Statistics 496, Applied Statistics for Industry II Name: _________________ Exam 2, Spring 2009 Site: ___________________ INSTRUCTIONS: You will have 1 hour and 30 minutes to complete the exam. There are 4 questions worth a total of 100 points. Not all questions have the same point value so gauge your time appropriately. Read the questions carefully and completely. Answer each question and show work in the space provided on the exam. Turn in the entire exam when you are done or when time is up. For essay questions, think before you write. 1. [30] The effects of three process variables; A: Seal Temperature (o F), B: Cooling Bar Temperature (o F), and C: % Polyethylene Additive on the seal strength (g/in) of a bread wrapper stock are studied with a 23 factorial experiment with 4 center points. The data are given below. A 225 285 225 285 225 285 225 285 255 255 255 255 B 46 46 64 64 46 46 64 64 55 55 55 55 C 0.5 0.5 0.5 0.5 1.7 1.7 1.7 1.7 1.1 1.1 1.1 1.1 Strength 6.6 6.9 7.9 6.1 9.2 6.8 10.4 7.3 10.4 9.5 9.8 9.9 The estimated full effects for this experiment are as follows: A: –1.75, B: 0.55, AB: –0.70, C: 1.55, AC: –1.00, BC: 0.30, and ABC: 0.35. The variance at the center points is 0.14. a) [6] Compute the standard error of an estimated full effect and the critical effect size (use t=3). Which of the estimated full effects are statistically significant? Explain briefly. 1 b) [5] Using only those effects that are statistically significant, give the prediction equation for seal strength. Be sure to explicitly define the variables in the prediction equation. c) [3] Using the prediction equation in (b), predict the seal strength for a seal temperature of 225oF, cooling bar temperature of 64oF and polyethylene additive of 1.7%. d) [5] Construct a prediction interval for your prediction in (c). e) [7] Is there evidence of curvature in the response? Be sure to include the mean of the factorial experiment and the mean for the center points as well as the value and interpretation of an appropriate test statistic. f) [4] In light of your result in (e), would you say your prediction in (c) is accurate? Explain briefly. 2 2. [20 pts] Golf ball manufacturers appeal to golfers with claims that their product goes farther, flies straighter or lands softer. Of particular interest is the driving distance of a golf ball. Some of the factors that may affect the distance a golf ball travels are: brand, compression, core and cover. Compression is a measure of the resiliency of the ball when it is struck by the golf club. Golf balls have either a one-piece core or a two-piece core (rubberized string wound around a solid or liquid inner core). The two types of cover commonly used are a hard cover (Surlyn) and a softer cover (Balata). Besides the characteristics of the golf ball, the golfer and weather/course conditions have a big effect on the distance a golf ball will travel. Better golfers can hit the ball straighter and farther than beginners. A 23 factorial experiment is run with a single golfer in a completely randomized design with 5 replications. All golf balls have two-piece cores. The factors are: Factor A: Brand B: Compression C: Cover Low (–1) Titleist 90 Balata High (+1) Maxfli 100 Surlyn The summarized data are: A B C –1 +1 –1 +1 –1 +1 –1 +1 –1 –1 +1 +1 –1 –1 +1 +1 –1 –1 –1 –1 +1 +1 +1 +1 Mean, Yi 260.8 259.8 258.8 257.4 266.0 276.2 275.8 272.6 ni 5 5 5 5 5 5 5 5 Variance, s i2 136.7 81.7 120.2 170.3 166.0 113.7 171.7 104.3 a) [6] Complete the following list of estimated full effects. Effect Name Y A B AB C AC BC ABC Estimate 265.925 0.45 13.45 2.35 2.65 –3.25 3 b) [2] Compute the MSrepError for this problem. c) [5] Calculate the standard error of an estimated effect and give the critical effect size, use t=3. What effect(s) is(are) significant? d) [7] In a brief paragraph, summarize your findings. This paragraph should be written so that it could be understood by someone with little or no knowledge of statistics. Be sure to comment on the limitations of this experiment. 