Chapter 19 Analyzing Accelerated Life Test Data William Q. Meeker and Luis A. Escobar Iowa State University and Louisiana State University 19 - 1 Copyright 1998-2008 W. Q. Meeker and L. A. Escobar. Based on the authors’ text Statistical Methods for Reliability Data, John Wiley & Sons Inc. 1998. December 14, 2015 8h 10min Example: Temperature-Accelerated Life Test on Device-A (from Hooper and Amster 1990) Data: Singly right censored observations from a temperatureaccelerated life test. Purpose: To determine if the device would meet its hazard function objective at 10,000 and 30,000 hours at operating temperature of 10◦C. 200 500 1000 2000 5000 10000 20000 50000 0 0/30 20 9/20 60 Degrees C 40 10/100 80 14/15 Device-A Hours Versus Temperature (Hooper and Amster 1990) 19 - 5 100 19 - 3 We will show how to fit an accelerated life regression model to these data to answer this and other questions. Hours Chapter 19 Analyzing Accelerated Life Test Data Objectives • Describe and illustrate nonparametric and graphical methods of analyzing and presenting accelerated life test data. • Describe and illustrate maximum likelihood methods of analyzing and making inferences from accelerated life test data. • Illustrate different kinds of data and ALT models. • Discuss some specialized applications of accelerated testing. • Describe pitfalls in accelerated testing. 19 - 2 Hours Versus Temperature Data from a Temperature-Accelerated Life Test on Device-A Hours Censored Status 1 1 ... 90 30 60 60 60 ... 60 40 40 ... 40 10 15 20 100 30 14/15 9/20 10/100 0/30 In Subexperiment Units Failures 5000 Failed Failed ... Censored ... 11 80 80 80 80 ... 80 Temperature ◦C 1298 1390 ... 5000 Failed Failed Failed ... Censored 1 1 1 1 ... 1 Number of Devices 581 925 1432 ... 5000 Failed Failed Failed Failed ... Censored 19 - 4 283 361 515 638 ... 5000 ALT Data Plot • Examine a scatter plot of lifetime versus stress data. • Use different symbols for censored observations. Note: Heavy censoring makes it difficult to identify the form of the life/stress relationship from this plot. 19 - 6 40 Deg C 1000 2000 5000 10000 20000 19 - 7 50000 19 - 9 80 Deg C 60 Deg C 200 40 Deg C 500 1000 2000 i 5000 10000 20000 19 - 8 50000 Weibull Multiple Probability Plot Giving Individual Weibull Fits to Each Level of Temperature for Device-A ALT Data h i log(t)−µ bi c [T (temp ) ≤ t] = Φ Pr , i = 40, 60, 80 sev i σ b .98 .9 .7 .5 .3 .2 .1 .05 .02 .01 .005 .003 .001 100 Hours .59 1.72 95% Approximate Confidence Interval Lower Upper 8.9 10.6 2.0 9.3 .27 8.0 7.5 Standard Error .42 .35 .70 1.17 1.0 8.64 .32 .55 6.7 ML Estimate 9.81 µ 1.19 .16 .21 Parameter µ σ .80 7.08 σ σ µ 19 - 12 The individual loglikelihoods were L40 = −115.46, L60 = −89.72, and L80 = −115.58. The confidence intervals are based on the normal approximation method. 80◦C 60◦C 40◦C Device-A ALT Lognormal ML Estimation Results at Individual Temperatures 19 - 10 Note: Either the lognormal or the Weibull distribution model provides a reasonable description for the device-A data. But the lognormal distribution provides a better fit to the individual subexperiments. • Try to identify a distributional model that fits the data well at all of the stress-levels. • Compute nonparametric estimates Fb for each level of accelerating variable; plot on a single probability plot. ALT Multiple Probability Plot of Nonparametric Estimates at Individual Levels of Accelerating Variable .0001 .0002 .0005 Proportion Failing Strategy for Analyzing ALT Data For ALT data consisting of a number of subexperiments, each having been run at a particular set of conditions: • Examine the data graphically: Scatter and probability plots. • Use a multiple probability plot to study the data from the individual subexperiments. • Fit an overall model involving a life/stress relationship. • Perform residual analysis and other diagnostic checks. • Perform a sensitivity analysis. i • Assess the reasonableness of using the ALT data to make the desired inferences. 