DEVELOPMENT OF THE PROCESS PARAMETER MAP FOR REFERENCE FREE PART ENCAPSULATION BY CEANI GUEVARA S.B., MECHANICAL ENGINEERING, 2000 MASSACHUSETTS INSTITUTE OF TECHNOLOGY SUBMITTED TO THE DEPARTMENT OF MECHANICAL ENGINEERING IN PARTIAL FULFILLMENT OF THE REQUIREMENTS FOR THE DEGREE OF MASTER OF SCIENCE IN MECHANICAL ENGINEERING AT THE MASSACHUSETTS INSTITUTE OF TECHNOLOGY BARKER JUNE2001 ~iMS CHUSETTS INSTIrUTE OFTECHNOLOGY C 2001 Massachusetts Institute of Technology JUL 16 2001 All rights reserved LIBRARIES -.- Author:.-.-. Certified by: Accepted by: Department of Mechanical Engineering May 11, 2001 ................. ....................... S a. S Sanjay E. Sarma Associate Professor of Mechanical Engineering Thesis Supervisor Ain A. Sonin Professor of Mechanical Engineering Chairman of the Graduate Thesis Committee Development of the Process Parameter Map for Reference Free Part Encapsulation by Ceani Guevara Submitted to the Department of Mechanical Engineering on May 11, 2001 in Partial Fulfillment of the Requirements for the Degree of Master of Science in Mechanical Engineering ABSTRACT A paradigm shift needs to occur so that manufacturing processes are able to simultaneously improve in quality, rate, and flexibility while reducing cost. Fixturing methods currently available represent an important constraint on manufacturing systems. The Reference Free Part Encapsulation (RFPE) concept, developed by Sarma and Wright, seems to be the paradigm shift required to improve the capabilities of the fixturing technology across the board. While Lee has proved the viability of the RFPE process experimentally, much work remains to be done before the process can complete the journey from idea to reality. Therein lies the motivation for this study: to establish a framework to understand RFPE, consolidate the existing knowledge, identify the critical factors that remain unexplored, determine the impact these factors have on the process, and thus develop a process parameter map of the RFPE concept. The following process parameters were identified: melt superheat temperature, mold preheat temperature, ejection temperature, cooling rate, packing pressure, aging, and alloy composition. These parameters were measured via metrics such as surface finish, porosity, dimensional accuracy, thermal drift, and rewelding strength. The RFPE Process Parameter Map was completed based on the information obtained through experimentation, analysis, and literature review. The melt superheat temperature, mold preheat temperature, packing pressure, and cooling have the potential to impact the precision of the system. These experiments have identified the process window within which the RFPE concept is not sensitive to variations in these process parameters. The ejection temperature, aging and alloy composition do not seem to have a significant impact on the precision of the process. The process parameter map forms a solid foundation from which future developments of the RFPE process can take place. Thesis Supervisor: Sanjay E. Sarma Title: Associate Professor of Mechanical Engineering Table of Contents CHAPTER 1: BACKGROUND AND MOTIVATION ............ 1.1. Role of Fixturing in Manufacturing.........................................................16 1.2. Functional Requirements of Fixturing.....................................................16 1.3. Current Fixturing Technology...................................................................19 1.3.1. 1.3.2. Modular Fixturing Systems ........................................................... Universal Fixturing Systems ........................................................ Conformable Clamps .................................................... 1.3.2.1. 19 20 20 Fluidized Bed................................................................ 21 1.3.2.2. 1.3.3. 15 1.3.2.3. Phase Change Material .................................................. Limitations of the Current Fixturing Technology .......................... 22 23 CHAPTER 2: REFERENCE FREE PART ENCAPSULATION....... 25 2.1. The Ideal Fixturing System.......................................................................25 2.2. The RFPE Concept .................................................................................... 26 2.3. Capabilities of RFPE ............................................................................... 28 2.4. Three Machining Strategies: 2D, 21/2 D, and 3D Milling ......................... 29 2.4.1. 2.4.2. 2.4 .3. 2.5. 2D M illing .................................................................................... 2 2D Milling .................................................................................. 3D M illing .................................................................................... 29 30 31 Motivation...................................................................................................32 CHAPTER 3: FRAMEWORK TO ANALYZE AND DEVELOP RFPE ................................................................................. 33 33 3.1. The Building Blocks of a System ............................................................. 3.2. Design and Process Parameters................................................................33 3.3. A Structured Approach to Developing the RFPE Process.....................36 CHAPTER 4: SYSTEMATIC EVALUATION OF PARAMETERS AND METRICS................ 4.1. 37 M etrics of the RFPE Process ................................................................... 37 4.1.1. 4.1.2. 4.1.3. 4.1.4. 4.1.5. Surface Finish................................................................................ Porosity........................................................................................... Dimensional Accuracy .................................................................... Thermal Drift.................................................................................. Rewelding Strength ........................................................................ 37 38 39 39 40 Process Parameters: an Overview........................................................... 41 4.2.1. Temperature.................................................................................... 4.2.1.1. Melt Superheat............................................................... 4.2.1.2. Mold Preheat Temperature ............................................ 4.2.1.3. Cooling Rate ................................................................. 4.2.1.4. Ejection Temperature.................................................... Packing Pressure............................................................................. Aging ............................................................................................. Alloy Composition ........................................................................ 42 42 43 43 44 44 47 47 4.3. The A Priori RFPE Process Parameter M ap ........................................... 48 4.4. Next Steps .................................................................................................. 50 4.2. 4.2.2. 4.2.3. 4.2.4. CHAPTER 5: EXPERIMENTAL PLAN................................................. 51 5.1. Objectives of the Experiments.................................................................. 51 5.2. Experimental Apparatus........................................................................... 51 5.2.1. 5.2.2. 51 5.3. The Mold ......................................................................................... Instrumentation................................................................................52 Experimental Procedure ............................................................................ 5.3.1. 5.3.2. 5.3.3. 5.3.4. 5.3.5. 5.3.6. 53 The Effect of and the Interaction between Melt Superheat and Mold Preheat Temperature ............................................................. 54 The Effect of Cooling Rate ............................................................ 55 The Effect of Ejection Temperature ............................................... 55 Aging Effects.................................................................................. 55 The Interaction between Packing Pressure and Cooling Rate........56 The Effects of Alloy Composition ................................................. 56 CHAPTER 6: THEORETICAL BACKGROUND FOR EXPERIMENTAL ANALYSIS ..................................... 6.1. The Impact of Surface Finish...................................................................57 6.1.1. 6.1.2. 6.1.3. 6.2. 57 58 The Mechanism of Surface Deflection Under Load ...................... Quantification of the Possible Deflection of the Asperities .......... 59 The Variables for Roughness Measurements as it Relates to . 60 D eflection ...................................................................................... Im pact of Porosity..................................................................................... 6.2.1. 6.2.2. 6.2.3. 61 61 Form ation of Porosity..................................................................... Classification of porosity: Macroporosity and Microporosity .......... 62 63 Porosity and the RFPE Process .................................................... 6.3. Temperature Drop from the Mold Cavity to the Thermocouple Well...63 6.4. Variations in Cooling Rate.......................................................................65 CHAPTER 7: EXPERIMENTAL RESULTS .................. 67 7.1. The Effect of Melt Superheat and Mold Preheat Temperature................67 7.2. The Effect of Ejection Temperature ......................................................... 7.3. The Effect of Cooling Rate.......................................................................69 7.4. Aging Effects.............................................................................................. 70 7.5. The Interaction between Packing Pressure and Cooling Rate .............. 71 7.6. The Effects of Alloy Composition........................................................... 71 69 CHAPTER 8: THE RFPE PROCESS PARAMETER MAP........ 73 CHAPTER 9: FUTURE WORK............................................................... 77 9.1. Study of Design Parameters.................................................................... 77 9.2. Design of a Field Trial Prototype ............................................................. 77 9.3. Development of a Rapid Prototyping Center ......................................... 78 APPENDIX A: AN INTRODUCTION TO THE RFPE DESIGN PARAM ETERS ........................................................... A.1. Parameters Affecting the Alloy Storage and Delivery........................... 83 A.1.1. The Reservoir ................................................................................. A. 1.1.1. Reservoir Temperature.................................................. 83 83 A.1.1.2. Proportion of New to Recycled Alloy .......................... A. 1.1.3. Reservoir Construction ................................................. Alloy Delivery............................................................................... A.l.2.1. Injection Pressure...........................................................86 84 84 85 A.1.2.2. Shot Size ........................................................................ 86 A.1.2.3. A.1.2.4. A.1.2.5. A.l.2.6. A.1.2.7. Rate of Change in Pressure ........................................... 87 Pressure on Opposing Sides of the Injection Piston .......... 87 Inertia Effects..................................................................87 Transfer Tubing Design.................................................87 Partial Blockages of the Metal Stream...........................88 A.1.2. A.2. 81 Parameters Affecting the Introduction and Behavior of Alloy Inside the Mold 88 A.2.1. Gate Velocity..................................................................................88 A.2.2. Cooling Direction...........................................................................89 A.2.3. Heating and Cooling of the Mold.................................................. 89 A.2.4. Mold Surface Finish...................................................................... 89 A.2.5. A.2.6. Mold Material Selection............................................................... Mold Locking Pressure ................................................................. 90 90 A.2.7. Mold Vents .................................................................................... 90 A.2.8. Compatibility of Gate and Machined Section Geometry .............. 91 REFERENCES...................................................................................... 93 List of Figures Figure 1: The lack of locating stability or deterministic workpiece location can introduce variations in the position or the orientation of the part. Even a small variation in orientation can cause a significant error in the precision of th e w ork p iece ..................................................................................................................... 17 Figure 2: Excessive clamping loads can deform a workpiece. This deformation can affect both the dimensional accuracy and the structural integrity of the w orkpiece ............................................................................................. 18 Figure 3: The inability of a workpiece to transmit the localized fixturing support force throughout the part causes a loss of dimensional accuracy. In effect, the workpiece deflection under machining loads results in a lack of to tal restraint. ..................................................................................................................... 18 Figure 4: Conformable clamp fixturing ...................................................................... 21 Figure 5: Fluidized bed fixturing .................................................................................. 22 Figure 6: Phase change fixturing .................................................................................. 23 Figure 7: The Reference Free Part Encapsulation (RFPE) Process ............................. 27 Figure 8: Sample parts produced with RFPE................................................................28 Figure 9: 2D M illing .................................................................................................... 29 Figure 10: 2!/2D M illing ................................................................................................ 30 Figure 11: 3D M illing .................................................................................................. 31 Figure 12: A plot of the relationship between each process parameter and each metric for a system facilitates an understanding of the system characteristics.....................................................................................................................34 Figure 13: Each process parameter typically impacts multiple metrics of the same system. Often, there is no optimum setting for the process parameter. Therefore, tradeoffs between the metrics are required. ................................................. 34 Figure 14: Design parameters determine the range of each process parameter that is feasible for each implementation of the concept................................................35 Figure 15: For the particular implementation modeled in this diagram, the choice was made to have the design parameters favor Metric #1 slightly over M etric # 2 ............................................................................................................................ 36 Figure 16: A surface finish can be categorized by the amount that it deviates from a perfectly flat surface. There are three ways in which this deviation occurs: form error, waviness, and roughness...............................................................38 Figure 17: H ow therm al drift occurs............................................................................. 40 Figure 18: Creation of weldline test specimens...........................................................41 Figure 19: The peak-to-valley heights of all specimens and inserts used to characterize surface finish............................................................................................. 45 Figure 20: RFPE process window for packing pressure versus mold surface rou gh ness ........................................................................................................................... 46 Figure 21: The A Priori RFPE Process Parameter Map ............................................... 48 Figure 22: Interaction matrix for the RFPE process parameters..................................49 Figure 23: Mold used to produce experimental specimens .......................................... 52 Figure 24: LabVIEW control program screen shot...........................................................53 Figure 25: Experim ental setup ...................................................................................... 54 Figure 26: Model of surfaces as flat, and in perfect contact........................................57 Figure 27: Asperities reduce the real to nominal surface area ratio ............................. 57 Figure 28: Profilometer trace for a 0.4 pm surface, with no wavelength filterin g ............................................................................................................................... 59 Figure 29: Temperature drop due to conductive resistance as a function of heat tran sfer rate.................................................................................................................64 Figure 30: Cooling rate of mold in air and in ice water...............................................70 Figure 31: Comparison of the cooling rate of a pressurized and unpressurized m o ld cav ity ......................................................................................................................... 71 Figure 32: Completed RFPE Process Parameter Map ................................................. 74 Figure 33: Completed interaction matrix for the RFPE process parameters ............... 75 Figure 34: Rapid Prototyping Center........................................................................... 78 Figure 35: The Rapid Prototyping Center will transform the manufacturing process from a heavy manual intervention process into a black box............................79 Figure 36: Proposed process flow for the Rapid Prototyping Center ........................... 80 List of Tables Table 1: Peak-to-valley depth for various surface roughness standards........................60 Table 2: Roughness, summit curvature, and deflection values of the surface roughness standards ...................................................................................................... 60 Table 3: Description of the surface condition as a function of the injection temperature and mold preheat temperature.................................................................. 