5/24/2010 LABORATORY SAFETY RULES Laboratory Safety Always be safety conscious. Move about the laboratory in a safe manner. Report all accidents. No accident is too small to report. Know the location of all of the safety equipment in the laboratory 1 5/24/2010 Laboratory Safety Plan ahead. Become familiar with all of the health and safety hazards of equipment and chemicals in use. If you are not sure, ask. MSDS – more later Wear safety goggles at all times Acid Damage 2 5/24/2010 Base Damage Broken Glass 3 5/24/2010 Laboratory Safety Wear a lab apron when handling corrosive chemicals Laboratory Safety Use Bunsen burners only at the direction of the teacher, and do not leave unattended Use a hot plate to heat flammable liquids Confine long hair – Watch for open flames Only do experiments assigned Do not eat or drink while in lab Wear closed toed shoes 4 5/24/2010 Laboratory Safety Do not return unused chemicals to the stock container Ask teacher about proper disposal techniques Clean all glassware and the lab area before leaving Wash your hands before leaving lab Laboratory Safety Failure to follow rules will not be tolerated and will result in the immediate removal from lab DO NOT play around in Lab 5 5/24/2010 Glassware Broken Glass – Clean up immediately with a brush and pan Do not put broken glass in the regular trash can Before inserting glass tubing or thermometers into corks or stoppers apply lubricating grease to glassware Avoiding Burns Keep lab table free of books and papers Point test tubes away from ALL people while heating Hot glass looks just like cold glass. Use care when touching glass objects that have been heated 6 5/24/2010 Handling Chemicals To smell the contents of a container use a “wafting” technique as demonstrated by your teacher Electrical Precautions Before connecting equipment to a power source, examine all wiring for electrical defects and improper installation. Make sure that all equipment is properly grounded and that you are NOT. Make sure that your hands are dry; that the work area is dry. Be certain that the proper voltage is available. Follow directions. If you are unsure of any procedure, ask your teacher. 7 5/24/2010 Acid Safety Always check the reagent bottle which contained the acid, or ask your teacher about the dangers of the acid. Always have on safety goggles whenever acids are present. It is also a good idea to wear an apron too. When mixing acid and water, always pour the acid into the water. ACID TO WATER never the reverse Acid Safety Never disturb an unmarked substance because it may be an acid. If an acid comes in contact with your skin wash it with soap, because the soap will neutralize the acid. Always clean up any spilled acid as soon as possible. Never allow the acid to come into contact with your skin unless your teacher says has told you that it is okay. 8 5/24/2010 Fire Safety Keep all combustible materials away from open flames unless specifically instructed to place them in the flame. Keep head, hair, and all loose clothing away from an open flame. Never leave unattended anything that is being heated or reacting. Always turn off burner when not in use. Basic Chemistry Lab Equipment Pipette For exact volume measurement s of liquids. 9 5/24/2010 Basic Chemistry Lab Equipment Pipette filler There are several styles of fillers used to draw liquids into a pipette. Never draw a liquid into a pipette with your mouth. Basic Chemistry Lab Equipment Filter flask Used in conjunction with a vacuum connection to a water faucet to speed up filtration. 10 5/24/2010 Basic Chemistry Lab Equipment Erlenmeyer flask Used to contain reaction solutions. Basic Chemistry Lab Equipment Florence flask Used to boil liquids. 11 5/24/2010 Basic Chemistry Lab Equipment Volumetric flask Used to make solutions Basic Chemistry Lab Equipment Beaker Used to contain chemical reactions 12 5/24/2010 Basic Chemistry Lab Equipment Graduated cylinder Used to make accurate measurements of liquid volumes. Basic Chemistry Lab Equipment Evaporating dish Used to recover dissolved solids by evaporation. 13 5/24/2010 Basic Chemistry Lab Equipment Watch glass Similar to an evaporating dish. Can be used to cover beakers. Basic Chemistry Lab Equipment Support ring Used to support glassware above the lab table. 