80 Deg C 60 Deg C 200 500 Lognormal Multiple Probability Plot Giving Individual Lognormal Fits to Each Level of Temperature for Device-A ALT Data h i log(t)−µ bi c [T (temp ) ≤ t] = Φ Pr , i = 40, 60, 80 nor i σ b .98 .9 .95 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 .005 .002 100 Hours b i, σ b i). ◮ Compute ML estimates (µ 19 - 11 Note: There are some small differences among the slopes that could be due to sampling error. • Assess the commonly used assumption that σi does not depend on Tempi and that Tempi only affects µi. b i, σ b i) cdfs on same plot. ◮ Plot the LOGNOR(µ Let Ti be the failure time at temperature Tempi. For the lognormal, Ti ∼ LOGNOR(µi, σi), assumed model: • For each individual level of accelerating variable compute the ML estimates. ALT Multiple Probability Plot of ML Estimates at Individual Levels of Accelerating Variable .0001 .0005 Proportion Failing # The Arrhenius-Lognormal Regression Model " log(t) − µ(x) Pr[T (temp) ≤ t] = Φnor σ •• •• •• • • 60 • •• •• •• •• 80 10% 5% 1% 19 - 13 100 19 - 15 80 Deg C 200 60 Deg C 500 40 Deg C 1000 2000 5000 10000 10 Deg C 20000 19 - 14 50000 Lognormal Multiple Probability Plot of the Arrhenius-Lognormal Log-Linear Regression Model Fit to the Device-A ALT Data h i log(t)−µ b(x) c [T (temp) ≤ t] = Φ b Pr , µ(x) = βb0 + βb1x nor σ b .98 .9 .95 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 .005 .002 100 Hours .98 .63 ML Estimate −13.5 .13 .08 Standard Error 2.9 .75 .47 1.28 .79 95% Approximate Confidence Intervals Lower Upper −19.1 −7.8 σ h b ). ◮ Compute ML estimates (βb0, βb1, σ h b i) = βb0 + βb1xi, σ b ◮ Plot the LOGNOR µ(x plot. i cdfs on same 19 - 18 −1 b for various values (p)σ ◮ Plot tbp(x) = exp βb0 + βb1x + Φnor of p and a range of values of x. i Let T (xi) be the failure time at xi = 11605/(Tempi + 273.15). For the, T (xi) ∼ LOGNOR(µ(xi) = β0 + β1xi, σ), lognormal SAFT assumed model: • To make inferences at levels of accelerating variable not used in the ALT, use a life/stress relationship to fit all the data. ALT Multiple Probability Plot of ML Estimates with an Assumed Life/Stress Relationship 19 - 16 The loglikelihood is L = −321.7. The confidence intervals are based on the normal approximation method. β1 Parameter β0 ML Estimation Results for the Device-A ALT Data and the Arrhenius-Lognormal Regression Model .0001 .0005 Proportion Failing The Arrhenius-lognormal regression model is where • µ(x) = β0 + β1x, • x = 11605/(temp K) = 11605/(temp ◦C + 273.15), • β1 = Ea is the activation energy, and • σ assumed to be constant. • • • 40 b µ(x) = βb0 + βb1x Scatter plot showing the Arrhenius-Lognormal Log-Linear Regression Model Fit to the Device-A ALT Data 20 −1 b b, log[tbp(x)] = µ(x) + Φnor (p)σ 50000 20000 10000 5000 2000 500 1000 200 50 100 0 Degrees C on Arrhenius scale 19 - 17 • −2(Lconst − Lunconst) = −2(−321.7 + 320.76) = 1.88 < 2 χ(.75,3) = 4.1, indicating that there is no evidence of inadequacy of the constrained model, relative to the unconstrained model. Lconst = −321.7 Lunconst = L40 + L60 + L80 = −320.76 • Use likelihood ratio test to check for lack of fit with respect to the constraints. • The Arrhenius-lognormal regression model can be viewed as a constrained model (µ linear in x and σ constant). • Distributions fit to individual levels of temperature can be viewed as an unconstrained model. Analytical