beneath the dam, and the lake drained catastrophically (Waitt, 1985). The maximum discharge of the largest flood was at least 17 million m3 s1 (Baker, 1973; Clarke et al., 1984; O’Connor and Baker, 1992). Floodwaters flowed into glacial Lake Columbia to the west, depositing a thick layer of gravel, sand, and silt on top of laminated silty glaciolacustrine sediments (Fig. 1; Atwater, 1984, 1986, 1987). Floodwaters also flowed across the Columbia Plateau, eroding Miocene basalt and Pleistocene loess (Fig. 1; Bretz, 1923, 1925, 1928). The floodwaters formed giant flood bars and current ripples, deposited fine-grained sediments in some Columbia River tributaries in southern Washington, and recharged Columbia River Basalt aquifers with isotopically depleted water (Bretz, 1925, 1928, 1929; Bretz et al., 1956; Baker, 1973; Waitt, 1980, 1985; Brown et al., 2010). They also backed up southward into Willamette Valley of western Oregon and deposited slackwater Author's personal copy 68 M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 Fig. 1. Study area showing locations mentioned in the text. The figure shows the maximum extent of the Cordilleran ice sheet as well as the maximum extent of glacial Lake Columbia. LCFR: Lower Clark Fork River; MV: Mission Valley; NC: Ninemile Creek; RL: Rail line. Darker gray areas were swept by floodwaters from glacial Lake Missoula. (Figure adapted from Waitt, 1985; Atwater, 1986; Levish, 1997). sediments there (Allison, 1978; Waitt, 1980, 1985; O’Connor et al., 2001). Within a few weeks, the floodwaters had reached the mouth of Columbia River, over 700 km from their source, where plumes of freshwater spread out into the northeast Pacific Ocean (Baker, 1973; Craig, 1987; O’Connor and Baker, 1992; Lopes and Mix, 2009; Denlinger and O’Connell, 2010). Turbidity currents triggered by the floods travelled an additional 1100 km southward along the floor of the eastern North Pacific Ocean (Zuffa et al., 2000), while a plume of finer sediment travelled northward along the coast (Gombiner et al., 2010). Glacial Lake Missoula may have drained and refilled approximately 90 times during the Fraser Glaciation (Waitt, 1985; Atwater, 1986). Most of the evidence for drainings of glacial Lake Missoula has come from study of flood deposits in Idaho, Washington, and Oregon (Bretz, 1925, 1928; Bretz et al.,1956; Baker, 1973; Allison, 1978; Waitt, 1980, 1985; Atwater, 1984, 1987; O’Connor et al., 2001). In contrast, relatively little research has been done in the glacial Lake Missoula basin itself. Pardee (1910, 1942) described the extent of the lake and landforms that led him to conclude that very large and rapid currents were involved in the draining of the lake. Chambers (1971, 1984) studied a section of cyclic, rhythmically bedded glaciolacustrine sand, silt, and clay units exposed in a highway cut near Ninemile Creek, Montana (Fig. 1). Most of the units1 at the Ninemile exposure comprise a thick layer of very fine sand and silt that grades upward into rhythmically laminated silt and clay beds that Chambers (1971, 1984) interpreted to be varves. The silteclay couplets thin upward within units that are separated by unconformable contacts. Thin beds of pebble gravel, weathering, and small frost wedges at the top of 22 of the 40 units led Chambers (1971, 1984) to conclude that glacial Lake Missoula drained at least 22 times to below 959 m above sea level (asl), which is 306e321 m below the highest elevation reached by the lake. Waitt (1980, 1985) ascribed rhythmically 1 In this paper, we define “unit” as an ensemble of lithofacies recording a single lake phase from filling through maximum stage to drainage. bedded slackwater flood sediments in southern Washington to these drainings and thus inferred that the drainings were catastrophic. Baker and Bunker (1985), however, argued that the slackwater beds are not proof that each draining was catastrophic. Levish (1997) studied exposures of rhythmically bedded sediments similar to those at Ninemile in Mission Valley, Montana (Fig. 1). He inferred 66 sedimentation units, each of which is recorded by approximately 30e60 varves that thin up-section and, collectively, represent 3240e3610 years of deposition in glacial Lake Missoula. He found no evidence of unconformities between the units and concluded that there was no evidence for repeated drainage of glacial Lake Missoula. Most recently, Smith (2006) described large gravel flood bars that underlie rhythmic silt and clay beds in several places along the lower Clark Fork River (Fig. 1). He attributed these features to catastrophic draining of glacial Lake Missoula and the finer beds at the Ninemile site to shallower, later stages of the lake when drainings were less energetic (Smith, 2006; Alho et al., 2010). This paper describes the stratigraphy and sedimentology of an important new section of rhythmically stratified sand, silt, and clay in the heart of the glacial Lake Missoula basin and compares it to the Ninemile section. The new section, which we refer to as the rail line section, provides evidence for several tens of substantial drainings of glacial Lake Missoula. These drainings repeatedly exposed the lake floor in the Clark Fork River valley at Missoula. Three new optical ages, two from the rail line site and one from the Ninemile site, better constrain the timing of glacial Lake Missoula flooding. 2. Section locations, stratigraphy, and sedimentology The Ninemile section is a 250-m-long exposure along Interstate Highway 90 near the confluence of Ninemile Creek and Clark Fork River in western Montana (N 47.0 , W 114.4 ; Fig. 1). The base and top of the section are, respectively, 936 m and 959 m asl. The base of the section is approximately 281 m above the base of the former ice dam, 200 km to the west. The rail line section is a 1.4-km-long, northwest-trending exposure along the former track of the Chicago Author's personal copy M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 Milwaukee St. Paul and Pacific Railroad west of the city limits of Missoula and approximately 26 km upstream of the Ninemile section (N 46.9 , W 114.1 ; Fig.1). The base and top of the section are, respectively, 963 m and 975 m asl. The highest glacial Lake Missoula shorelines around Missoula are 1265e1280 m asl, 290e315 m above the top of the rail line section (Pardee, 1942; Smith, 2006). 69 2.1. Ninemile Creek section The Ninemile Creek section comprises 34 units of rhythmically stratified, graded beds of fine sand, silt, and clay (Figs. 2 and 3A) and, at the base of the section, at least 1 m of coarse to fine sand and pebble-cobble gravel. The uppermost 3 units were too weathered Fig. 2. Stratigraphic log of the Ninemile Creek section, Montana. Author's personal copy 70 M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 to describe in detail. The sediments comprise three lithofacies: a gravelesand facies, a sandesilt facies, and a silteclay facies. The sequence of lithofacies in most units, from bottom to top, is gravelesand, sandesilt, and silteclay facies. 2.1.1. Gravelesand facies This facies comprises thin beds of coarse sand and, in some cases, granule to medium pebble gravel. It lies at the base of nine of the 34 units (Figs. 2 and 3B) and ranges from less than 1e20 cm thick; the thinnest beds are discontinuous. Most gravel clasts are subrounded to subangular. The gravelesand facies also fills wedgeshaped cracks at the top of the five lowest units (Fig. 3C). 2.1.2. Sandesilt facies The sandesilt facies is present in each of the 34 rhythmically stratified units and comprises very fine sand or silt (Figs. 2 and 3D). Individual occurrences of the facies range from 9e220 cm thick. Lower contacts are commonly sharp and planar or undulating; 16 of the contacts are clearly erosional. Some of the lower contacts, however, are loaded, producing convoluted bedding above or below the contact (Figs. 2 and 4A). The sandesilt facies is characterized by planar or undulating laminae ranging from <1e4 mm thick. About half of the strata of the sandesilt facies contain ripples (Figs. 2 and 3D); in one case, the ripples are overturned. Both type-A and type-B ripples are present Fig. 3. Rhythmically bedded sand, silt, and clay units at the Ninemile section. (A) One unit comprising sandesilt facies (below) and silteclay facies (above). The contact between the two facies is gradational. Unit is 320 cm thick. Varves thin upward as the silt content decreases. (B) Gravelesand facies at the base of a unit. Sand is w6 cm thick. (C) Wedge-shaped feature at the top of a unit, infilled with gravel and sand. Feature is w15 cm long. (D) Type-A and type-B climbing ripples in sandesilt facies. (E) Loaded silt laminae and water escape structures in sandesilt facies. Author's personal copy M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 (Jopling and Walker, 1968). Most ripples indicate flow to the northwest; in one instance, flow was to the southeast (Fig. 2). Other common sedimentary structures in the sandesilt facies are loaded laminae and beds, diapirs, dish structures, and flame structures (Figs. 2, 3E, 4A, and B). Thin (w2 mm) clay laminae are present locally within the facies, commonly near the top and generally associated with laminated silt. 2.1.3. Silteclay facies The silteclay facies is also present in each of the 34 rhythmically stratified units and comprises sets of silt and clay couplets that resemble varves (Figs. 2 and 4C). The number of couplets per rhythmically stratified unit ranges from two to 44 and averages 19. Couplets are 0.3e20 cm thick. Within each unit, couplet thickness decreases upward from an average of 4.3e0.8 cm (Fig. 3A). The lower part of each couplet consists of massive silt with few clay laminae; the upper part is clay, in some cases with thin silt interlaminae (Fig. 4C). Lower contacts of individual couplets are sharp but the boundary between the silt layer and overlying clay layer in each couplet is gradational (Fig. 4C). The thickness of the clay layer changes little upward within a unit; thin couplets have a higher ratio of clay to silt than thick couplets and the thinnest ones are approximately 80 percent clay. Thinner couplets also have fewer 71 internal laminations than thicker couplets. Near the top of three of the units, couplets are separated by anomalously thick (1.5e5 cm) silt beds (Fig. 4D). The three silt beds have sharp, planar lower and upper contacts, and include planar and undulating laminae and ripples. 