67 Table 4: Measurement of specimen diameters.............................................................68 TkanL You To mg familg To mg friends To mg mentors I dedicate this thesis to the memory of M 3 Grandfather, Opa, Ernst 5. Who taught me Keizer Math, Persistence, UJnderstanding and to M Grandmother, Oma, Kuth Keizer Who taught me the power of Kindness and Listening. Chapter 1: Background and Motivation Manufactured goods are prevalent in our society. These goods decrease the time, reduce the effort, or provide the tools required to accomplish a task. The span of these goods ranges from the very mundane, such as scissors or a wrench, to the highly complex, such as an automobile or a heart pump. We use manufactured products daily, yet most of us rarely stop to question how they were produced. When we purchase them, we want them to be cheap, yet we expect them to be durable and perform as advertised. These requirements percolate through to drive the goal of manufacturing systems: to produce high quality, low cost products quickly in flexible set-ups. Unfortunately, these goals tend to be competitive in nature, with advances in one area often requiring concessions from the other metrics. In this way, incremental advances to the existing manufacturing systems can only have extremely limited effects. Thus, a paradigm shift is needed to raise the bar simultaneously on all four criteria used to evaluate manufacturing systems. The first question we may want to ask is where this paradigm shift needs to occur. Do we need to change the entire manufacturing process as we know it, or is it possible to identify a key aspect that will enable the overall improvement we are looking for? In any system, some areas are always more capable than others. Whichever aspect lags behind the others becomes a critical link, limiting the overall potential of the system. Chapter 1 of this thesis argues that current fixturing technology is this critical link of both the design process and of most manufacturing systems. Once the motivation for developing a novel fixturing system is established, Chapter 2 introduces the Reference Free Part Encapsulation (RFPE) concept-a paradigm shift. Chapter 3 establishes a framework for the foundation necessary to analyze and develop the RFPE process. With this structure in place, Chapter 4 both identifies the parameters of this process that have the potential to affect the outcome and defines RFPE's measurable objectives. This chapter also summarizes the insights gained from a literature review and from previous research. Next, Chapter 5 discusses the design of experiments conducted to fill in the gaps in understanding the impact of and interaction between the various process parameters. The theoretical background necessary to analyze the data from these experiments is presented in Chapter 6. Chapter 7 presents the results of these experiments. Then, Chapter 8 presents the RFPE Process Parameter Map. The understanding provided by this map will help unearth the full potential of the RFPE process. Chapter 9 suggests avenues for further research, and speculates about RFPE's effect on the manufacturing process. To realize the potential contribution of RFPE, it is important to understand the role of fixturing in manufacturing. Section 1.1 begins by discussing the role of fixturing in manufacturing and its repercussions on the design process. Next, Section 1.2 reviews the functional requirements of fixturing. Finally, Section 1.3 presents the current fixturing technology. 15 1.1. Role of Fixturing in Manufacturing Manufacturing is the process by which a product is brought from design to production, from idea to reality. In an ideal scenario, the design will achieve the functional requirements set by the designer in the simplest possible manner. However, in reality, the designer must take into account various limitations. In particular, the designer must consider the cost and physical limitations of the different manufacturing processes. One important limitation in manufacturing is defined by the capabilities of the fixturing systems available. Fixturing is the critical link between idea and reality in a unit production system. Fixturing holds the workpiece in the desired orientation so that various manufacturing processes can be brought to bear on the component. In many ways, the quality of the component is determined by the limitations of the fixturing system itself. Furthermore, demands that a particular design places on a fixturing system translate directly into financial and temporal costs born by the final product. These challenges can be illustrated through an examination of the impact of fixturing on machining processes. Machine tools, especially with the aid of CNC, are capable of creating a great variety of geometries. Recent strides in precision machine design have resulted in continued improvement in the precision, power, and flexibility of tools. However, limitations in current fixturing technology greatly restrict the shapes that can actually be produced. In fact, designers must often increase the complexity of the part and the production process to compensate for deficiencies in the fixturing systems. This, in turn, leads to an increase in the cost and a decrease in the production in order to produce the part at all. Thus, the creativity of the designer is curbed by the capabilities of the fixturing systems available. Advances in this field would clearly have a positive impact on the manufacturing world. Therefore, a new fixturing system would be most welcome. The goals of this new fixturing system are driven by the functional requirements of fixturing and the characteristics and limitations of the current workholding systems. 1.2. Functional Requirements of Fixturing In order to compare a variety of fixturing methodologies, it is important to establish the goals of a fixturing system. This permits an objective evaluation of each system. Any fixturing device must achieve some basic characteristics for it to be called a fixture. For example, a fixture must provide the machine with access to the workpiece. Additionally, a fixture should not destroy a workpiece. If the "fixture" does not meet either of these characteristics, the device is effectively useless. For the purpose of discussion within this thesis, these basic characteristics are assumed to be met implicitly by any device called a fixture. Additionally, it is assumed that in evaluating fixtures, the goals of manufacturing will be considered. Therefore, properties such as the production rate and production cost dictated by the fixture need to be considered. However, before we can even begin discussing these properties, we need to discover how well different fixtures perform their 16 duty. To do this, there are some finer requirements that these fixtures should achieve to enable them to perform their function properly. These functional requirements of fixturing systems are fourfold: locating stability, deterministic workpiece location, clamping stability, and total restraint.* Locating stability implies that the workpiece must achieve a stable position as it is placed into a fixturing device. Deterministic workpiece location signifies that the position of a workpiece must be precisely known to ensure the accuracy of the machining operations. Clamping stability establishes that the equilibrium and accuracy of the workpiece position should not be disturbed while the clamping forces are applied. Total restraint means that once the clamping forces have been applied to the workpiece, it should remain immobile for the duration of the machining operation. The quality of a machined part is limited by the fixturing system used during the production process. Even with the use of the best machine tools available, machining processes can achieve the desired level of quality only if the fixture satisfies its four functional requirements. The fixture's limitations in achieving these functional requirements lead to errors introduced into the workpiece. For example, the lack of locating stability or deterministic workpiece location can introduce variations in the position or the orientation of the part. Figure li shows that even a small variation in orientation can cause a significant error in the precision of the workpiece. .,-Material to DESIRED CUT -Actual material ORIENTATION ERROR PART AFTER MACHINING Figure 1: The lack of locating stability or deterministic workpiece location can introduce variations in the position or the orientation of the part. Even a small variation in orientation can cause a significant error in the precision of the workpiece. The fixture's ability to locate the part accurately is not sufficient in and of itself. Any precision gained through locational accuracy and stability is readily lost when clamping loads are applied incorrectly. Figure 2 shows how excessive clamping loads applied to a * i Chou, Y.-C., Srinivas, R.A., and Saraf, S., "Automatic Design of Machining Fixtures: Conceptual Design," InternationalJournalofAdvanced Manufacturing Technology, Vol. 9, 1994, pp. 3-12. Kapoor, S., "New FEM Modeling Results for Fixture/Part Contact," AMRI Machine Tool Workshop on Agile Fixturing, The University of Michigan, Ann Arbor, MI, July 25, 1996, p. 4. Ibid. 17 workpiece can result in deformation of the part. This deformation causes too much material to be removed during the machining operations. Such an error can affect both the dimensional accuracy and the structural integrity of the workpiece. Material to DESIRED CUT Actual material EXCESSIVE CLAMPING LOADS PART AFTER MACHINING LEAD TO PART DEFORMATION Figure 2: Excessive clamping loads can deform a workpiece. This deformation can affect both the dimensional accuracy and the structural integrity of the workpiece. Finally, one cannot neglect total restraint, the fourth and final functional requirement of fixturing systems. Unfortunately, this requirement is often difficult to achieve. Ideally, once the workpiece has been clamped to its supporting elements, the fixture prevents the workpiece from shifting from its desired position, regardless of the machining operations that are performed on it. In reality, the supporting elements and holding forces are typically applied over localized regions of the workpiece. This localized contact results from tradeoffs between the capabilities of the fixturing system, the part geometry, and the access required by the machine tool. Unfortunately, this localized contact means that total restraint relies on the workpiece being capable of transmitting that support or force throughout the part. Complex geometries, especially ones with thin cross sections, tend to be unable to do so effectively. Thus, the workpiece can deflect under machining loads, resulting in a loss of dimensional accuracy. Figure 3 illustrates how this loss of dimensional accuracy can occur. End'i1 renweaed Materiatto-1 be reimavae- DESIRED CUT INABILITY OF PART TO TRANSMIT LOCALIZED FORCES LEADS TO PART DEFORMATION PART AFTER MACHINING Figure 3: The inability of a workpiece to transmit the localized fixturing support force throughout the part causes a loss of dimensional accuracy. In effect, the workpiece deflection under machining loads results in a lack of total restraint. 18 Thus, the inability of a fixture to meet all four functional requirements of a workholding device satisfactorily can result in errors introduced through a number of avenues. These errors, if not corrected, combine to severely degrade not only the quality of the machining process, but the quality of the resultant part. If the errors render the part out of specification, significant time and effort must be expended to bring the part back to a usable condition. Unfortunately, the error often cannot be mitigated and the part has to be discarded. Given the crucial role that fixturing systems play in determining the quality of unit manufacturing processes, one must closely monitor their ability to meet their functional requirements. Section 1.3 reviews the current fixturing technologies. In particular, the advantages and limitations of each process, along with their impact on manufacturing, are examined. 1.3. Current Fixturing Technology Current fixturing technologies can be divided into two broad categories: modular fixtures and universal fixtures. Each category, along with their capabilities and limitations, are discussed in Sections 1.3.1 and 1.3.2. 1.3.1. Modular Fixturing Systems Modular fixturing systems are the dominant class of workholding devices used in manufacturing today. As their name suggests, modular fixtures use a number of elements, such as v-blocks, vices, and toe clamps, in conjunction, to fixture a workpiece. These elements have standardized interfaces that allow them to be assembled into a variety of configurations. Thus, the use of basic elements allows modular fixtures to hold a variety of regular shapes. Ball and socket assemblies, along with other innovations in the modular elements, have greatly improved the modular fixturing system's flexibility. Work on fixturing design and analysis* has improved the siting of clamping points. However, despite these improvements, these systems still suffer severe performance degradations when applied to complex geometries. Generally, even increasing the fixture's geometric complexity significantly can only marginally improve the clamping stability. This limitation is due to the constant tradeoff between the increased restraint that can be achieved by a fixturing assembly and the resultant reduction in access for the machine tool. * Asada, H. and By, A., "Kinematics of Workpart Fixturing," IEEE International Conference on Robotics and Automation, 1985, pp. 337-345. Chou, Y.-C., Srinivas, R.A., and Saraf, S., "Automatic Design of Machining Fixtures: Conceptual Design," International Journal of Advanced Manufacturing Technology, Vol. 9, 1994, pp. 3-12. 19 In addition to the geometric limitations of modular fixtures, one must take into account the cost of a particular fixture in terms of time, money, and resources. Even slight increases in part complexity can result in great leaps in the complexity of the fixturing assemblies. This is costly not only in terms of the time and resources required to design the workholding device, but in terms of the time and resources required to build and set up the fixturing assemblies for each set of machining operations. For modular fixturing systems, the cost of these activities is very high for low volume production. This class of workholding devices becomes more reasonable only in mass production processes, where the cost can be amortized over large unit volumes and long production runs. Thus, the capital investment and lead-time required to construct new fixtures becomes a significant cost that must be considered in bringing each new product to market. Innovations such as pallet-mounted fixtures allow the set up to be accomplished outside the machine tool, thus improving the uptime of the system. However, the use of the pallets merely reduces the setup time while increasing the temporal and material costs for design and storage of the fixtures. However, while these innovations have brought about improvements in throughput, modular fixturing systems remain a visible obstacle between design and production that limits the creativity of the designer. 1.3.2. Universal Fixturing Systems In order to minimize the impact of fixturing on the design-to-production process, universal fixturing concepts were developed as potential replacements for modular fixtures. Universal fixturing systems use a single fixture to handle a multiplicity of geometries. The ability of these concepts to handle various workpieces without the need for redesign provides a number of advantages. First, one avoids the cost of designing and building unique fixturing elements and setups. Second, the use of a single flexible fixture removes the need for storing and maintaining unique fixtures. Third, the use of a standard fixture, or set of fixtures, greatly simplifies the requirements for toolpath generation since, with known fixtures, there is no longer a need to constantly generate new patterns to cope with the interference presented by the fixturing assembly. Currently, there are three common types of universal fixtures: conformable clamps, fluidized bed, and phase change technology. 1.3.2.1. Conformable Clamps Conformable clamps are a category of universal fixturing systems that use sliding and pivoting elements to establish contact with the workpiece. These flexible elements adapt to fit a large range of geometries. Once the workpiece is in the desired location and 20 orientation, the movable elements are locked into place. Figure 4* displays a cross-sectional view of a conformable clamp fixture holding a part. Figure 4: Conformable clamp fixturing An application of conformable clamps can be found in turbine blade manufacturing. During set-up, the stock from which the turbine will be machined is placed into the clamping assembly. The blade is then adjusted until it is in the required location and orientation. As the workpiece is adjusted, the movable elements shift to conform to the part. Once the desired position has been reached, the clamping assembly is actuated to lock the elements in place. The entire workpiece-clamping assembly can be transferred from machine to machine so that the same reference frame is maintained throughout the machining process. This greatly reduces the possibility of an error, or a stack of errors, being introduced which would affect the locational accuracy of the part. Due to the large number of moving parts, however, the conformable clamp concept is vulnerable to jamming by the debris that enters the clamping assembly during the course of machining. The introduction of this debris may impact the fixture's ability to deterministically locate subsequent parts. Like modular fixturing systems, the conformable clamps rely on the workpiece to transfer locally applied support and forces to the whole structure in order to maintain clamping stability. While this is ideal for rigid workpieces such as turbine blades, it is less than ideal for parts with thin cross-sections. Furthermore, the fixturing elements can only provide limited damping for the workpiece. This, along with the dependence on workpiece rigidity, limits the degree to which total restraint can be achieved during machining. Finally, conformable clamps are generally unable to provide adequate access to compact workpieces. 1.3.2.2. Fluidized Bed The second universal fixturing concept utilizes the functionality of a fluidized bed. In preparation for workpiece insertion, a gas, typically air, is pumped into the bottom of the bed of particles at a controlled rate. In this state, the air-particle mixture behaves like a * Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 14. 21 fluid. This makes it quite easy to insert the workpiece into the fluidized bed. Once the part has been positioned properly, the gas is withdrawn from the fluidized bed to compact it. Often, vacuum or magnetic forces are applied to aid in the compacting process. The compacted bed, which now behaves like a solid, grips the workpiece securely, as Figure 5* shows. Figure 5: Fluidized bed fixturing The fluidized bed fixturing system has many advantages. The particle bed is infinitely adaptable and can accept extremely complex geometries. The simple action of the mechanism means that the cycle time for the device is very short. Fortunately, the simplicity of the action required for fluidized bed fixturing also contributes to the reliability of the system. However, like the conformable clamp system, the fluidized bed system requires external assistance to locate the workpiece. In addition, given that the penetration of the machine tool into the bed would destroy the integrity of the bed, care must be taken to ensure adequate access for the machine tool. Furthermore, while the pressure exerted by the fluidized bed against the contours of the part fully supports the immersed workpiece, the fluidized bed may not be sufficiently strong to retain the workpiece against machining forces. Finally, the packing of the bed cannot reliably achieve the optimal packing density. As a result, voids left in the bed may allow the workpiece to shift, adversely affecting locational stability. 