Comparison of Individual and Arrhenius-Lognormal Model ML Estimates of Device-A Data Hours ML Estimation for the Device-A Lognormal Distribution F (30,000) at 10◦C = −13.469 + .6279 × 11605/(10 + 273.15) = 12.2641 b µ(x) = βb0 + βb1x # = " .287 .048 .048 .0176 1 # . b σ b = [log(30,000) − 12.2641]/.9778 ζce = [log(te) − µ]/ = −2.000 " d µ) d µ, b b σ b) Var( Cov( d µ, d σ b σ b ) Var( b) Cov( Fb (30,000) = Φnor (ζce) = Φnor (−2.000) = .02281 Σ̂µb,σb = ) 19 - 19 φ(ζce) d 2 c2Var( cCov( d σ d µ, b) b σ b) + ζ b + 2ζ Var(µ) sceFb = e e b σ φ(−2.000) h = .286 + 2 × (−2.000) × .047 + (−2.000)2 × .0176 .9778 = .0225. Checking Model Assumptions • • 0.10 • •• •• •• 0.20 • •• •• •• •• 0.50 • •• • • •• • • • • • • 1.00 Standardized Residuals • 2.00 5.00 Confidence Interval for the Device-A Lognormal Distribution F (30,000) at 10◦C " Fb , Fb + (1 − Fb ) × w .14] # .02281 .02281 + (1 − .02281)/w Fb Fb + (1 − Fb )/w .02281 , .02281 + (1 − .02281) × w = [.0032, = Fe (te )] = A 95% normal-approximation confidence interval based on the assumption that Zlogit(Fb) ∼ NOR(0, 1) is [F (te ), e where = exp{(1.96 × .0225)/[.02281(1 − .02281)]} = 7.232. w = exp{(z(1−α/2)sceFb )/[Fb (1 − Fb )]} 19 - 20 This wide interval reflects sampling uncertainty when activation energy is unknown. The interval does not reflect model uncertainty. With given activation energy, the confidence intervals would be much narrower. • •• •• • • • • 3 2x10 3 •• •• •• • • 5x10 3 10 4 •• • • 2x10 Fitted Values 4 5x10 4 10 5 2x10 5 5 19 - 22 5x10 Plot of Standardized Residuals Versus Fitted Values for the Arrhenius-Lognormal Log-Linear Regression Model Fit to the Device-A ALT Data 5.00 2.00 1.00 0.50 0.20 0.10 0.05 0.02 10 Some Practical Suggestions • See Nelson (1990). 19 - 24 • Design tests to limit the amount extrapolation needed for desired inferences. • Seek physical justification for life/stress relationships. • Use results from physical failure mode analysis. • Seek physical understanding of cause of failure. • Use pilot experiments; evaluate the effect of stress on degradation and life. • Build on previous experience with similar products and materials. Standardized Residuals It is important to check model assumptions by using residual analysis and other model diagnostics ( log[t(xi)] − βb0 − βb1xi b σ • Define standardized residuals as exp where t(xi) is a failure time at xi. • Residuals corresponding to censored observations are called censored standardized residuals. • Plot residuals versus the fitted values given by exp βb0 + βb1xi . • Do a probability plot of the residuals. 19 - 21 Note: For the Device-A data, these plots do not conflict with the model assumptions. .9 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 .005 .002 0.05 19 - 23 Probability Plot of the Residuals from the Arrhenius-Lognormal Log-Linear Regression Model fit to the Device-A ALT Data Probability 4 3 2 1 0 • •• • • • 100 • •• • •• • • •• • • • • 150 i • •• •• • kV/mm 200 250 300 19 - 26 350 400 • •• • • • • Breakdown Times in Minutes of a Mylar-Polyurethane Insulating Structure (from Kalkanis and Rosso 1989) 10 10 10 10 10 -1 10 .99 .98 .9 .95 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 .99 .98 .9 .95 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 10 10 -1 -2 361.4 kV/mm 10 361.4 -1 0 10 0 10 10 219.0 1 1 219.0 10 i 157.1 Minutes 10 2 3 10 100.3 Minutes 10 2 122.4 10 4 3 100.3 10 10 5 50 kV/mm 6 10 10 10 4 7 19 - 30 Lognormal Probability Plot of the Inverse Power Relationship-Lognormal Model Fitted to the Mylar-Polyurethane Data Including 361.4 kV/mm h i log(t)−µ bi c [T (temp ) ≤ t] = Φ Pr , i = 100.3, . . . , 361.4 nor i σ b 19 - 28 Lognormal Probability