2.1.4. Correlation with Chambers’ work Chambers (1971, 1984) counted six more units at the Ninemile site than we did, although he was only able to describe 32 in detail; the remaining units were at the top of the exposure and were too weathered to describe in detail. Based on unit thickness, elevation, and sedimentological characteristics, such as the presence of the sand-gravel facies and ripple-drift sequences in the silt, we are able, with few exceptions, to correlate our units with Chambers’ units. Just above our 10-m level, Chambers identifies one additional unit. We are confident, however, in our decision to include his thin unit (18.5 cm thick) within the unit that underlies it. Above the 17.5-m level, correlation is more difficult. Chambers’ 22nd unit from the base is 1.5 m thick, which does not match the thickness of any of our units. A possible explanation for this discrepancy is that Chambers’ 22nd unit represents two of our units, which occur between 17.4 m and 18.6 m. Chambers also described one more unit than we were able to near the top of the exposure, below the weathered zone. Fig. 4. Sedimentary features at the Ninemile section. (A) Loaded lower part of unit with diapiric structure in gravelesand facies and dish structures in the sandesilt facies. (B) Flame structures within lower part of sandesilt facies. (C) Nine varves with sharp lower contacts, gradational internal contacts, and internal laminations. (D) Event beds at the top of silteclay facies. Author's personal copy 72 M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 Finally, above the 17.5-m level, Chambers also has one occurrence of sand and gravel, whereas we identified six. A possible explanation for the discrepancy is the discontinuous nature of this facies. Chambers’ total varve count is 716; ours is 583. His counts are higher for nearly all units that we can confidently correlate. We offer two explanations for this discrepancy: (1) weathering of the upper part of the exposure over the past several decades did not allow us to observe all of the varves in the uppermost units; (2) we erred by grouping varves into composite varves, or Chambers erred by subdividing composite varves. The latter explanation is more likely in the sandesilt facies, where thin clay laminae might be interpreted to be part of a composite varve or the top of a noncomposite varve. 2.2. Rail line section We studied the rail line section in detail where the exposed sediments are thickest (11.8 m; Fig. 5). All but the lowest sediments are well exposed on the northeast-facing side of the railway cut; the lowest sediments were documented on the southwest-facing side of the cut. The exposed sediments include 29 upward-thinning units of rhythmically bedded fine sand, silt, and clay (Figs. 5 and 6A). A zone of highly disturbed sediments approximately 6 m above the base of the exposure is thicker than the units directly above and below it (Fig. 5). Judging from the average thickness of adjacent units, we estimate that the disturbed zone includes 3 units, bringing the total count to 31. Units consist of three lithofacies similar to those at the Ninemile site. The three lithofacies, in the order in which they generally occur from bottom to top, are the sand, silt, and silteclay facies. We describe the facies in detail because some of their characteristics differ from those at the Ninemile site. 2.2.1. Sand facies The sand facies, which resembles the gravelesand facies at the Ninemile site, occurs below 10 units, all in the lower half of the exposure (Fig. 5). The facies comprises well-sorted, very fine to fine sand (Fig. 6A and B). The lower contact of each of the 10 beds is erosional, and most contacts are planar (Fig. 6B). The facies ranges in thickness from <1 cm to 6 cm; the thinner occurrences are discontinuous. The sand is normally graded, commonly rippled at the top, and, in some cases, laminated at the base. Type-A ripples, commonly containing silt stringers or clay rip-ups that were eroded from underlying sediments, indicate flow to the northeast (Fig. 5). The thick sand at the base of the third lowest unit (Fig. 5) is different in character from the sand layers at the base of the other 9 units. It is 64 cm thick and mostly massive, but with some laminations and type-A ripple-drift cross-laminae in the upper 9 cm of the bed. 2.2.2. Silt facies The silt facies is limited to two beds, 14 cm and 35 cm thick, in the two lowest units (Fig. 5). The two silt beds resemble most of the beds of the sandesilt facies at the Ninemile site. Lower contacts are sharp and erosive. The facies consists of thinly laminated, coarse to fine silt with type-B ripple-drift cross-laminae (Fig. 7A). A few thin (w2 mm) clay laminae occur within silt beds near the top of the facies. 2.2.3. Silteclay facies The dominant facies at the rail line section is silteclay couplets similar to those at the Ninemile site. In most of the units, the silteclay facies either drapes the sand facies (Fig. 6B) or unconformably overlies silteclay couplets of the next lower unit (Fig. 6C). Fig. 5. Stratigraphic log of the rail line section, Montana. See Fig. 2 for legend. The number of couplets per unit ranges from 15 to 42 and averages 24. Couplets range in thickness from 0.4e12 cm. Couplet thickness decreases upward within each unit from an average of 3.4e0.7 cm (Fig. 6A). The lower contact of each couplet is sharp (Fig. 6D). Each couplet comprises a lower lamina or bed of massive silt, in some cases with a few thin laminae of clay near Author's personal copy M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 73 Fig. 6. Rhythmically bedded sand, silt, and clay units at the rail line section. Arrows indicate unit contacts. (A) A sedimentary unit comprising sand facies (below) and silteclay facies (above). Varves thin upward as the silt content decreases. Square shows location of photo B. (B) Sand facies with type-A ripples and an erosional lower contact. Silt and clay varves are draped over ripples. (C) The basal sediment of the upper unit unconformably drapes the sediments of the unit below. The uppermost 2 cm of each unit were disturbed during draining of the lake. (D) Silt and clay varves. Note clay laminations within silt beds. Contacts between couplets and internal contacts are sharp and planar. Undulation of laminations is caused by post-depositional desiccation. the top, and an upper clay cap (Fig. 6D). Most contacts between the massive silt and the clay cap are sharp (Fig. 6D); only in a few cases are they gradational. The clay caps range in thickness from 0.2e0.7 cm and appear to be normally graded. Few of the clay caps contain silt laminae. As at the Ninemile site, the ratio of the thickness of the clay cap to that of the associated silt layer increases upward within units; the uppermost couplets are approximately 80 percent clay. Thinner couplets also have fewer internal laminations. The uppermost 15 cm of ten of the units are brecciated and include rip-ups of silt and clay couplets (Figs. 5 and 6C). These disturbed zones have a sharp and probably erosive lower contact. Silteclay couplets in other glacial Lake Missoula sediments identical to those described here have been interpreted to be varves by Chambers (1971, 1984), Waitt (1980), Fritz and Smith (1993), and Levish (1997). We interpret these silteclay couplets, as well as those as the Ninemile site, to be varves. The silteclay couplets meet five criteria of varves: (1) they are thin, regular, fine-grained, and commonly contain no current structures; (2) there is little or no fining in the silt layer, whereas the clay cap fines upward; (3) the thickness of the clay cap changes little from couplet to couplet, unlike the thickness of the silt layer; (4) couplets thin and fine laterally in a down-lake direction; and (5) couplets are found at all elevations within the lake basin (Ashley, 1975, 2002; Smith and Ashley, 1985). 2.2.4. Boundaries between units The contacts between successive units at the rail line section are unconformable. Even where the basal sand facies is absent, there is evidence of erosion of up to seven varves at the top of each unit. Tilted and broken varves are also present in the upper few centimetres of many units. These broken varves form small concave-up features 2e3 cm wide and less than 2 cm deep (Fig. 6A and B). Eight units are characterised by small, downward-tapering clastic wedges that do not cross the contact with the overlying unit (Figs. 5 and 7B). These wedge-shaped structures are filled with silt and clay derived from the adjacent sediment; in some cases brecciated fragments of varves occur within the casts (Fig. 7B). The cracks extend down to 26 cm from unit contacts. The tops of the cracks range from 0.5e15 cm wide (Fig. 7B). Varves in the adjacent sediment are bent downward at the margins of the cracks, and micro-faults in sediment adjacent to the largest crack parallel the crack walls (Fig. 7B). Author's personal copy 74 M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 Fig. 7. Unique characteristics of sediments at the rail line section. (A) Laminated and rippled silt facies with clay laminations. Arrow indicates lower contact. (B) Largest wedgeshaped crack, measuring 15 by 26 cm. Crack is infilled with adjacent varved silt and clay. Varves are downturned toward the crack. Micro-faulting can be seen to the right of the wedge-shaped crack (squares). A secondary similar feature from the overlying unit crosscuts the main feature (arrows). 