1.3.2.3. Phase Change Material In the third type of universal fixturing system, the phase change concept, a molten material, such as low temperature plastic or metallic alloy, is poured into a mold. The molten material flows around the contours of the workpiece and is allowed to solidify. Upon solidification, the workpiece is firmly embedded within the phase change material, as Figure 6 shows. * Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 14. * Ibid. 22 Figure 6: Phase change fixturing The phase change material provides full support for the workpiece. In addition, it has excellent damping properties, thus helping reduce errors introduced through vibrations induced by the cutting process. Furthermore, if the phase change material is poured into a regularly shaped die, the encapsulated workpiece can be handled and fixtured easily. The regular geometry facilitates the handling process. Thus, the phase change concept satisfies the locational stability, clamping stability, and total restraint requirements of fixturing. However, like the other two universal fixturing processes, a die is required to align the part accurately. In order to assure deterministic location, care must be taken in the mold and in the fixture design. In addition, the phase change process is highly hardware-intensive. Finally, the heat transfer requirements of the process introduce an added layer of complexity to phase change fixturing systems. 1.3.3. Limitations of the Current Fixturing Technology Modular fixturing systems are capable of achieving the four functional requirements of workholding devices when used to fixture workpieces with regular geometries. However, as the geometries become more complex, modular fixtures become less and less able to meet these requirements. This limitation is especially evident with regard to clamping stability and total restraint. The precision that can be achieved with modular fixturing systems is not aided by the need to switch to a new setup for each machining operation. With each fixture change, the locational reference is lost and an opportunity exists for errors to be introduced into the process. Of the three universal fixturing concepts, the conformable clamping concept is the most closely linked in functionality to the modular fixturing systems. It is not surprising that, while they possess a number of advantages over the modular systems, these concepts share many problems. The ability of the conformable clamps to secure irregular geometries provides an improvement in locational and clamping stability over modular fixturing. With proper metrological support during insertion, deterministic workpiece location can also be achieved. Unfortunately, like modular systems, conformable clamp systems cannot be adjusted during the machining process without the loss of locational 23 reference. In addition, conformable clamping is unable to secure compact shapes while providing sufficient access for the machine tool. Finally, due to the limitations of locally applied forces and supports, the use for this fixturing concept is limited to rigid geometries for which it can comply with the total restraint requirement. The fluidized bed concept can accommodate a wider variety of geometries than either modular fixturing or conformable clamps can due to the ability of the particles to conform to the workpiece. The simplicity of operations and the quick cycle time is also quite desirable. However, the instability of the packing process, along with the low retaining forces exerted by the particle bed, severely degrade the concept's ability to achieve locational stability, deterministic work piece location, and total restraint. These drawbacks limit the utility of the fluidized bed concept. The phase change system shows the most promise of the three universal fixturing concepts. The phase change material is capable of capturing a range of geometries that is on the order of that captured by the fluidized bed concepts. In addition, the phase change material can provide much higher holding forces than those exerted by the particles of a fluidized bed. This increase in holding forces, damping ability, and support of the workpieces is a function of the material property rather than a function of the geometrical structure of the mechanism. This ensures that the fixturing quality remains stable regardless of the complexity of the workpiece. While this has not been the general practice, the phase change material also allows access by the machine. This can take place over much of the enclosed surface without degrading the fixture's workholding capabilities. The downside of the process is that it is hardware-intensive and the cycle time is dictated by the physics of the heat transfer process involved. From this examination of the advantages and disadvantages of the modular and universal fixturing systems, it is clear that there are a variety of problems inherent in the fixturing systems available today. In particular, it should be noted that none of the currently available systems satisfies all four functional requirements of a fixture: locating stability, deterministic workpiece location, clamping stability, and total restraint. In particular, deterministic workpiece location has typically been sacrificed to allow for the other three requirements and for machine access to the workpiece. This requires that a significant portion of the manufacturing time be spent establishing reference planes each time the part is fixtured. This process is not only time intensive, but also results in a loss of accuracy since each of these references is established independently. Thus, there is a need for a new fixturing system that is able to achieve all four functional requirements. 24 Chapter 2: Reference Free Part Encapsulation From the discussion in Section 1.3, it is evident that modular fixturing systems, despite improvements in quality and speed, place severe limitations on the design and production process. In addition, the cost of maintaining, storing, designing, and building modular fixtures plays a large role in determining product cost and viability. Universal fixtures, on the other hand, provide a great deal of flexibility in terms of the geometry they can be used for. These fixtures greatly simplify manufacturing planning and can be reused for multiple products, but pay for it in terms of a higher degree of mechanical complexity. In addition, the conformable clamps and the fluidized bed systems suffer from reduced clamping reliability and total restraint in exchange for the flexibility they offer. The phase change process is slow, hardware intensive, and requires precise secondary dies to locate the workpiece. It is not immediately evident that any change to these existing systems, modular or universal, would generate the meaningful, across-the-board improvement in fixturing methods that is necessary to substantially improve the manufacturing process. Clearly, a new approach is necessary to yield a significant improvement over current fixturing methods. 2.1. The Ideal Fixturing System To enable this paradigm shift, it helps to develop an ideal fixturing system and determine if it, or something close to it, is feasible. One could consider the imaginary scenario in which a stock of metal could be suspended midair using non-contact forces, such as magnetic forces. In this situation, all faces of the stock would be exposed for machining. This means that any part could be machined from a workpiece in a single set-up, as long as the machine has sufficient degrees of freedom. This imaginary scenario fulfills all four functional requirements for fixturing systems. Thus, we can establish this as an ideal fixturing system. Initially, it seems impossible to bring this ideal system out of the imaginary world. In reality, we must rely on physical contact and frictional forces to immobilize objects. These means, by definition, require contact with the workpiece. Unfortunately, this contact inhibits machine tool access to the workpiece in the regions where the forces are applied. Thus, the need to access the entire workpiece requires moving the force delivering mechanisms at least once during the machining process. However, all locational information is lost when these force-delivering mechanisms are removed. It does not seem possible to ensure free access to the workpiece while maintaining an accurate locational reference. However, instead of discarding this ideal fixturing system as not feasible in reality, one may question whether it is possible to conceptually freeze the component in space a different way. 25 2.2. The RFPE Concept Sanjay Sarma* argues that this conceptual freezing of an object in space is possible. RFPE locates, secures, and supports a workpiece by encapsulating it with another material. This results in a cubical shape with the workpiece embedded inside the cube. Thus, instead of suspending the workpiece in air, RFPE suspends it in a metal medium. After the workpiece is initially encapsulated, it is cyclically machined and reencapsulated. The reencapsulation step allows the position of the workpiece to be stationary within a constant cubical structure. The material that the cube is formed of may change, but the geometry in which the workpiece is suspended does not. In this way, by keeping the workpiece stationary within the cube, one can always determine the part's location and orientation. Thus, the workpiece is conceptually frozen in space. This means that every time one places the part on the machine, one can choose the orientation that one wants that particular time. However, it is not necessary to relocate the part's references. Thus, by rotating the encapsulated workpiece, RFPE allows one to access all sides of the workpiece without having to relocate the part. Once the machining operations are completed, the encapsulation metal is melted away, leaving the part that was desired. Figure 7t describes the RFPE process pictorially. * Sarma, S.E., A Methodologyfor Integrating CAD and CAM in Milling, Ph.D. Thesis, University of California, Berkeley, 1995, p. 32. Lee, E.C., Development of an EncapsulationProcessfor use in a Universal Automated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 21. 26 START: RAW STOCK(EMBEDDED) ENCAPSULATOR ORIENT MACHINE REFILL SIDE 1 SIDE2 SIDE N FINISH: Figure 7: The Reference Free Part Encapsulation (RFPE) Process 27 2.3. Capabilities of RFPE RFPE is clearly the paradigm shift that was needed to achieve the four functional requirements of a fixture. Once the workpiece has been encapsulated, its position is constant with respect to the surface of the encapsulated workpiece. Thus, locating stability can be achieved. Furthermore, the regular geometry of the encapsulated workpiece permits the use of simple, precise fixtures, thus enabling deterministic workpiece location. In addition, the RFPE process provides workholding capabilities superior to the current fixturing systems. The use of a phase change material to secure the workpiece means that no excessive force capable of deforming the workpiece can be applied during the encapsulation process. Once the workpiece has been completely enclosed, all the surfaces of the part are supported. This not only ensures clamping stability but also allows the system to achieve total restraint. Thus, the encapsulated workpiece is totally located, supported, and secured. Therefore, RFPE has the potential to produce high quality components while minimizing the obstacles for both design and production. Figure 8* shows some sample parts produced with RFPE. Figure 8: Sample parts produced with RFPE * Lee, B.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 35. 28 2.4. Three Machining Strategies: 2D, 2%D, and 3D Milling RFPE suspends a workpiece in space and allows access to all of its faces. However, having the encapsulated workpiece immobilize, support, and locate a part can result in a high level of complexity. Sarma* recognized that not all tasks warrant a high level of fixturing complexity. Therefore, in order to realize the RFPE concept with a level of complexity commensurate with the difficulty of the task, he developed three distinct machining strategies: 2D, 2 D, and 3D. The complexity permitted in the machining operations increases as one progresses from the 2D to the 3D Milling Strategy. It should be noted that, as one progresses from the 2D to the 3D milling strategy, the complexity permitted in the machining operations increases. Unfortunately, tied to this increase in flexibility is an increase in the complexity and cost of the encapsulation equipment. 2.4.1. 2D Milling 2D milling is the simplest machining strategy. As Figure 9 shows, this machining strategy allows 2 parallel faces of the workpiece to be accessed, using the other four faces to attach the workpiece to a fixturing device. Figure 9: 2D Milling This fixturing device provides the contact between the encapsulated workpiece and both the machine and the encapsulation system. Additionally, if one leaves this fixturing device attached to the encapsulated workpiece for the duration of the machining and reencapsulation cycles, the fixturing device can take over the locational function from the encapsulated workpiece. Sarma, S.E., A Methodologyfor IntegratingCAD and CAM in Milling, Ph.D. Thesis, University of California, Berkeley, 1995, p. 46. Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 48. 29 Since the fixturing device performs the locating function in 2D milling, the requirements for the encapsulated workpiece can be relaxed. Given that the surface of the encapsulated workpiece is not used to reference the location of the part, this machining strategy requires neither precise surface finish nor exact dimensional repeatability. This significantly reduces the complexity of the encapsulation machine. 2.4.2. 2%D Milling Often, more than two faces of a workpiece need to be accessed to produce a part. In these cases, 2D milling is clearly not applicable. However, only rarely does the production of a part require all six faces of the encapsulated workpiece to be accessed. It is in these cases that that 21/2D milling can be exploited. This machining strategy is not as simple as 2D milling, but one can still reap significant benefits from not having to access all six sides. In 2/2D milling, a locating pallet covers one of the faces of the workpiece. As Figure 10* shows, this leaves five faces of the encapsulated workpiece free to be machined. Figure 10: 2%D Milling The locating pallet serves as the link between the encapsulated workpiece and both the machine tool and the encapsulation system. As in 2D milling, the fixture serves as the locational device, while the encapsulating material provides the immobilization and support required. * Lee, B.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 48. 30 2.4.3. 3D Milling If the complexity of the part being produced requires all six sides of the workpiece to be machined, the full power of RFPE needs to be unleashed. In this case, the 3D milling strategy, the most flexible of the machining strategies, is the most appropriate. In this strategy, the encapsulated workpiece can be placed on the machine with any face up during any given portion of the machining cycle and can be turned as needed. Thus, as Figure 11* shows, this strategy permits access to the workpiece from all directions. (7E-- 10 Figure 11: 3D Milling The flexibility of the 3D milling strategy allows complex geometries, even those with thin cross-sections, to be generated with great precision. In this strategy, the encapsulation is responsible for ensuring compliance with all four functional requirements of a fixture. This means that the encapsulation must not only retain and support the workpiece against machining forces, but it must also maintain the locational reference for the workpiece. Since the encapsulated workpiece may be placed in any orientation, variations in the encapsulation may affect the precision of the RFPE. This need for precision increases the rigor of the requirements for the encapsulation process and equipment. * Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 48. 31 2.5. Motivation Clearly, the RFPE concept can be the lever that is needed to significantly improve the manufacturing process. It has the ability to satisfy-without compromise-all the functional requirements of a fixture, and yet, in conjunction with the three machining strategies, is flexible enough to work in a great variety of situations. The question then is whether this concept is actually feasible in reality. Given the difficulties in modeling the RFPE process analytically, initially much of the work to prove the viability of the concept had to be done experimentally. Lee built an encapsulation system at MIT, which has proved the viability of the process. However, as expected, it also left significant room for improvement. RFPE can only advance once basic knowledge has been gathered in all the critical areas. Therein lies the motivation for this study: to establish a framework to understand RFPE, consolidate the existing knowledge, identify the critical factors that remain unexplored, determine the impact these factors have on the process, and thus develop the RFPE Process Parameter Map. This map will guide future designs and developments of the concept. 32 Chapter 3: Framework to Analyze and Develop RFPE The goal of this study is to establish a foundation of knowledge on which the future work on the RFPE process can be based. Without this foundation, systematic improvement of the process cannot be achieved. The key to a solid foundation is a structured approach to the discovery and layout of the basic building blocks. Section 3.1 begins with a description of this approach. 3.1. The Building Blocks of a System For any engineering problem, the information can be divided into three parts: the system, the inputs, and the outputs. For this study, the system in question is the RFPE concept. At this level of abstraction, the concept encompasses all aspects of the process and apparatus. The outputs are the values by which the system is judged. In particular, these are the attributes, or metrics, that determine how well the RFPE process meets its goals, including the functional requirements of fixturing and other aspects as esoteric as the floor space that needs to be dedicated to the device. The inputs, in turn, consist of the variables that can impact the quality of the process. These inputs can be further classified into environmental variables and parameters. Environmental variables are those factors, such as atmospheric pressure, that cannot easily be controlled. On the other hand, parameters are set either during the design of the apparatus or during the operation of the process. 3.2. Design and Process Parameters It is important to distinguish between design and process parameters. While both of these affect the operation of the system and may affect the same metrics, they represent very different things. Process parameters are indisputable properties of the concept, dictated by the physical laws of nature. On the other hand, design parameters are the particular characteristics selected for a particular implementation of the concept. Thus, any implementation of a system has the exact same process parameters as another implementation. However, two different implementations of a particular system are likely to have different design parameters. Process parameters denote the conditions that can be theoretically varied for a given process. Depending on the sensitivity of the metrics to a particular parameter, the variation can impact the quality of the product produced. Thus, it is important to identify the process parameters for any system and investigate the relationship between each process parameter and each metric for the system. Figure 12 shows how the plot of a process parameter versus a metric can simplify the analysis of where the system should be run to maximize that particular metric. 