Strong-field Physics with Ultrafast Optical Resonators by William Putnam MASSACHUSETTS INSTITUTE OF TECHNOLOLGY B.S. Physics and B.S. Electrical Science and Engineering, Massachusetts Institute of Technology (2008) JUL 0 7 2015 LIBRARIES M.Eng. Electrical Engineering and Computer Science, Massachusetts Institute of Technology (2008) Submitted to the Department of Electrical Engineering and Computer Science in partial fulfillment of the requirements for the degree of Doctor of Philosophy in Electrical Engineering at the MASSACHUSETTS INSTITUTE OF TECHNOLOGY June 2015 0 Massachusetts Institute of Technology 2015. All rights reserved. Author ................... Signature redacted .............. Department of tietrical Engineering and Computer Science February 23, 2015 Certified by .................... Signature redacted .......... Franz X. Kartner Adjunct Professor of Electrical Engineering Thesis Supervisor Certified by ................... Signature redacted Erich P. Ippen Elihu Thomson Professor of Electrical Engineering Professor of Physics Thesis Supervisor Accepted by.................... Signature redacted I (Qfeslie A. Kolodziejski Chair of the Committee on Graduate Students 2 Strong-field Physics with Ultrafast Optical Resonators by William Putnam Submitted to the Department of Electrical Engineering and Computer Science on February 23, 2015, in partial fulfillment of the requirements for the degree of Doctor of Philosophy in Electrical Engineering Abstract Light fields from modern high-intensity, femtosecond laser systems can produce electrical forces that rival the binding forces in atomic and solid-state systems. In this strong-field regime, conventional non-linear optics gives way to novel phenomena such as the production of attosecond bursts of electrons and photons. Strong laser fields are generally achieved with amplified, ultrafast laser pulses. In this thesis we explore phenomena unique to strong-fields by using optical resonators to passively enhance ultrafast laser pulses. We pursue two major themes in the area of ultrafast resonator-enhanced strongfield physics. First, we use plasmonic nanoparticles as nano-optical resonators to explore strong-field photoemission near nanostructures on the surface of a chip. We demonstrate strong-field photoemission with our chip-scale devices under ambient conditions. Additionally, we use the strong-field photoemission current to probe the ultrafast temporal response of the plasmonic nano-optical field around the nanoparticle emitters. We also show a carrier-envelope sensitive component of the photoemission current and develop a simple model to predict this sensitivity. Second, we investigate cavity-enhanced high-harmonic generation. In particular, we explore the design of novel optical cavities based on Bessel-Gauss modes. Such cavities might have the capability to allow perfect out-coupling for intra-cavity generated harmonics as well as to provide for extremely large mode areas on the cavity mirrors. We prototype a particular Bessel-Gauss cavity design and discuss the limitations of this approach. Thesis Supervisor: Franz X. Kdrtner Title: Adjunct Professor of Electrical Engineering Thesis Supervisor: Erich P. Ippen Title: Elihu Thomson Professor of Electrical Engineering Professor of Physics 3 4 Acknowledgments Having attended MIT as an undergraduate and graduate student, I have now spent more than a third of my life working, playing, and living in the MIT community. The people here at MIT are far and away the institute's most valuable resource, and I am thankful to many of them for their help, support, and care over my many years here. Firstly, I need to thank my doctoral advisor, Prof. Franz Kdrtner. Throughout my years working with Franz, he has always provided energetic and enthusiastic support for me and my research pursuits. I would also like to thank my thesis committee members Prof. Erich Ippen and Prof. Karl Berggren. I have known both Erich and Karl since my time as an undergraduate, and throughout my MIT career they have always had open doors and a great willingness to share their time and knowledge. Additionally, I have to thank all my research collaborators over the years: in particular, Richard Hobbs for all the fantastic electron-beam lithography work and insightful discussions, Jim Daley for all the invaluable assistance through my various catastrophic pursuits in fabrication, Xiaolong Hu for helping teach me the ropes of nano-fabrication oh-so-many years ago, and the entire optics and quantum electronics group, especially Andrew Benedick, Gilberto Abram, Jon Cox, Shu-Wei Huang, and Donnie Keathley for all the stimulating conversations and good times in the lab. Beyond my co-workers, I also need to thank my family and friends for all the love and support they have given me through the ups and downs of my graduate studies. My parents Mary and Peter have never wavered in their support and encouragement through all my pursuits. My sister Julie, my brother James, and the rest of my family as well as my friends Tim, Patrick, Eric, and Luke have always been there for me through the good and bad times with a reassuring word or humorous distraction. Lastly and most importantly, I need to thank Maria. Since our first days together as graduate students at MIT, Maria has been my partner in this entire experience. From difficult times in our early years of graduate school to right now as I write these words, Maria has always been there for me with endless care and willingness to give. 5 6 Contents 1 Strong-fields . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27 1.1.1 'Conventional' non-linear optics and strong-field physics . . . . 27 1.1.2 Multiphoton to strong-field photoemission . . . . . . . . . . . 30 Reaching the strong-field regime . . . . . . . . . . . . . . . . . . . . . 34 1.2.1 Ultrafast pulses . . . . . . . . . . . . . . . . . . . . . . . . . . 34 1.2.2 Ultrafast laser amplifiers . . . . . . . . . . . . . . . . . . . . . 38 1.3 Strong-fields at the nanoscale and HHG . . . . . . . . . . . . . . . . . 40 1.4 Outline of this thesis . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 1.1 1.2 2 45 Theory of photoemission from solid surfaces 2.1 2.2 2.3 3 25 Introduction . . . . . . . . . . . . . . . . . . . . . 45 2.1.1 Field emission . . . . . . . . . . . . . . . . . . . . . . . . . . . 46 2.1.2 Photo-assisted field emission . . . . . . . . . . . . . . . . . . . 49 2.1.3 Multiphoton and strong-field photoemission . . . . . . . . . . 51 Strong-field photoemission . . . . . . . . . . . . . . . . . . . . . . . . 58 . . . . . . . . . . . . . . . . . 59 . . . . . . . . . . . . . . . . . . . . 60 Electron emission fundamentals 2.2.1 Ultrafast optical pulse emission 2.2.2 Continuous-wave emission 2.2.3 Alternative emission rate formulations . . . . . . . . . . . . . 66 2.2.4 Time-dependent emission . . . . . . . . . . . . . . . . . . . . . 67 Carrier-envelope phase effects . . . . . . . . . . . . . . . . . . . . . . 70 Plasmonic nanoparticles and optical resonators 75 3.1 Surface Plasmons and nanoparticle resonators . . . . . . . . . . . . . 75 3.2 Circuit model for nanoparticle resonators . . . . . . . . . . . . . . . . 79 3.2.1 Frequency domain - susceptibility and extinction . . . . . . . 81 3.2.2 Time-domain ultrashort pulse broadening . . . . . . . . . . . 82 . . . . . . . . . . . . . 84 3.3 Nanoparticle fabrication and characterization 7 CONTENTS 87 Photoemission from plasmonic nanoparticles 4.3 . . . . . . . . . . . 87 Previous results and ongoing work . . . . . . . . . . . . . . . 89 . . . . . . . . . . . . . . . . . . . . . . . . . 91 . . 4.1.1 . Strong-fields on a chip Flattened nano-tips on a chip . . . . . . . . . . . . . . . . . 92 4.2.2 On-chip nanoparticle emitter arrays . . . . . . . . . . . . . . 94 . . . . . . . . . . . . . . . . . . . . . . . . . . 97 . . . . . . . . . . . . . 97 . 4.2.1 . 4.2 . . . . . . . . Strong-fields near nanostructures Experimental details . 4.1 Pulse measurement . . . . . . . . . . . . . . . . . . . . . . . 98 4.3.3 Carrier-envelope phase stabilization . . . . . . . . . . . . . . 100 4.3.4 Device alignment . . . . . . . . . . . . . . . . . . . . . . . . 101 . . . . . . . . . . . . . . . . . . . . . 103 4.4.1 Collector and emitter currents . . . . . . . . . . . . . . . . . 103 4.4.2 Photoemission current versus pulse energy . . . . . . . . . . . 104 4.4.3 Device degradation . . . . . . . . . . . . . . . . . . . . . . . 108 4.5 Probing the plasmonic field via IAC . . . . . . . . . . . . . . . . . . 110 4.6 Carrier-envelope phase sensitivity . . . . . . . . . . . . . . . . . . . 113 . . . . . . Photoemission measurements . 4.4 . 4.3.2 119 119 . Few-cycle Er:fiber based laser source . 4.3.1 . 4 121 5 Enhancement cavities for high-harmonic generation 5.1 Enhancement cavities for strong-field physics . . . . 5.2 Enhancement cavity design for HHG . . . . . . . . 6 Bessel-Gauss beams 6.1 Bessel beams to Bessel-Gauss beams . . . . . . 6.2 Constructing Bessel-Gauss beams . . . . . . . . 6.3 Focal properties of Bessel-Gauss beams . . . . . 6.4 Bessel-Gauss beams and simple optical elements 125 155 B Evolution operator basics 159 C Volkov waves 165 . 135 141 . 133 143 . . A Pulse trains in the time and frequency domains . 141 128 . 7 Bessel-Gauss beam enhancement cavities 7.1 Bessel-Gauss beam cavity design . . . . . . . . . . . 7.1.1 Confocal Bessel-Gauss cavity . . . . . . . . 7.2 Confocal Bessel-Gauss cavity demonstration . . . . 125 . . . . . 8 . . . . 147 CONTENTS D Bessel-Gauss beam spatial phase 169 9 CONTENTS 10 List of Figures 1-1 1-2 1-3 1-4 Multiphoton photoemission. Photons of different colors excite electrons from the Fermi level to an energy above the vacuum level, and the excited electrons subsequently leave the metal. The violet, red, and green squiggles represent violet, red, and green photons of energy hvv. hvr, and hvg respectively. U represents energy, and x is the spatial coordinate normal to the metal surface. Urn is a sketch of the metal's binding potential, and WF represents the work function. . . . . . . . 31 Strong-field photoemission. At high field strengths, the strong fields distort the metal's binding potential and results in electron tunneling emission from the metal. . . . . . . . . . . . . . . . . . . . . . 33 Progress in ultrafast laser sources and amplifiers. a. The achievable minimum laser pulse duration as a function of year. The arrow indicates the first demonstration of SHG [2]. b. The achievable maximum focused laser intensity as a function of year. The 107 W/cm2 mark shows the intensity used in the first demonstration of SHG [2]. Note the tremendous growth in achievable intensity since the development of chirped pulse amplification (CPA). (Images borrowed from Ref. [5] without permission). . . . . . . . . . . . . . . . . . . . . 34 Ultrashort optical pulse train from a mode-locked laser. A single optical pulse circulates in the laser cavity (sketched in the upper left) with a circulation period TR. The pulse periodically leaks out of the cavity forming a pulse train with temporal spacing TR = 1fR. Each pulse contains an energy Ep and has a full-width at half maximum duration of TFWHM . . . . . . . . . . . . . . . . . . . . . . . . .35 11 LIST OF FIGURES 1-5 Ultrafast optical pulses and pulse trains in the frequency domain. a. The spectrum of an isolated ultrafast optical pulse with central frequency f, and CEP ,CCEO. b. The spectrum of an ultrafast optical pulse train with repetition rate fR, central frequency f,, and carrier-envelope offset frequency fCEO . . . . . . . . . . . 1-6 .. . . . .36 Ultrashort laser pulse amplifiers and resonators. a. Picture of a typical commercial CPA laser system capable of generating multi-mJ femtosecond laser pulses in a strong-field physics laboratory (photo courtesy of P. D. Keathley). b. Sketch on an ultrafast optical en- hancement cavity. An optical pulse circulates in the resonator with amplitude ares. It is excited by an incident pulse train with amplitude a . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-7 Strong-field photoemission near nanostructures. a. 39 Strong- field photoemission from plasmonic nanoparticles. A femtosecond laser pulse illuminates the nanoparticles, and they photo-emit electrons (illustration borrowed from Ref. [22] without permission). b. Electron energy spectra measured from strong-field photoemission experiment with differing excitation pulse energies (picture borrowed from Ref. [23] without permission). . . . . . . . . . . . . . . . . . . . . . . . . . 1-8 41 Characteristics of HHG and cavity-enhanced HHG. a. Example of an HHG spectrum. For this example, the driving laser light wavelength varies but for the pink trace A = 1.8 prm or the photon energy ~ 0.7 eV. Note the large plateau of hundreds of harmonics; this plateau resembles the plateau in the electron energy spectra from Figure 1-7b (this data was borrowed without permission from Ref. [3]). b. Basic arrangement for cavity-enhanced HHG. An ultrafast laser pulse is enhanced in a bow-tie ring cavity where high-harmonics are produced and out-coupled via a sapphire plate (the pictured harmonics are borrowed from Ref. [26] without permission). 12 . . . . . . . . . . . 