Plot of the Individual Tests in the Mylar-Polyurethane ALT i h log(t)−µ bi c [T (temp ) ≤ t] = Φ , i = 100.3, . . . , 361.4 Pr nor i σ b Minutes Inferences from AT Experiments • Inferences or predictions from ATs require important assumptions about: ◮ Focused correctly on relevant failure modes. ◮ Adequacy of AT model for extrapolation. ◮ AT manufacturing testing processes can be related to actual manufacturing/use of product. • Important sources of variability usually overlooked. • Deming would call ATs analytic studies (see Hahn and Meeker 1993, American Statistician). 19 - 25 Accelerated Life Test of a Mylar-Polyurethane Laminated Direct Current High Voltage Insulating Structure • Data from Kalkanis and Rosso (1989) • Time to dielectric breakdown of units tested at 100.3, 122.4, 157.1, 219.0, and 361.4 kV/mm. • Needed to evaluate the reliability of the insulating structure and to estimate the life distribution at system design voltages (e.g. 50 kV/mm). • Except for the highest level of voltage, the relation between log life and log voltage appears to be approximately linear. 19 - 27 • Failure mechanism probably different at 361.4 kV/mm. # Inverse Power Relationship-Lognormal Model • The inverse power relationship-lognormal model is " log(t) − µ(x) F (t) = Pr[T (volt) ≤ t] = Φnor σ where µ(x) = β0 + β1x, and x = log(Voltage Stress). • σ assumed to be constant. 19 - 29 Proportion Failing Proportion Failing 50 • •• •• •• •••• • 100 • • •• • 200 • •• •• • 500 10% 50% 90% b µ(x) = βb0 + βb1x • • •• •• kV/mm on log scale 19 - 31 Plot of Inverse Power Relationship-Lognormal Model Fitted to the Mylar-Polyurethane Data Including 361.4 kV/mm 8 7 6 5 4 3 2 1 0 20 −1 b b, log[tbp(x)] = µ(x) + Φnor (p)σ 10 10 10 10 10 10 10 10 -1 10 10 0 219.0 1 10 157.1 2 122.4 10 100.3 10 3 4 50 kV/mm 10 10 5 19 - 33 Lognormal Probability Plot of the Inverse Power Relationship-Lognormal Model Fitted to the Mylar-Polyurethane Data W/O the 361.4 kV/mm Data i h log(t)−µ b(x) c [T (temp) ≤ t] = Φ b , µ(x) = βb0 + βb1x Pr nor σ b 10 ML Estimate 27.5 .12 .60 Standard Error 3.0 .83 −5.46 1.32 −3.11 1 • • • •• • • • 5 20 •• • • •• • • 100 Fitted Values • • •• • •• • • 500 • • •• • • • • 2000 • •• • • • 19 - 32 Lognormal Plot of the Standardized Residuals versus b exp(µ(x)) for the Inverse Power Relationship-Lognormal Model Fitted to the Mylar-Polyurethane Data with the 361.4 kV/mm Data 20.0 10.0 5.0 2.0 1.0 0.5 0.2 0.1 8 7 6 5 4 3 2 1 0 50 • •• •• •• •••• • 100 • • •• • 200 • •• •• • 500 10% 50% 90% b µ(x) = βb0 + βb1x • • •• •• kV/mm on log scale 19 - 34 Plot of Inverse Power Relationship-Lognormal Model Fitted to the Mylar-Polyurethane Data (also Showing 361.4 kV/mm Data Omitted from the ML Estimation) 10 10 10 10 10 10 10 10 10 -1 10 20 −1 b b, log[tbp(x)] = µ(x) + Φnor (p)σ 10.0 5.0 2.0 1.0 0.5 0.2 0.1 50 •• • • •• • • 100 200 • • •• • •• • • Fitted Values 500 • • •• • • • • 1000 • • • • • • 2000 19 - 36 5000 Lognormal Plot of the Standardized Residuals versus b for the Inverse Power Relationship-Lognormal exp(µ) Model Fitted to the Mylar-Polyurethane Data W/O the 361.4 kV/mm Data Minutes .99 .98 .9 .95 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 Minutes 1.05 −4.29 95% Approximate Confidence Intervals Lower Upper 21.6 33.4 Inverse Power Relationship-Lognormal Model ML Estimation Results for the Mylar-Polyurethane ALT Data Parameter β0 σ β1 The loglikelihood is L = −271.4. The confidence intervals are based on the normal approximation method. 