33 Metric Process Parameter Figure 12: A plot of the relationship between each process parameter and each metric for a system facilitates an understanding of the system characteristics Theoretically, there are no limits to the extent to which a process parameter can be varied. However, in reality, the range of each process parameter is bounded by physical limitations. For example, if we consider two metrics that are affected by the same process parameter, we could imagine facing the situation depicted in Figure 13. Metric #1 Metric #2 Metric Process Parameter Figure 13: Each process parameter typically impacts multiple metrics of the same system. Often, there is no optimum setting for the process parameter. Therefore, tradeoffs between the metrics are required. In this case, it would be impossible to select a setting for the process parameter without knowing the details of the situation so that we can make an informed tradeoff. Ideally, this means that in designing a system we would allow the user utmost flexibility to set the process parameter to whatever setting is best for the application at hand. However, in reality, we cannot feasibly build a machine that will allow all possible values of a given process parameter. Thus, as Figure 14 shows, for any given apparatus, there is a window within which the user can define the setting that is best for their particular application. 34 The boundaries of this window are defined by the choices made-implicitly or explicitly-during the equipment design process. Range permitted by design parameters Process Parameter Settings Figure 14: Design parameters determine the range of each process parameter that is feasible for each implementation of the concept. Design parameters are the characteristics of the device that determine the extent to which a piece of machinery can carry out its desired functionality. The particular design parameters for a given system are selected based on the specific objectives of the implementation being designed. These objectives guide the tradeoffs that are required by the often-contradictory nature of the process parameters, as shown in Figure 13. Additionally, factors such as the cost of the process and the apparatus, production rate, and the quality specifications that the design has to meet also influence the choice of design parameters. Ultimately, the design parameters determine the extent to which a piece of machinery can carry out its desired functionality. Ideally, design parameters are set such that they allow the end-user utmost flexibility in choosing the process parameter setting. In the process modeled by Figure 15, it is not possible to maximize both Metric #1 and Metric #2 simultaneously. Thus, the end user needs to select the setting that is best for the case at hand. Unfortunately, physical and cost limitations often do not allow for an apparatus that gives the user the ability to select a setting in the entire range. Thus, a particular implementation of the concept becomes a version of the concept optimized for a particular application. 35 Range permitted by design parameters selected. Combination Metric (a function of Metrics #1 & #2) Metric #1 Vetric #2 Process Parameter Figure 15: For the particular implementation modeled in this diagram, the choice was made to have the design parameters favor Metric #1 slightly over Metric #2. This means that, in order to design an optimal system, it is important to first determine the process parameters. With the process parameters defined, one can then investigate the effect that they have on each other and on the metrics. Then, with this basic understanding in place, one can choose the applications that one wants to satisfy with one particular design and select the design parameters accordingly. In this way, systems satisfying the requirements can be built at a reasonable cost within a reasonable amount of time. For a different set of requirements, a slightly different implementation of the same process can be built. 3.3. A Structured Approach to Developing the RFPE Process The goal of this study is to develop a roadmap that will guide the future development of the RFPE concept. In order to do this, one must develop a means to systematically evaluate the importance of various factors. This evaluation can be accomplished through the identification of the critical metrics for the concept. By determining the process parameters that can potentially influence these metrics, one captures the core variables whose interrelationship will shape the quality of the product. The next step in the journey lies in discovering the shape of these interrelationships. This can be done through a combination of literature review of similar processes, mathematical analysis, and experimentation. The factors that have negligible impact can be discarded. Those that are crucial to the success of the concept will receive further attention to determine the concept's sensitivity to variation in these areas. 36 Chapter 4: Systematic Evaluation of Parameters and Metrics This chapter establishes the foundation for a systematic evaluation of the criteria that may impact the RFPE concept. In particular, this chapter focuses on consolidating knowledge, presenting parameters of known significance, and identifying parameters whose effect remains to be determined. Section 4.1 presents the metrics for the RFPE concept. Section 4.2 introduces the process parameters and summarizes both a literature review and the current research on how the process parameters impact the metrics. Section 4.3 consolidates this information and presents the RFPE Process Parameter Map. Section 4.4 presents the next steps based on the current state of knowledge. 4.1. Metrics of the RFPE Process The metrics selected to evaluate the performance of the RFPE process are measures of the quality of the encapsulated workpiece. These properties of the workpiece determine how well the process fulfills the functional requirements of fixturing. The metrics are divided into two categories: those that affect the precision of the process and those that affect the integrity of the encapsulation. The precision of the RFPE process is determined by the surface finish, porosity, shrinkage, and thermal drift of the encapsulated workpiece. These factors, in turn determine the minimal dimensional tolerance that one can achieve with this system. Additionally, the integrity of the encapsulation is affected by the rewelding strength as well as the presence of porosity. Sections 4.1.1 through 4.1.5 discuss these metrics. 4.1.1. Surface Finish Surface finish refers to the relative roughness and flatness of the encapsulation surface. Since the surface of the encapsulation forms the load-bearing surface through which the encapsulated workpiece is fixtured, variations in surface finish can impact the dimensional accuracy of the process. The surface finish can be characterized by the amount that the surface deviates from perfect flatness. As displayed in Figure 16,* there are three types of deviations: gross deviation, surface waviness, and roughness. Gross deviation is called form error. Minor deviations can be called surface waviness or roughness. The distinction between waviness and roughness is a function of the frequency of the undulations. For the purpose of this study, the two will be considered as one single category and referred to as roughness. Tencor P-10 Reference, P/N 412937 Rev. A, 1996, pp. 3-8. 37 Rougfroes Formn Errr Waviness Figure 16: A surface finish can be categorized by the amount that it deviates from a perfectly flat surface. There are three ways in which this deviation occurs: form error, waviness, and roughness. Form error can be measured with a coordinate measurement machine. Surface roughness can be measured with a profilometer. Profilometers are capable of greater resolution than the coordinate measurement machines and can provide a better characterization of the micro-scale features of the surface. While these methods provide a fairly accurate way to characterize the flatness of a surface, this degree of precision is not always required. In many cases, the surface deformities do not affect a process as long as the roughness does not exceed a certain threshold value. In this instance, the use of a "go/no-go" gauge would be appropriate. An example of such a roughness gauge would be a surface roughness standard, which contains a variety of roughness samples that one can compare to the target surface. 4.1.2. Porosity Porosity refers to the presence of voids in the encapsulation. These voids are formed either by shrinkage or by gases trapped during the molding process. Section 6.2 describes the porosity generating mechanisms more in-depth. The presence of porosity on the surface of the encapsulation forms defects that, in sufficient numbers, compromise the load-bearing capability of the encapsulation. The added deflection resulting from the compression of the defect-ridden surface impacts the accuracy of the process. Furthermore, the presence of porosity inside the encapsulation can compromise the workholding ability of the encapsulation against the embedded workpiece. Finally, porosity in the encapsulation weakens the encapsulation since the voids reduce the amount of material available to withstand tensile and compressive loads. The presence of porosity, both internal and external, has the potential to impact the quality of the RFPE process. The presence of voids in the encapsulation can be detected by comparing the encapsulation density against the tin-bismuth density. The weight can be obtained with a balance. The volume can be found by depositing the specimen into a graduated cylinder filled with water. The displaced volume of water will be equivalent to 38 the volume of the encapsulation. With sufficiently fine resolution on the balance and on the graduated cylinder, deviations from the tin-bismuth density can be determined quite accurately. Since it is also the location, not just the presence of porosity, that determines the impact on the RFPE process, visual inspection and identification of the voids is an important component of the measurement process. If necessary, instruments with the appropriate resolution can measure the size of the voids. However, often the short sample length of a profilometer limits the size of the voids that it can measure accurately. For internal voids, it is necessary to section a specimen to determine their presence, frequency of occurrence, and location. 4.1.3. Dimensional Accuracy Dimensional accuracy refers to how closely the specimen geometry matches the expected geometry. Ideally, to simplify the mold design process, this means that the specimen geometry mirrors the geometry of the mold. Unfortunately, the expansion and contraction of the mold and the specimen due to the changes in temperature makes this a difficult goal to achieve. This variation is determined by the material's properties, in particular the coefficient of thermal expansion and the geometry of the part in question. If the dimensions of the part or the temperature change involved are sufficiently large, the dimensional variation can impact the dimensional accuracy of the RFPE process. Thus, it is important to determine the effect of each process parameter on this metric and methods to mitigate unwanted variation. Two-dimensional measurement of dimensional accuracy can be accomplished using calipers and micrometers. Higher precision, non-contact instruments such as lasers can also be used, although the precision advantages are often offset by errors introduced by variation in the optical properties of the surface. For a three-dimensional measurement of dimensional variation, a coordinate measurement machine is necessary. 4.1.4. Thermal Drift One of the advantages of RFPE over conventional fixturing processes is that the workholding is accomplished using the material properties of the metallic alloy. While this is much more stable and offers better damping than the structural stiffness provided by conventional fixtures, one must be aware of the errors that can be introduced by thermal drift. Thermal drift describes the shifting of the encapsulated workpiece as the encapsulation temperature reaches or exceeds the melting point. As Figure 17* shows, this results in a softened zone within which the workpiece can shift. If this occurs, the locational references for the part would be lost. Unfortunately, if thermal drift is present * Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 23. 39 in the process, the error will only be spotted after the encapsulation material is removed following the completion of the part. Therefore, it is important that no thermal drift takes place. I - - New Encapsulatio.10 Workpiece Sofiened Zone Previous Encapsulation Figure 17: How thermal drift occurs 4.1.5. Rewelding Strength Rewelding refers to the process by which new alloy is introduced into the encapsulated workpiece to restore it to its original shape. In order to ensure the integrity of the encapsulation, a strong bond must exist between the new and the old alloy. Otherwise, under thermal or machining-induced stresses, the encapsulation would disintegrate. This would cause the locational references to be lost. Like thermal drift, rewelding cannot be readily measured before the encapsulation fails. As such, it is a factor that is better avoided in the RFPE process. The measurement of rewelding strength is best carried out using tensile-strength specimens created according to the flow chart in Figure 18.* The yield strength of the weldline can be determined with the use of an Instron tensile test machine, as carried out by Valdivia.t Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 90. t Lee, E., Valdivia, P., Fan, W., Sarma, S.E., "The Process Window for Reference Free Part Encapsulation," To appear in ASME JournalofManufacturing Science & Engineering,p. 8. * 40 Cavity Gate A ir Sprue A Molded specimen SDecimen broken in half Parting line Tensile test specimen mold Final tensile test specimen with desired weldline 0:- Broken half placed back into mold and re-injected eldlile Figure 18: Creation of weldline test specimens 4.2. Process Parameters: an Overview The process parameters of RFPE fall into four main categories: temperature, packing pressure, aging, and alloy composition. The temperature parameter is separated into a number of subcategories. These are melt superheat, mold preheat temperature, cooling rate, and ejection temperature. Packing pressure is the pressure maintained during the cooling process. Aging refers to the changes in a workpiece's dimensions as a function of the time between a casting operation and the actual machining operation. The alloy composition also affects the quality of the encapsulation. Each of these categories will be examined for their potential impact on the RFPE process. The information provided below is based on a literature review of related manufacturing processes and on work previously conducted in the development of RFPE. 41 4.2.1. Temperature There are four temperatures that affect the RFPE process: melt superheat, mold preheat temperature, cooling rate, and ejection temperature. 4.2.1.1. Melt Superheat The melt superheat denotes the amount by which the molten material is heated above the melting point of the alloy at the point of entry into the mold cavity. If the injection temperature cannot be measured, the reservoir temperature can be monitored. The reservoir temperature should be the desired injection temperature plus the temperature difference necessary to account for the heat loss during alloy delivery to the mold. The melt superheat has a direct impact on the quality of the casting. If the melt superheat is not sufficiently high, cold shuts may occur and trapped air may not be able to escape before the alloy solidifies. Furthermore, one must consider the effect of the melt superheat on rewelding and thermal drift.* During reencapsulation, contamination on the surface of the alloy prevents proper diffusion and bonding between the existing and the new alloy. This results in poor adhesion and greatly reduced structural strength. There are two ways to remove the contaminants: chemical agents and superheating. Chemical agents, such as reagents, fluxes, and solvents, will strip away the contaminants. However, the difficulties in automation, as well as safety and environmental considerations, make the chemical option impractical. Therefore, superheating is preferred. By superheating the molten alloy, sufficient heat transfer takes place to displace the melt front into the existing alloy. This allows the new alloy to penetrate the layer of contaminants to achieve a good weld. Given that the contaminant layer has a thickness of approximately 1 pm, a penetration of at least 1 mm must be achieved to ensure the dispersion of the contaminant layer. However, caution must be taken as too much superheat may result in thermal drift of the workpiece within the encapsulation. The melt superheat temperature, along with other factors such as the mold preheat temperature, determines the extent of the penetration. Lee has developed a model to analyze the effects of melt superheat and mold preheat temperature on thermal drift and rewelding. Valdivia experimentally verified the rewelding aspects of the model. They concluded that good quality rewelding can be achieved through a combination of high melt superheat and mold preheat temperatures. t The desired interpenetration between the alloys can be achieved within twenty seconds. This rewelding time should be kept under forty seconds to avoid thermal drift. Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p 22. t Lee, E., Valdivia, P., Fan, W., Sarma, S.E., "The Process Window for Reference Free Part Encapsulation," To appear in ASME JournalofManufacturingScience & Engineering,p. 12. * 42 Depending on the design of the encapsulation system, the melt superheat may also play a role in ensuring the dimensional accuracy of the encapsulation. If the encapsulation is extracted from the mold based on a set cooling time, varying injection temperatures will result in varied dimensions. Thus, to ensure dimensional stability, it is best if the melt superheat stays as constant as possible. Further methods to maintain dimensional stability will be addressed in the following sections. Porosity is another metric that may be impacted by the melt superheat. If the injection temperature is too close to the melting point of tin-bismuth, there may not be sufficient time for the air to vent completely from the mold prior to alloy solidification. In this case, the melt superheat will contribute toward the formation of porosity in the mold. This porosity may be within or on the surface of the encapsulation. Finally, high reservoir temperatures used to generate high melt superheat may result in alloy segregation as well as the formation of oxides. Alloy segregation would lead to variable structural strength and temperature response. On the other hand, formation of oxides would result in contamination of the mold and encapsulation, degrading both the surface finish and the integrity of the encapsulation. 4.2.1.2. Mold Preheat Temperature The temperature of the mold also plays an important role in determining the quality of the encapsulation. During injection, a high mold preheat temperature is necessary to prevent cold shuts and early solidification.* In addition to the impact on the surface finish, the premature solidification can prevent trapped air from escaping, thus causing porosity. Furthermore, a low mold preheat temperature will result in the rapid solidification of the encapsulation. The surface of the encapsulation has the potential to warp due to stress induced through thermal expansion and contraction. The final mold temperature is also important as it determines the thermal expansion of the mold and the associated errors in the encapsulated workpiece. Finally, the high temperature needs to be maintained during packing so that rewelding occurs.t 4.2.1.3. Cooling Rate The cooling of the mold must proceed slowly enough that the material strength and ductility are not compromised.t A slow cooling rate ensures that thermal factors dominate and kinetic factors are damped out. This helps minimize the impact on both * I Allsop, D.F., and Kennedy, D., PressureDiecasting; Part2, Pergamon Press, New York.1983, pp. 6-7. Lee, E., Valdivia, P., Fan, W., Sarma, S.E., "The Process Window for Reference Free Part Encapsulation," To appear in ASME JournalofManufacturingScience & Engineering,p. 12. Murray, M.T., Griffiths, J.R., "The Design of Feed Systems for Thin-Walled Zinc High-Pressure Die Castings," Metallurgicaland Materials Transactions,Vol. 27B, February 1996, p. 115. 