42 LIST OF FIGURES 2-1 2-2 Field emission and models. a. Basic model for metallic surface. The interior of the metal is treated as a free electron gas, and the metal surface is modeled as a simple rectangular step of height WF. As before, the metal potential is denoted as Um(x) with x the coordinate normal to the surface. The real part of the electron wavefunction at the Fermi energy is drawn in red (calculated numerically). b. Potential with an applied static bias. With an applied bias the rectangular step is deflected, and electrons can tunnel through the barrier and into the vacuum. The real part of the wavefunction is again drawn in red (numerical calculation). Also, note that we assume no field penetration into the metal. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 Photo-assisted field emission. a. Photo-thermal emission. An optical excitation locally heats the electron gas in a metal (see the lightly shaded region labeled THot). This heating results in a stretched Fermi-Dirac distribution. Higher energy levels are now increasingly thermally occupied and can undergo field emission. The real part of the electron wavefunction at 2 eV above the Fermi energy is drawn in red (calculated numerically) with a static field of Estat = E0 = 10 V/nm. b. Photo-field emission. An optical excitation resonantly excites electrons to higher energy levels, and these excited electron field-emit. The real part of the electron wavefunction at 3 eV (three photons at a wavelength of 1.2 pm) above the Fermi energy is drawn in red (calculated numerically) with a static field of Estat = Eo = 10 V /nm . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50 Multiphoton photoemission. The rectangular step potential is illustrated in black. We see it wiggles only a small amount in response to the relatively weak field E(t) (see dashed). The real part of the initial wavefunction #(x, t) is drawn in red, and the real part of a potential final state (that is also a eigenstate of the unperturbed step potential) is drawn in blue. This state has an energy of 3 eV above the drawn vacuum level (both wavefunctions are numerically calculated). ..... 55 2-4 Strong-field perturbation theory. The terms in Eq. (2.25) can be interpreted via these simple diagrams . . . . . . . . . . . . . . . . . . 56 2-3 13 LIST OF FIGURES 2-5 Strong-field photoemission. The rectangular step potential is illustrated in black. We see it wiggles dramatically with the strong field E(t) with Eo = 10 V/nm (see dashed sketch). The real part of the initial wavefunction O(x) is drawn in red (numerically calculated), and the real part of a potential final state (that is a length gauge Volkov wave) is drawn in blue. This state has an energy of 3 eV above the drawn vacuum level and an additional pondermotive energy of 1.8 eV. 2-6 58 Multiphoton and tunneling emission. At low fields (high -y), we expect the photoemission current to resemble the multiphoton scaling i.e. oc En (drawn in red). Above a critical field (y a 1) and for low y, we expect the photoemission current scaling to resemble the FowlerNordheim equation (drawn in black). The parameters used above are for gold being illuminated by light with a wavelength of 1.2 pm. . . . 2-7 59 Strong-field photoemission with an ultrafast pulse. The photoemission current is plotted for an ultrafast pulse with a central wavelength A, = 1.2 pm and a pulse duration r= The pulse is of a cos 2 9.5 fs (WF= 5.1 eV). shape. Additionally, the photoemission rate for the continuous wave case with a wavelength A = 1.2 pm is plotted for com parison. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-8 61 Strong-field photoemission with continuous-wave excitation. The photoemission current is plotted for a continuous-wave excitation at a central wavelength of A = 1.2 Am. As before WF= 5.1 eV. The numerical calculation is plotted in pink and the analytical result is draw n in blue. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-9 64 Strong-field photoemission in the time domain. The pink shows the electric field that drives photoemission from a gold surface with WF = 5.1 eV. The field has strength E0 = 30 V/nm and wavelength A = 1.2 pm. The blue shows the probability current as found via numerical solution of the TDSE. The dashed black shows the quasistatic tunneling current. The peaks of these currents are shifted from that of the field as they are calculated a short distance from the surface. Additionally, the inset shows the potential model for the simulation (note that the potential is truncated = 0.5 nm from the surface for simplicity in caculation). . . . . . . . . . . . . . . . . . . . . . . . . . 14 68 LIST OF FIGURES 2-10 Strong-field photoemission in space and time. The wavefunction amplitude for the simple rectangular step potential modeled in Figure 2-9 is displayed in space and time. Note the surface is located at x = 0 nm. Also, note the large current spike near t = 0 fs. . . . . . . . . . . 69 2-11 Threshold nature of CEP sensitivity. Two short pulses and two long pulses are illustrated with carrier-envelope phases p = r and 7r/2. The shifted CEP strongly affects the peak field for the short pulses (the CEP dictates whether the peak field in this case is above or below Et), while the CEP shift has a minimal effect on the peak field of the longer pulses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71 2-12 CEP model for a simple pulse. The top plots show a simple 9.5 fs cos 2 shaped laser pulse (red) and the resulting quasi-static emission current (Fowler-Nordheim) for the one- and two-sided emission cases. The middle plots show the emitted charge as a function of the CEP (note the two-sided charge has been magnified by a factor of 103). The bottom plot shows the Fourier series coefficients for the emitted charge. 73 2-13 CEP model for a real pulse. The top plots show the measured 9.5 fs, 1.2 pm wavelength laser pulse used in our experiments (red) and the resulting quasi-static emission current (Fowler-Nordheim) for the one- and two-sided emission cases. The middle plots show the emitted charge as a function of the CEP (note the two-sided charge has been magnified by a factor of 10). The bottom plot shows the Fourier series coefficients for the emitted charge. . . . . . . . . . . . . . . . . . . . . 74 Surface plasmons on a metal surface. a. At a metal-dielectric interface (dielectric above the dashed line and metal below the dashed line), longitudinal surface charge oscillations can be excited. These charge oscillations are the origin of the surface plasmon polariton modes and have wavelength Aspp. b. The electric and magnetic fields produced from these longitudinal surface charge oscillations. Since the fields originate from the surface charge oscillations, they are largely confined to a region near the metal's surface (see green sketch of mode profile). (Images in a. and b. were borrowed without permission from [401). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77 3-1 15 LIST OF FIGURES 3-2 Optical cavities and plasmonic nanoparticle resonators. a. The fundamental operation of a familiar optical cavity. Between the cavity mirrors an optical pulse circulates. Energy is fed into the intra-cavity pulse by an external pulse train. b. Plasmonic nanoparticle resonators, for example nano-rods or nano-triangles, are analogous to the familiar optical cavity. They support surface plasmonic electromagnetic modes that can propagate up and down the nanoparticles. Inset shows the transverse intensity profile of such a mode on a nano-rod resonator with a circular cross-section and a diameter of 20 nm (image borrowed from Ref. [41] without permission). 3-3 . . . . . . . . . . . . . . . . . . . 78 Circuit model for plasmonic nanoparticle resonators. a. Image of nano-rod resonator and cartoon of basic optical cavity-like operation. b. Second-order RLC circuit model for nano-rod resonator. 3-4 . . . . . 80 Example extinction spectrum and fit. The blue curve represents the measured extinction spectrum for an array of nano-triangles with pitch 400 nm, altitude 200 nm and base 150 nm. The dashed red curve shows the fit via Eq. (3.3). . . . . . . . . . . . . . . . . . . . . . . . . 3-5 82 Ultrafast optical pulse broadening in a nanoparticle resonator. The resonator used has a resonant wavelength of 1256 nm and a damping time of 7.4 fs. The black trace shows the excitation pulse envelope (central wavelength of 1.2 pm). The blue trace shows the envelope of the response on the nanoparticle resonator. . . . . . . . . . . . . . . . 3-6 83 Chip overview. a. Picture of the actual chip. b. Zoomed in microscope image of the arrays of devices. c. Zoom in of the purple region outlined in part b. d., and e. electron micrographs of the blue and red regions outlined in part c. 3-7 . . . . . . . . . . . . . . . . . . . . . . Extinction spectra for the nano-rod devices. 84 The blue traces are measurement and the red dashed traces are model fits according to Eq. (3.3). The dark blue trace is for the nano-rod with resonant wavelength 1041 nm . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-8 Extinction spectra for the nano-triangle devices. 85 The blue traces are measurement and the red dashed traces are model fits according to Eq. (3.3). The dark blue trace is for the nano-triangle with resonant wavelength 1059 nm. . . . . . . . . . . . . . . . . . . . . . . 16 85 LIST OF FIGURES 3-9 Image and sketch of chip layout. a. Microscope image of set of eighteen fabricated device arrays. b. Sketch showing the resonant wavelengths of each array. The R and T labels indicate whether the array is a nano-rod array or a nano-triangle device array. 4-1 . . . . . . . 86 Strong-field physics with nanostructures. a. Schematic of nanotip emitter operation. b. Basic layout for nanoparticle emitter experiments. c. Example data set showing carrier-envelope phase effects in the emitted electron's energy spectra from nano-tip emitters. d. Energy spectra showing large re-scattered plateau of emitted electrons from nanoparticles. (illustrations and pictures in a-d borrowed from Refs. [10, 22] without permission). 4-2 . . . . . . . . . . . . . . . . . . . 90 Nano-tip emitter experiments on a chip. a. Conventional nanotip emitter experimental arrangement (illustration borrowed from Ref. [10] without permission). b. Basic layout of one of our flattened onchip nano-emitting tips. 4-3 . . . . . . . . . . . . . . . . . . . . . . . . . 92 Electrical currents across large gaps under ambient conditions. a. Basic experimental arrangement. Electrical emission from gold whisker on photo-lithographically defined pad. b. Measured electrical currents: emitter current, collector current, and current difference. All currents were measured sequentially, i.e. one after the other. 4-4 94 Nanoparticle emitter device layout (optical microscope image). The substrate is composed of a sapphire chip coated in indium tin oxide (ITO). An array of nanoparticle emitters is fabricated on the ITO layer (enclosed by the red box in the image and an example show in the inset). The ITO is patterned into two regions: an emitter that connects to the nanoparticles and a collector. The collector is separated from the emitter by a few micron gap. . . . . . . . . . . . . 4-5 95 Nanoparticle emitter device layout (optical microscope image) and basic experimental setup. Femtosecond laser pulses are focused by an objective (Obj.) to a small spot-size on the nanoparticle array. The excitation laser pulses result in strong-field photoemission from the devices, and the photo-emitted electrons jump from emitter to collector. The three main elements of the following few chapters are num bered. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 96 LIST OF FIGURES 4-6 Femtosecond laser system overview. Schematics and pictures of the Er:fiber oscillator and the supercontinuum generation stages are shown. At the output of the femtosecond laser system is the dispersive wave spectrum spanning 1-1.4 pm as shown. The dispersive wave pulses are sent from the laser system output to the pulse measurement setup, the carrier-envelope phase stabilization/characterization setup, and the actual strong-field experiments. . . . . . . . . . . . . . . . . . 4-7 Dispersive wave pulse measurement. a. persive wave pulse used in the experiments. 98 Spectrum of the disb. Measured optical pulse shape from the 2DSI (blue) and the ideal transform-limited pulse (dashed-red). c. Interferometric autocorrelation measurements (note the early delay data is poor due to an error in the calibration at the start of this trace). d. Image of the 2DSI setup. . . . . . . . . . . . . 4-8 99 Carrier-envelope phase stabilization and characterization. a. Overview of the modifications to the femtosecond laser system to allow carrier-envelope phase locking. The physical meaning of the CEP is also illustrated to the right. b. Results from the out-of-loop f - 2f interferometer when the carrier-envelope offset frequency is locked to o Hz. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 1 4-9 Alignment microscope setup and focused spot characterization. a. Picture of the confocal alignment microscope and the device mount (right). b. Knife-edge measurements of the focused laser spot in both transverse planes (measurement made by scanning a 10 Am wide gold wire across the laser spot). c. Example microscope image recorded on the CCD. Old devices are shown with very high spatial resolution. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 102 4-10 Collector and emitter currents from a nano-triangle array. The upper plot shows the simultaneous measurement of the collector and emitter currents and the stability of these currents. The bottom plot shows the relative phase between the collector and emitter currents. The right image shows a reminder of our basic experimental arrangement. The nano-triangle array has ARes = 1059 nm and 5 .8 fs. Trd = . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 104 LIST OF FIGURES 4-11 Photoemission current versus pulse energy for a nano-triangle array. The array has ARes = 1105 nm and rsad = 6.4 fs. The current scaling is measured for four different collector biases. energies the current scales as ~ scaling falls off to - I. 5., At low pulse while at higher pulse energies this The blue dot at the top right of the graph labels a data point that shows 42.6 nA of current which corresponds to approximately 37 electrons per pulse per emitter. . . . . . . . . . . 105 4-12 Photoemission current versus pulse energy for a nano-rod array. The array has 1041 nm and ARes = Trad = 4.8 fs. The current scaling is measured for four different collector biases. At low pulse energies the current scales as - I" , while at higher pulse energies this scaling falls off to ~ I2. The blue dot at the top right of the graph labels a data point that shows 34.3 nA of current which corresponds to approximately 21 electrons per pulse per emitter. . . . . . . . . . . 106 4-13 Photoemission current versus pulse energy (nano-triangle). The four nano-triangle arrays have ARes = 951, 1059, 1158, and 1256 nm. The measurements were made at 30 V bias. . . . . . . . . . . . . 107 4-14 Photoemission current versus pulse energy (nano-rod). The four nano-rod arrays have AR,, = 968, 1041, 1177, and 1238 nm. The measurements were made at 30 V bias. . . . . . . . . . . . . . . . . . 4-15 Repeatable photoemission current scalings. was made at 30 V from a nano-triangle array with and TRad 108 The measurement ARes = 1105 nm = 6.4 fs. The red trace is the same measurement as shown from Figure 4-7. The blue trace is measured by sweeping the intensity in the opposite direction several minutes later. . . . . . . . . . . . . . 4-16 Emitter array degradation. a. 109 Microscope image of extensively used device arrays (the labeled array was used in this condition to measure the ARes = 1158 nm trace from Figure 4-13). The light colored strip near the collector edge forms during device operation. b. SEM image of the labeled device array. The light colored strip from the microscope image appears to be ITO de-lamination. . . . . . . . . . . 19 110 LIST OF FIGURES 4-17 Interferometric autocorrelation measurement performed with the strong-field photoemission current. The device used in this 7.4 fs. ARes = 1256 nm and r7ad - measurement is a nano-triangle array with The top trace shows the measured autocorrelation (red), the expected autocorrelation from our time-domain model (blue), and the second-harmonic generation (SHG) autocorrelation measured previously. The bottom panel shows the measured pulse (black) that excites the nano-resonator array and the expected pulse from our time-domain m odel (blue). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 111 4-18 Interferometric autocorrelation measurement performed with the strong-field photoemission current. The device used in this measurement is a nano-triangle array with ARes = 1105 nm and 'rad = 6.4 fs. The top trace shows the measured autocorrelation (red), the expected autocorrelation from our time-domain model (blue), and the second-harmonic generation (SHG) autocorrelation measured previously. The bottom panel shows the measured pulse (black) that excites the nano-resonator array and the expected pulse from our time-domain m odel (blue). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 112 4-19 Interferometric autocorrelation measurement performed with the strong-field photoemission current. The device used in this measurement is a nano-triangle array with 4.8 fs. ARes = 1041 nm and rad = The top trace shows the measured autocorrelation (red), the expected autocorrelation from our time-domain model (blue), and the second-harmonic generation (SHG) autocorrelation measured previously. The bottom panel shows the measured pulse (black) that excites the nano-resonator array and the expected pulse from our time-domain m odel (blue). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 113 4-20 Geometry of strong-field emission. Nano-triangles and nano-rods are illuminated by femtosecond laser pulses (here labeled F(t)). The Nano-triangles will only emit from their apex and therefore only emit for half of the pulse's optical cycles, while the nano-rods emit from every cycle. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20 114 LIST OF FIGURES 4-21 Initial CEP sensitivity measurement. The top trace shows the RF spectrum of the emitter current for a nano-triangle array and the bottom trace for a nano-rod array with the fCEO locked to 2 kHz. The noise data corresponds to when the fCEO is unlocked. The units dBpA are equivalent to 20logio(JE/1 pA). . . . . . . . . . . . . . . . . . . . 115 4-22 Absolute phase stepping measurement. A barium fluoride wedge is stepped through the excitation pulse train shifting the absolute CEP of the pulse train. The response is measured via lock-in detection. . . 4-23 CEP sensitivity versus ARes. 116 a. RF traces of the emitter currents from five different nano-triangle arrays are displayed (note each trace is measured from 1.94 - 2.06 kHz). b. The corresponding sensitivity is plotted for these five devices and two additional ones. . . . . . . . . . 5-1 Operation of a femtosecond enhancement-cavity. a. 118 In the time domain, small portions of the incident pulse train are transmitted into the cavity and add to the circulating intra-cavity pulse. If the cavity parameters are properly tuned, these transmitted pulses will constructively add and build-up the energy of the intra-cavity pulse. b. In the frequency domain, the cavity has a comb of resonances spaced by the free-spectral range of the cavity. If each spectral mode of the incident optical pulse train overlaps a cavity resonance, the pulse train will be enhanced. 5-2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 120 Bow-tie ring cavities and popular out-coupling schemes for intra-cavity HHG. a. A sapphire plate is placed in the cavity and Brewster's angle to couple out the generated HHG beam. b. An EUV grating is etched on to a highly reflecting cavity mirror to diffract out the generated high harmonics. . . . . . . . . . . . . . . . . . . . . . . 6-1 123 k-space distribution for a Bessel and a Bessel-Gauss beam. a. The k-space distribution for a Bessel beam at the focal plane z = 0. b. The k-space distribution for a Bessel-Gauss beam at the focal plane z = 0. 6-2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 127 Decentered Gaussian beam. At the focal plane z = 0 (shaded), the beam has a Gaussian distribution that is displaced from the origin by rd = (rd, -/). Away from the focal plane the beam resembles a tilted Gaussian beam, propagating at an angle p to the optical axis, i.e. the z-ax is. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21 129 LIST OF FIGURES 6-3 Constructing Bessel-Gauss beams. a. We superpose many decentered Gaussian beams with differing -y. This amounts in superposing many decentered Gaussian beams along the surface of a cone or a frustum (rd 74= 0). b. (rd = 0) An overlay of the transverse intensity profile after the superposition. Note the annular form of the generalize Bessel-Gauss beam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-4 131 Types of Bessel-Gauss beams. a.-c. Illustrations of r - z plane cross-sections of gBG, BG, and mBG beams respectively. d.-f. Plots of the amplitude in the r - z plane for gBG (A p = 0.21 , r= and mBG (A 6-5 = 1 pm, wo = 200 pm, 0.25 mm), BG (A = 1 pm, wo = 200 pm, p = 0.29'), = 1 pm, wo = 200 pm, rd = 1 mm) beams respectively.. 132 BG beam focal properties and intensity gain. a. Plot of amplitude cross-section in the z = 0 plane of a BG beam with A = 1 pm, wo = 200 pm, and semi-aperture angle p = 0.29' (same parameters from BG beam plotted in Figure 6-4e). Cross-section of the focus in the y-direction is on the right with 2 WB labeled. b. Plot of approximate (orange dashed) and exact (solid green) intensity gain of BG beams with A = 1 pm, wo = 30 pm, and semi-aperture angles p of 10, 20, 30 , and 40 at distance z. The intensity gain of a Gaussian beam with A = 1 pm and wo = 30 pm (blue curve) is also included. c. Plot of the amplitude cross-section in the z = 20 cm plane of the BG beam from plot a. Cross-section in the y-direction is included on the right with w and r, labeled . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-6 gBG beam transformations. 135 a. Example 1 geometry: an mBG beam reflecting from a curved mirror. b. r - z plane cross-section of numerically simulated amplitude for example 1 (note z-axis corresponds to reflecting geometry). c. r-direction cross-sections of field's spatial amplitude and phase at the end of propagation (numerically simulated (blue) and analytical (red-dashed)). d. Example 2 geometry: an mBG beam reflecting from a reflecting axicon. e and f are as b and c but for example 2. g Example 3 geometry: an mBG beam reflecting from a toroidal optic. h and i are as b and c) but for example 138 3.............................................. 22 LIST OF FIGURES 7-1 Gaussian cavities and Bessel-Gauss cavities. a. Illustration of a Gaussian beam enhancement cavity. Note that the harmonics (purple pulse) are generated collinearly with the driving beam. b. The intracavity Gaussian mode intensity on the cavity mirrors in the x - y plane. The dashed white circles indicate roughly where two of the cavity mirrors lie. c. Illustration of a Bessel-Gauss enhancement cavity. This cavity is rotationally symmetric about the z-axis (as indicated by the red circle). Also, note that the harmonics propagate along the zaxis. d. Intra-cavity Bessel-Gauss mode intensity on the segmented cavity mirror in the x - y plane. The dashed white circles roughly show the boundaries between the different sections of the segmented mirror. 142 7-2 Single-mode selection in the confocal BG cavity. a. Cavity mirror with patterned annular (donut-shaped) region of high-reflectivity. b. Cross-section of patterned cavity mirror with incident beams. . . . 144 7-3 Patterned-mirror confocal BG cavity simulation. a. r - z plane cross-section of fundamental BG mode amplitude. b. Normalized mode intensity at mirror surface plotted against r (as labeled in (a)). c. Mode intensity at focus plotted against r (same normalization as (b) and labeled in (a)). . . . . . . . . . . . . . . . . . . . . . . . . . . 145 7-4 Patterned mirror confocal cavity scaling. a. Intensity gain, Ig, scaling with repetition rate (i.e. cavity length and mirror radius of curvature). b. Effective waist, weff, scaling with repetition rate (i.e. cavity length and mirror radius of curvature). For all cavities in these plots Ar = 3.1Wmin . . . . . .. .. . . .146 . . . . . . .. . . . . . . . 7-5 Confocal Bessel-Gauss cavity mirrors a. Illustration of patterned cavity mirror with intra-cavity mode intensity overlaid (not to scale). Inset is a microscope image of a section of a patterned mirror used in the experiment. b. Photograph of actual patterned cavity mirror in the experimental setup. . . . . . . . . . . . . . . . . . . . . . . . . . 148 7-6 Confocal Bessel-Gauss prototype cavity. a. Experimental arrangement (sampling pellicle and CCD not shown). The photodiode signal is used to lock the cavity (input-coupling mirror is actuated with a piezo). b. Simulated field (r - z plane cross-section) traversing the coupling optics/cavity system. . . . . . . . . . . . . . . . . . . . . . . 149 23 LIST OF FIGURES 7-7 Images of the transmitted cavity mode. Images are normalized and taken when the cavity is a. misaligned and the cavity length is swept (the dashed ring is added for ease of illustration), b. well-aligned and the cavity length is swept c. locked from a well-aligned state. 7-8 . . 150 Effective finesse in the presence of curvature variations. The solid line (green) is the analytical model i.e. Eq. (7.4). The dots (black) represent simulation results. The dashed line (red) shows the value of ravg/w used in the experiment. The inset illustrates the simple model for estimating curvature variations. A-1 . . . . . . . . . . . . . . . 151 An optical pulse train in the time and frequency domains. In the above, we proceed step by step from the time domain to the frequency dom ain . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 156 A-2 The basic f-2f interferometer. In the basic f-2f interferometer a low frequency component from the spectrum is frequency doubled via second-harmonic generation (SHG) and mixed with a high frequency component. The mixing process yields a beat-note at the fCEO- 24 - -. 