3. Optical dating Optical dating provides an estimate of the time elapsed since deposition and burial of quartz or feldspar grains (see Lian and Roberts, 2006 and Wintle, 2008 for detailed descriptions of the method). For this work, quartz was prepared from two samples of the sand facies at the rail line section (samples MAH-3 and MAH-5) and from one sample of the gravelesand facies at the Ninemile section (sample MAH-8). These facies were chosen for dating based on our interpretation that they were deposited in shallow fluvial environments on the exposed floor of the lake between ponding events and before lake refilling (see Section 4.1). 3.1. Sample collection and preparation We collected samples from horizons free of gravel indicative of high-energy deposition and avoided sediments showing evidence of post-depositional disturbance that could have mixed grains of different ages. Each sample was collected by inserting an aluminum cylinder (w40 cm long and 10 cm in diameter) into a cleaned face; the sampled sediment included both the target sand bed and bounding silt and clay. The cylinder then was excavated and its ends were filled with fabric and taped to keep the contents immobile and to retain water content. In the laboratory, the outer 0.5e1 cm of the sediment from each end of the cylinder was removed under controlled lighting conditions. Some of this sediment was dried and used for dosimetry and the remainder was discarded. The sand was then separated from the surrounding silt and clay for optical dating. All sand samples were treated with hydrochloric acid to dissolve carbonates and then sieved to isolate the 180e250 mm size fraction. Samples then were treated with concentrated hydrofluoric acid for 40 min to dissolve feldspar grains and to etch from quartz grains outer material that had been affected by alpha radiation in the environment. Quartz grains were separated from heavier minerals using a sodium polytungstate solution with a density of 2.68 g ml1. The separated quartz grains were mounted on 9.8-mm-diameter aluminum discs using silicone oil as an adhesive. In principle, each aliquot should be as small as possible, but in practice aliquot size is dependent on the sensitivity of the quartz grains. For our samples, each aliquot contained 50 to 100 grains, therefore it is likely that the measured luminescence was dominated by that originating from fewer than 10 grains (Duller et al., 2000). 3.2. Environmental dose rate determination The radiation dose absorbed by the sample grains after deposition comes from alpha (a), beta (b), and gamma (g) radiation produced by decay of U, Th, their daughter products, and 40K. The radiation absorbed by the mineral grains of interest originates in the surrounding sediment and within the sampled grains themselves; there is also a contribution from cosmic rays. Samples used for dosimetry were dried, milled, and sent to a commercial laboratory for neutron-activation analysis to determine 40K, U, and Th contents; results are presented in Table 1. From these data, dose rates (in Gy ka1) caused by g and b radiation were calculated using standard formulae (Aitken, 1985; Berger, 1988; Lian et al., 1995) and the dose rate conversion factors of Adamiec and Aitken (1998; Table 2). In each case, we assumed that the U and Th decay chains have been in secular equilibrium since deposition of the sediment. This assumption generally has been found to be valid for welldrained mineral sediments (Prescott and Hutton, 1995; Olley et al., 1996). Pore water in the sediment matrix attenuates or absorbs radiation differently from mineral matter, and therefore it has to be accounted for in the dose rate calculations. When the sediments were overlain by a lake, it is likely they were saturated with water. The sediments, however, have spent the vast majority of the time since deposition as well-drained subaerial deposits, thus we used the as-collected water contents with an appropriate uncertainty to account for any reasonable variance (Table 1). For samples near the ground surface, cosmic-ray radiation can contribute significantly to the environmental dose rate, but its Author's personal copy M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 75 Table 1 Sample depths, K, U, and Th contents, and water content. Sample Site d (m)a K (%)b U (mg/g)b Th (mg/g)b Dw c MAH-3 MAH-5 MAH-8 Rail line Rail line Ninemile Creek 7.6 8.5 2.9 3.61 0.17 3.46 0.18 3.29 0.16 3.06 0.12 3.27 0.13 3.18 0.13 13.0 0.5 13.4 0.5 13.0 0.5 0.172 0.017 0.172 0.017 0.115 0.012 a d: sample depth beneath the ground surface. K, U, and Th contents were determined using neutron-activation analysis of a dried and milled subsample of the bulk material sampled for dating. c Dw: water content ¼ water mass/mineral mass. For each sample, the as-collected water content was used in the dose rate calculation, with an uncertainty that is thought to account for any reasonable variation at 2s. b effect diminishes rapidly with burial depth (Prescott and Hutton, 1994). For the samples dated here, cosmic-ray radiation constitutes less than three percent of the total dose rate (Table 2). 3.3. Equivalent dose determination Luminescence measurements were made using a Risø TL/OSL DA-20 reader. The separated quartz grains were stimulated using light-emitting diodes that delivered 45 mW cm2 of blue (470 20 nm) light to the sample. Ultraviolet emissions (w350 nm) were detected by an Electron Tubes Ltd. 9235QB photomultiplier tube placed behind a 7.5-mm-thick Hoya U-340 optical filter. Laboratory irradiations were applied with a calibrated 90Sr/90Y bsource mounted on the reader that delivered 6.38 0.12 Gy min1 to fine sand quartz grains mounted on an aluminum substrate. The equivalent dose (De; Table 2) of each sample was determined using the standard single-aliquot regenerative dose (SAR) protocol of Murray and Wintle (2000) but with the inclusion of an infrared wash to remove any luminescence resulting from K-feldspar contamination (Olley et al., 2004; Wintle and Murray, 2006; see Fig. 8 for details), which typically was found to be less than one percent of that measured from the quartz fraction. A zero-dose point was included to assess the severity of preheat-induced thermal transfer and one of the regenerative-dose points was repeated to assess the efficacy of the test dose to correct for sensitivity change. Of the 73, 49, and 48 aliquots prepared for samples MAH-3, MAH-5, and MAH-8, respectively, 58, 40, and 35 aliquots were accepted. For each sample, De values determined using SAR were plotted on radial plots (Galbraith et al., 1999; Galbraith, 2010), which display the distributions of De values about mean values (Fig. 9). The De values for the samples are distributed approximately evenly about their respective mean values and thus show no obvious discrete De populations. Therefore, a representative De used in the calculation of sample burial age was determined using the central age model (CAM) of Galbraith et al. (1999). This model determines the weighted De and its associated standard error and takes into account over-dispersion of the data, which is the variation between individual De values above and beyond that associated with Table 2 Dose rates, equivalent doses, and optical ages. Sample _ c ðGy=kaÞa D D_ T ðGy=kaÞb De (Gy)c Optical age (ka)d MAH-3 MAH-5 MAH-8 0.067 0.003 0.060 0.003 0.129 0.006 4.38 0.3 4.32 0.3 4.45 0.3 65.0 2.0 54.6 1.4 67.2 1.1 14.8 0.7 12.6 0.6 15.1 0.6 a _ Dc : dose rate due to cosmic rays, calculated using present burial depths and the relationship of Prescott and Hutton (1994). b _ DT : total dose rates (that due to cosmic rays plus that due to a, b, and g radiation). Only an internal dose rate applies for a radiation, and an estimate of 0.03 Gy/ ka was used (Olley et al., 2004). c De: equivalent dose found using the central age model. d Apparent optical ages and their analytical uncertainties at 1s. Fig. 8. (A) Flow chart showing the modified single-aliquot regenerative dose (SAR) method used to date the rail line and Ninemile samples. Li is the luminescence measured after administration of a regenerative dose, Di. In this case the regenerative doses (i ¼ 1 to 5) were 15.9, 31.8. 