43 surface finish and dimensional accuracy. Finally, too high a cooling rate may result in air being trapped in the encapsulation, thus increasing the amount of porosity. 4.2.1.4. Ejection Temperature Many casting processes utilize cooling time to determine the ejection of the casting from the mold. However, as Section 4.3.1.2 discusses, packing pressure and cooling rate have complementary effects. These, along with the mold preheat temperature, the melt superheat, and the cooling rate of the mold, impact the workpiece temperature at any given point in time. Variations in the ejection temperature seem likely to have an important impact on the precision of the RFPE process. Ejection of the encapsulated workpiece at too high temperatures can result in warping of the surface as shrinkage takes place. This may have an effect on both surface finish and dimensional accuracy. Varying ejection temperatures will result in varying shrinkage rates, thus introducing errors into the critical dimensions of the encapsulated workpiece.t Therefore, the ability to reliably achieve consistency in casting dimensions can be better accomplished by following a temperature-based ejection scheme than a time-controlled one. 4.2.2. Packing Pressure The packing pressure has the potential to impact the porosity and surface finish of the encapsulation. Experiments have shown that, as long as packing pressures above 60 psig are used, the reflected surface finish on the encapsulation will closely approximate that of the mold. Figure 19 shows the difference between the mold surface finish and its reflection on the corresponding specimen as a function of pressure. From the data obtained in the experiments, a reflected surface roughness on the order of 64 to 125 micro inches will have a negligible effect on the precision of the RFPE process. Thus, the mold can be manufactured using standard machining processes. * Allsop, D.F., and Kennedy, D., PressureDiecasting;Part2, Pergamon Press, New York.1983, p. 15. t Ibid. Fan, W., The Effect of Surface Roughness on the Precision of the EncapsulatedFixturing System, S.M. Thesis, Massachusetts Institute of Technology, 2000, p. 51. 44 60 - - - - Mold Ra =3.2 Roughness beyond profilometer range 50 X Nom. Ra = 3.2 -..-.. Mold Ra= 1.6 Nom. Ra =1.6 - -Mold Ra =0.4 1040 5 30--- ModR= : 10 . om R2=0. 30 10 0 - - - - - - - - - -~- 40 20 - - - ------ - - - 60 80 Pressure (psi gauge) Figure 19: The peak-to-valley heights of all specimens and inserts used to characterize surface finish The packing pressure also aids in the dimensional accuracy of the encapsulation. By forcing the molten alloy to conform to the surface of the mold until solidification has taken place, packing pressure minimizes the dimensional variation due to the expansion or contraction of the alloy due to changes in temperature. From the experimental data, Fan also developed a correlation between packing pressure and the acceptable mold surface finish. Figure 20* shows the resultant process window. * Fan, W., The Effect of Surface Roughness on the Precision of the EncapsulatedFixturingSystem, S.M. Thesis, Massachusetts Institute of Technology, 2000, p. 57. 45 - 3.5 -.-0 32.5 :a - 2- 0 W Z, 1.5 Tolerable Roughnes s (microns) - Process Incapable Process Capable 10.5- 0 20 40 60 80 100 Molding Pressure (psi gauge) Figure 20: RFPE process window for packing pressure versus mold surface roughness A higher packing pressure has the potential of compressing the air that remains inside the mold. This results in smaller air bubbles. El Mahallawy has shown that there is no macroporosity at pressures beyond 10,000 psig.* This should help ensure the structural integrity of the encapsulation. This, in turn, would increase the strength and ductility of the encapsulation. In RFPE, the use of packing pressure that is two orders of magnitude lower than that spacified by El Mahallawy means that there is likely to be some porosity present both on the surface and throughout the encapsulation. However, the level of porosity should not be sufficient to affect the surface finish, the porosity of the surface, or the structural integrity of the encapsulated workpiece. High packing pressure also minimizes the air gap between the mold and the molten alloy. This increases the heat transfer by eliminating the insulation layer. Since a high packing pressure has a similar effect as increasing the cooling rate,t the former can be applied to provide more flexibility for the latter parameter. However, one should note that pressurized gas in the bubbles might form blisters upon reheating as the trapped air expands.t This should not be of concern, as the reencapsulation will take place in a pressurized environment. * El Mahallawy, N. A., Taha, M. A. and Zamzam, M. L., "On the Microstructure and Mechanical Properties of Squeeze-Cast Al-7 wt% Si Alloy," JournalofMaterials ProcessingTechnology, 40, 1993. p. 83. Ibid, p. 83. Allsop, D.F., and Kennedy, D., PressureDiecasting;Part2, Pergamon Press, New York.1983, pp. 6-7. 46 The most important effect of packing pressure is on the dimensional accuracy and stability. The packing pressure helps offset shrinkage effects and maintain the dimensional accuracy. Consistent packing pressure is required to ensure repeatable results. 4.2.3. Aging During casting processes, stress can be introduced into the material by effects such as shrinkage, turbulence, and premature solidification. This results in a state of tension that may dissipate slowly over a period of time following the casting process. The casting will continue releasing the stress until equilibrium has been reached. Depending on the material and the strength of the induced stresses, this may result in dimensional variations that are large enough to affect the precision of the process. Zinc castings have been noted to shrink between 0.075% to 0.12% over several months.* It is unclear as to the effect that aging has on tin-bismuth. The effect that aging has on the surface finish is equally unclear. This, along with the time period over which the aging process takes place, form possible avenues for experimental verification. 4.2.4. Alloy Composition As the RFPE process proceeds, new encapsulation alloy must be added to the reservoir to replace the consumed alloy. As new and recycled alloy are mixed in the reservoir, the introduction of contaminants is unavoidable. The contaminants can be impurities contained within the ingots, chemicals used to treat the outside of the ingots to prevent oxidation, particles and fluids introduced during machining, or oxides generated during the heating process. These impurities contaminate the mold. This, along with any contaminants that may aggregate on the surface of the workpiece, may contribute to a poor surface finish. The contamination of machined surfaces, along with the contaminants present in the alloy, may lead to rewelding problems. The presence of contaminants on the mold and alloy surface may lead to air being trapped on the surface, thus causing porosity. Finally, sufficient oxide-induced defects may affect the dimensional accuracy of the encapsulation. Repeated heating of the alloy may result in segregation of the elements and variations in mechanical and thermal properties of the encapsulation material. Careful selection and usage will be necessary to minimize the impact of alloy composition on the RFPE process. * Murray, M.T., Griffiths, J.R., "The Design of Feed Systems for Thin-Walled Zinc High-Pressure Die Castings," Metallurgicaland Materials Transactions,Vol. 27B, February, 1996, p. 115. 47 4.3. The A Priori RFPE Process Parameter Map From the information provided in Sections 4.1 and 4.2, a process parameter map was created showing the relationship between the RFPE process parameters and metrics. Figure 21 presents the RFPE Process Parameter Map. The process parameter effects are divided into three categories. The shaded blocks indicate that the process parameter and the metric are materially independent. The check-marked blocks have been investigated. The remainder represents the relationships that have a potential to impact the RFPE process and, thus, are worthy of further exploration. Metrics Dimensional Thermal Rewelding Accuracy drift strength Melt superheat [Lee 2001] [Lee 2001] Mold preheat temperature [/ [/ [Lee 2001] [Lee 2001] Cooling rate [Lee 2001] Process Parameters . Surface Po__sity finish Ejection temperature Packing pressure [Fan 2000] [Fan 2000] [Fan 2000] Aging Alloy Composition Relationship to be determined / [Source] Map completed Materially Independent Figure 21: The A Priori RFPE Process Parameter Map In addition to the relationship between the metrics and the process parameters, one must also consider the relationship between the various process parameters. These relationships are laid out in the interaction matrix shown in Figure 22. The question mark indicates those parameters that have a potentially positive interaction. 48 r q Process Parameters Melt superheat Mold preheat temperature Cooling rate Ejection temperature Packing pressure Aging Alloy composition Melt superheat Mold preheat temperature Cooling rate Ejection temperature Packing pressure Aging Alloy composition Materially independent Relationship to be determined Redundant Spaces Figure 22: Interaction matrix for the RFPE process parameters 4.4. Next Steps The research into the status of the RFPE process highlighted the areas that have been mapped. Additionally, the literary research pinpointed many areas that are materially independent and have no impact on the process. However, there still remains much unexplored ground in the process parameter map that needs to be understood. The study of these parameters will help identify the impact of and relationships between the process parameters. This is the first step in further developing the RFPE process. 50 Chapter 5: Experimental Plan Chapter 4 identifies a number of process parameters that have the potential to impact the quality of the RFPE process. Experimentation was necessary to determine the actual effects. Section 5.1 reviews the objectives of the experiments. Next, Section 5.2 provides an overview of the experimental apparatus designed for these experiments. Section 5.3 provides, in detail, the experimental procedure. 5.1. Objectives of the Experiments The objective of the experiments carried out in this study was to explore the effects of process parameters that could potentially impact the quality of the RFPE process. In particular, the experiments explored the effects of melt superheat, mold preheat temperature, and cooling rate on the surface finish, porosity, and dimensional accuracy of the encapsulation. The effect of ejection temperature and aging on surface finish and dimensional accuracy was also examined. By evaluating the results of the experiments, information regarding the effects of alloy composition was collected. 5.2. Experimental Apparatus 5.2.1. The Mold A mold was made to produce tin-bismuth specimens for the various experiments. Figure 23 displays the mold with the top removed. In order to increase the number of experiments that could be carried out within a given period of time, two molds were used in the experiments. The molds are labeled Mold A and Mold B respectively. 51 Figure 23: Mold used to produce experimental specimens The mold used to produce the specimens is a four-part mold. It has a parting line along the length of the cylindrical cavity to facilitate removal of the specimens. The air used to supply pressure to the molds is introduced through the quick-release fittings attached to the top plate. To facilitate removal of specimens, clamps were used to assemble the mold. Ideally, a thermocouple would be inserted into the mold cavity to monitor the specimen temperature directly during specimen production. Unfortunately, the difficulties involved in sealing the mold cavity and in extracting the specimen made this option impractical. Thus, as an alternative, the mold thermocouple was inserted into a shaft on the side of the mold that put the tip of the thermocouple 0.1 inches away from the wall of the mold cavity. 5.2.2. Instrumentation The packing pressure, the reservoir temperature, and the mold cavity temperature required control and monitoring. A pressure regulator controlled the compressed air feed from the building compressed air system. The pressure to the mold was switched on and off via a SMC NVFS3300-3FZ automatic valve with a subplate. The temperature of the mold and the tin-bismuth reservoir were measured using a J-Type thermocouple. A LabVIEW program was written for three purposes: data monitoring, data collection, and pressure actuation. The program tracked the temperature inputs from the various 52 thermocouples. Temperature alarms built into the system can be set to aid in the operation of the apparatus. The temperature data was stored every second in a designated text file, along with binary pressure data, and counter information. The program also provided the interface displayed in Figure 24 to actuate the pressure. Figure 24: LabVIEW control program screen shot* A Gar Electroforming M- 15 Surface Roughness Standard Set was used for the threshold surface roughness measurements. A micrometer accurate up to ± 0.0001 inches was used for dimensional measurements. 5.3. Experimental Procedure Experiments were designed to test the effect of the process parameters on each other and on the metrics of RFPE. For each experiment, the mold and the molten alloy were heated in the setup displayed in Figure 25. The alloy was melted and brought to the desired * The LabVIEW program can gather data for 3 molds, however the cycle time of the experiments limited the use to the two molds mentioned in Section 5.2.1. 53 temperature in a stainless steel pot on an electric heating element. The mold was heated from the bottom surface using another electric heating element to a temperature slightly above the desired set point. Then, the mold was removed from the heating element. Figure 25: Experimental setup Once the mold reached the desired set point, the molten alloy was poured in, the top plate secured, and the mold pressurized. Eutectic tin-bismuth was used. The mold temperature was monitored until it reached the desired ejection temperature. At that point, the pressure was relieved, the mold disassembled, and the specimen removed. The diameter of the specimen, which is the critical parameter for these experiments, was measured with the micrometer upon extraction from the mold. The specimen then underwent visual inspection for surface porosity and other defects. Surface finish measurements were also made using the surface roughness standard. Finally, the temperature information was extracted from the LabVIEW program for analysis. 5.3.1. The Effect of and the Interaction between Melt Superheat and Mold Preheat Temperature The effects of melt superheat and mold preheat temperature on surface finish, porosity, and dimensional accuracy were determined using the same experiment. This experiment also determined the relationship between the two parameters. The melt superheat temperatures were selected to range from just above melting point to a high degree of superheat. The temperature of the tin-bismuth should not exceed 450'F, since the oxidation of the alloy increases significantly beyond this point. In particular, the melt Widely available, this eutectic binary alloy is composed of 58% bismuth and 42% tin. The alloy has a low melting point of 281*F. It has a reasonably high Young's Modulus of 7.5 GPa and an adequate 0 yield strength of 60 MPa. Its thermal conductivity is 18.4 W/m K, while its thermal expansion 6 0 coefficient is 15x10- / K [Lee 1999]. 54 superheat was set to 293.5'F, 331 F, 368.5'F, and 406'F, while the mold preheat temperature was varied between 200'F, 225'F, 250'F, and 275'F. Aside from the two process parameters under consideration, all other variables were held constant. The packing pressure was set to 70 psig. The specimen ejection temperature was set to 200'F. Finally, natural convection was used to cool the mold. 5.3.2. The Effect of Cooling Rate A second experiment was conducted to determine the effect of the cooling rate on surface finish, porosity, and dimensional accuracy. There were two sets of test runs. The first set was carried out utilizing natural convective cooling with ambient air. In the other set, the mold was placed into a bath that contained an ice-water mixture. When the thermocouple reached the ejection temperature, the mold was removed from the water and the specimen extracted. For this experiment, the melt superheat was set to 331 'F, while the ejection temperature was set to 200'F. The mold preheat temperature was varied between 225 F, 250'F, and 275'F. The packing pressure was set to 70 psig. 5.3.3. The Effect of Ejection Temperature A third experiment was conducted to determine the effect of ejection temperature on surface finish and dimensional accuracy. The ejection temperature was tested at 150 0F, 200 0 F, and 250'F. For this trial, the melt superheat was set to 33 1F and the mold preheat temperature was varied between 225'F, 250 0 F, and 275'F. The packing pressure was set to 70 psig. The molds were cooled through natural convection in ambient air. 5.3.4. Aging Effects The goal of this experiment was to determine whether aging has an impact on the surface finish and the dimensional accuracy. To do this, the specimen diameter and surface roughness of the parts created for the previous four experiments were measured both at the time of removal and at discrete time intervals ranging from a few hours up to four weeks after specimen production. 55 5.3.5. The Interaction between Packing Pressure and Cooling Rate Literature research* suggests that the application of packing pressure can increase the cooling rate. To determine to what extent this relationship can affect the RFPE process, two sets of trials were conducted. In the first series, pressure was applied shortly after the molten alloy was poured into the cavity. In the second series, the specimens were left to cool at atmospheric pressure. For this experiment, the melt superheat was set to 331 'F, the ejection temperature was set to 200'F, and the mold preheat temperature was varied between 225 F, 250'F, and 275*F. The packing pressure was set to 70 psig. 5.3.6. The Effects of Alloy Composition Finally, throughout all the experiments, observations were made regarding the formation of oxides in the molten alloy and their effect on the process. Particular attention was paid to the mold and the surface finish of the specimens. The porosity information of the surface was also recorded. El Mahallawy, N.A., Taha, M.A., Zamzam, M.L. "On the microstructure and Mechanical Properties of Squeeze-Cast Al-7 wt% Si Alloy," Journalof MaterialsProcessing Technology, Vol. 40, 1994, p. 83. 56 Chapter 6: Theoretical Background for Experimental Analysis In order to analyze the data obtained from the experiments discussed in Chapter 5, some theoretical background is necessary. This chapter begins with an analysis of the asperity deflection mechanism. Then, the analysis of the experimental setup is presented. In particular, the expected temperature drop from the tip of the mold shaft to the thermocouple well is calculated. Additionally, the cooling rate of the mold in air and in ice water needs to be determined. 6.1. The Impact of Surface Finish As Figure 26* shows, surfaces are often idealized as perfectly flat. As such, perfect contact is assumed. However, in reality, the surface deviates from perfect flatness in a number of ways. Figure 26: Model of surfaces as flat, and in perfect contact As Section 4.1.1 mentioned, gross deviations from flatness are called form error. Smaller, higher frequency error is called waviness or roughness. These deviations result in a real contact area that is a fraction of the nominal contact area, as Figure 27 shows. Figure 27: Asperities reduce the real to nominal surface area ratio * Fan, W.,The Effect of Surface Roughness on the Precisionof the EncapsulatedFixturingSystem, S.M. Thesis, Massachusetts Institute of Technology, 2000, p. 27. 