157 Chapter 1 Introduction These days one would be hard pressed to walk down a corridor in a university's applied physics department and not glimpse an advertisement for a talk or see a research poster with a title involving the prefixes pico- (10-12), femto- (10-15), or atto- (10-18). Since the advent of scientific investigation, researchers have sought instruments to explore and probe the world around them with ever finer resolution, and in the past several decades, the laser physics community has pushed the temporal resolution of our measurement capabilities, i.e. the temporal duration of the shortest achievable bursts of light, from the picosecond to the femtosecond scale and, recently, towards the attosecond level. The advantages of short pico- or femtosecond laser pulses extend beyond just the temporal resolution they can provide. Femtosecond laser pulses from a mode-locked laser oscillator are typically emitted as a train of pulses with each pulse carrying an optical energy on the order of nanojoules (nJ). Consider the optical power at the peak of such a laser pulse. This peak power is on the order of nanojoules, i.e. 10- J (1 nJ), divided by femtoseconds, i.e. 1015 s (1 fs); that is, this peak power is on the order of megawatts, i.e. 106 W (1 MW)! Over the past several decades, developments in short pulse laser amplifiers have made the amplification of these nanojoule laser pulses to the millijoule level commonplace. Accordingly, remarkable peak powers in the range of terawattsi, i.e. 1012 W (1 TW), can be achieved with commercial, table-top femtosecond laser systems. Just over fifty years ago, and only a year after the development of the first laser, researchers illuminated a quartz crystal with millisecond-duration laser pulses and produced second-harmonic generation [2]. The illuminating laser pulses contained 'To establish a sense of scale for a terawatt, note that the mean global power consumption in the year 2012 was approximately 2.6 terawatts [1]. 25 CHAPTER 1. INTRODUCTION three joules (3 J) of energy in their one millisecond (1 ms) duration and had a peak power of around three kilowatts (3 kW). This was the first demonstration of second-harmonic generation (SHG) and a major milestone in the early days of nonlinear optics. Nowadays, with near terawatt peak power femtosecond laser pulses, researchers have pushed non-linear optics to a new frontier. With such extreme optical peak powers, harmonics of the hundredth order and higher have been generated from non-linear optical media [3, 4, 5, 6, 7]; pulses of extreme-ultraviolet (EUV) light under a hundred attoseconds in duration have been produced in this high-harmonic generation (HHG) process [8, 9]; and individual optical cycles of femtosecond laser pulses have been used to switch on-and-off photoemission currents near nanostructures and to steer the resulting sub-optical cycle duration electron bursts near such nanostructures [10, 11, 121. This extreme regime of non-linear optics is known as the 'strong-field' regime. In this thesis we will explore the strong-field regime of non-linear optics with ultrafast, femtosecond laser pulses and passive optical resonators. Passive optical resonators offer a means to enhance the optical energy in a femtosecond laser pulse and achieve the high peak powers necessary for strong-field physics without the complexity and limitations of traditional femtosecond laser amplifiers. In particular, in this thesis we will focus on two different areas in the broad topic of strong-field physics with ultrafast optical resonators. First, we will make use of plasmonic nanoparticle optical resonators to explore strong-field physics near nanostructures. We will switch on and off photoemission currents from nanoparticle resonators with individual optical cycles of a femtosecond laser pulse. We will use this photoemission current to characterize the femtosecond dynamics of the nanoparticle's excited plasmonic field and demonstrate carrier-envelope phase sensitivity of the photoemission current. Second, we will explore novel optical resonator designs for cavity-enhanced highharmonic generation. We will design and prototype optical enhancement cavities supporting Bessel-Gauss intra-cavity modes, and we will explore the advantages and limitations of these cavities for cavity-enhanced HHG. We begin this thesis by reviewing the what, how, and why of strong-field physics. First, we trace the origins of strong-field physics from traditional non-linear optics and define the strong-field regime. We next discuss how the field strengths necessary for strong-field phenomena can be achieved. In particular, we will review the basics of ultrafast, femtosecond laser pulses and femtosecond pulse amplification and resonator techniques. Next, we motivate our interest in this high-intensity regime and explain why strong-field physics has garnered such attention from the laser physics 26 CHAPTER 1. INTRODUCTION community. Lastly, we provide an overview of the specific goals of this thesis and an outline of the coming chapters. 1.1 Strong-fields In this section, we develop the concept of the strong-field regime from the basic principles of linear and non-linear optics. Additionally, we provide a brief detour to consider just how strong strong-fields really are, and we go through a simple, relevant first example of strong-field phenomena: strong-field photoemission. 1.1.1 'Conventional' non-linear optics and strong-field physics Since the 'field' part of strong-field refers to the electric field of an electromagnetic wave, and we are interested in light interacting with matter, a reasonable starting point is the wave equation for an electromagnetic wave in some material. V2E - a2p 1 (92E c2 E= [- (9t2 at2 (1.1) In the above, E is the electric field of the wave, c is the speed of light in vacuum, and P is the polarization response of the material, i.e. the dipole moment per unit volume produced in the material in response to the electromagnetic wave. The wave equation in Eq. (1.1) takes the form of a 'driven' or inhomogeneous wave equation. Qualitatively, the left-hand side of the equation describes freely propagating electromagnetic waves, and the right-hand side represents a driving term that can provide sources or sinks for these waves. In linear optics, we assume that the polarization response is proportional to the electric field P = CoX( E In the above, X( (1.2) is the linear susceptibility. In the familiar regime of linear optics, with the driving polarization term proportional to the electric field, the right hand side of Eq. (1.1) can be lumped in with the time derivative of the electric field on the left-hand side. The result is a homogeneous wave equation with a modified wave speed: c/n = c//1 + X), where n is the familiar index of refraction. Physically, in the linear optical regime, the electric field of the wave produces a proportional polarization in the material which subsequently radiates electromagnetic waves of the same frequency. 27 CHAPTER 1. INTRODUCTION As the strength of the electric field increases, the polarization response deviates from the simple linear form. This is the regime of non-linear optics. The polarization is now a non-linear function of the electric field, i.e. P = P(E). In conventional nonlinear optics, we assume that the polarization's departure from the linear response is small. We can therefore expand P(E) in the perturbative form P(E) = co(X( 1)E + X )E2 + X 3 )E 3 +.. .) (1.3) In the above, XM again corresponds to the linear susceptibility, and the higherorder X(') terms (i.e. with n > 1) correspond to the non-linear susceptibilities. From these non-linear susceptibilities and higher-powers of the electric field come the classic phenomena of conventional non-linear optics, e.g. second-harmonic generation derives from the X) E 2 term. Note that in the perturbative expansion we have implicitly assumed that X(1) >> x() >> X(). We can re-write Eq. (1.3) in a more intuitive form as P(E) = coX(')E + a2 I + ai + . .2. (1.4) Here we have factored the linear response out of the polarization and expressed the higher-order terms as ratios of the electric field to some critical field strength Ec. The parameters a1 and a 2 for many materials are comparable and close to unity. In this form, the assumption of the perturbative expansion is very clear. When E << Ec the higher-order terms are small and the series expansion is valid. From this analysis we see that when E approaches E, the conventional, perturbative approach of non-linear optics breaks down. This is the strong-field regime. Here the non-linear response takes on a non-perturbative character and fundamentally new non-linear optical phenomena can be observed. We will discuss some of these phenomena and exciting applications in the following sections and in the course of this thesis. However, before this discussion let us first consider the boundary of the strong-field regime. Let us consider the value of Ec. A first guess at the value of E, might be the characteristic binding field strength of the material 2 . However, the characteristic binding field strength is not exactly a 2 If we use for Ec the atomic unit of electric field Eat = e/47rcoa2, i.e. the electric field experienced by an electron in a Coulomb potential at a Bohr radius (ao), and note that XM) is of order unity 1 1 for most materials, we can approximate X xM /E2 2 im/V and xj) = )/E2 3.78 x 10-24. Note that here we have assumed that a,, a 2 : 1. These values are actually comparable to the X(2 ) and X(3 ) values for many materials (see Ref. [13]). 28 CHAPTER 1. INTRODUCTION familiar quantity. Instead, let us compare the characteristic binding energy Eb of the material to the characteristic energy of the oscillating electric field, i.e. to the pondermotive potential Up. The pondermotive potential of an oscillating electric field represents the average kinetic energy of an electron wiggling in this field. Consider an electron (mass m and charge -e) in an electric field E(t) = Eo cos(wt). The electron's spatial position x(t) is given as a solution to the simple equation of motion d2 x2 (t) -d E(t) x(t) = e E02 e cos(wt) (1.5) Note that in the above we have disregarded any initial velocity of the electron. From the electron's spatial trajectory x(t) we can calculate the electron's average kinetic energy, i.e. Up = m(,(t)2 )/2, and we find UP e 2 E2 = 4mW 2 (1.6) This pondermotive potential Up is the characteristic energy scale associated with the electric field. We expect that when this energy exceeds the characteristic binding energy of the material Eb, the field of the electromagnetic wave will be strong relative to the fields in the material, and we will enter the non-perturbative regime of strongfield physics. Therefore we expect the transition to the strong-field regime to be defined by Up ~ Eb. In fact, as we will elaborate on in Chapter 2, the boundary to the strong-field regime will be defined by a slightly modified parameter known as the Keldysh parameter -y. This parameter is defined as ly = Eb U--= 2Up 2mEb (1.7) w eE0 When -y < 1 we expect the electric field strength of the incident electromagnetic wave to exceed the field strengths in the material, and we expect non-perturbative, strong-field effects. Now, to provide a more tangible physical picture of the strongfield regime let us consider a specific physical example: strong-field photoemission. However, before moving on to this example let us actually consider some numbers here and consider how strong strong-fields really are. 29 CHAPTER 1. INTRODUCTION How strong are strong-fields? Consider light with a wavelength of 1.2 pm illuminating a gold surface (gold has a 5.1 eV [14]). With these numbers 4 we see that to reach -y ~ 1, we must have Eo 12 V/nm. This field strength is on , binding energy or work function3 of Eb = WF the order of volts per Angstrom. For solid-state systems like the gold surface we are considering, typical lattice constants are at the Angstrom level and typical binding energies are at the volt level, so this field strength is exactly in the expected range. Let us now consider how strong a 12 V/nm electric field is compared to a force and field we are more familiar with and experience everyday: gravity. Typical gravitational acceleration here on earth is g ~ 9.8 M/s 2 . The acceleration of an electron in a 12 V/nm electric field is approximately a ~ 2.2 x 1021 M/s 2 This is obviously a tremendous acceleration. near the edge of a black hole is ~ 1027 g's 2.2 x 1020 g's. In fact, the gravitational acceleration [5], so we are talking about some pretty extreme conditions! 1.1.2 Multiphoton to strong-field photoemission Photoemission is the emission of electrons from a material surface by light. The conventional picture of photoemission involves energy, i.e. photon, absorption (see Figure 1-1). An optical field illuminates a metal surface (for the purposes of this thesis, the photo-emitting material will be metallic, in our case gold), and the optical field wiggles an electron in the metal. We model the metallic binding potential as a simple, smoothed rectangular step of a height given by the work function WF. When illuminated by light (in the case of Figure 1-1, violet, red, and green light), the electrons in the metal slowly pick up energy. Eventually they can absorb enough energy to hop over the binding potential barrier and out into the vacuum. The photo-emitted electrons can absorb one or more photons from the illuminating optical field. Conventionally, the electrons only absorb the number of photons required to surmount the work-function barrier 5 ; see, for example, that in Figure 1-1 three red photons are required to overcome the barrier, two green photons are required, and just one violet photon is required. This multiphoton absorption and 3 Depending on various conditions, the work function of gold varies around 5 eV by several tenths of an eV. For the purposes of this thesis we will use the value of 5.1 eV [14]. 'These numbers are typical of our experiments described in Chapter 4. 'We are taking a very simplistic approach to photoemission here for the purpose of illustrating the essential physical phenomena. Photo-emitted electrons can absorb more photons than are required to surmount the work-function. This phenomena is known as above-threshold photoemission. 