63.6, 127.2, and 0 Gy; the 0 Gy data point is used to check for thermal transfer resulting from the preheat, which was 220 C for 10 s. An aliquot was rejected if the luminescence measured at the 0 Gy step was more than 5 percent of that of the natural. Ti is the luminescence measured following a test dose of 12.7 Gy and a cut-heat of 160 C. For each aliquot, the 15.9 Gy dose (arbitrary choice) was repeated to determine the effectiveness of the test dose for correcting for sensitivity change; only aliquots that had a recycling ratio within 10 percent of unity were accepted. (B) Example of a luminescence decay curve for an aliquot of sample MAH-3, which is typical of those generated from natural aliquots of the three samples. The initial measured signal is dominated by the thermally stable fast component, which decays to about 10 percent of its initial intensity in w2 s. The inset graph shows doseresponse data for this aliquot, determined from the sensitivity corrected luminescence (Li/Ti) measured over the first 0.4 s of stimulation, minus that recorded during the last 20 s. The data are fitted with a saturating exponential curve, onto which the natural luminescence is interpolated in order to determine the equivalent dose (De). Author's personal copy 76 M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 analytical uncertainties (Galbraith et al., 1999; Lian and Roberts, 2006; Jacobs and Roberts, 2007). Even in cases where aliquots consisted only of grains that were exposed to sufficient sunlight prior to burial, over-dispersion values can be as high as 20 percent (see references cited in Lian and Roberts, 2006, p. 2459). All of the samples that we analyzed have over-dispersion values of approximately 20 percent (sample MAH-3) or much less than 20 percent (samples MAH-5 and -8; Fig. 9). These relatively low values suggest that the aliquots used to determine De had not been significantly contaminated with older grains that were insufficiently exposed to sunlight prior to burial. The results are consistent with our interpretation that the sands were deposited in a shallow, non-turbid fluvial environment (see Section 4.1). It is possible, although unlikely, that the size of the aliquots has masked the presence of younger or older grain populations. When one cannot be certain that the luminescence signal measured from the sampled grains was properly reset prior to burial or when the nature of the distribution of De values suggests the presence of more than one age population, it is common to apply the minimum age model (MAM) of Galbraith et al. (1999). MAM calculations were performed on all three samples, and in each case the MAM yielded De values that are consistent with those found using the CAM. These results support our supposition that the sampled quartz grains were exposed to adequate sunlight before burial. To test whether or not the SAR protocol used here is appropriate for our quartz samples, we performed dose recovery experiments (Roberts et al., 1999; Murray and Wintle, 2003) on 24 aliquots each of samples MAH-3 and MAH-8. Aliquots were exposed to natural sunlight for 10 min to remove the natural light-sensitive luminescence signal and then each aliquot was given a laboratory radiation dose similar to the De determined previously using the CAM. We then attempted to recover the laboratory dose using the same SAR protocol that we used to determine natural De values. In both cases, the recovered dose was at least 99 percent of the applied dose. 3.4. Optical ages The two samples collected from the rail line section yielded burial ages, in calendar years, of 14.8 0.7 ka (MAH-3) and 12.6 0.6 ka (MAH-5; Table 2). The samples were taken from directly below the 5th and 7th units of glacial Lake Missoula sediments, numbered from the base of the section (Fig. 5). The single sample from the Ninemile section (MAH-8) returned an age of 15.1 0.6 ka (Table 2). It was collected directly below the 1st unit of glacial Lake Missoula sediments, as numbered from the base of the exposure (Fig. 2). 4. Discussion 4.1. Sedimentology The rhythmic units at the rail line site are similar to those at the Ninemile site, as well as to those in Mission Valley described by Levish (1997), except for the lack of unconformities between units in Mission Valley. Thin gravelesand and sand beds separate rhythmic units in the Ninemile and rail line sections. These are likely the gravel-filled channels described by Chambers (1971, 1984). Such sediments can be deposited by underflows, but based Fig. 9. Radial plots showing the distribution of equivalent doses determined from aliquots of samples (A) MAH-3, (B) MAH-5, and (C) MAH-8. More precise data plot farther from the origin. In each case, the gray bands, which are generated by the radial plot software, are centered on the weighted mean equivalent dose (De) values provided by the central age model (CAM). De values that plot within the gray bands are consistent with the mean at a 95 percent confidence interval. De values that showed poor recycling ratios or unacceptably high thermal transfer (recuperation) were not included in the CAM calculations. The uncertainty in the weighted mean De used in the age calculation is provided by CAM. Over-dispersion values are 25 4, 16 2, and 9.5 1.3 percent for samples MAH-3, -5, and -8, respectively. Author's personal copy M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 on evidence for exposure of the underlying unit (see below), we interpret the gravel and sand to be non-channelized fluvial sediments deposited in shallow water on the floor of the lake before refilling; Chambers (1971) reached a similar conclusion at the Ninemile site. Thick, laminated and rippled basal silt beds are present throughout the Ninemile section but were found only in the two lowest units at the rail line section. At Ninemile, these beds have been interpreted by Shaw et al. (1999) as deposits of turbidity currents generated by periodic jökulhlaups from beneath the Cordilleran ice sheet in the Rocky Mountain Trench. This explanation does not explain, however, why upwardly thinning varves above this facies indicate a deepening lake over time after deposition of the sand and silt. Nor does this explanation account for what we interpret as evidence for subaerial exposure (see below) below this facies. The climbing ripple-drift sequences indicate a high influx of suspended sediment and high accumulation rates. Soft-sediment deformation structures, which are present at Ninemile but absent from the two similar units at the rail line section, are evidence of rapid deposition causing differential loading and consequent dewatering of the sediments (Lowe and LoPiccolo, 1974; Rust, 1977). These characteristics, combined with the erosive lower contact, leads us to conclude that these two thick silt beds were likely deposited by turbidity currents but at relatively shallow depths as glacial Lake Missoula began to fill, a conclusion also reached by Chambers (1971, 1984) at the Ninemile site. The sand and silt beds at both sites grade up into silteclay varves that were deposited in deeper water. The varves thin upward within each unit, evidence of continued deepening of the lake over time and increasing the distance from sediment sources. The general decrease in the number of varves per unit up-section at each site is consistent with a thinning ice dam toward the end of the Fraser Glaciation. The 1.5e5-cm-thick silt beds that interrupt the thinning-upward sequence near the top of some units at Ninemile (Fig. 4D) are deposits of rare, high-energy events, possibly turbidity currents. They are not separate, thin, lake-ponding units because they are abruptly and conformably overlain by varves and because the varves above the silt beds are similar in thickness and in clay-silt ratios to those directly below them. Deformed beds at the top of 10 units at the rail line section (Fig. 6C) are likely related to the unconformity directly above. We exclude the possibility that these deformed beds could be caused by rapid loading and sedimentation from underflows because these beds have erosive lower contacts and are not consistently overlain by the silt facies that could have produced the loading. These beds possibly result from erosion and rapid re-deposition of saturated glaciolacustrine sediment during draining of the lake. We cannot conclusively correlate the rail line and Ninemile sections on the basis of their stratigraphy and sedimentology. Units at the base of the rail line section, however, are similar to units throughout the Ninemile section, indicating that at least the lower part of the rail line section possibly overlaps with the Ninemile section, which also appears to be older based on our ages. If there is no overlap between the two sections, then the 31 units at rail line are missing from the top of the Ninemile section. In this scenario, it would be difficult to explain how earlier glacial Lake Missoula units were preserved at the Ninemile site, but later ones were eroded, given that the later lake draining events probably were less erosive because the ice sheet was thinning and the lakes were smaller. Thus, there is likely some overlap between the two sites. The broken and tilted varves and the concave-up features at the top of the rail line units probably record desiccation caused by subaerial exposure. We tentatively interpret the large wedge-like cracks as ice-wedge casts because: (1) they are infilled with adjacent varved sediment; (2) adjacent varves are bent down toward 77 the cracks implying secondary infill; and (3) micro-faults occur in adjacent sediment (Harry and Gozdzik, 1988; Murton and French, 1993; Gao, 2005). Chambers (1971, 1984) described similar cracks at the Ninemile site that he interpreted to be frost wedges filled with the gravelesand facies. Shaw et al. (2000) did not observe cracks at Ninemile, but argued that they could be dewatering structures associated with loading caused by rapid deposition of the overlying sandesilt units. The cracks at Ninemile, however, are filled with the gravelesand facies, which nowhere appears substantial enough to load the underlying varved sediment. Similarly at the rail line site, what we interpret to be ice-wedge casts are filled with adjacent sediment, not overlying sediment as would be expected from injection of liquefied sediment into fractures caused by rapid sedimentation. Unfortunately, due to the nature of the exposure, we could not examine these features in plan view, which bears on our interpretation of them as ice-wedge casts. If the wedges are ice-wedge casts, the lake floor must have been exposed between units. The interpretation of the depositional environment of each of the facies and of the boundaries between units is subject to different interpretations, but considering all the evidence together, we believe we have made a credible case for repeated draining and filling of glacial Lake Missoula at the Ninemile and rail line sites. Desiccation in the upper few centimetres and possible ice-wedge casts at the tops of units indicate subaerial exposure of varved units. Overlying laminated and rippled sand and gravel represent initial infilling of the lake; laminated and ripple-drift sand and silt sequences represent increased