19 - 35 Standardized Residuals Standardized Residuals Minutes Proportion Failing Analysis of Interval ALT Data on a New-Technology IC Device • Tests were run at 150, 175, 200, 250, and 300◦C. • Developers interested in estimating activation energy of the suspected failure mode and the long-life reliability. • Failures had been found only at the two higher temperatures. • After early failures at 250 and 300◦C, there was some concern that no failures would be observed at 175◦C before decision time. i 19 - 37 • Thus the 200◦C test was started later than the others. 100 200 500 2000 300 Degrees C 1000 Hours 250 Degrees C 5000 19 - 39 10000 Lognormal Probability Plot of the Failures at 250 and 300◦C for the New-Technology Integrated Circuit Device ALT Experiment h i log(t)−µ bi c [T (temp ) ≤ t] = Φ Pr , i = 250, 300 nor i σ b .9 .95 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 .005 .002 .9 .95 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 .005 .002 .0005 .0001 10 300 Deg C 2 250 3 10 200 10 4 175 Hours 150 10 5 6 100 10 10 7 19 - 41 Lognormal Probability Plot Showing the Arrhenius-Lognormal Model ML Estimation Results for the New-Technology IC Device h i log(t)−µ b(x) c [T (temp) ≤ t] = Φ b Pr , µ(x) = βb0 + βb1x nor σ b .0001 .0005 Proportion Failing Proportion Failing Status Right Censored Right Censored Right Censored Failed Failed Failed Right Censored Failed Failed Failed Right Censored Number of Devices 50 50 50 1 3 5 41 4 27 16 3 Temperature ◦C 150 175 200 250 250 250 250 300 300 300 300 New-Technology IC Device ALT Data Hours Lower Upper 1536 1536 96 384 788 788 1536 1536 2304 2304 384 788 1536 1536 192 384 788 19 - 38 Individual Lognormal ML Estimation Results for the New-Technology IC Device 250◦C σ σ µ Parameter µ .46 .87 6.56 ML Estimate 8.54 .05 .26 .07 Standard Error .33 .36 .48 6.4 .58 1.57 6.7 95% Approximate Confidence Intervals Lower Upper 7.9 9.2 300◦C The loglikelihood were L250 = −32.16 and L300 = −53.85. The confidence intervals are based on the normal approximation method. 19 - 40 Arrhenius-Lognormal Model ML Estimation Results for the New-Technology IC Device .83 ML Estimate −10.2 .06 .07 Standard Error 1.5 .42 .68 .64 .97 95% Approximate Confidence Intervals Lower Upper −13.2 −7.2 .52 Parameter β0 σ β1 The loglikelihood is L = −88.36. Comparing the constrained and unconstrained models Luconst = L250+L300 = −86.01 and for the constrained model, Lconst = −88.36. The comparison has just one degree of freedom and 2 −2(−88.36 + 86.01) = 4.7 > χ(.95,1) = 3.84, again indicating that there is some lack of fit in the constant-σ Arrheniuslognormal model. 19 - 42 x x x 300 50% 10% 1% 350 b µ(x) = βb0 + βb1x x x x 250 19 - 43 300 Deg C 2 3 10 250 200 10 4 175 150 10 5 6 100 10 10 7 19 - 44 Lognormal Probability Plot Showing the Arrhenius-Lognormal Model ML Estimation Results for the New-Technology IC Device with Given Ea = .8 h i log(t)−µ b(x) c [T (temp) ≤ t] = Φ b Pr , µ(x) = βb0 + Ea x nor σ b .9 .95 .8 .7 .6 .5 .4 .3 .2 .1 .05 .02 .01 .005 .002 10 Hours 19 - 46 19 - 48 • Plan ATs that will allow effective prediction of failure time distributions at desired ratio (or ratios) of time scales. • With multiple time scales, understand ratio or ratios of time scales that arise in actual use. • Need to use the appropriate time scale(s) for evaluation of each failure mechanism. Suggestions: Dealing with Multiple Time Scales ◮ Use sensitivity analysis to assess the effect of departures from model assumptions and uncertainty in other inputs. ◮ Use confidence intervals to quantify statistical uncertainty. • Suggestions: • Confidence intervals ignore model uncertainty (which can be tremendously amplified by extrapolation in Accelerated Testing). • Standard statistical confidence intervals quantify uncertainty arising from limited data. • There is uncertainty in statistical estimates. Pitfall 2: Failure to Properly Quantify Uncertainty .0001 .0005 Proportion Failing Arrhenius Plot Showing ALT Data and the Arrhenius-Lognormal Model ML Estimation Results for the New-Technology IC Device. 