30 CHAPTER 1. INTRODUCTION hv,+ hV,+ h, vacuum i'J - -(x U 1 W_ Figure 1-1: Multiphoton photoemission. Photons of different colors excite electrons from the Fermi level to an energy above the vacuum level, and the excited electrons subsequently leave the metal. The violet, red, and green squiggles represent violet, red, and green photons of energy hvv. hvr, and hvg respectively. U represents energy, and x is the spatial coordinate normal to the metal surface. Un is a sketch of the metal's binding potential, and WF represents the work function. photoemission is a well-known non-linear optical effect [13, 15], and we can write the total photoemission current as J = a 1, + 02)I2 + C()13 (1.8) In the above, J represents the photo-emitted electrical current, and I, Ir, and I are the optical intensities of the violet, red, and green light respectively. The constants a(), a(2), and a() describe the relative contributions of the one-, two-, and three-photon components to the total current, and, similar to the non-linear susceptibilities we previously discussed, a0) >> a 2 ) >> a(3 ). Paralleling our preceding development, we can re-write Eq. (1.8) as J= (1 (v) + 0(2) g + p( (1.9) Where in the above, O(n) = a()I . Here we have factored out a critical intensity, Ic, and in this form the /(n) terms for many materials are of the same order, i.e. 31 CHAPTER 1. INTRODUCTION #3(1) ~ (2) ,~ (3). It is clear that when the optical intensity is less than the critical intensity, I << Ic, the higher-order multiphoton terms will provide relatively small contributions to the total photo-emitted current. This is exactly what is observed in conventional photoemission experiments. However, when the optical intensity approaches the critical intensity I ~Ic, or when the electric field of the optical wave approaches the associated critical field E ~ Ec, we see that all the multiphoton orders will become comparable; here we enter the strong-field photoemission regime, and as we will see, the basic physical picture of photoemission changes. Something not considered in the previous discussion is that the optical field actually wiggles the metallic binding potential. In the vacuum half-space the electric field of the illuminating light creates a potential Um(x) - exE(t) where Um(x) is the metal's binding potential, x is the spatial coordinate normal to the metal surface, and E(t) is the electric field of the illuminating light' (see Figure 1-2). As the intensity approaches the critical intensity 1, and the field strength grows toward Ec, the barrier can become extremely distorted as drawn in Figure 1-2. Near the critical field strength Ec, the potential barrier is collapsed to such an extreme degree that electrons from the metal can tunnel through. We imagine that this tunneling current will become significant when the barrier is collapsed for a sufficiently long duration such that a sizable number of electrons can traverse the barrier. Assume that it takes an electron approximately the time Tt to tunnel through the barrier, and let us define the oscillation period of illuminating electric field, i.e. the cycle-time, to be Tcyc. Then if Ftun < 7cy,, we expect a sizable tunneling current. We can quantify this condition by calculating the tunneling time rtss. However, tunneling time is a tricky and historically debated quantity [16, 17]. We will elaborate on how to estimate the tunneling time in Chapter 2; however, for now we will just use the result Ttn = V2mWF/eEo where E0 is the electric field deflecting the barrier. Using this result and writing the cycle time Tcyc = 1/w where w is the angular frequency of the optical field 7 , we find that the tunneling current becomes significant when Ttun y = - rcyc w __- 2mWF eEo E = <1 (1.10) 2Up Note that this ratio that defines when the optically-driven tunneling current becomes 6 For simplicity in this intuitive discussion, we are assuming that the field is constant in space. This is a reasonable assumption if we are considering dynamics occurring only very close to the metallic surface. 'This cycle time is the optical period divided by 27r. This definition is to maintain consistency with the standard form of the Keldysh parameter [7, 18]. 32 CHAPTER 1. INTRODUCTION hvv vacuum U ---- e o- -- +- - UmJz) ---------- cxE(t) Figure 1-2: Strong-field photoemission. At high field strengths, the strong fields distort the metal's binding potential and results in electron tunneling emission from the metal. sizable is the same Keldysh parameter we defined earlier (note WF = Eb). We previously saw that this parameter defined a boundary where the energy scale of the field, Up, began to compare to the energy scale of the material, Eb. We see here that the boundary to the strong-field regime also defines the boundary to the optically-driven tunneling regime. In other words, when -y ~ 1, the physics of the photoemission process begin to depart from the simple picture of electrons wiggling and grabbing energy from the optical field and begin to resemble an electron tunneling process in which the binding potential is deflected by the optical field and electrons tunnel through. This picture of optically driven tunneling is central to strong-field photoemission. There are several interesting characteristics to this optically-driven tunneling regime I that largely explain the tremendous interest in this physical process. In the coming chapters we will elaborate theoretically and experimentally on these characteristics. 'in the following photoemission related discussions we will use the terms 'strong-field regime' or 'optically-driven tunneling regime' interchangeably; they both refer to the same extreme-field region of photoemission. 33 CHAPTER 1. INTRODUCTION Reaching the strong-field regime 1.2 Now that we have a sense for what defines the strong-field regime, let us explore how we actually go about reaching the field strengths necessary for strong-field physics like strong-field photoemission. As mentioned, it was the development of the first laser that allowed researchers to reach the required peak optical powers and field strengths to explore some of the first non-linear optical phenomena, namely secondharmonic generation. It has largely been the development of ultrafast, femtosecond laser and amplifier technologies that have likewise provided researchers with the tools to achieve the peak optical powers and field strengths necessary to explore the strongfield regime of non-linear optics. In Figure 1-3, we chart the progress of ultrafast laser sources and amplifiers over the past few decades. In this section we provide a brief review of some fundamental concepts in the treatment of ultrafast optical pulses as . well as some basic information on ultrafast laser amplifiers9 b a r lops CPA 1021 1020 ps-- E .1019 100 fs . . 10 p 1017 W 0J 010 fs - 107 W/cm 2 6isfs 1960 1970 1990 1980 2000 1960 2010 1970 1980 1990 2000 2010 Year Year Figure 1-3: Progress in ultrafast laser sources and amplifiers. a. The achievable minimum laser pulse duration as a function of year. The arrow indicates the first demonstration of SHG [2]. b. The achievable maximum focused laser 2 7 intensity as a function of year. The 10 W/cm mark shows the intensity used in the first demonstration of SHG [2]. Note the tremendous growth in achievable intensity since the development of chirped pulse amplification (CPA). (Images borrowed from Ref. [5] without permission). 1.2.1 Ultrafast pulses For the purposes of this thesis, we consider only the electric field of an ultrashort optical pulse and model this field as a slowly varying pulse envelope modulating a rapidly varying optical carrier-wave. Our model for an ultrashort optical pulse can then be written as 9 For a more elaborate treatment on these subjects see Refs. [4, 19] 34 CHAPTER 1. INTRODUCTION E(t) = E0 x P(t) cos(27rfct + (OCEO) (1.11) where E(t) is the electric field of the pulse, E0 is the peak electric field, P(t) is a normalized pulse envelope shape, f, is the central frequency of the carrier-wave, and LCEO is a phase-shift called the carrier-envelope offset phase (CEP). The CEP describes the displacement of the carrier-wave maximum, or field maximum, from the pulse envelope maximum (see Figure 1-4). Note that the CEP defines the shape of the optical electric field of each pulse. 'rFWHfM Ewas TR =A IfR Figure 1-4: Ultrashort optical pulse train from a mode-locked laser. A single optical pulse circulates in the laser cavity (sketched in the upper left) with a circulation period TR. The pulse periodically leaks out of the cavity forming a pulse train with temporal spacing TR = 1/fR. Each pulse contains an energy Ep and has a full-width at half maximum duration of TFWHM A train of optical pulses as emitted by a mode-locked laser is illustrated in Figure 1-4. In Figure 1-4, we see that a single optical pulse circulates in the mode-locked laser's resonator with period TR (illustrated in the upper left of Figure 1-4). The pulse leaks out and forms the illustrated train of pulses with each pulse copy separated by the repetition rate period TR (the repetition rate frequency is fR = 1/TR). Each pulse has an associated pulse energy Ep and an associated full-width at half maximum duration rFWHM1 . From Figure 1-4, we also see that from pulse to pulse ,0 CEO shifts by some fixed amount AZo. This shift is due to group and phase velocity mismatch in the mode-locked laser resonator. The frequency at which this phase "0 The pulse duration will often also be written as just r and is conventionally defined as the fullwidth at half maximum of the intensity envelope (hence the seemingly odd location of the labeling in Figure 1-4). 35 CHAPTER 1. INTRODUCTION shifts is known as the carrier-envelope offset frequency fCEO, and can be defined as (A/27r) x fR. The CEP and the fCEO will be important parameters in our experiments (further discussion on their properties is provided in Appendix A). fCEO = It is worthwhile to make some brief comments on the frequency domain structure of the considered ultrafast optical pulses and pulse trains. A sketch of the spectrum for an isolated ultrafast optical pulse and a pulse train are provided in Figure 1-5a and b respectively. Note that the spectrum of the isolated ultrafast pulse is clearly very broad and the carrier-envelope phase appears as a constant, absolute phase across the entire spectrum. For the pulse train the broad spectrum is broken into harmonics appearing at the repetition rate fR. The fCEO becomes important as it provides an offset to each of the comb lines comprising this frequency comb spectrum (more details on time and frequency domain structure as well as WCEO and fCEO are provided in Appendix A). a :.f b fR xe~& nfA+fcEo Figure 1-5: Ultrafast optical pulses and pulse trains in the frequency domain. a. The spectrum of an isolated ultrafast optical pulse with central frequency f, and CEP WCEO. b. The spectrum of an ultrafast optical pulse train with repetition rate fR, central frequency f,, and carrier-envelope offset frequency fCEOConsidering the above definitions, let us now look at some typical parameters for an ultrafast optical pulse train. Consider the femtosecond laser pulse train we will use in our experiments in Chapter 4: the repetition rate is fR = 78 MHz; the pulse energy is Ep - 0.2 nJ; and the pulse duration is 'FWHM ~ 9 fs. The average power of this pulse train is then Pvg = fR x Ep = 15.6 mW. This relatively low power is comparable to the average power emitted by many compact continuous-wave lasers, 22 kW. e.g. laser pointers"1 . However, the peak power is Pp = Ep/TFWHM Consider tightly focusing one of these laser pulses to a beam radius of wo 2.6 pm (typical of our experimental conditions in Chapter 4). With this beam radius and "This is not a coincidence. The laser pulse energy in a mode-locked laser is dictated by the energy storage capabilities of the laser gain medium, so we expect these powers to be comparable [13]. 36 CHAPTER 1. INTRODUCTION the above peak power, we can estimate the peak optical intensity Ip and the peak electric field E0 , of one of these laser pulses. We find" ~ 2E 7T'UO2/FWHM 2.1 x 10" W/cm2 -- + Eo 1.3 V/nm (1.12) Although tremendous optical fields are achievable directly at the output of femtosecond mode-locked laser oscillators, the field strengths still generally fall short of the strong-field regime levels (for our above example, 1.3 V/nm << 12 V/nm). The second major technological development that has given researchers the ability to reach the strong-field regime is ultrafast laser pulse amplification, in particular chirped pulse amplification. However, before considering ultrafast laser amplifiers let us take a brief detour to consider just how fast ultrafast optical pulses are. How fast is ultrafast? For our purposes, ultrafast or ultrashort laser pulses are on the femtosecond scale. Although increasingly common in research labs and industrial applications, it is difficult to grasp just how short a femtosecond is. The otherworldly nature of the femtosecond is not terribly surprising considering that the average firing rates of most synapses in our brains are only on the order of 10-100 Hz i.e. with a period of 10-100 ms [20]. To get a sense for how small a femtosecond is, let us consider the following ratio' 3 8 fs 1 minute 1 minute Age of the universe With this sense of scale for the femtosecond, one is left wondering how we are able to make lasers emitting such short pulses or why we might be interested in such an absurdly small unit to begin with. The answer is found simply through some Planck's constant gymnastics. Considering the energy-time uncertainty relation, AtAE - h, we find that for At ~1 fs, AE ~ 0.7 eV. Energy-level spacings in molecules and solids are generally on the eV-level, so accordingly, the dynamics of molecules and solids occur in the femtosecond domain. Additionally, by no coincidence, photon energies of visible light are in the few eV regime, and therefore, the oscillation pe2 The factor of two in the Ip expression in Eq. (1.12) emerges for Gaussian beams. Additionally, the relation used here (and for the rest of this thesis) between the intensity and the electric field strength is the usual expression for plane electromagnetic waves: I = E 2 /2ZO where Zo is the impedance of free-space, Zo = /po/co ~ 377 Q. 1 3 The age of the universe approximation comes from Ref. [21]. 