sedimentation in a shallow but deepening lake. Lastly, varved sediment with couplets that decrease in thickness upward indicate that the lake deepened until the ice dam failed, after which some of the lake sediment became disturbed and the lake bottom exposed. Subaerial exposure at the top of every unit at the rail line section indicates that glacial Lake Missoula drained or partially drained at least 29 times. Each time, the lake lowered below 960 m asl. The existence of possible ice-wedge casts in some units suggests that the lake floor was exposed for at least several years. This length of exposure is longer than one would expect from simple lake-level fluctuations and is consistent with the fact that it might take several years after the lake drained for the lake to refill to the elevation of this exposure. Twenty-two of the units at the Ninemile site show evidence of subaerial exposure, including erosional contacts, frost wedges, or overlying fluvial sand and gravel. This evidence indicates that the majority of the lake drainings were significant enough to lower the lake to below 936 m asl. Loaded contacts between varves and overlying sandesilt beds at three of the contacts at Ninemile possibly support the argument that glacial Lake Missoula did not drain completely each time the ice dam failed. The hypothesis of repeated draining of glacial Lake Missoula is consistent with the conclusions drawn by Chambers (1971, 1984) and Waitt (1980) at the Ninemile site. It is contrary, however, to the conclusions of Levish (1997) based on his study of similar glacial Lake Missoula sediments in Mission Valley. He argued that these sediments show no evidence of repeated subaerial exposure and that the silt beds at the base of rhythmic beds could be attributed to episodic surging of the Flathead lobe of the Cordilleran ice sheet, which increased sedimentation in Mission Valley. Levish did not describe any features at the contacts between units that would indicate subaerial exposure, thus we assume that his interpretation of continuous sedimentation is correct. Levish’s interpretations are sedimentologically plausible, but there are two other explanations for rhythmic sedimentation with no evidence of subaerial exposure that would be more consistent with evidence of repeated glacial Lake Missoula draining found elsewhere in the basin. First, it is Author's personal copy 78 M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 possible that the Mission Valley sediments were deposited at a different time than the sediments at the Ninemile and rail line sites; Levish’s optical ages (19.2e16.0 ka ago) would seem to support this interpretation. Levish argued on the basis of regional topography, however, that no more than approximately 100 years of sediment could be missing from the top of the record, implying that the exposures represent the later phases of glacial Lake Missoula, as do the sediments at the Ninemile and rail line sites. Second, Levish’s sites are in the deepest part of the glacial Lake Missoula basin and thus conceivably remained inundated when part of the lake drained. Clarke et al. (1984) considered this possibility when modelling glacial Lake Missoula outburst floods and found that not all models resulted in complete lake drainage. Some model runs left up to 22 percent of the water in the lake. A water depth of greater than 220 m, approximately 35 percent the maximum lake depth, would have inundated most of the exposures in Mission Valley (Levish, 1997; Smith, 2006). Significant fluctuations in water level at these sites, caused by partial drainage, may explain the cyclicity of the units and the rippled sand and silt facies. In contrast, the rail line and Ninemile sites require a minimum lake depth of about 370 m, or approximately 60 percent of the maximum lake depth, to remain inundated during a potential partial draining and thus would more likely be exposed during such events. Although there is strong evidence for repeated draining of glacial Lake Missoula in both the rail line and Ninemile sections, we cannot conclusively demonstrate that these drainings were complete or catastrophic. Excellent preservation of sediment at the two sites suggests that flow out of the basin at these localities did not significantly erode the lake floor. Hydraulic modelling by Alho et al. (2010) indicates that the sediments at the rail line section could be preserved during most lake drainings, even during higherenergy floods. It is likely, however, that the sediments at Ninemile would only be preserved during smaller, less energetic lake draining events (Alho et al., 2010), which is consistent with our optical ages that situate these exposures toward the end of the existence of glacial Lake Missoula (see Section 4.2). 4.2. Chronology Radiocarbon ages associated with the advance of the Cordilleran ice sheet into eastern Washington, with glacial Lake Missoula flood sediments in Oregon, with low salinity anomalies inferred from freshwater diatom abundances off the southern Oregon coast that have been attributed to glacial Lake Missoula flooding, and with glacial Lake Missoula sediment in the North Pacific all place the onset of glacial Lake Missoula flooding at or after 23.0 to 19.0 ka ago2 (Clague et al., 1980; Benito and O’Connor, 2003; Lopes and Mix, 2009; Gombiner et al., 2010). Based on varve counts and optical dating of the clay portion of glacial Lake Missoula varves in Mission Valley, Levish (1997) concluded that the lake existed from approximately 19.2e16.0 ka ago. Similarly, on the basis of a radiocarbon age and varve counts, Atwater (1986) argued that the 89 glacial Lake Missoula floods he identified occurred over a period of 2000e3000 years between 19.4 and 14.7 ka ago. Mount St. Helens set S (Sg and So) tephra, dated to between 18.5 and 13.3 ka ago (Mullineaux et al., 1975, 1978; Crandell et al., 1981; Baker and Bunker, 1985; Waitt, 1985; Clynne et al., 2008) lies at the top of one flood bed, at least 11 flood beds from the top of slackwater flood sediment sequences in southern Washington (Waitt, 1980, 2 All calibrated radiocarbon ages discussed are reported directly from the source or have been calibrated with OxCal 4.1 using the IntCal09 calibration curve (Bronk Ramsey, 2009; Reimer et al., 2009). 1985). Using this tephra and paleomagnetic secular variation records from three slackwater sediment exposures in Washington, Clague et al. (2003) placed the period of glacial Lake Missoula flooding between either 18.5 and 13.1 or 21.0 and 16.1 ka ago, depending on the age of the tephra and the number of years between floods. Radiocarbon ages on turbidites in the North Pacific extend flooding to between 13.0 and 12.6 ka ago (Zuffa et al., 2000). The last flood from glacial Lake Missoula, however, must have occurred before approximately 13.7e13.4 ka ago (Kuehn et al., 2009), when Glacier Peak tephras G and B blanketed parts of Washington and Montana, including Mission Valley (Fryxell, 1965; Porter, 1978; Mehringer et al., 1984; Foit et al., 1993; Sperazza et al., 2002; Hendrix et al., 2004; Kuehn et al., 2009; Hofmann and Hendrix, 2010). Hofmann and Hendrix (2010) recovered a pine needle from a varved sediment sequence in Flathead Lake in northern Montana; it yielded an age of 14,150 150 yr BP. They inferred that this varve sequence, which dates back to at least 14,475 150 yr BP, was deposited in a proglacial lake dammed by a terminal moraine, the Polson moraine, that was built after glacial Lake Missoula ceased to exist. The three new optical ages reported in this paper contribute to the discussion of the age and duration of glacial Lake Missoula and its outburst floods. The stratigraphic positions of the optical ages are shown in Figs. 2 and 5. The ages indicate that the Ninemile section is slightly older than the rail line section, consistent with the stratigraphy, which shows that the lower beds at rail line are similar to most beds at the Ninemile site. The two ages at the rail line site do not differ statistically when their analytical uncertainties are taken into account at two standard deviations, although the mean ages are stratigraphically reversed. We see no reason to favour one age over the other and thus adjust the age of the upper sample to that of the lower by assuming that w100 years separate the two dated horizons. With this adjustment, the weighted mean of the two ages, referenced to the lower sample, is 13.5 0.5 ka (Fig. 5). The main potential source of uncertainty in optical dating arises from the assumption that effective bleaching of the relevant electron traps resets the measured luminescence signal of all the grains immediately before final burial. Anomalously old ages would arise if a significant number of electron traps had not been emptied before deposition and burial. In particular, dating of glaciolacustrine sediments can be problematic because the grains are commonly transported in turbid water (Berger et al., 1987; Berger, 1988; Lian and Hicock, 2001). Our strategy was to avoid this problem by dating sand deposited in fluvial environments on the exposed floor of glacial Lake Missoula between ponding events. Our supposition was that the sand grains would be well exposed to sunlight in this environment before being buried. Rendell et al. (1994) concluded that the optical signal from quartz and feldspar grains in relatively clear water approximately 10 m deep is thoroughly reset in 3 h. If, however, the water is turbid, as is common in proglacial environments, the optical signal might not be reset. Ditfelsen (1992) found that feldspar grains only 75 cm deep in turbid water are not reset after 20 h of exposure to light. The problem is exacerbated by the fact that fluvial grains are not always equally reset e coarser grains are more likely to be reset than finer ones (Murray et al., 1995; Olley et al., 