7 6 5 4 3 2 200 Degrees C on Arrhenius scale 150 −1 b b, log[tbp(x)] = µ(x) + Φnor (p)σ 10 10 10 10 10 10 100 • Suggestions: ◮ Determine failure mode of failing units. ◮ Analyze failure modes separately. Pitfall 3: Multiple Time Scales • Composite material 19 - 47 ◮ On/off cycles of a print operation (thermal cycling of substrate and printhead lamination). ◮ Characters or pages printed (ink supply, resistor degradation). ◮ Real time (corrosion) • Inkjet pen ◮ On-off cycles induce thermal and mechanical shocks that can lead to fatigue cracks. ◮ Filament evaporates during burn time. • Incandescent light bulbs ◮ Stress cycles during use lead to initiation and growth of cracks. ◮ Chemical degradation over time changes material ductility. 19 - 45 • Other failure modes, if not recognized in data analysis, can lead to incorrect conclusions. • High levels of accelerating factors can induce failure modes that would not be observed at normal operating conditions (or otherwise change the life-acceleration factor relationship). Pitfall 1: Multiple (Unrecognized) Failure Modes Hours 10 10 10 10 10 10 6 5 4 3 2 1 60 Degrees C 80 100 120 Temperature-Accelerated Life Test for an IC Device 40 Pitfall 4: Masked Failure Mode ◮ Identify failure modes of all failures. Comparison of Two Products II Questionable Comparison 120 10% 10% Vendor 2 10% 140 19 - 49 19 - 51 6 5 4 3 2 1 6 5 4 3 2 1 60 60 80 Degrees C Degrees C 80 100 100 10% Mode 2 10% Mode 1 120 10% 140 19 - 50 19 - 52 140 Vendor 1 10% Vendor 2 120 Comparison of Two Products I Simple Comparison 40 Unmasked Failure Mode with Lower Activation Energy for an IC Device 10 10 10 10 10 10 10 10 10 10 10 10 40 Pitfall 5: Faulty Comparison • It is sometimes claimed that Accelerated Testing is not useful for predicting reliability, but is useful for comparing alternatives. 19 - 54 ◮ Understand the physical reason for any differences. ◮ Analyze failure modes separately. ◮ Identify failure modes of all failures. ◮ Know (anticipate) different failure modes. • Comparisons can, however, also be misleading. 1 2 5 140 • Beware of comparing products that have different kinds of failures. 100 4 80 Degrees C 19 - 53 • Suggestions: 60 Hours Hours 3 6 ◮ Analyze failure modes separately. 10 10 10 10 10 10 40 Vendor 1 ◮ Limit acceleration and test at levels of accelerating variables such that each failure mode will be observed at two or more levels of the accelerating variable. ◮ Know (anticipate) different failure modes. • Suggestions: • Masked failure modes could dominate in the field. • Masked failure modes may be the first one to show up in the field. • Accelerated test may focus on one known failure mode, masking another! Hours Hours Pitfall 6: Acceleration Factors Can Cause Deceleration! • Increased temperature in an accelerated circuit-pack reliability audit resulted in fewer failures than in the field because of lower humidity in the accelerated test. Pitfall 7: Untested Design/Production Changes • Lead-acid battery cell designed for 40 years of service. • New epoxy seal to inhibit creep of electrolyte up the positive post. • Accelerated life test described in published article demonstrated 40 year life under normal operating conditions. • Automobile air conditioners failed due to a material drying out degradation, lack of use in winter (not seen in continuous accelerated testing). • Improper epoxy cure combined with charge/discharge cycles hastened failure. • First failure after 2 years of service; third and fourth failures followed shortly thereafter. • 200,000 units in service after 2 years of manufacturing. • Inkjet pens fail from infrequent use. • Entire population had to be replaced with a re-designed cell. • Higher than usual use rate of a mechanical device in an accelerated test inhibited a corrosion mechanism that eventually caused serious field problems. • Suggestion: Understand failure mechanisms and how they are affected by experimental variables. 