4 3. [20 pts] An engineer is interested in the effects of cutting speed (A), tool geometry (B), and cutting angle (C) on the life (in hours) of a machine tool. The levels of each of the 3 factors are given below. low (–1) 50 rpm Type 1 5o A: cutting speed B: tool geometry C: cutting angle high (+1) 100 rpm Type 2 10o Since the hardness of the raw material being tooled may vary, heats of raw material are used as blocks. Below are the data. A –1 +1 –1 +1 –1 +1 –1 +1 B –1 –1 +1 +1 –1 –1 +1 +1 Block Mean C –1 –1 –1 –1 +1 +1 +1 +1 I 22 32 35 45 43 36 50 47 38.75 Block II 31 43 50 55 45 38 61 43 45.75 III 25 30 35 47 38 40 54 39 38.5 Mean 26 35 40 49 42 38 55 43 41.0 For this experiment SSrepError = 474.0 with 16 degrees of freedom. Then estimated full effects are: A: 0.5, B: 11.5, AB: –2.0, C: 7.0, AC: –8.5, BC: –2.5, ABC: –2.0. a) [4] Below is a plot of the main effects. Comment on the apparent effects of the three factors. 5 b) [5] Below are plots of the A: Speed by C: Angle interactions for Type 1 and Type 2 Geometries. What do these plots indicate about the possible interaction between A and C? What do they indicate about the 3-way interaction? c) [8] What is the standard error of an estimated full effect? d) [3] What effects are statistically significant? Use t=3. 6 4. [30 pts] A 24 un-replicated factorial experiment was conducted on the polymer resin, PMR-II-50 to see the effect of four factors on weight loss. The four factors and their levels are given below. Factor Oven Position Kapton Preprocessing Dianhydride Low Level (–1) Position 1 no kapton (0) Time 15 minutes Type Polymer grade (1) High Level (+1) Position 2 with kapton (1) 120 minutes Electronic grade (2) All specimens, which initially had about the same mass, are baked at 600oF for 936 hours. The percent weight loss (wghtloss) is the measured response. The output of the analysis of the 16 observations is given below. Fractional Factorial Fit Estimated Full Effects and Parameter Estimates for wghtloss Term Constant Position Kapton Time Type Position*Kapton Position*Time Position*Type Kapton*Time Kapton*Type Time*Type Position*Kapton*Time Position*Kapton*Type Position*Time*Type Kapton*Time*Type Position*Kapton*Time*Type Full Effect 4.3375 0.2750 0.0750 –0.0500 –1.0500 0.0750 0.0500 –0.2500 –0.0500 –0.2000 –0.0250 0.0500 0.1000 0.0750 –0.0750 0.1250 Parameter Estimate 0.1375 0.0375 –0.0250 –0.5250 0.0375 0.0250 –0.1250 –0.0250 –0.1000 –0.0125 0.0250 0.0500 0.0375 –0.0375 0.0635 Analysis of Variance for wghtloss Source Main Effects 2-Way Interactions 3-Way Interactions 4-Way Interactions Residual Error Total DF 4 6 4 1 0 15 SS 4.74500 0.45500 0.09500 0.06250 0.00000 5.35750 MS 1.18625 0.07583 0.02375 0.06250 0.00000 On the next page is a normal probability plot of estimated full effects. 7 a) [5] On the normal plot above, clearly label, with their names, the effects that you suspect are significant. b) [8] If we use the 3-Way and 4-Way interactions to produce an error term, which main effect(s) and interaction(s) would be statistically significant? Justify your answer and use t=3. 8 An alternative analysis would drop Time and look at the analysis of the 23 experiment in Position, Kapton and Type. The output of that analysis is given below. Fractional Factorial Fit Estimated Full Effects and Parameter Estimates for wghtloss Term Full Effect 4.3375 0.2750 0.0750 –1.0500 0.0750 –0.2500 –0.2000 0.1000 Constant Position Kapton Type Position*Kapton Position*Type Kapton*Type Position*Kapton*Type Parameter Estimate 0.1375 0.0375 –0.5250 0.0375 –0.1250 –0.1000 0.0500 Analysis of Variance for wghtloss Source Main Effects 2-Way Interactions 3-Way Interactions Residual Error Pure Error Total DF 3 3 1 8 8 15 SS 4.73500 0.43250 0.04000 0.15000 0.15000 5.35750 MS 1.57833 0.14417 0.04000 0.01875 0.01875 c) [7] Using this alternative analysis, which main effect(s) and interaction(s) are statistically significant? Justify your answer and use t=3. 9 d) [3] Is there another factor that can be dropped from the model? If so, which factor? e) [7] Give the prediction equation for the model with only significant terms. Use this model to make recommendations on how to set all of the factors to give the least amount of weight loss. What is the predicted weigh loss at this recommendation? 10