5Ibid, p. 28. 57 As a result, the areas in contact are under much higher compressive loads than expected for a given nominal area. Deflection of the surface under this load condition has the potential of affecting the precision of the RFPE process. In order to understand this potential impact, the mechanism of deflection under load must be understood. 6.1.1. The Mechanism of Surface Deflection Under Load When a surface is placed under load, elastic and plastic deformation may occur. It is important to determine how much of the deflection is plastic, as that will result in a change in the encapsulation dimensions. It is also important to determine the maximum surface deflection that is possible with a given surface. The elastic deflection of asperities can be modeled by adapting the Hertzian theory of elastic contact between solids of revolution.* Equation (1) shows the deflection sustained by the asperity at the onset of yield. 81;- 2Y2 R E*2 16 where the Y is the yield strength of the material, R is the radius of curvature, and E* is the modulus of elasticity. The radius of curvature of the asperity is difficult to measure, but can be approximated from the profilometry data by the root mean square curvature, O . Equation (2) defines the root mean square curvature. i=N K7 1/2 N j=1 where N is the number of samples and Equation (3). K K is the summit curvature as defined by zz+1 -2z, +zu 1 2 +(3) h2 where z is the height from the graphical centerline determined by the profilometer and h is the sampling interval defined by Equation (4). h =- L N (4) Fan, W., The Effect of Surface Roughness on the Precision of the EncapsulatedFixturing System, S.M. Thesis, Massachusetts Institute of Technology, 2000, p. 3 6 . 58 With the onset of yield, plastic deformation of the asperity material begins. Theoretically, the material continues deforming until perfect contact has been achieved. However, there has been documented research that shows that asperities typically persist even under high compressive loads.* According to Childs,t the asperity interactions can be modeled using plasticity mechanics. The attainable real to nominal contact area ratio is expected to be between 0.56 and 0.65, with the lower theoretical limit being 0.5. Thus, the maximum possible deflection of the asperities is half the peak-to-valley height of the surface. 6.1.2. Quantification of the Possible Deflection of the Asperities As Section 4.1.1 discusses, profilometers can be used to characterize a surface. Figure 281 shows a typical profilometer trace of a surface. 20000 15000 U) E 10000 0 5000 0 L-5000 -10000 dL IL r 111) -200 IF I HIVIV ALJVV 3 Do -15000 -20000 Data Number Figure 28: Profilometer trace for a 0.4 ptm surface, with no wavelength filtering From the profilometer traces of a series of surface roughness standards, their peak-to-valley depth can be determined. Table 1 presents this data. Moore, A.J.W., "Deformation of Metals in Static and in Sliding Contact," Proceedingsof the Royal Society (London), Vol. A195, 1948, pp. 231. Uppal, A.H. & Probert, S.D., "Deformation of Single and Multiple Asperities on Metal Surfaces," Wear, Vol. 20, 1972, pp. 381 Childs, T.H.C., "The Persistence of Asperities in Indentation Experiments," Wear, Volume 25, 1973, p. 16. Fan, W., The Effect of Surface Roughness on the Precision of the EncapsulatedFixturingSystem, S.M. Thesis, Massachusetts Institute of Technology, 2000, p. 40. § Ibid, p. 42. 59 Table 1: Peak-to-valley depth for various surface roughness standards Ra (tm) 0.05 0.1 0.2 0.4 0.8 1.6 6 (PM) 0.0138 0.009855 0.008811 0.004428 0.004545 0.003258 Peak-to-valley Depth (pm) 0.397 0.753 1.528 3.167 4.239 9.680 The elastic deflection calculated using profilometry data for the same range of surface roughness is shown in Table 2*. Table 2: Roughness, summit curvature, and deflection values of the surface roughness standards Nominal KLA-Tencor Matlab calculations Ra (pm) Ra (pm) RRMS (pm) Ra (pm) RRMS (Am) K (M') 8y (pm) 0.05 0.1 0.2 0.4 0.8 1.6 0.0473 0.079 0.233 0.353 0.673 1.383 0.060 0.106 0.278 0.442 0.837 1.747 0.057 0.096 0.235 0.441 0.620 2.055 0.074 0.140 0.297 0.553 0.789 2.636 37150 51920 58040 115580 112540 157000 0.0138 0.009855 0.008811 0.004428 0.004545 0.003258 Clearly, the postulated elastic deflection is at least an order of magnitude less than the half peak-to-valley height available. Thus, the majority of the deflection will be plastic, with a permanent change in the dimension of the encapsulation. 6.1.3. The Variables for Roughness Measurements as it Relates to Deflection With this understanding of the asperity deflection mechanism, one can develop a methodology to evaluate the impact of surface roughness on the precision of the RFPE process. The surface roughness is characterized by a number of roughness parameters.t Equation (5) defines the first of these parameters, Ra, the average roughness. The average roughness is a measure of the deviation from an artificially imposed centerline. Fan, W., The Effect of Surface Roughness on the Precision of the EncapsulatedFixturingSystem, S.M. Thesis, Massachusetts Institute of Technology, 2000, p. 41. * Tencor P-10 Reference, P/N 412937 Rev. A, 1996, p. 3-8. 60 Ra = fy I dx (5) 0 where L represents the sampling length, while y is the height of the profile measured relative to a graphical centerline computed by the profilometer. x is the incremental distance traversed by the profilometer along the sampling length. For most uniform, well-behaved surfaces, the Ra is a sufficient means to evaluate the characteristics of the surface. Coupled with the data presented in Section 6.1.2, this allows the evaluation of the impact that surface finish has on the RFPE process in Section 7.1. 6.2. Impact of Porosity The encapsulation material is used to locate, secure, and support a workpiece during machining operations. To fulfill its functions, the encapsulation material must remain intact, except in the specific areas that need to be removed for the particular machining operation under consideration. These excised portions should be planned out in advance to prevent a loss of structural integrity of the encapsulated workpiece. Porosity disrupts the microstructure of the encapsulation in an unpredictable fashion. This microstructure directly affects the structural integrity and the surface topography of the encapsulation. As such, it has the potential to impact the RFPE process. 6.2.1. Formation of Porosity As mentioned in Section 4.2.2, porosity is composed of voids that remain when the molten metal solidifies. Porosity has the potential to weaken the strength of the casting. In particular, it can degrade the casting's fatigue resistance* and provide crack nucleation sites.t The presence of surface porosity, through the generation of cold shuts, can impact both the accuracy and the aesthetic quality of the casting.t Anson, J.P., Gruzleski, J.E., "The Quantitative Discrimination between Shrinkage and Gas Microporosity in Cast Aluminum Alloys using Spatial Data Analysis," Materials Characterization,Vol. 43, 1999, p. 319. t Atwood, R.C., Sridhar, S., Lee, P.D., "Equations for Nucleation of Hydrogen Gas Pores during Solidification of Aluminum Seven Weight Percent Silicon Alloy," Scripta Materialia,Vol. 41, No. 12, 1999, p. 1255. I Boileau, James M., Zindel, Jacob W., Allison, John E., "The effect of solidification time on the mechanical properties in a cast A356-T6 Aluminum Alloy," Society ofAutomotive Engineers Technical Paper Series, no. 970019, 1997, p. 62. * 61 These voids, or pores, are generated by three mechanisms. The first type of porosity is generated by shrinkage. As the material in one location of the casting cools and contracts, molten material is drawn from another part of the casting to compensate for the reduction in volume. This mechanism, which usually takes place in long freezing range alloys, is referred to as feeding. Feeding takes place through interdendritic channels. As solidification continues, feeding becomes more and more difficult until the channels are blocked off. To relieve the stress that builds up as shrinkage continues, small pores are formed. These pores tend to form along dendritic channels and are characterized by their long shapes. The second mechanism of porosity generation is through the improper degassing of the molten alloy. The most common of these is the presence of hydrogen in aluminum. The change in solubility of hydrogen as the aluminum alloy transitions from liquid to solid state causes gas pores to form.t The third porosity generation mechanism is gas entrainment.t Gas present in the mold during the injection process can become trapped. Common causes for pores generated by gas entrainment are the presence of turbulence in the mold and inadequate vents. Both types of gas pores are usually spherical in nature. Turbulence induced pores can be distinguished due to their elongated profile. 6.2.2. Classification of porosity: Macroporosity and Microporosity As discussed in Section 6.2.1, there are three types of porosity. While one can describe a surface by the types of porosity present, often one is looking only for a characterization of the surface regardless of the cause of the porosity. In this case, it is helpful to determine whether there is microporosity or macroporosity, or both, present on the surface. Microporosity refers to defects that are less than one millimeter in size. On the other hand, macroporosity refers to any defects that are greater than one millimeter in size. Macroporosity can include cold shuts and misruns.** Anson, J.P., Gruzleski, J.E., "The Quantitative Discrimination between Shrinkage and Gas Microporosity in Cast Aluminum Alloys using Spatial Data Analysis," Materials Characterization, Vol. 43, 1999, p. 320. Kuznetsov, A.V., Vafai, K., "Development and Investigation of Three-Phase Model of the Mushy Zone for Analysis of Porosity Formation in Solidifying Castings," InternationalJournalofHeat Mass Transfer, Vol. 38, No. 14, 1995, pp. 2557-2559. t Saikawa, S., Nakai, K., Sugiura, Y., Kamio, A., "Effects of Hydrogen Gas Content on Generation of Porosity in Al-Li Casting Alloys," Materials Transactions,JIM, Vol. 40, No. 1, 1999, p. 57. I Bar-Meir, G., Eckert, E.R.G., Goldstein, R.J., "Pressure Die Casting: A Model of Vacuum Pumping," JournalofManufacturingScience and Engineering,Vol. 118, May, 1996, pp. 259. § Medeiros, S.C., "Failure Analysis of an Aluminum Casting," Advanced Materials & Processes,April, 1999, p. 4 2 . ** Ibid. * 62 6.2.3. Porosity and the RFPE Process Most of the research on porosity tends to focus on aluminum alloys, particularly on the elimination of shrinkage and hydrogen gas pores. Others work on specific materials with unique properties, geometries, and conditions. The models used for porosity prediction are mostly derived from experimental correlations and are particular to the type of alloy and operating condition. The material in these studies is of limited use because the phenomena are extraordinarily specific. However, they do provide a sense of the parameters that may impact porosity formation. In addition, design rules to significantly reduce porosity, such as proper vent sizing and siting, were developed by Bar-Meir.* One must also keep in mind that the function of the encapsulation differs greatly from that of typical casting components. While most cast components are design to exceed the service life of the systems of which they will be a part, the RFPE encapsulation is strictly for temporary service. It is intended to function as the fixturing medium for the duration of the machining operations on the workpiece. Then it will be melted down for recycling. During this short life cycle, the encapsulation will only be exposed to a limited number of load cycles. This means that fatigue failure is not of great concern in this application. The only concern engendered by porosity is the presence of pores in sufficient quantities that the strength and accuracy of the encapsulation is compromised. This would prevent the encapsulation from carrying out its function to locate, hold, and support the workpiece. The presence of internal pores that will affect the strength of the encapsulation is largely a function of design parameters and is outside the scope of this study. The experiments outlined in Chapter 5 examine the effects of various process parameters on the amount on external porosity present on the encapsulation specimens. 6.3. Temperature Drop from the Mold Cavity to the Thermocouple Well To be able to interpret the data obtained during the experiments, it is important to determine the temperature drop across the distance from the tip of the hole to the mold cavity. The thermal resistance across that distance is composed of two elements: conductive resistance and contact resistance. The temperature drop due to conduction across that distance was determined approximately using the equation for radial conductive heat transfer.t Rearranging the equation to solve for the temperature drop yields Equation (6). Bar-Meir, G., Eckert, E.R.G., Goldstein, R.J., "Pressure Die Casting: A Model of Vacuum Pumping," JournalofManufacturingScience and Engineering,Vol. 118, May, 1996. t Mills, A.F., Basic Heat and Mass Transfer,Richard D. Irwin, Inc., Chicago, USA, 1995, p. 69. 63 AT = ln(r 2 / )Q 2,zkL (6) where rj and r2 are the inner and out radii respectively, Q is the heat transfer rate, k is the thermal conductivity, and L is the height of the mold. Figure 29 shows this temperature drop from the cavity of the mold to the tip of the thermocouple as a function of the rate of heat transfer. 0 15- o1 05- E 0 0 0 800 400 600 200 Heat Transfer Rate (W) 1000 Figure 29: Temperature drop due to conductive resistance as a function of heat transfer rate Over the range of temperatures we are concerned with, the temperature drop as a function of the heat transfer rate is effectively linear. In order to gain a sense of the maximum pressure drop possible, an approximate Q was calculated using one-dimensional heat transfer and the electrical analogy. The heat transfer from molten alloy at 406'F to ambient air temperature at 60'F is approximately 42 W. Therefore, the maximum temperature drop due to conductive resistance is 0.6'K, or 0.108'F. The measure of the contact resistance is given in terms of an equivalent interfacial heat transfer coefficient, hi. Equation (7) solves for the temperature drop given the equivalent heat transfer coefficient. AT= h1A Q represents (7) the heat transfer rate as determined above. A represents the tip area of the thermocouple. AT represents the temperature drop across the interface. The contact resistance for a stainless steel to aluminum interface is approximately 4000 W/m 2 K.* Based on a heat transfer rate of 42 W and a tip area of 7.9x10- 6 M2 , this would only result in a temperature drop of 0.133'K, or 0.24'F. When the contributions of the two thermal resistances are added together, this results in a maximum temperature drop of 0.35*F. This is insignificant when compared to the error margin of the thermocouple. Therefore, * Mills, A.F., Basic Heat and Mass Transfer, Richard D. Irwin, Inc., Chicago, USA, 1995, p. 69. 64 the thermocouple provides an acceptable means of determining the conditions within the mold cavity. 6.4. Variations in Cooling Rate The experiment outlined in Section 5.3.2 explores the effect of different cooling rates on the dimensional accuracy of the process. The cooling rates using different mediums are calculated in the following analysis. The simplest way to determine the cooling rate would be to use the lumped parameter approximation* defined in Equation (8). This validity of this approximation can be verified with the final result. dT = (T -T,) pVc dt (8) where h is the convective heat transfer coefficient, p is the density, V is the volume, c is the heat capacity and T and Te represent the mold and environmental temperatures respectively. The suitability of the lumped parameter approximation can be tested using the Biot numbert defined in Equation (9). Bi - Rinternal _ Rexternal hL (9) k The laminar convective heat transfer coefficient can be calculated using the correlation developed by Churchill and Chu shown in Equation (10).1 RaL =GrPr Gr = ATgL V2 9/16 -16/9 0 (10) L= NuL 0.68+0.67(RaLTY h- NuLk L * Mills, A.F., Basic Heat and Mass Transfer,Richard D. Irwin, Inc., Chicago, USA, 1995, p. 30. SIbid, p. 32. + Ibid, pp.293-29 4 . 65 Where RaL, Gr, V NUL, and h are the Rayleigh number, Grashof number, Prandtl number function, Nusselt number, and the convection heat transfer coefficient respectively. , A T, g, L, v, Pr,and k represent the volumetric coefficient of expansion, the temperature change, gravitational acceleration, length of the convective surface, kinematic viscosity, Prandtl number, and thermal conductivity respectively. Using an initial mold temperature of 330'F, ambient air temperature of 70'F, ice water temperature of 32'F, and a vertical distance of 4 inches, the heat transfer coefficients were calculated. The heat transfer coefficient is 8.03 W/m 2 K for ambient air and 259 W/m 2 K for the ice-water bath. The Biot numbers for the air and the ice water baths conditions are both much smaller than 0.1. Therefore, the lumped parameter approximation is suitable for the current calculations. From Equation (8), the predicted cooling rate for ambient air is 0.02750 K/s, or 0.0500 F/s. The predicted cooling rate for an ice water bath is 0.886*K/s, or 1.60'F/s. 66 Chapter 7: Experimental Results With the understanding of the experimental apparatus developed in Chapter 6, we are now ready to consider the experimental results of the experiments described in Chapter 5. 