14 5/24/2010 Basic Chemistry Lab Equipment Utility clamp Used to hold large test type or Florence flask above the lab table. Basic Chemistry Lab Equipment Crucible & Cover Used as a container when something requires strong heating. 15 5/24/2010 Basic Chemistry Lab Equipment Crucible tongs For picking up crucibles and crucible covers ONLY Basic Chemistry Lab Equipment Wire gauze Will support glassware when placed across a support ring. 16 5/24/2010 Basic Chemistry Lab Equipment Striker Used to light a lab burner. Not a toy noisemaker during lab. Basic Chemistry Lab Equipment Mortar and Pestle To grind solids into powders. 17 5/24/2010 Basic Chemistry Lab Equipment Test tube holder To hold test tubes while heating. Basic Chemistry Lab Equipment Filter funnel When lined with filter paper, used to filter suspended solids from a liquid. 18 5/24/2010 Basic Chemistry Lab Equipment Wash bottle For washing solids out of a container when filtering. Basic Chemistry Lab Equipment Chemical spoon / Spatula To transfer solids from their original bottle to a scale for weighing. 19 5/24/2010 Basic Chemistry Lab Equipment Hose clamps Used to close hoses by pinching them together. Basic Chemistry Lab Equipment This is not a complete listing of all the equipment in our lab. Additional equipment is available, if needed for the exercise. 20 5/24/2010 NFPA 704 Hazard Identification System National Fire Protection Agency RED-- Flammability RED BLUE-- Health Hazard BLUE YELLOW-- Reactivity YELLOW WHITE- Special WHITEPrecautions Protective Gear Required NFPA 704 Hazard Identification System National Fire Protection Agency Hazard Rating 4 Severe 3 Serious 2 Dangerous 1 Minor 0 Slight 21 5/24/2010 Flammability Hazard Rating 4 3 2 1 0 = = = = = Severe – flash point <730C Serious – flash point < 1000C Dangerous – flash point b/t 100100-200 Minor – flash point >200oC Slight – will not burn Health Hazard Carcinogens Mutagens Cancer causing Cause mutations Can affect your future children Teratogens Affect developing fetuses 22 5/24/2010 Specific Hazards Corrosive materials Acids Bases Oxidizers Unstable compounds Reactivity Explosive materials Almost instantaneous release of large or small amounts of pressure, gas, and heat when subjected to sudden shock, pressure, or high temperature 23 5/24/2010 MSDS MSDS- Material Safety Data Sheets MSDSSheets-- Gives important information on chemicals such as: Product identification Hazardous components Physical data Fire and explosion Hazards Health hazards Fire and explosion data Spill and disposal procedures Protective equipment Storage and handling procedures Transportation data and additional information MSDS 24 5/24/2010 Section 1 Source and Nomenclature The name, address, and telephone number of the manufacturer or supplier of the product. The trade name and synonyms for a mixture of chemicals, a basic structural material, or for a process material NFPA Hazard Rating Section 1 25 5/24/2010 Section 2 Hazardous Ingredients Chemical or widely recognized common name of all hazardous ingredients The approximate percentage by weight or volume which each hazardous ingredient of the mixture bears to the whole mixture. Basis for toxicity for each hazardous material such as an established standard in appropriate units Section 2 26 5/24/2010 Section 3 Physical Data Boiling Point Melting Point Appearance Odor Etc. Section 3 27 5/24/2010 Section 4 Fire and Explosion Hazard Data Flammability and Reactivity Information What to do in case of emergency Section 4 28 5/24/2010 Section 5 Health Hazard Data Toxic level for total compound or mixture Effects of exposure, and emergency and firstfirstaid procedures Section 5 29 5/24/2010 Section 6 Reactivity Data Chemical stability Section 6 30 5/24/2010 Section 7 Spill or Leak Procedures Detailed procedures to be followed with emphasis on precautions to be taken in cleaning up and safe disposal Section 7 31 5/24/2010 Section 8 Special Protection Information Requirements for personal protective equipment, such as respirators, eye protection, protective clothing, and ventilation Section 8 32 5/24/2010 Section 9 Special Precautions Any other precautionary information Section 9 33