37 CHAPTER 1. INTRODUCTION riod of optical electromagnetic waves must be on the order of a few femtoseconds. So, although seemingly bizarrely small, the femtosecond is a very natural unit for interactions, transitions, and dynamics in molecules and solids. It is with these interactions, transitions, and dynamics that ferntosecond laser pulses are made and a large reason why (aside from the tremendous peak power they offer) ultrafast, femtosecond laser sources are of great interest. 1.2.2 Ultrafast laser amplifiers In addition to ultrafast laser pulses, the development of ultrafast laser amplifiers have been critical to achieving the field strengths necessary for strong-field physics. The most predominant form of ultrafast laser amplifier is the chirped pulse amplifier (CPA). The basic mechanism behind chirped pulse amplification is as follows: CPAs broaden ultrafast laser pulses to limit their peak power, amplify or build-up the pulse energy of the resulting broadened pulses, and then re-compress the amplified pulses into extremely high peak power ultrashort optical pulses [4, 19]. Typical commercial CPA systems can provide millijoule pulse energies in laser pulses of around 20-30 fs. This amounts in peak optical powers of Pp a 1 mJ/20 fs e 50 GW. Imagine increasing the tightly focused 0.2 nJ laser pulse discussed previously to 1 mJ pulse energy. This would result in a peak intensity of Ip 1018 W/cm 2 and a peak field of E0 - 2800 V/nm, well into the strong-field regime! Although chirped pulse amplifiers offer access to tremendous optical peak intensities and field strengths (see Figure 1-5), they are not without drawbacks. Their primary limitations come in two forms: repetition rate restrictions and complexity. Firstly, chirped pulse amplifier systems reduce the repetition rate of the amplified optical pulse train. CPAs generally take a e 100 MHz optical pulse train from a modelocked oscillator seed and dramatically amplify the pulse train but also dramatically reduce the repetition rate of the train to just a few kHz. This drop in repetition rate is largely associated with average power limitations: a 1 mJ pulse train at 100 MHz repetition rate would have an average power of 100 kW! This decrease in repetition rate however dramatically limits the potential flux of the products of strong-field interactions. For example, if we are interested in using the high-harmonics produced via a strong-field non-linear optical process as a source of short-wavelength light, then this source will have a flux limited by this kHz repetition rate. The second major restriction of CPA systems is complexity. Looking at Figure 1-6a, although these CPA systems are table-top in size, they can sometimes stretch the definition of a table-top. 38 CHAPTER 1. INTRODUCTION b a a, r. t Figure 1-6: Ultrashort laser pulse amplifiers and resonators. a. Picture of a typical commercial CPA laser system capable of generating multi-mJ femtosecond laser pulses in a strong-field physics laboratory (photo courtesy of P. D. Keathley). b. Sketch on an ultrafast optical enhancement cavity. An optical pulse circulates in the resonator with amplitude ares. It is excited by an incident pulse train with amplitude aj. An alternative route to achieving the field strengths necessary for the strong-field regime while bypassing repetition rate restrictions or the complexity of these large amplifier systems is therefore very desirable. To this end researchers have pursued using passive optical resonators to achieve these strong-fields directly from the output of mode-locked laser oscillators. The essential idea behind passive optical resonators is illustrated in Figure 1-6b. In Figure 1-6b, we have a two mirror arrangement confining an optical pulse. The pulse circulates between the two mirrors with amplitude ares. If we assume in this simplistic treatment that one of the mirrors is a perfect reflector and the other has reflectivity, r, and transmissivity, t, then we find that the pulse amplitude in the resonator, are,, must be related to the incident pulse train amplitude ai by ares = - rares + itai it i ai 1 - r (1.13) (1.14) Therefore, tremendous intra-resonator pulse amplitudes can be built up without active amplification! The above analysis has obviously been a very simplistic one, and there are many restrictions to passive pulse amplification with optical resonators. We will discuss these throughout this thesis as we pursue strong-field physics with optical 39 CHAPTER 1. INTRODUCTION resonators. In the following section, we first will give some details on applications of strong-field physics and motivate interest in this resonator approach. 1.3 Strong-fields at the nanoscale and HHG Thus far we have described the what and the how of strong-field physics. We have defined the strong-field regime and provided a relevant example, and we have reviewed how we can reach this strong-field regime with ultrafast laser pulses and amplifiers. Additionally, we suggested the possible advantages in using optical resonators to reach the necessary field strengths for strong-field physics. In this section we will build on this discussion; we highlight the two application areas of strong-field physics that will be the focus of this thesis, and we describe the utility of optical resonators in these applications. The first application area of interest is strong-field photoemission near nanostructures. As we mentioned earlier, when an optical field reaches a critical strength the fundamental physical picture of photoemission changes. In the strong-field regime of photoemission, sub-optical cycle bursts of electrons can be ripped from material surfaces. These electrical bursts can be switched on and off with individual cycles of the excitation laser pulse, and after emission these electrical bursts wiggle in the driving laser field. They can be driven back into the material surface where they can re-scatter and extract more energy from the laser field. The prospect of using these sub-optical cycle electron bursts for scientific investigations of solid-state surface dynamics as well as the prospect of steering these electron bursts with optical waves for technological purposes have made strong-field photoemission a hot research topic in the past decade. In particular, nanostructure surfaces offer several particular advantages to the strong-field photoemission experiments. One such advantage is the field-enhancement present at a nanostructure. This field-enhancement eliminates the need for repetition rate reducing, complex laser amplifiers. This field-enhancement near plasmonic nanoparticles also takes on an optical resonator like character. Figure 1-7 illustrates the basic arrangement for strong-field photoemission from nanostructures and a representative dataset. The second application area of interest is high-harmonic generation. As discussed, when the optical fields approach a critical strength, the perturbative description of non-linear optical processes breaks down. In this strong-field regime familiar phe- nomena like second-harmonic generation are replaced by non-perturbative phenomena. Illuminating gas jets [3, 4, 5, 6, 7] with high peak power, ultrafast laser pulses, 40 CHAPTER 1. INTRODUCTION b 0.2 pi 0.2fp. fsIgr0 2 4 G 8~ 10 1 Electron energy (eV) Figure 1-7: Strong-field photoemission near nanostructures. a. Strong-field photoemission from plasmonic nanoparticles. A femtosecond laser pulse illuminates the nanoparticles, and they photo-emit electrons (illustration borrowed from Ref. [22] without permission). b. Electron energy spectra measured from strong-field photoemission experiment with differing excitation pulse energies (picture borrowed from Ref. [23] without permission). researchers have generated hundreds of harmonics. The process that leads to this generation is creatively named high-harmonic generation (HHG). The essential physics of HHG is closely linked to strong-field photoemission. HHG can be understood as a simple three-step process [24, 25]. First, an intense laser field results in strong-field ionization of an electron from a host atom. The emitted electron, like those in strong-field photoemission, is sub-optical cycle in duration and subsequently wiggles in the oscillating laser field acquiring energy. This electron can be sent by the laser field back towards its parent atom where it can recombine and emit a high-energy photon. From this simple physical picture of HHG, we predict a broad spectrum of harmonics with a plateau-like structure (see example in Figure 1-8a). The generated high harmonics have excited researchers as they might furnish routes towards table-top, coherent sources of light in the hard-to-reach spectral region of the extreme ultraviolet (EUV) or soft x-ray range. However, as we have mentioned, the amplification necessary to achieve the required field strengths for HHG limits the achievable flux of HHG based short-wavelength sources. In order to push the repetition rate of HHG sources from the kHz regime of CPA systems to the 100 MHz regime of mode-locked laser oscillators, passive optical resonators, i.e. enhancement cavities have been employed (see Figure 1-8b). We will discuss the benefits and drawbacks of these cavities and the general approach in subsequent chapters. 41 CHAPTER 1. INTRODUCTION a b 20 40i 60' so 100 120 140 Out-coupWd high harmonics 160 Pluom~ ensrgy (sy) Figure 1-8: Characteristics of HHG and cavity-enhanced HHG. a. Example of an HHG spectrum. For this example, the driving laser light wavelength varies but for the pink trace A = 1.8 Mm or the photon energy ~ 0.7 eV. Note the large plateau of hundreds of harmonics; this plateau resembles the plateau in the electron energy spectra from Figure 1-7b (this data was borrowed without permission from Ref. [3]). b. Basic arrangement for cavity-enhanced HHG. An ultrafast laser pulse is enhanced in a bow-tie ring cavity where high-harmonics are produced and out-coupled via a sapphire plate (the pictured harmonics are borrowed from Ref. [26] without permission). 1.4 Outline of this thesis As a final section to this introductory chapter, we reiterate the purpose of this thesis and outline the following chapters. The course of this thesis research has spanned many projects and a wide range of topics. We have unified two of the main projects in the broad category of strong-field physics with ultrafast optical resonators. We present work on the two main application areas outlined above. First, we use plasmonic nanoparticle optical resonators to explore strong-field physics near nanostructures. We will switch on and off photoemission currents from nanoparticle resonators with individual optical cycles of a femtosecond laser pulse. We will use this photoemission current to characterize the femtosecond dynamics of the nanoparti- cle's excited nanoplasmonic field and demonstrate carrier-envelope phase sensitivity of the photoemission current. Second, we will explore novel optical resonator designs for cavity-enhanced high-harmonic generation. We will design and prototype optical enhancement cavities supporting Bessel-Gauss intra-cavity modes, and we will demonstrate that such cavity modes might allow the major obstacles to efficient cavity-enhanced HHG to be overcome. The outline of the following chapters is as follows: 42 CHAPTER 1. INTRODUCTION Chapter 2 - Theory of photoemission from solid surfaces The main goal of this chapter is to develop a qualitative physical picture and quantitative model for strong-field photoemission. We first consider some fundamental elements of electron emission; in particular, we discuss field emission and photo-assisted field emission. We develop a basic theoretical framework to study photoemission, and we analyze photoemission rates in the multiphoton and strong-field regimes. We additionally consider the time-dependence of strong-field photoemission currents and the carrier-envelope phase sensitivity of the strong-field photoemission process. Chapter 3 - Plasmonic nanoparticles and optical resonators Here we discuss the fundamentals of plasmonic nanoparticle resonators. We begin with an intuitive review of surface plasmons and build a conceptual physical picture of the operation of nanoparticle resonators, and we construct a simple circuit model that can accurately describe and predict the response of plasmonic nanoparticles when excited by femtosecond optical pulses. Lastly, we mention some details of our nanoparticle fabrication procedure, describe the overall layout of our nanoparticle emitter chips, and present fits of our nanoparticle properties to the simple, second-order circuit model. Chapter 4 - Photoemission from plasmonic nanoparticles In this chapter we present the experimental results from our investigations into on-chip strong-field photoemission from plasmonic nanoparticle emitters. We motivate our results by providing some background on strong-field physics with nanostructures. We then move to provide details regarding the experimental system: we discuss the femtosecond laser source, the laser pulse measurement system, the carrier-envelope phase stabilization technique, and the device alignment microscope. We then discuss basic scaling properties of the photoemission from the nanoparticles and demonstrate signatures of the strong-field regime. We use the strong-field photoemission current to perform interferometric autocorrelations and characterize the nano-plasmonic, ultrafast optical field on the nanoparticles. Lastly, we demonstrate the carrier-envelope phase sensitiv- ity of the photoemission signal and develop a simple model for predicting this carrier-envelope phase response. 