7.1. The Effect of Melt Superheat and Mold Preheat Temperature The melt superheat and the mold preheat temperature have the potential to affect surface finish, porosity, and dimensional accuracy. In particular, this effect was determined by the difference between the melt superheat temperature and the mold preheat temperature as well as the two temperature settings relative to the melting point of tin-bismuth. The experiments were intended to determine the effect of these two process parameters on the metrics. Table 3 presents the visual observations of the surface. The surface finish was good when the melt superheat was greater than or equal to 331 'F and the mold preheat temperature was greater than or equal to 250'F. At these settings, only microporosity was present on the surface. Below those temperature levels, the surface was marred by both macroporosity and microporosity. Table 3: Description of the surface condition as a function of the injection temperature and mold preheat temperature Mold Preheat Temperature (*F) 275 250 225 200 Injection Temperature (*F) 293.5 331 368.5 406 Small pores distributed Smooth surface with tiny, almost invisible pores. across surface. A few very small pores across surface. Small pores with path lines around edge. No flow lines evident. Flow lines and pores Small pores sprinkled across surface. present. Small amount of flow lines. Premature freezing of alloy. Pores and flow lines present. However, aside from the extreme cases, these indications do not seem to impact the surface finish beyond mere aesthetics. The specimen surface, as expected at this pressure, is a near-mirror reflection of the mold surface. Regardless of the melt superheat and mold preheat temperature, the surface roughness was always less than 1.6 pm. From Table 1, this corresponds to a peak-to-valley height of approximately 9.68 pIm. The maximum possible deflection of the surface is the half height, which is 4.84 pIm, or 0.00019 inches. This is more than an order of magnitude less than the desired tolerance 67 of 0.005 inches for the RFPE process. Therefore, one can conclude that the process is robust against surface finish and surface porosity variations introduced by the melt superheat and mold preheat temperatures. Table 4 contains the specimen diameters measured upon extraction from the mold. The average diameter is 1.0104 inches, with a standard deviation of 0.0004 inches. The specimen diameters were found to be 1.0104 inches, with a standard deviation of 0.000378 inches, for Mold A and 1.0104 inches, with a standard deviation of 0.000417 inches, for Mold B. The variation overall and between the molds is within the tolerance of the micrometer. Table 4: Measurement of specimen diameters Mold Temperature (*F) 275 250 225 200 Injection Terperature (IF) 293.5 1.011 1.011 1.010 1.010 331 1.0105 1.010 1.0010 1.0105 368.5 1.011 1.0010 1.0105 1.0105 406 1.0105 1.0010 1.0105 1.0105 Variations in the melt superheat and the mold preheat temperature did not seem to have a significant difference on the dimensional accuracy of the specimens. The difference between the measurements and the 1.008 inches diameter of the mold cavity is due to the thermal expansion of the mold. Aluminum's coefficient of thermal expansion is 22x10-6/OK. The 211OF, or 1 17.2'K, difference between the ambient environmental temperature and the melting point results in a thermal strain of 0.00258 for the aluminum. At 281 OF, this would give the mold cavity an expanded diameter of 1.0106 inches. This corresponds well to the measurements of the specimens. The coefficient of thermal expansion seems to be the dominant effect affecting the dimensional accuracy of the RFPE process. For encapsulation mold design, this variation will have to be considered carefully in order to achieve an encapsulated workpiece of the desired dimension. In addition, the mold temperature at which the embedded workpiece is reinserted for reencapsulation will have to be carefully controlled to minimize induced stresses due to thermal expansion. Finally, the controlled preheating temperature will permit the mold to fit and seal properly around the encapsulated workpiece. 68 7.2. The Effect of Ejection Temperature The temperature at which the specimens are ejected from the mold has the potential to impact the surface finish and dimensional accuracy of the specimens. In order to determine the sensitivity of these metrics, specimens were ejected from the mold at 150 0F, 200 0 F, and 250*F. When the specimen was produced at a high melt superheat with an initial low mold temperature, there were some instances where the alloy had not completely solidified when the specimen was extracted. There was insufficient time for the entire specimen to cool below the tin-bismuth's melting point. Care should be taken to ensure that this does not take place during the actual encapsulation. Despite this, no additional variations in surface finish beyond those caused by melt superheat and mold preheat temperature was noted. The difference in dimension was accounted for by the thermal expansion of the mold. Therefore, one may conclude that both the surface finish and dimensional accuracy of the RFPE process are independent of the ejection temperature over the range tested. 7.3. The Effect of Cooling Rate One of the concerns with using a phase change process was the relatively long cycle time compared to the other universal fixturing concepts. This is due to the requirement for heat transfer into and out of the encapsulation. Therefore, it is desirable for the cooling time to be reduced as much as possible in order to reduce the cycle time. However, counterbalancing that requirement was the potential for a rapid cooling rate to negatively impact the surface finish, porosity, and dimensional accuracy of the RFPE process. Figure 30 shows the cooling rate of the specimen using both air and ice water as the convective medium. The air and ice water medium yielded cooling rates of 2.407'F/s and 0.0776 0 F/s. This is similar to the predicted cooling rates of 1.6 0 F/s and 0.05'F/s. The difference can be explained by environmental factors that resulted in forced convection, such as air conditioning and mixing of the ice bath as the mold was inserted. There were no surface finish, porosity, and dimensional accuracy variations attributable to the variation in the cooling rate. The results of the experiments show that, regardless of whether the specimen was cooled in an ice water bath or in ambient air, the surface finish, porosity and dimensional accuracy was not affected at a level detectable by visual inspection and by the instruments used. 69 280 270 260 L- -cAir Cooled 4) 250 i 240 E 230 - Ice Water Bath 220 210 -IL 200 1 201 401 601 801 Time (s) Figure 30: Cooling rate of mold in air and in ice water 7.4. Aging Effects As mentioned in Section 4.2.3, aging is caused by the presence of thermal and kinetic stress. These stresses can be created by shrinkage, turbulence, and premature solidification. The gradual relaxation of these stresses over a period of time as the specimen tends towards equilibrium may result in changes in the specimen dimension and surface finish. The specimens from the previous three experiments were measured immediately following ejection, several hours later and once weekly after that. The only variation that was noted can be attributed to thermal expansion as discussed in Section 7.1. There were no changes in dimension between the second, third and fourth weeks. The surface inspections and comparisons between the specimens and the surface roughness standard did not detect any variations. There were no detectable changes in porosity. The lack of variation during to aging is due to two reasons. First, the experiments were carried out by hand-pouring the alloy into the mold. The low rate of alloy introduction into the mold minimizes the amount of turbulence present, thus neutralizing the kinetic effects. Second, the slow rate of solidification, even with the ice water bath, provided sufficient time for the thermal effects to dampen out. From this, one may conclude that, as long as the process operates in moderate injection and cooling regimes, the metrics of surface finish and dimensional accuracy are not sensitive to aging effects over the range and duration of operations of the RFPE process. 70 7.5. The Interaction between Packing Pressure and Cooling Rate An experiment was conducted to determine the effect of pressure on cooling rate. Figure 31 shows the cooling rate of the specimen at atmospheric pressure and at 60 psig. The cooling rate with pressure was 0.089 0F/s compared to 0.049 0 F/s when the mold was at atmospheric pressure. The 83% increase in cooling rate demonstrates the positive correlation between packing pressure and cooling rate described in Section 4.2.2. 270 o-% 260 Atmospheric 250 L Pressure 240 E 230 0, M- 220 60 psig 210 200 M- C LO, 04 0) (O MO T_ (0j Mv MC MC NlIO- M 0M N T01 Cv, 0 L( 0) N0) 0 a, (%. T_ CO, Time (s) Figure 31: Comparison of the cooling rate of a pressurized and unpressurized mold cavity 7.6. The Effects of Alloy Composition Alloy composition plays an important role in the RFPE process. This is especially true given the dependence of the process on the alloy material properties. Lee, Valdivia, and Fan* have addressed a number of issues regarding alloy composition: rewelding, thermal drift, and the use of eutectic tin-bismuth. It was noted during the experiments that high temperature, rapid changes of temperature, and agitation all result in the rapid generation of oxides. These oxides are less dense than the tin-bismuth alloy and float to the top of the reservoir. While the presence of oxides * Lee, E., Valdivia, P., Fan, W., Sarma, S.E., "The Process Window for Reference Free Part Encapsulation," To appear in ASME JournalofManufacturingScience & Engineering. 71 does not seem to affect dimensional accuracy, it has shown the potential of affecting the RFPE process in terms of surface finish and porosity. The oxides tend to aggregate on the surface of the specimen. This causes blemishes on the specimen surface. In addition, the oxides contaminate the surface of the mold. This makes it easier for air bubbles to be trapped on the specimen-mold interface. The simplest solution to the oxide issue is to avoid introducing it into the alloy stream. This can be best accomplished by locating the alloy intake at a small distance above the bottom of the reservoir. This would allow the intake to both avoid the layer of oxide lying on top and any debris that may have settled on the bottom of the reservoir. Secondly, agitation of the alloy should be kept to a minimum to avoid both the generation of oxides and the mixing of the oxides into the alloy stream. The amount of oxide present in the system can be avoided by using filtering systems to continuously skim off the oxide on the surface of the reservoir. Finally, temperature control, both in the avoidance of high temperatures and of high rates of temperature change, would be required to minimize oxide generation. 72 Chapter 8: The RFPE Process Parameter Map Current fixturing technology is the critical link in manufacturing. Fixturing is the choke point that impedes the flow of ideas from design to production. The limitations of current fixturing systems severely restrict the component geometries that can be produced at a reasonable cost. It forces the designer to take roundabout routes, such as dividing the part into smaller, simpler components or embedding locational or workholding attachments into the design, in order to produce the component. The universal fixturing technologies provide a much greater flexibility. However, this flexibility comes at the cost of robustness. Conformable clamp systems have poor damping capabilities and are mechanically unreliable. Fluidized bed technologies are flexible and allow relatively fast turnovers, but are limited to low workholding forces and often sacrifice accuracy when the bed settles. Phase change systems have excellent workholding properties, but the relatively slow cycle time and hardware-intensive systems used to establish the locational reference form major detractors. Sarma* developed a paradigm shift for fixturing systems: the Reference Free Part Encapsulation Concept. Since the viability of this concept has been proven experimentally, it was important to fully understand the RFPE process to allow further development. In order to do this, a literature review of similar processes was conducted. Additionally, research to date was examined to see what knowledge we have already gained. With this foundation, the RFPE process parameters and metrics were defined and an initial process parameter map was constructed. As Figure 21 shows, the effects on packing pressure on all the parameterst had been examined in addition to the causes of thermal drift and re-welding strength.t However, the effects of melt superheat, mold preheat temperature, ejection temperature, cooling rate, aging, and alloy composition on surface finish, porosity, and dimensional accuracy had yet to be examined. This study explored these areas through a literature review, theoretical analysis, and experimentation. This investigation resulted in a completed RFPE Process Parameter Map, presented in Figure 32. This study also explored the relationships between the following process parameters: melt superheat and mold preheat temperature, melt superheat and ejection temperature, melt superheat and alloy composition, mold preheat temperature and cooling rate, mold preheat temperature and ejection temperature, cooling rate and ejection temperature, cooling rate and packing pressure, and cooling rate and aging. The Final RFPE Interaction Matrix is presented in Figure 32. Sarma, S.E., A Methodologyfor IntegratingCAD and CAM in Milling, Ph.D. Thesis, University of California, Berkeley, 1995, pp. 28-57. * Fan, W., The Effect of Surface Roughness on the Precision of the EncapsulatedFixturing System, S.M. Thesis, Massachusetts Institute of Technology, 2000, p. 51. Lee, E., Valdivia, P., Fan, W., Sarma, S.E., "The Process Window for Reference Free Part Encapsulation," To appear in ASME JournalofManufacturingScience & Engineering. 4 73 -Metrics *I Process Parameters Surface finish Porosity Dimensional Accuracv Thermal drift Melt superheat Mold preheat temperature Cooling rate Ejection temperature Packing pressure Aging Alloy Composition [This thesis] [Source] [This thesis] Materially Independent Map completed Figure 32: Completed RFPE Process Parameter Map 74 Rewelding strength _____________ Process Parameters Melt superheat Mold preheat temperature q Cooling rate p Ejection temperature p Packing pressure p Aging Alloy composition Melt superheat preheat temperature Cooling rate Ejection temperature Packing pressure Aging Alloy composition Materially independent Relationship Characterized Redundant Spaces Figure 33: Completed interaction matrix for the RFPE process parameters Chapter 9: Future Work The completion of the Process Parameter Map is the critical first step in further developing the RFPE process. From this point, there are a number of avenues of research that can be pursued. As discussed in Section 3.2, once the process parameters are established, the design parameters can be coherently selected for any particular implementation of the system. This is the next step in bringing RFPE to life. In order to do this, the design parameters of the process must be defined. Once these design parameters have been defined, any interdependencies between the process and design parameters must be explored. This will allow us to expand the RFPE Interaction Matrix. With this foundation in place, a field prototype can be developed. With the lessons learned from this field prototype, a coherent rapid prototyping system can be built. 9.1. Study of Design Parameters Since the process parameters have been identified, the mapping of the design parameters can begin. This will identify the factors that have a major impact on the quality, cost, and cycle time of the RFPE apparatus. As Appendix A discusses, there are many design parameters that must be considered when designing the apparatus, including orifice size, injection pressure, shot size, cooling direction, mold surface finish, mold locking pressure, siting of vents, and siting of injection ports. These parameters denote the limits of the process that can be achieved with a given apparatus built to certain specifications. Interrelationships between design parameters also help determine additional design variables. An example of this is the relationship between orifice size, vent siting, and injection pressure that determines the injection velocity, the cavity fill time, and the turbulence during the molding process. Finally, one must study the interaction between process and design parameters. 9.2. Design of a Field Trial Prototype Once the RFPE Design Parameter Map has been developed, the apparatus can be designed according to the optimal settings and ranges. The design should include not only the encapsulation machine, but also the associated encapsulated workpiece fixture. In addition, procedures will have to be developed for the application, machining, and removal of the tin-bismuth. Field trials can then be carried out to validate the function of this design. From the understanding gained during these trials, the design and procedures can be fine-tuned. The objective of these trials will be to demonstrate the optimal capabilities of the RFPE process. This test may include some or all of the machining strategies. 77 9.3. Development of a Rapid Prototyping Center Once the RFPE System is fully developed, we envision using it as the core component of a Rapid Prototyping Center. Figure 34* shows an RFPE System and three milling machines in a model of one of these Centers. Figure 34: Rapid Prototyping Center This Rapid Prototyping Center will further transform the manufacturing process. Unique designs will no longer require individual attention. Instead, the manufacturing process will be a black box. As Figure 35t displays, the inputs to this process will be a unique G-code and raw stock while the outputs will be the unique products. * Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 17. Ibid, p. 378. 78 E~1\ Customer A Customer B >24 Unique G code Figure 35: The Rapid Prototyping Center will transform the manufacturing process from a heavy manual intervention process into a black box The power of this Center is that the planning and set up time will be virtually eliminated. In fact, manufacturing will move from requiring intensive human decision making to one where the majority of the energy can be dedicated toward design work. This will drastically reduce the cost of manufacturing. In fact, in this Rapid Prototyping Center, a central computer controller can control the entire process, as Figure 36* shows. * Lee, E.C., Development of an EncapsulationProcessfor use in a Universal Automated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 38. 79 Encapsulation Machine Queue 2 Queue 1 noCentral Computer Controller MachineTool Queue 4 Queue 3 Figure 36: Proposed process flow for the Rapid Prototyping Center If we take this a step further, we can take advantage of other technology under development and have the central computer controller have a single input: the CAD drawing of each part that is desired. This controller uses tool path generation* to generate the G-code. This G-code is parsed into machining passes. These machining passes are then automatically controlled, with reencapsulation occurring in between consecutive machining operations. Thus, the designer only needs to worry about putting his or her ideas down on paper. The rest will be taken care of by the Rapid Prototyping Center. Thus, Rapid Prototyping Centers will have the ability to "revolutionize the way engineers and designers think about product development and manufacturing. Just as the concepts of mass production-assembly lines, interchangeable parts--have revolutionize [d] manufacturing, so shall rapid prototyping through machine tools. The ability to create one part as quickly, efficiently, and as economically as creating a thousand of those parts, that is the next frontier in manufacturing and product development."f This may all sound like a dream-but dreams give us a goal. Lee took the first step in proving Sarma's idea. The development of the Process Parameter Map completed the next step in the process. With the efforts of others in pursuing the next stages of development, Rapid Prototyping Centers can become a reality. Institute Balasubramaniam, M., Automatic 5 Axis NC Toolpath Generation,Ph.D. thesis, Massachusetts of Technology, 2001. Fixturing t Lee, B.C., Development of an EncapsulationProcessfor use in a UniversalAutomated System, S.M. Thesis, Massachusetts Institute of Technology, 1999, p. 18. * 80 Appendix A: An Introduction to the RFPE Design Parameters In the course of conducting the literature review for the RFPE process parameters, some information was gathered on the design parameters. In an attempt to avoid duplicating effort in the next stage of RFPE process development, this Appendix presents these initial findings. The design parameters for the RFPE System can be divided into two categories. The first category affects the storage and delivery of the molten alloy. The second category affects the introduction and behavior of alloy inside the mold. A.1. Parameters Affecting the Alloy Storage and Delivery In the RFPE process, the material properties of the phase change material determine the workholding, damping and support characteristics of the fixturing system. While this ensures that the fixturing quality remains stable regardless of the part geometry, variations in the alloy composition will impact the reliability of the system. Therefore, it is imperative that all avenues for potential degradation of alloy quality be identified and neutralized. This section will examine a number of such avenues. A.1.1. The Reservoir The reservoir forms an inseparable part of any encapsulation machine. It is the location where the alloy is melted down and stored in preparation for injection into the mold. The objective of reservoir design is to create a system that can provide alloy in the desired state with a minimum of contaminants. There are three design parameters to be considered: reservoir temperature, proportion of new to recycled alloy, and reservoir construction. A.1.1.1. Reservoir Temperature The reservoir temperature is the temperature of the tin-bismuth awaiting injection. The desired reservoir temperature is determined by the melt superheat process parameter and by the physical layout of the machine. The experiments discussed in Section 7.1 established the desired melt superheat. The physical layout of the apparatus determines the heat loss that takes place between the reservoir and the injection point into the mold. The reservoir temperature is, in essence, the desired injection temperature plus the temperature difference necessary to account for the heat loss during alloy delivery. The correct setting of this design parameter has an important impact on the metrics used to measure the quality of the encapsulation. If the reservoir temperature is set too low, there will not be sufficient melt superheat. This will result in poor surface finish and porosity as outlined in Section 7.1. Variation in the reservoir temperature will lead to 83 variation in the thermal expansion of the encapsulation, thus resulting in varying dimensional accuracy.