1998). The sand grains that we dated, however, were probably deposited in water no deeper than 10 cm. The sediments sampled for dating came from thin sheets, rather than thick channel deposits, and were more likely deposited by non-channelized sheet flow on the exposed lake floor than in channels. The sands are well sorted and thus were probably deposited in relatively clear water. The radial plots (Fig. 9) do not display multiple age populations that would indicate a significant number of grains had not been properly reset, as would be expected Author's personal copy M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 in turbid water, thus reaffirming our interpretation of the depositional environment of these facies. If these sediments had been deposited by turbidity currents, we would expect a larger spread (over-dispersion) in the single-aliquot De values. It is possible that our optical ages underestimate the true burial ages of the sediments of interest, in spite of the fact that our quartz samples passed all quality-control tests mentioned above. Reports of this scenario are rare, but one example was provided recently by Steffen et al. (2009) who attempted to date quartz collected from alluvial fan and terrace sediments in Peru using a SAR protocol similar to the one that we used in this study. Steffen et al. (2009) concluded that their calculated quartz ages were too low when compared to independent age information, probably due to the influence of an unstable component in the measured luminescence signal. This unwanted component can be seen in their luminescence decay data, and it is especially evident when compared to that measured from a standard, well-behaved quartz sample (Steffen et al., 2009, their Fig. 9). It is clear, however, that the luminescence decay data recorded from our samples (a representative curve is shown in Fig. 8B) closely resembles that of the standard quartz sample; both are dominated by the thermally stable fast component over the first w2 s of stimulation. It is therefore unlikely that our samples suffer from this effect. Despite these favourable results, additional confidence in our optical ages could be attained via three supplementary methods: (1) comparison of our ages with those derived from chemically and physically similar quartz sediment in the region for which the age has been determined previously by an independent method or methods; (2) the analysis of single grains of quartz, and subsequently looking for and eliminating data derived from grains that show abnormal luminescence behaviour (cf. Jacobs et al., 2006; Demuro et al., 2008). Additionally, if single-grain ages can be successfully determined, then the finite mixture model (Roberts et al., 2000; Jacobs and Roberts, 2007; Arnold and Roberts, 2009) may be applied to distinguish age populations, if there are any, from the sample. Single-grain analysis may, however, be impractical due to the sensitivity of the quartz in the region; and (3) comparison of our quartz ages with those derived from the feldspar fractions of the samples (cf. Steffen et al., 2009) after correction for anomalous fading. The three optical ages lie within the range of ages that constrain the time when glacial Lake Missoula could exist (21.4e13.4 ka ago). They are near the young end of this age range, which is consistent with the stratigraphy (Smith, 2006). The rail line samples, for example, are from beneath the 25th- and 27th-to-the-last glacial Lake Missoula sediment units there. Three wells drilled on the surface adjacent to the top of the rail line section indicate that glacial Lake Missoula sediments extend another 30e40 m below the base of the section (www.mbmggwic. mtech.edu). The units at rail line systematically increase in thickness downward and this trend probably continues below the base of the section. Thus a reasonable estimate of the number of units below the base of the section, based on the average thickness of the lowest 5 units (0.80 m), is 38e50, for a total of 69e81 units in the Missoula basin. These numbers are consistent with Levish (1997) and Atwater (1986) estimates of, respectively, the number of glacial Lake Missoula units and flood events. The total number of varves exposed at the rail line section, based on the average count for each unit, adding a reasonable number of varves for the disturbed units in the middle of the section, and assuming that the lower silt facies capped by clay is one varve, is 732. The total number of varves at the Ninemile section is 583. These are minimum estimates, because some varves probably were eroded from the top of each unit and because they do not include the length of time it took the ice dam to re-establish itself and the 79 lake to refill to the elevations of the sections. Ice-wedge casts can commence growth within a year after a surface is exposed and expand up to 3 cm per year (Mackay and Burn, 2002), thus indicating that some surfaces were exposed for a few years. Estimated refilling times for glacial Lake Missoula range from w20 years to 110 years. Atwater (1986) counted the number of varves between successive glacial Lake Missoula flood beds in a sequence of glacial Lake Columbia sediments. The numbers decrease from 45 to 55 near the base of the sequence to two between the last two flood beds. Similarly, Waitt (1984, 1985) counted 20e55 varves between glacial Lake Missoula flood beds in three exposures in Idaho and Washington. Many of these counts are minima for the number of years between floods because they do not include varves eroded by the floodwaters. Waitt (1985) calculated a refilling time for a maximum glacial Lake Missoula of less than 65 years. He based this estimate on the assumption that the rate of discharge into glacial Lake Missoula during the Fraser Glaciation was twice the present-day rate of discharge into the basin. He also estimated that it would take 40 years to fill glacial Lake Missoula to half its maximum volume. Waitt (1985) estimates of refilling times seem reasonable in light of the glacial Lake Columbia varve counts of Waitt (1984, 1985) and Atwater (1986). Levish (1997) counted 20e107 varves per unit in glacial Lake Missoula sediments in Mission Valley; most units have 30e60 varves. Assuming that the cyclicity of the units in Mission Valley corresponds to the draining cycle of glacial Lake Missoula, Levish’s data provide constraints on glacial Lake Missoula refilling times. Precise stratigraphic correlation of the rail line section and the upper part of Levish's (1997) Landslide Bend section is not possible, but based on our previous discussion, we argue that these exposures record the same time interval. In an attempt to improve our estimate of the age of the rail line sediments, we attempted to correlate the 31 rail line units and the last 41 Landslide Bend units based on the number of varves per unit. In this scenario, all units at the rail line site have fewer varves than corresponding units at Landslide Bend owing to erosion during lake draining. Some gaps between units at rail line are required to make this scenario feasible. The last 41 units at Landslide Bend record 1348 years of glacial Lake Missoula sedimentation. If the overlap is valid, 616 varves are missing from the rail line site, an average of 20 varves per unit. It is likely, however, that there are also missing units at the top of the rail line section because of erosion and weathering. Using this number and the weighted mean of the two optical ages, the base and top of the rail line section would date to, respectively, 13.7 0.5 and 12.4 0.5 ka ago. We make a similar provisional match of the 34 Ninemile units with units 18e51, numbered from the top, at Landslide Bend, which record 1505 years of glacial Lake Missoula sedimentation. Assuming this amount of time is recorded at Ninemile, the top of that section would date to approximately 13.6 0.6 ka ago. Our chronology accords with the known maximum age for the advance of the Cordilleran ice sheet into northern Idaho (21.4e19.6 ka; Clague et al., 1980) and with an age that pre-dates glacial Lake Missoula flooding in Oregon (23.3e22.3 ka; Benito and O’Connor, 2003). It is consistent with radiocarbon ages on glacial Lake Missoula sediment in the Pacific Ocean that indicate flooding occurred between 19.6 and 12.6 ka ago (Zuffa et al., 2000). Although on the young side, our chronology is consistent with Smith's (2006) interpretation that the glacial Lake Missoula rhythmic silt and clay deposits date to the later stages of the lake. Waitt (1980, 1985) inferred, and Atwater (1987) attempted, bed-for-bed correlations between beds at Ninemile and, respectively, the Touchet Beds and alternating glaciolacustrine and glacial Lake Missoula flood beds in glacial Lake Columbia. Based on the age of the set S tephra, known limits of the Cordilleran ice sheet advance and retreat, and the Author's personal copy 80 M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 estimated period between floods, Waitt (1985) postulated that glacial Lake Missoula existed for 2000e2500 years between w18.8 and 14.2 ka ago, which is fairly consistent with our chronology. Based on varve counts and constrained by a radiocarbon age in glacial Lake Columbia sediment, Atwater (1986) proposed that the Ninemile beds correlate with flood beds in glacial Lake Columbia that were deposited during the early half of his record (19.4ew17.1 ka), which is older than the inferred ages of our sections. Our chronology corresponds well with the younger of the intervals proposed by Clague et al. (2003) based on paleomagnetic secular variation correlations and different ages of the Mount St. Helens set S tephra (w18.5e13.1 ka). The inferred ages of the two exposures are considerably younger than the optical ages of Levish (1997; 19.2e16.0 ka) and Lopes and Mix (2009) chronology for low