19 - 56 5 4 3 2 1 0 5 Degrees C 45 Degrees C 85 Degrees C 30 996 cen 196 cen 40 174 cen 496 cen 48 cen 49 cen 50 49 cen 156 cen 60 70 19 - 59 0 20 40 60 80 100 .2 .1 .05 .03 .02 .01 .005 .003 .001 .0005 .0003 4/1000 35 10 4/200 40 85 Deg C, 35 V 85 Deg C, 40.6 V 85 Deg C, 46.5 V 85 Deg C, 51.5 V 45 Deg C, 46.5 V 5 Deg C, 62.5 V 50 2/50 6/502 1/175 45 200 4/53 50 Volts Hours 500 2000 55 1/50 i 5000 60 18/174 20000 65 19 - 60 50000 Weibull Probability Plot for the Individual Voltage and Temperature Level Combinations for the Tantalum Capacitors ALT, with ML Estimates of Weibull cdfs h i log(t)−µ bi c [T (temp ) ≤ t] = Φ Pr sev i σ b 19 - 58 Tantalum Capacitors ALT Design Showing Fraction Failing at Each Point 19 - 55 Temperature/Voltage ALT Data on Tantalum Electrolytic Capacitors • Two-factor ALT • Non-rectangular unbalanced design • Much censoring • The Weibull distribution seems to provide a reasonable model for the failures at those conditions with enough failures to make a judgment. • Temperature effect is not as strong. 19 - 57 • Data analyzed in Singpurwalla, Castellino, and Goldschen (1975) 10 10 10 10 10 10 20 Volts Degrees C Proportion Failing Scatter Plot of Failures in the Tantalum Capacitors ALT Showing Hours to Failure Versus Voltage with Temperature Indicated by Different Symbols Hours Model 1: µ(x) = β0 + β1x1 + β2x2 Tantalum Capacitors ALT Weibull/Arrhenius/Inverse Power Relationship Models Model 2: µ(x) = β0 + β1x1 + β2x2 + β3x1x2 where x1 = log(volt), x2 = 11605/(temp K), and β2 = Ea. • Coefficients of the regression model are highly sensitive to whether the interaction term is included in the model or not (because of the nonrectangular design with highly unbalanced allocation). • Data provide no evidence of interaction. 2 85 Deg C, 35 V 85 Deg C, 40.6 V 85 Deg C, 46.5 V 85 Deg C, 51.5 V 45 Deg C, 46.5 V 5 Deg C, 62.5 V 10 10 3 4 30 Deg C, 24 V 10 10 5 19 - 61 −20.1 ML Estimate 84.4 4.4 Standard Error 13.6 1.72 −.04 −28.8 .69 −11.4 95% Approximate Confidence Interval Lower Upper 57.8 111. β1 .36 .19 3.16 .33 72.35 135.1 2.33 −32.5 −292.3 σ 26.7 .40 11.6 109.0 −1.35 19.9 3.3 1.72 −2.8 -78.6 .80 β0 β2 Parameter β0 Tantalum Capacitor ALT Weibull-Inverse Power Relationship Regression ML Estimation Results Model 1 Model 2 5.13 .36 β1 β2 2.33 −1.17 3.16 σ 19 - 62 β3 Loglikelihoods L1 = −539.63 and L2 = −538.40 1 2 3 4 5 6 7 8 9 10 10 10 10 10 10 10 10 10 10 10 20 85 Deg C 45 Deg C 5 Deg C 30 40 Volts 85 50 70 5 Degrees C 45 60 19 - 64 ML Estimates of t0.01 for the Tantalum Capacitor Life Using the Arrhenius-Inverse Power Relationship Weibull Model Hours • Strong evidence for an important voltage effect on life. 1 19 - 65 19 - 63 Weibull Multiple Probability Plot of the Tantalum Capacitor ALT Data Arrhenius-Inverse Power Relationship Weibull Model (with no Interaction) i h log(t)−µ b(x) c [T (temp) ≤ t] = Φ b x) = βb0 + βb1x1 + βb2x2 , µ( Pr sev σ b .5 .2 .1 .05 .02 .01 .005 .003 .001 10 Hours Other Topics in Chapter 19 • Environmental stress screening. • Burn-in. • Environmental stress and STRIFE testing. • Highly accelerated life tests (HALT). Discussion of .000005 .000003 .00001 .00002 .00005 .0001 .0002 .0005 Proportion Failing