* If the reservoir temperature is too high, the resultant excessive superheat has the potential of causing thermal drift of the encapsulated workpiece. Finally, the reservoir temperature will likely have an impact on the microstructure of the alloy.' This, in turn, will impact the strength of the encapsulation. The reservoir temperature also has an effect on the process parameters. The relationship between the reservoir temperature and the melt superheat has already been outlined above. In addition, the reservoir temperature, by setting one end of the temperature gradient, plays a part in determining the cooling rate. Finally, the reservoir temperature will have a large effect on the alloy composition. In particular, high reservoir temperatures, as well as sharp temperature fluctuations, tend to encourage oxide formation. This was born out by experimental observation noted in Section 7.6. A.1.1.2. Proportion of New to Recycled Alloy Once machining operations are complete, the encapsulation is melted off the embedded workpiece and, along with any scraps generated, returned to the reservoir. The alloy is then recycled for future operations. The use of recycled alloy provides an avenue for the introduction of contaminants such as cutting fluid, metal scraps, and oxides. Methods for dealing with the contaminants are covered in Section A. 1.1.3. The inevitable loss of alloy during the machining process means that new alloy will have to be introduced. The tradeoff lies between introducing the minimum amount of new alloy necessary to replenish losses to optimize the economics of the process and providing sufficient pure alloy to ensure alloy quality in the process. Inability to ensure alloy quality may result in poor surface finish and porosity as contaminants are introduced into the mold. In sufficient quantities, these contaminants have the potential to affect the strength of the rewelding between old and new portions of the encapsulation. Finally, the introduction of metal chips and other contaminants into the encapsulation machine may negatively impact the reliability of the system. A.1.1.3. Reservoir Construction In addition to the above design considerations, the construction of the reservoir will heavily influence the quality of the alloy available for encapsulation. This influence is transmitted through three design considerations: construction materials, heater selection and siting, and contaminant containment. * Allsop, D.F., and Kennedy, D., PressureDiecasting;Part2, Pergamon Press, New York. 1983, p. 15. t Murray, M.T., Griffiths, J.R., "The Design of Feed Systems for Thin-Walled Zing High-Pressure Die Castings," Metallurgicaland Materials Transactions,Vol. 27B, February, 1996, p. 115. 84 The material used to construct the reservoir must meet three basic requirements. It must be suitable for long duration, high temperature service. The reservoir surface must be durable against impacts and not contribute contaminants to the melt. Finally, the reservoir material must be chemically inert when placed into contact with the molten alloy at operating conditions. The heaters must be sited to minimize the heat transfer resistance between the heater and the molten alloy. The location of the heaters also plays an important part in ensuring the even distribution of temperature. This will avoid the creation of hot spots that would result in oxide generation. Finally, heaters and associated control systems must be selected so that the system is responsive within the operational range and is capable of maintaining the desired temperature with minimal fluctuations. The final consideration of reservoir construction is contaminant containment. This refers to the goal of ensuring alloy quality by preventing the introduction of contaminants into the encapsulation machine. Since the oxides tend to float on the surface of the melt and debris such as metal chips tend to sink to the bottom, one solution would be to locate the alloy intake at a set distance above the bottom of the reservoir. This will not only avoid the oxide floating on the surface, but will also provide a sump to allow metal chips to settle. To further improve the alloy quality, filtration systems can be installed. Studies of filtration systems used with other casting materials and processes will provide a useful first step in this endeavor*. A.1.2. Alloy Delivery Once the alloy has been heated to the correct temperature, it is ready to be injected into the mold. The alloy is pumped from the reservoir to the mold using a piston cylinder arrangement. The piston can be actuated pneumatically or hydraulically. While hydraulic cylinders allow higher reaction times and pressures, these qualities are not necessary for the RFPE process. The functionality of the pneumatic cylinders was quite sufficient for this application. In addition, the pneumatics cylinders have an advantage in terms of cost and ease of use.t A number of design parameters affect the efficacy of this process, including injection pressure, shot size, rate of change of pressure, opposing pressures on each side of the piston, inertia, transfer tubing design, and partial blockages of the metal stream. * 1 Neff, D.V., "The Filtering and Degassing of Aluminum Die Casting Alloy" Die CastingEngineer, Vol. 18 2 4 30, No. 5, September-October, 1986, pp. - . Lee, E.C., Development of an EncapsulationProcessfor use in a UniversalAutomated Fixturing System, S.M. Thesis, Massachusetts Institute of Technology, 1999, pp. 50-51. 85 A.1.2.1. Injection Pressure The injection pressure refers to the pressure of the molten encapsulation machine as it enters the mold cavity. This design parameter can impact the surface finish, porosity, rewelding strength, and in extreme cases, the dimensional accuracy of the encapsulated workpiece. A high injection pressure leads to a high injection velocity, which results in a lower fill time and increased turbulence. While the lower fill time may be desirable to improve the cycle time of the encapsulation system, the increased turbulence causes the molten alloy to mix with the air in the cavity. If the encapsulation solidifies before the alloy can settle, air bubbles are trapped in the encapsulated workpiece. This trapped air causes porosity.* If air bubbles are trapped on the surface, the surface finish of the part can be affected. In extreme cases, the dimensional accuracy of the encapsulated workpiece can be sacrificed as the voids on the surface compromise the load bearing ability of the encapsulation. The injection pressure should not affect the location of the encapsulated piece unless the internal porosity level is sufficiently high to degrade the mechanical properties of the encapsulation. This may lead to the failure of the encapsulation during machining. There is no known effect of injection pressure on rewelding strength. The injection pressure is affected by a number of other parameters detailed below. A.1.2.2. Shot Size The shot size is the amount of alloy that can be ejected by the piston-cylinder assembly. A shot size must be larger than the mold volume in order to generate good quality castings. Otherwise, incomplete filling of the mold would occur. The unstable injection pressure, along with the increased presence of air in the system, would increase the chance for porosity. This would compromise both the surface finish and, potentially, the strength of the encapsulation. When the injection piston plays an additional role as the packing pressure applicator, an adequate shot size becomes even more important. An incomplete filling of the mold, or short shot, will not only result in the defects detailed above, but it will also eliminate the hydraulic lock the piston needs to apply the packing pressure. The lack of pressure on the casting would result in an even larger percentage of porosity and lower dimensional accuracy due to the lack of pressure compensation for shrinkage. Finally, the shot size has no known effect on the thermal drift and rewelding strength. * Bar-Meir, G., Eckert, E.R.G., Goldstein, R.J., "Pressure die casting: A Model of Vacuum Pumping," JournalofManufacturing Science and Engineering, Vol. 118, May, 1996, p. 256. 86 A.1.2.3. Rate of Change in Pressure The rate of change of pressure can negatively affect the precision of the RFPE process. The packing pressure effects on surface finish and porosity were explored by Fan.* Variations in the injection pressure will result in varying degrees of air entrapment. This air entrapment can impact surface finish, porosity, dimensional accuracy and rewelding strength. If the rate of change of pressure cannot be applied in a consistent manner, the reliability of the process will be negatively impacted. A.1.2.4. Pressure on Opposing Sides of the Injection Piston Another parameter that may cause variation in the injection pressure is the pressure present on opposing sides of the injection piston. This pressure can vary depending on the design of the piston cylinder, the environmental pressure, and the design of the apparatus. The presence of pressure on the other side of the injection piston will reduce the actual available injection pressure and potentially result in the negative effects outlined in Section A. 1.2.1. A.1.2.5. Inertia Effects While inertia effects have played a part in determining the quality of die casting processes,t it is not clear how inertia effect will impact the RFPE process. Further research, both in the form of literature review and in experimentation, is necessary. A.1.2.6. Transfer Tubing Design Transfer tubing refers to the tubing that connects the reservoir to the mold. The tubing should be as short as possible to minimize heat loss to the environment. In addition, high and low loops should be avoided as much as possible to avoid trapping air or debris in the line. The air and the debris, if injected along with the alloy, have the potential to affect the surface finish, porosity, and dimensional accuracy of the encapsulation. * I Fan, W., The Effect of Surface Roughness on the Precision of the EncapsulatedFixturingSystem, S.M. Thesis, Massachusetts Institute of Technology, 2000. Upton, B., PressureDiecasting;Part 1, Pergamon Press, New York, 1982, p. 42. 87 A.1.2.7. Partial Blockages of the Metal Stream Partial freezing of the alloy in the metal stream or blockages in the pathway can affect the surface finish and porosity of the encapsulated workpiece. Any blockages in the alloy pathway can increase turbulence, increasing the amount of trapped air bubbles. These air bubbles result in porosity as the encapsulated workpiece solidifies. The partial freezing of the alloy in the metal stream introduces random variation in the encapsulation structure with resultant variations on mechanical properties. This is a particularly important issue to consider since it affects the reliability of the encapsulation strength. One approach towards mitigating this issue is to minimize the flow path of the alloy from the reservoir to the mold. Alternatively, heaters can be used on or near the transfer tubing to ensure that the alloy remains above the melting point during the entire operation. A.2. Parameters Affecting the Introduction and Behavior of Alloy Inside the Mold Once the alloy has been delivered to the mold, one must be aware of the kinetic and thermal effects that will ultimately have an effect on the quality of the encapsulation. The following sections will examine various design parameters that will control these effects. These parameters include gate velocity, cooling direction, heat and cooling of the mold, mold surface finish, mold material selection, mold locking pressure, mold vents and compatibility of gate and machined section geometry. A.2.1. Gate Velocity The gate velocity is the rate at which the alloy enters the mold. The velocity, which determines the cavity fill time, is a function of the orifice size, injection pressure, and frictional effects on the alloy. This parameter has the potential to impact the surface finish, porosity and dimensional accuracy of the encapsulation. A high gate velocity will result in a great deal of turbulence. On the other hand, too slow a gate velocity means that the alloy will cool before the mold is entirely filled, causing cold shuts. Allsop recommends a two stage filling strategy.t The first stage is at a lower velocity to reduce turbulence and permit air to vent from the mold. The second stage is at a higher velocity to complete filling the mold before solidification takes place. In this fashion, the turbulence, and thus the amount of porosity generated, will be greatly reduced. * Upton, B., PressureDiecasting;Part1, Pergamon Press, New York, 1982, p. 42. t Allsop, D.F., and Kennedy, D., PressureDiecasting;Part2, Pergamon Press, New York. 1983, p. 6-7. 88 A.2.2. Cooling Direction The application of directional cooling to the mold may help ensure the quality of the encapsulation by improving the surface finish and dimensional accuracy and lowering the porosity. A mold that is cooled from the bottom up will provide more time for air bubbles to escape, thus reducing porosity. In a mold where the gate is located at the top, the shrinkage effect will also be minimized, as packing pressure will be applied until the moment the gate freezes. Experiments should be carried out to determine the effect that directional cooling has on the microstructure of the encapsulation. This may have an impact on the strength of the encapsulation. A.2.3. Heating and Cooling of the Mold The temperature of the mold, along with the temperature of the melt, controls the temperature gradient and, thus, the heat transfer rate from the encapsulation to the environment. The implementation of heating and cooling channels on the mold body would allow the cooling rate to be varied in a programmed fashion. Although this would increase the complexity of the apparatus, such a heat transfer control system may be necessary to achieve the cooling requirements laid down by Lee* to maximize rewelding strength while minimizing the risk for thermal drift. Directional cooling may also be implemented once such a system is in place. Finally, this type of system will allow cooling to be controlled so that the kinetic effects have an opportunity to dampen out and allow thermal effects to dominate in the solidification process.t A.2.4. Mold Surface Finish The mold surface finish is very important to the RFPE process. The process parameter windows have been selected to replicate the mold surface finish. As long as a fine mold surface finish is selected, coupled with a packing pressure above 60 psi, the surface finish of the encapsulated workpiece will closely follow that of the mold. The mold surface finish should be selected considering the tradeoff between a fine mold finish and its cost and durability. Since a surface that wears out quickly can have a detrimental effect on dimensional accuracy, it would be wise to select the roughest, least delicate surface possible that would suffice. From the results in Section 7.1, mold surface finish with a surface roughness of 1.6 pm is capable of generating an encapsulation surface with an Lee, E., Valdivia, P., Fan, W., Sarma, S.E., "The Process Window for Reference Free Part Encapsulation," To appear in ASME JournalofManufacturingScience & Engineering. T Murray, M.T., Griffiths, J.R., "The Design of Feed Systems for Thin-Walled Zing High-Pressure Die Castings," Metallurgicaland Materials Transactions,Vol. 27B, February, 1996, p. 115. 89 error that is more than an order of magnitude smaller than the tolerance of the RFPE process. This is a surface finish that is achievable using normal machining techniques and repressents a good compromise between fineness and durability. A.2.5. Mold Material Selection The mold surface finish may also be affected by the mold material. In the experiments conducted to examine the process parameters, aluminum molds were used. Aluminum was sufficiently durable for the low number of trials carried out on the experimental molds. However, some scarring patterns developed toward the end of the test. This may be due to wear of the aluminum during the molding process, chemical interactions between the aluminum and the tin-bismuth, and desposition of oxides or other contaminants onto the mold surface. For improved wear resistance, the actual molds used in the encapsulation machines will likely be fabricated out of harder and tougher materials, such as steels. Combined with a surface finish selected with the criteria outlined above, a durable mold that manufactures parts with consistent quality can be fabricated at a reasonable cost. A.2.6. Mold Locking Pressure Mold locking pressure is another avenue by which the dimensional accuracy of the encapsulation may be impacted. Care must be taken during the design process to ensure that sufficient pressure is applied toward locking the mold to overcome the injection pressure. Otherwise, the injection pressure may force the mold open along the parting lines, thus introducing dimensional errors into the encapsulation. A.2.7. Mold Vents The use of mold vents may be necessary in order to evacuate air from the mold. The successful location and sizing of the vents will significantly reduce the amount of air trapped in the mold. Correspondingly, this will reduce the amount of porosity due to air entrapment and improve the surface finish of the encapsulated workpiece. Bar-Meir has developed a methodology for vacuum venting.* This methodology also includes a model for optimizing the vent area, which may be a helpful first step should the need for such vents appear. * Bar-Meir, G., Eckert, E.R.G., Goldstein, R.J., "Pressure die casting: A Model of Vacuum Pumping," JournalofManufacturing Science and Engineering,Vol. 118, May, 1996, pp. 256-265. 90 A.2.8. Compatibility of Gate and Machined Section Geometry Finally, the geometry of the machined section that needs to be refilled needs to be considered. Depending on the mold design, some limitations may have to be placed on the cavity geometries that can be refilled. This must be considered in conjunction with the positioning of the encapsulated workpiece within the mold during reencapsulation. Otherwise, if the cavity or the gate is poorly located, air may be trapped, causing porosity. 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