43 CHAPTER 1. INTRODUCTION Chapter 5 - Enhancement cavities for high-harmonic generation In this chapter we outline the basics of cavity-enhanced high-harmonic generation. The essential motivation for enhancement cavities for strong-field physics is discussed, and the concept of passive amplification inside an ultrafast, femtosecond enhancement cavity is reviewed. We discuss the requirements for an effective enhancement cavity for HHG and the challenges associated with the design of such a cavity. Chapter 6 - Bessel-Gauss beams Here we introduce Bessel-Gauss beams. We construct Bessel-Gauss beam solutions by superposing familiar Gaussian-like beams. We describe the focal and far-field properties of Bessel-Gauss beams and illustrate their advantages for strong-field enhancement cavities. Lastly, in preparation for design of such cavities with Bessel-Gauss modes, we analyze how Bessel-Gauss beams transform as they traverse simple optical elements. Chapter 7 - Bessel-Gauss beam enhancement cavities In this chapter we build upon the properties of Bessel-Gauss beams to analyze Bessel-Gauss beam enhancement cavities. We consider the overall design principles of Bessel-Gauss beam cavities and how to build such cavities from fundamental Gaussian designs. We discuss a specific design: the confocal Bessel-Gauss cavity and possible arrangements for high-harmonic generation applications. We discuss a continuous-wave experimental demonstration of the confocal Bessel-Gauss cavity and highlight the limitations of Bessel-Gauss modes illuminated by this demonstration. 44 Chapter 2 Theory of photoemission from solid surfaces In the next three chapters, we will discuss strong-field photoemission from nanostructures, in particular plasmonic nanoparticle resonators. We begin the discussion in this chapter with an introduction to the theory underlying photoemission from solid surfaces. Our main goal will be to develop a qualitative physical picture and quantitative model for photoemission in the strong-field regime. Towards this end, we first look at some fundamental elements of electron emission. We discuss the basics of field emission i.e. electron emission from a material in the presence of a static bias field; we briefly discuss photo-assisted field emission mechanisms; and we consider the basic theoretical formalism behind photoemission. We build on this discussion to analyze the basics of strong-field perturbation theory, and we calculate average photoemission currents in the strong-field regime. We carry out these calculations for illumination with an ultrashort optical pulse and with a continuous-wave, monochromatic excitation. Next, we discuss the time-dependence of photoemission in the strong-field regime and develop a simple quasi-static model. Lastly, we consider carrier-envelope phase effects in strong-field photoemission. We briefly discuss their origins and present a simple model to predict their strength. 2.1 Electron emission fundamentals Electrons can be coerced to leave solid surfaces by a variety of means. As mentioned in the previous chapter for the purposes of this thesis we will be concerned with metallic surfaces, in particular gold surfaces. In the previous chapter, we briefly discussed 45 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES a particular electron emission mechanism, multiphoton photoemission, in which electrons in a metal can absorb optical energy and hop over their binding potential and out of the metal and into vacuum. In addition to this optically-driven photoemission mechanism, many other physical mechanisms for electron emission exist. We divide these emission mechanisms into three logical categories: field emission, photo-assisted field emission, and photoemission. These three categories of electron emission are divided according to whether they rely on a static bias field, a static field and an optical field, or just an optical field. The field emission mechanism relies on a static bias applied to the metal surface that allows electrons to tunnel from the metal and into vacuum. The photo-assisted field emission mechanism involves a mixture of optical and static field effects. For example, in photothermal emission an optical source heats the electrons in a metal, and these hot electrons then field-emit from the metal surface in the presence of a static field. Lastly, the photoemission mechanism, as has been discussed, involves an optically driven form of emission. In the following, we discuss each of these electron emission mechanisms, and we build towards an understanding of photoemission in the strong-field regime. 2.1.1 Field emission In the field emission regime, static fields lead to electron emission from a metal surface. The static electric field deflects the electron's binding potential such that electron's can tunnel from their host material. We can make an extremely simple, yet insightful, model for this phenomenon. We can model the metal's binding potential at the surface as a simple rectangular step (as we did for our discussion of multiphoton photoemission in the previous chapter). We can then write the time-independent Schr6dinger equation h2 d2 2 2m dx + (WF + EF - eXEstat)U(X) In the above, #(x) O(x) = EF(x) (2.1) is the wavefunction for a single electron in the metal at the Fermi energy EF, WF is the work function, and u(x) is a step-function. Additionally, as before -e and m are the electron charge and mass 2 respectively. The coordinate x denotes distance in the direction normal to the metal's surface, and Estat denotes the 'We define the step-function as u(x) = 1 if x > 0 and u(x) = 0 if x < 0. 2 Note that we use the bare electron mass, m, in Eq. (2.1) instead of the effective mass, m*U, in gold. The reason for this will be elaborated upon in a later section. 46 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES static applied bias field'. The basic model and wavefunction for the Etat = 0 and Estat = Eo = 10 V/nm cases are illustrated in Figure 2-1. Note that from the form of Eq. (2.1), we are assuming there is no field penetration in the metal. Here and in the following, we use the normal parameters for a gold surface [14, 27], EF = 5.5 eV and WF = 5.1 eV. b a vacuum vacuum 5 -5(x) S - E= 10 V/- W? -- - EF ---- -51 -5 -2 -1.5 -1 -0.5 0 0.5 1 1.5 -2 -1.5 -1 -0.5 0 0.5 1 1.5 X (1m1) :r(1111) Figure 2-1: Field emission and models. a. Basic model for metallic surface. The interior of the metal is treated as a free electron gas, and the metal surface is modeled as a simple rectangular step of height WF. As before, the metal potential is denoted as Urnm(x) with x the coordinate normal to the surface. The real part of the electron wavefunction at the Fermi energy is drawn in red (calculated numerically). b. Potential with an applied static bias. With an applied bias the rectangular step is deflected, and electrons can tunnel through the barrier and into the vacuum. The real part of the wavefunction is again drawn in red (numerical calculation). With Estat = 0, Eq. (2.1) can easily be solved, and the wavefunction is found to be oscillatory in the metal; it is composed of forward and backward plane wave components reflecting off the potential step. Under the barrier the wavefunction takes on an evanescent form. Under the barrier (for x > 0) the wavefunction takes the general form #(x) oc exp(-ax) with 3 We a= 2mWF/h (2.2) should make a short note concerning notation. Tragically, the poor choice was made to use the letter E for both energies and for electric field. Hopefully, context will indicate which quantity we are discussing. 47 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES This general behavior is illustrated in Figure 2-la. With an applied static field, (2.1) becomes more challenging to solve analytically. However, we can use Eq. the Wentzel-Kramers-Brillouin (WKB) approximation to estimate the wavefunction under the barrier as #(x) oc exp - dx'P(x')) with p(x) = 2m,(WF - exEstat)/h (2.3) The above form of the wavefunction only applies to the under-barrier region i.e. 0 < x < d where d is the barrier exit (or tunnel exit). The essence of the WKB approximation used above is to separate the problem into two length scales. The relatively large length scale over which variations in V(x) = WF + EF - exEstat occur, and the far shorter length scale defined by A = h/p(x). Since this wavelength A is generally very small compared to the scale of variations in V(x), the potential can be approximated as quasi-static, and the above form of the wavefunction is found. The general intuition behind this quasi-static concept will be applied in future sections to analyze the time-dependent behavior of photoemission. Using the WKB form of the wavefunction, we can estimate the energy-dependent barrier transmission, T(E), by considering the wavefunction at the barrier or tunnel exit T(EF) c (d) I2 cx exp - dx N2m(WF - exEstat) (2.4) In the above, d again refers to the tunnel exit, and T(EF) is the barrier transmission at the Fermi energy. The above integration can easily be performed, and we find T(EF) oc exp where Et,, = 4/2mWF/3he -tun (_Estat) (2.5) (~ 78.7 V/nm for our parameters) is a characeristic tunneling field strength. The form of T(EF) gives a sense for the extreme exponential nature and sensitivity of the tunneling process. A complete field emission tunneling current can be calculated from the above transmission function by integrating the transmission of all the electron states in the metal weighted by their incident electron velocity and probability of occupation. Carrying out this operation [28], we find the well-known Fowler-Nordheim equation for the tunneling current as a function of the applied static field 48 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES Jitn(Estat) = 2 ( Estat (Etun exp ) Eun (2.6) (Estat The above simple model and the Fowler-Nordheim equation have been used extensively to model field emission devices in their many applications. In later sections we will make use of this simple model to trace the time dynamics of strong-field photoemission. However, before proceeding towards this goal and our discussion of other emission mechanisms, we look at one last quantity of interest that we can extract from this simple static model: the tunneling time. Tunneling time Loosely defined, the tunneling time here refers to the duration the electron takes to traverse the barrier. Tunneling time is a tricky and debated quantity however with this simple definitition in mind, we can formulate an esimate for this time via our WKB expression for the wavefunction [16, 17]. Previously, we found that under the barrier the electron momentum in out model takes the form p(x) = -/2m(WF - exEstat). We can estimate the velocity under the barrier as v(x) = p(x)/n, and accordingly we can crudely estimate the time it takes for an electron to traverse the barrier as fdx n To v(x) 0 d n(2.7) 2(WF - ex Estat) e Estat In the above, d again refers to the tunnel exit position, and we see that we obtain the . tunneling time used in the previous chapter4 2.1.2 Photo-assisted field emission The next category of electron emission processes involves a mixture of static and optical field effects. These emission mechanisms generally involve two basic steps. In the first step, light excites the electrons in a metal in some way. At their higher, excited energy levels, the electrons see an effectively lowered work function, and, when a static field is applied, they field-emit out of the metal. In Figure 2-2 we illustrate two common photo-assisted field emission mechanisms: photo-thermal emission and photo-field emission. In the following, we briefly discuss these mechanisms. 4We should reiterate that this tunneling time derivation is not intended to be rigorous, but intuitive. For more thorough treatments and discussion of tunneling time see Refs. [7, 16, 17]. 