salinity anomalies in the Pacific Ocean that are likely due to inputs of water from glacial Lake Missoula (19.0e17.0 ka). Levish dated glaciolacustrine sediments, and it seems likely that a significant number of grains in his samples were not sufficiently reset prior to burial, leading to apparently old ages. Radiocarbon-dated material in the cores analysed by Lopes and Mix (2009) could be considerably older than the sediment in which it lies. Our chronology is also not consistent with Hofmann and Hendrix's (2010) calibrated radiocarbon age of 14,150 150 yr BP from glaciolacustrine sediments in Flathead Lake. It is possible, if not likely, that the needle they dated is older than the enclosing sediments. Notably, the age assigned to the top of the rail line section is younger than the most likely age for Glacier Peak G and B tephras (13.7e13.4 ka; Kuehn et al., 2009) before which glacial Lake Missoula had ceased to exist. This discrepancy may reflect our inability to precisely define the intervals represented by these two exposures because of the amount of time missing from each unit due to erosion and lake refilling. The sediment at the rail line site was deposited near the end of the Fraser Glaciation. As the ice sheet began to retreat, a thinning ice dam would have produced more frequent floods, decreasing the flood recurrence interval and thus the number of years per unit toward the top of the exposures. Unfortunately, there is no way to accurately model this decreasing recurrence interval. 5. Summary The rail line section in Missoula, Montana, exposes 29 units of rhythmically bedded sand, silt, and clay similar to other deposits that have been attributed to deposition in glacial Lake Missoula. Each of the units records partial or complete emptying of glacial Lake Missoula, and the entire sequence spans approximately 1350 years. The Ninemile section exposes 34 units of rhythmically bedded sand, silt, and clay and spans approximately 1500 years. Recurrent draining and subaerial exposure of the lake floor at both sites are indicated by unconformities, desiccation, possible icewedge casts, and fluvial gravel and sand beds. Three new optical ages limit the time of marine oxygen isotope stage 2 glacial Lake Missoula flooding. Based on a tentative correlation between our two sites and Levish's (1997) Landslide Bend site, the Ninemile section spans the period 15.1 to 13.6 0.6 ka ago, and the rail line section spans the period 13.7 to 12.4 0.5 ka ago. Acknowledgements Our research was supported by the Natural Sciences and Engineering Research Council (NSERC) of Canada through Discovery grants to Clague and Lian and through an NSERC PGS B Scholarship to Hanson. M. Al Suwaidi, J. Dykstra, and C. Reiss assisted in the field, and N. Cox, L. Day, and W. Moon assisted with analyses in the Luminescence Dating Laboratory at University of the Fraser Valley. Thoughtful and careful reviews by V. Baker and an anonymous reviewer greatly improved the paper. References Adamiec, G., Aitken, M.J., 1998. Dose-rate conversion factors: update. Ancient TL 16, 37e49. Aitken, M.J., 1985. Thermoluminescence Dating. Academic Press, New York. Alho, P., Baker, V.R., Smith, L.N., 2010. Paleohydraulic reconstruction of the largest glacial Lake Missoula draining(s). Quaternary Science Reviews 29, 3067e3078. Allison, I.S., 1978. Late Pleistocene sediments and floods in the Willamette valley. The Ore Bin 40, 177e191. and 193e202. Arnold, L.J., Roberts, R.G., 2009. Stochastic modelling of multi-grain equivalent dose (De) distributions: implications for OSL dating of sediment mixtures. Quaternary Geochronology 4, 204e230. Ashley, G.M., 1975. Rhythmic sedimentation in glacial Lake Hitchcock, Massachusetts-Connecticut. In: Jopling, A.V., McDonald, B.V. (Eds.), Glaciofluvial and Glaciolacustrine Sedimentation. Society of Economic Paleontologists and Mineralogists Special Paper, vol. 23, pp. 304e320. Ashley, G.M., 2002. Glaciolacustrine environments. In: Menzies, J. (Ed.), Modern and Past Glacial Environments. Butterworth-Heinemann Publications, Oxford, pp. 335e362. Atwater, B.F., 1984. Periodic floods from glacial Lake Missoula into the Sanpoil Arm of glacial Lake Columbia, northeastern Washington. Geology 12, 464e467. Atwater, B.F., 1986. Pleistocene glacial lake deposits of the Sanpoil River valley, northeastern Washington. U.S. Geological Survey Bulletin 1661, 1e39. Atwater, B.F., 1987. Status of glacial Lake Columbia during the last floods from glacial Lake Missoula. Quaternary Research 27, 182e201. Baker, V.R., 1973. In: Paleohydrology and Sedimentology of Lake Missoula Flooding in Eastern Washington. Geological Society of America Special Paper, vol. 144. Baker, V.R., Bunker, R.C., 1985. Cataclysmic late Pleistocene flooding from glacial Lake Missoula: a review. Quaternary Science Reviews 4, 1e41. Benito, G., O’Connor, J.E., 2003. Number and size of last-glacial Missoula floods in the Columbia River valley between the Pasco Basin, Washington, and Portland, Oregon. Geological Society of America Bulletin 115, 624e638. Berger, G.W., 1988. Dating Quaternary events by luminescence. In: Easterbrook, D.J. (Ed.), Quaternary Sediments. Geological Society of America Special Paper, vol. 227, pp. 13e50. Berger, G.W., Clague, J.J., Huntley, D.J., 1987. Thermoluminescence dating applied to glaciolacustrine sediments in central British Columbia. Canadian Journal of Earth Sciences 24, 425e434. Bretz, J.H., 1923. Glacial drainage on the Columbia Plateau. Geological Society of America Bulletin 34, 573e608. Bretz, J.H., 1925. The Spokane flood beyond the Channeled Scablands. Journal of Geology 33, 97e115. and 236e259. Bretz, J.H., 1928. Bars of Channeled Scabland. Geological Society of America Bulletin 39, 643e701. Bretz, J.H., 1929. Valley deposits immediately east of the Channeled Scabland of Washington. Journal of Geology 37, 393e427. and 505e541. Bretz, J.H., 1969. The Lake Missoula floods and the Channeled Scablands. Journal of Geology 77, 505e543. Bretz, J.H., Smith, H.T.U., Neff, G.E., 1956. Channeled Scabland of Washington: new data and interpretations. Geological Society of America Bulletin 67, 957e1049. Bronk Ramsey, C., 2009. Bayesian analysis of radiocarbon dates. Radiocarbon 51, 337e360. Brown, K.B., McIntosh, J.C., Baker, V.R., Gosch, D., 2010. Isotopically-depleted late Pleistocene groundwater in Columbia River Basalt aquifers: evidence for recharge of glacial Lake Missoula floodwaters. Geophysical Research Letters 37. doi:10.1029/2010GL044992. Chambers, R.L., 1971. Sedimentation in glacial Lake Missoula. M.Sc. Thesis, University of Montana, Missoula, MT. Chambers, R.L., 1984. Sedimentary evidence for multiple glacial lakes Missoula. In: McBane, J.D., Garrison, P.B. (Eds.), Northwest Montana and Adjacent Canada. Montana Geological Society, Billings, pp. 189e199. Clague, J.J., Armstrong, J.E., Mathews, W.H., 1980. Advance of the late Wisconsinan Cordilleran ice sheet in southern British Columbia since 22,000 yr BP. Quaternary Research 13, 322e326. Clague, J.J., Barendregt, R., Enkin, R.J., Foit Jr., F.F., 2003. Paleomagnetic and tephra evidence for tens of Missoula floods in southern Washington. Geology 31, 247e250. Clarke, G.K.C., Mathews, W.H., Pack, R.T., 1984. Outburst floods from glacial Lake Missoula. Quaternary Research 22, 289e299. Clynne, M.A., Calvert, A.T., Wolfe, E.W., Evarts, R.C., Fleck, R.J., Lanphere, M.A., 2008. The Pleistocene eruptive history of Mount St. Helens, Washington, from 300,000 to 12,800 years before present. In: Sherrod, D.R., Scott, W.E., Stauffer, P.H. (Eds.), A Volcano Rekindled: The Renewed Eruption of Mount St. Helens, 2004e2006. U.S. Geological Survey Professional Paper, vol. 1750, pp. 593e627. Craig, R.G., 1987. Dynamics of a Missoula flood. In: Mayer, L., Nash, D. (Eds.), Catastrophic Flooding. Allen and Unwin, London, pp. 305e332. Crandell, D.R., Mullineaux, D.R., Rubin, M., Spiker, E., Kelley, M.L., 1981. Radiocarbon Dates from Volcanic Deposits at Mount St. Helens. U.S. Geological Survey OpenFile Report, Washington. 81e844. Demuro, M., Roberts, R.G., Froese, D.G., Arnold, L.J., Brock, F., Bronk Ramsey, C., 2008. Optically stimulated luminescence dating of single and multiple grains of Author's personal copy M.A. Hanson et al. / Quaternary Science Reviews 31 (2012) 67e81 quartz from perennially frozen loess in western Yukon Territory, Canada: comparison with radiocarbon chronologies for the late Pleistocene Dawson tephra. Quaternary Geochronology 3, 346e364. Denlinger, R.P., O’Connell, D.R.H., 2010. Simulations of cataclysmic outburst floods from Pleistocene glacial Lake Missoula. Geological Society of America Bulletin 122, 678e689. Ditfelsen, C., 1992. Bleaching of K-feldspars in turbid water suspensions: a comparison of photo- and thermoluminescence signals. Quaternary Science Reviews 11, 33e38. Duller, G.A.T., Bøtter-Jensen, L., Murray, A.S., 2000. Optical dating of single sandsized grains of quartz: sources of variability. Radiation Measurements 32, 453e457. Foit Jr., F.F., Mehringer Jr., P.J., Sheppard, J.C., 1993. Age, distribution, and stratigraphy of Glacier Peak tephra in eastern Washington and western Montana, United States. Canadian Journal of Earth Sciences 30, 535e552. Fritz, W.J., Smith, G.A., 1993. Revisiting the Ninemile section: problems with relating glacial Lake Missoula stratigraphy to the Scablands-floods stratigraphy. Eos (Transactions American Geophysical Union) 74, 302. Fryxell, R., 1965. Mazama and Glacier Peak volcanic ash layers: relative ages. Science 147, 1288e1290. Galbraith, R.F., 2010. On plotting OSL equivalent doses. Ancient TL 28, 1e9. Galbraith, R.F., Roberts, R.G., Laslett, G.M., Yoshida, H., Olley, J.M., 1999. Optical dating of single and multiple grains of quartz from Jinmium rock shelter, northern Australia. Part I: experimental design and statistical models. Archaeometry 41, 339e364. Gao, C., 2005. Ice-wedge casts in Late Wisconsinan glaciofluvial deposits, southern Ontario, Canada. Canadian Journal of Earth Sciences 42, 2117e2126. Gombiner, J., Hendy, I.L., Hemming, S.R., Fleisher, M.Q., Pierce, E., Mesko, G., Dale, C.L., 2010. Spatial and temporal variation of the last ice age mega-floods in the Pacific Northwest: sediment provenance using single-aliquot K/Ar dating. American Geophysical Union 2010 Fall Meeting. American Geophysical Union, San Francisco, California, Abstract PP21A-1663. Harry, D.G., Gozdzik, J.S., 1988. Ice wedges: growth, thaw transformation, and palaeoenvironmental significance. Journal of Quaternary Science 3, 39e55. Hendrix, M.S., Bondurant, A.K., Timmerman, G., Salmon III, E.L., 2004. Preliminary results from geologic mapping and sedimentologic analysis of late Pleistocene glacial and post-glacial deposits, southern Flathead and northern Mission valleys, western Montana. Geological Society of America Abstracts with Programs 36, 287. Hofmann, M.H., Hendrix, M.S., 2010. Depositional processes and the inferred history of ice-margin retreat associated with the deglaciation of the Cordilleran ice sheet: the sedimentary record from Flathead Lake, northwest Montana, USA. Sedimentary Geology 223, 61e74. Jacobs, Z., Roberts, R.G., 2007. Advances in optically stimulated luminescence dating of individual grains of quartz from archeological deposits. Evolutionary Anthropology 16, 210e223. Jacobs, Z., Duller, G.A.T., Wintle, A.G., 2006. Interpretation of single grain De distributions and calculation of De. Radiation Measurements 41, 264e277. Jopling, A.V., Walker, R.G., 1968. Morphology and origin of ripple-drift cross-lamination, with examples from the Pleistocene of Massachusetts. Journal of Sedimentary Petrology 38, 971e984. Kuehn, S.C., Froese, D.G., Carrara, P.E., Foit Jr., F.F., Pearce, N.J.G., Rotheisler, P., 2009. Major- and trace-element characterization, expanded distribution, and a new chronology for the latest Pleistocene Glacier Peak tephras in western North America. Quaternary Research 71, 201e216. Levish, D.R., 1997. Late Pleistocene Sedimentation in Glacial Lake Missoula and Revised Glacial History of the Flathead Lobe of the Cordilleran Ice Sheet, Mission Valley, Montana. Ph.D. Thesis, University of Colorado, Boulder, CO. Lian, O.B., Hicock, S.R., 2001. Lithostratigraphy and limiting optical ages of the Pleistocene fill, Fraser valley, near Clinton, south-central British Columbia. Canadian Journal of Earth Sciences 38, 839e850. Lian, O.B., Roberts, R.G., 2006. Dating the Quaternary: progress in luminescence dating of sediments. Quaternary Science Reviews 25, 2449e2468. Lian, O.B., Hu, J., Huntley, D.J., Hicock, S.R., 1995. Optical dating studies of Quaternary organic-rich sediments from southwestern British Columbia and northwestern Washington State. Canadian Journal of Earth Sciences 32, 1194e1207. Lopes, C., Mix, A.C., 2009. Pleistocene megafloods in the northeast Pacific. Geology 37, 79e82. Lowe, D.R., LoPiccolo, R.D., 1974. The characteristics and origins of dish and pillar structures. Journal of Sedimentary Petrology 44, 484e501. Mackay, J.R., Burn, C.R., 2002. The first 20 years (1978e1979 to 1998e1999) of icewedge growth at the Illisarvik experimental drained lake site, western Arctic coast, Canada. Canadian Journal of Earth Sciences 39, 95e111. Mehringer, P.J., Sheppard, J.C., Foit Jr., F.F., 1984. The age of Glacier Peak tephra in west-central Montana. Quaternary Research 21, 36e41. Mullineaux, D.R., Hyde, J.H., Rubin, M., 1975. Widespread Late Glacial and postglacial tephra deposits from Mount St. Helens volcano, Washington. Journal of Research of the U.S. Geological Survey 3, 329e335. Mullineaux, D.R., Wilcox, R.E., Ebaugh, W.F., Fryxel, R., Rubin, M., 1978. Age of the last major Scabland flood of the Columbia Plateau in eastern Washington. Quaternary Research 10, 171e180. Murray, A.S., Wintle, A.G., 2000. Luminescence dating of quartz using an improved regenerative-dose protocol. Radiation Measurements 32, 57e73. Murray, A.S., Wintle, A.G., 2003. The single aliquot regenerative dose protocol: potential for improvements in reliability. Radiation Measurements 37, 377e381. 81 Murray, A.S., Olley, J.M., Caitcheon, G.G., 1995. Measurement of equivalent doses in quartz from contemporary water-lain sediments using optically stimulated luminescence. Quaternary Science Reviews 14, 365e371. Murton, J.B., French, H., 1993. Thaw modifications of frost-fissure wedges, Richards Island, Pleistocene Mackenzie Delta, western Arctic Canada. Journal of Quaternary Science 8, 185e196. Olley, J.M., Murray, A., Roberts, R.G., 1996. The effects of disequilibria in the uranium and thorium decay chains on burial dose rates in fluvial sediments. Quaternary Science Reviews 15, 751e760. Olley, J., Caitcheon, G., Murray, A., 1998. The distribution of apparent dose as determined by optically stimulated luminescence in small aliquots of fluvial quartz: implications for dating young sediments. Quaternary Geochronology 17, 1033e1040. Olley, J.M., Pietsch, T., Roberts, R.G., 2004. Optical dating of Holocene sediments from a variety of geomorphic settings using single grains of quartz. Geomorphology 60, 337e358. O’Connor, J.E., Baker, V.R., 1992. Magnitudes and implications of peak discharges from glacial Lake Missoula. Geological Society of America Bulletin 104, 267e279. O’Connor, J.E., Sarna-Wojcicki, A., Wozniak, K.C., Polette, D.J., Fleck, R.J., 2001. Origin, Extent, and Thickness of Quaternary Geologic Units in the Willamette Valley, Oregon. U.S. Geological Survey Professional Paper, vol. 1620. Pardee, J.T., 1910. The glacial Lake Missoula, Montana. Journal of Geology 18, 376e386. Pardee, J.T., 1942. Unusual currents in glacial Lake Missoula, Montana. Geological Society of America Bulletin 53, 1570e1599. Porter, S.C., 1978. Glacier Peak tephra in the north Cascade range, Washington: stratigraphy, distribution, and relationship to Lateglacial events. Quaternary Research 10, 30e41. Prescott, J.R., Hutton, J.T., 1994. Cosmic ray contributions to dose rates for luminescence and ESR dating: large depths and long-term time variations. Radiation Measurements 23, 497e500. Prescott, J.R., Hutton, J.T., 1995. Environmental dose rates and radioactive disequilibrium from some Australian luminescence dating sites. Quaternary Science Reviews 14, 439e448. Reimer, P.J., Baillie, M.G.L., Bard, E., Bayliss, A., Beck, J.W., Blackwell, P.G., Bronk Ramsey, C., Buck, C.E., Burr, G.S., Edwards, R.L., Friedrich, M., Grootes, P.M., Guilderson, T.P., Hajdas, I., Heaton, T.J., Hogg, A.G., Hughen, K.A., Kaiser, K.F., Kromer, B., McCormac, F.G., Manning, S.W., Reimer, R.W., Richards, D.A., Southon, J.R., Talamo, S., Turney, C.S.M., van der Plicht, J., Weyhenmeyer, C.E., 2009. IntCal09 and Marine09 radiocarbon age calibration curves, 0e50,000 years cal BP. Radiocarbon 51, 1111e1150. Rendell, H.M., Webster, S.E., Sheffer, N.L., 1994. Underwater bleaching of signals from sediment grains: new experimental data. Quaternary Science Reviews 13, 433e435. Roberts, R.G., Galbraith, R.F., Olley, J.M., Yoshida, H., Laslett, G.M., 1999. Optical dating of single and multiple grains of quartz from Jinmium rock shelter, northern Australia: part II, results and implications. Archaeometry 41, 365e395. Roberts, R.G., Galbraith, R.F., Yoshida, H., Laslett, G.M., Olley, J.M., 2000. Distinguishing dose populations in sediment mixtures: a test of single-grain optical dating procedures using mixtures of laboratory-dosed quartz. Radiation Measurements 32, 459e465. Rust, B.R., 1977. Mass flow deposits in a Quaternary succession near Ottawa, Canada: diagnostic criteria for subaqueous outwash. Canadian Journal of Earth Sciences 14, 175e184. Shaw, J., Munro-Stasiuk, M., Sawyer, B., Beaney, C., Lesemann, J.-E., Musacchio, A., Rains, B., Young, R.R., 1999. The Channeled Scabland: back to Bretz? Geology 27, 605e608. Shaw, J., Munro-Stasiuk, M., Sawyer, B., Beaney, C., Lesemann, J.-E., Musacchio, A., Rains, B., Young, R.R., 2000. The Channeled Scabland: back to Bretz? Geology 28, 576. Smith, L.N., 2006. Stratigraphic evidence for multiple drainings of glacial Lake Missoula along the Clark Fork River, Montana, USA. Quaternary Research 66, 311e322. Smith, N.D., Ashley, G., 1985. Proglacial lacustrine environment. In: Ashley, G.M., Shaw, J., Smith, N.D. (Eds.), Glacial Sedimentary Environments. Society of Economic Paleontologists and Mineralogists Short Course, vol. 16, pp. 135e216. Sperazza, M., Thomas, G., Hendrix, M.S., Moore, J.N., 2002. Record of late Pleistocene through Holocene climate change in a regional lake system: Flathead Lake basin, northwestern Montana. Eos (Transactions American Geophysical Union) 83, F941. Steffen, D., Preusser, F., Schlunegger, F., 2009. OSL quartz age underestimation due to unstable signal components. Quaternary Geochronology 4, 353e362. Waitt, R.B., 1980. About forty last-glacial Lake Missoula jökulhlaups through southern Washington. Journal of Geology 88, 653e679. Waitt, R.B., 1984. Periodic jökulhlaups from Pleistocene glacial Lake Missoula e new evidence from varved sediment in northern Idaho and Washington. Quaternary Research 22, 46e58. Waitt, R.B., 1985. Case for periodic, colossal jökulhlaups from Pleistocene glacial Lake Missoula. Geological Society of America Bulletin 96, 1271e1286. Wintle, A.G., 2008. Luminescence dating: where it has been and where it is going. Boreas 37, 471e482. Wintle, A.G., Murray, A.S., 2006. A review of quartz optically stimulated luminescence characteristics and their relevance in single-aliquot regeneration dating protocols. Radiation Measurements 41 396e391. Zuffa, G.G., Normark, W.R., Serra, F., Brunner, C.A., 2000. Turbidite megabeds in an oceanic rift valley recording jökulhlaups of late Pleistocene glacial floods of the western United States. Journal of Geology 108, 253e274.