49 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES hv, hv, a b vacuum vacuum 5 F4)= 10 E0 10 V/11111' ----------VV VV V --- ----------------- ---- -- ------ 3hv 0 Ep EF ---------------------------------- --------------- ------------------- -5 -2 ft -------------------------- n TH.t. -1.5 -1 -0.5 -5 0 0.5 1 1.5 -2 x (niii) J -1.5 -1 -0.5 0 0.5 1 1.5 x (nimi) Figure 2-2: Photo-assisted field emission. a. Photo-thermal emission. An optical excitation locally heats the electron gas in a metal (see the lightly shaded region labeled THot). This heating results in a stretched Fermi-Dirac distribution. Higher energy levels are now increasingly thermally occupied and can undergo field emission. The real part of the electron wavefunction at 2 eV above the Fermi energy is drawn in red (calculated numerically) with a static field of Estat = E0 = 10 V/nm. b. Photo-field emission. An optical excitation resonantly excites electrons to higher energy levels, and these excited electron field-emit. The real part of the electron wavefunction at 3 eV (three photons at a wavelength of 1.2 pm) above the Fermi energy is drawn in red (calculated numerically) with a static field of Estat = E0 = 10 V/nm. Photo-thermal emission As mentioned, in photo-thermal emission an optical excitation heats the electron gas. In our simple model we can think of the Fermi-Dirac distribution broadening dramatically in response to the heating (see Figure 2-2a). At the high optical field strengths achievable with an ultrafast laser pulse, this heating can be dramatic. The electron gas can be heated to thousands of degrees K before thermalizing with the lattice over hundreds of femtoseconds (note the electron temperature is distinct from the bulk temperature of the gold i.e. the lattice temperature, so the electron temperature can be thousands of K with no apparent damage or melting occurring). When a static field is applied this hot electron gas can result in large field emission currents. These currents should occur over the duration of the electron gas thermalization and should be extremely sensitive to the applied static bias due to the field emission nature of the process [29]. Although important to mention, photothermal emission will not 50 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES play a major role in our experiments as will be evidenced by the lack of static bias sensitivity mentioned later in Chapter 4. Photo-field emission Photo-field emission is similar to photothermal emission. In photo-field emission, incident photons excite electrons in the metal to higher energy levels, and these electrons subsequently field-emit in the presence of a static bias field. This emission mechanism is distinct from photo-thermal emission in that it involves the generation of a highly non-equilibrium electron distribution. In other words, electrons are optically excited and field-emit before the electron gas can thermalize into a hot Fermi-Dirac distribution. This emission mechanism can also involve the resonant excitation of electrons between bands. In Figure 2-2b, the photo-field emission process is illustrated with a three-photon, 3 eV excitation. This gap actually closely corresponds to an available transition in gold between the d-band and the sp-band [30]. As for photo-thermal emission, we expect that photo-field emission will be very sensitive to the applied static bias due to its field emission nature. As we mentioned, we will largely rule out photo-field emission due to the relatively weak static field effects we will observe in our experiments in Chapter 4; however, future studies of photo-field emission are warranted. 2.1.3 Multiphoton and strong-field photoemission Our final category of electron emission is photoemission. As we have mentioned, photoemission involves the optical exciation of electrons from the metal, and in photoemission, static bias field effects are relatively weak. In the following, we first formulate the basic framework for the calculation of photoemission currents. Next, we discuss photoemission currents and calculation techniques in the multiphoton regime and in the strong-field regime. Photoemission involves a time-dependent, optical excitation. Therefore, all the interesting behavior will emerge from the time-dependent Schrddinger equation i )= H(t) 10) (2.8) In the above our state ket is 10). We should mention that in the following we will be rather loose with our state definitions and bounce between the spatial or momentum domain wavefunction representations. Additionally, our problem will be entirely one- 51 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES dimensional, and we will denote operators with a hat (e.g. k is the momentum operator). Our time-dependent Hamiltonian is written as H(t). We consider again the simple rectangular step potential from the preceding discussions. In this case our Hamiltonian can be written as the sum of several parts H K+V +-F p2 - 2m (2.9) (WF + EF)u(-x) - exE(t) (2.10) In the above, K corresponds to the kinetic portion of the Hamiltonian, V corresponds to the potential component (note that to simplify later calculations, we have shifted V from our earlier Hamiltonian such that the vacuum level is set to an energy of zero), and F corresponds to the field component. Note that the field component is written in the length gauge with the dipole approximation 5 . Now denoting the time evolution operator associated with H(t) as U(t, to), we can write a simple expression for the time evolution of an initial state 1#) (see Appendix B) |V)(0)) = 1#( )) - (2.11) dt' U(t, t') F(t') #(t')) - In the above, the state J(t)) starts in the initial state 1#) at time t = to. Additionally, 1#(t)) denotes the time evolution of the state 1#(to)) in the absence of F (see Appendix B). For the photoemission problem we are considering, the wavefunction of this initial state is given by the O(x) expression we found in Eq. (2.2). We can then also easily find q(t)) by incorporating the time-dependence into O(x) in the absense of F. Incorporating this time-dependence into the wavefunction, we find 0(x, t) oc exp(-ax + iWFlh) (2.12) We are interested in excitations from this initial state to higher energy states that are not bound to the metal; we are interested in the emission of electrons. This excitation is represented by the evolution of 1#) in the presence of F to 10). To analyze the excitation of 1#) into these higher energy unbound states, we take the overlap of the time evolution of 1') with a family of such unbound final states that we denote 'Also, note that unlike our previous Hamiltonian, in Eq. (2.10), our time-dependent field now penetrates the metal (there is not a step-function multiplying the field component). This follows because, as we will see, we are only concerned with the x > 0 region, so omitting the step-function is unimportant. 52 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES as {IXa)} where a is some continuous or discrete label. This overlap gives martix elements describing the excitation AMa(t) (2.13) (Xa(t)#(t)) = -t dt' (Xa|I U (1, i') F(t') #(t')) (2.14) In the above, we have shifted the initial time such that to = -oc. Additionally, we have assumed the initial state is orthogonal to the family of excited states, i.e. (Xa|1) = 0. The matrix elements Ala describe the amplitude of the transition from the intial state 1#) to the unbound, excited state IXa); however, we are interested in transition rates or currents. We can define a transition or exctiation rate or current in the usual way 1 t-+oo t Pa = lim - Ma(t) 2 (2.15) In the above, Fa is the photoemission rate from the initial state 10) to the final, excited state IXa). We have now established a basic framework for considering photoemission, and thus far, all our developements have been exact. We now turn to approximate methods, in particular time-dependent perturbation theory, to provide us with an estimate for the time evolution operator U(t, t') in the above equations and point us towards an appropriate set of final states, { IXa) }. In the following, we look at this perturbation theory for two particular examples of photoemission under different approximations. In particular we consider multiphoton and strong-field photoemission. Multiphoton photoemission In the regime of multiphoton photoemission the essential approximation we make is that the field component of the Hamiltonian is small. We treat the field portion of the Hamiltonian as a perturbation. We can then rewrite our photoemission Hamiltonian in Eq. (2.10), as 53 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES H K-+V+F = (2.16) (WF + EF)U(-X) _ 2m Ho - + exE(t) (2.17) F (2.18) + V. Now treating F as a small quanity, we can Where we have defined Ho as K write a perturbative expansion for the evolution operator (see Appendix B) U(t, to) Uo(t, to) - i dt'Uo(t, t')F(t') (2.19) to dt' dt"Uo(t, t')F(t')Uo(t', t")F(t") + - In the above expression, we make use of the unperturbed time evolution operator Uo(t, to). This is the time evolution operator for the unperturbed Hamiltonian Ho. Now before proceeding we must define the form of the excitation field. Using a continuous-wave, monochromatic field for simplicity we can write F(t) = -exEo cos wt (2.20) With this field Hamiltonian, we now have a complete problem we can solve. However, we still have two decisions to make before we proceed. First, we must decide on a suitable set of final states to consider emission into, and second, we must decide how to truncate our expansion for the evolution operator in Eq. (2.19). The first decision is rather straightforward. Since we are considering the field portion of the Hamiltonian to be weak, we will just consider emission into eigenstates of the unperturbed Hamiltonian, Ho. We can call this family of eigenstates { #q)} where q is a continuous parameter denoting the momentum of the states. The initial wavefunction and a candidate final wavefunction are illustrated in Figure 2-3. The second decision actually makes itself. If we consider the actual expansion in Eq. (2.19) under the rotating wave approximation6 , we find that a single term dominates. This term is the n - 1 term where n is defined as the lowest term such that nhw - Eq where Eq is the energy of 10q). This term involves n - 1 integrations 6 For a more elaborate description of the various approximations that go into multiphoton pho- toemission calculations see Refs. [13, 15]. 54 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES 1210- 2- -EF -2 -4 -0.5 0 0.5 1 1.5 2 xi (ii) Figure 2-3: Multiphoton photoemission. The rectangular step potential is illustrated in black. We see it wiggles only a small amount in response to the relatively weak field E(t) (see dashed). The real part of the initial wavefunction #(x, t) is drawn in red, and the real part of a potential final state (that is also a eigenstate of the unperturbed step potential) is drawn in blue. This state has an energy of 3 eV above the drawn vacuum level (both wavefunctions are numerically calculated). and accordingly the resulting matrix element is proportional to E01. Making use of this term to then calculate the total photoemission rate, we find that fMP oc0 (2.21) This general form the multiphoton photoemission rate, rMP, is exactly of the form we described in the previous chapter. Note that in deriving this form, we relied on the assumption that the field component of the Hamiltonian is small relative to the potential and the kinetic components. When this assumption breaks down our above expression will fail. We will explore this regime in the following. Strong-field photoemission As we discussed in the previous chapter, in the strong-field regime the field strength becomes such that the characteristic energy associated with the field is stronger than the binding potential itself. In this regime, we must shift the approximations made in the multiphoton case. In the multiphoton case we treated the field as weak relative to the potential. Here we treat the potential as weak relative to the field. We can then split our Hamiltonian as 55 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES H = = K+F+V (ex 2m = '4 (2.22) E(t)) (2.23) - (WF + EF)U(-X) V HF (2.24) Where we have defined HF as the 'free-field' Hamiltonian K + F. Now treating V as a small quanity, we can write a perturbative expansion for the evolution operator U(t, to) = UF(t, 0o) - I hto dt' - (2.25) dt'UF(t, t)V dt"UF (t, t')VUF(t + ..- In the above, we use the evolution operator UF(t, to). This is the evolution operator associated with the free-field Hamiltonian, HF, only. The above perturbative expansion is very interesting. We can diagrammatically interpret each term as shown in Figure 2-4. 1 2 + + 0 Figure 2-4: Strong-field perturbation theory. The terms in Eq. (2.25) can be interpreted via these simple diagrams. In Figure 2-4 we see each term in the expansion corresponds to an interaction, or scattering event, with the binding potential. The zeroth order term corresponds to no interaction with the potential, V; the first order term corresponds to a single interaction; and the second order term corresponds to two interactions. Here we are interested in only the total current, so we make an approximation and only consider the direct electrons i.e. we only consider the zeroth order term (more detailed analysis shows that the higher order terms are primarily of interest in characterizing the energy spectrum of the emitted electrons [7]). In other words, we make the approximation 56 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES U (t, tO) ~_ UF (t, tO) (2.26) We totally ignore the binding potential, and only treat the field component of the Hamiltonian in the evolution operator. The binding potential only plays a role in setting the initial state. Following Eq. (2.11), we can then write an expression for our final state as =|(t)) q5t)- t ]dt'UF-(t, t')F(t') |5(t')) (2.27) Additionally, like in the multiphoton case we must choose a final set of states to consider emission into. Since we are assuming the field is very strong compared to the potential, we want to choose our family of final states to be the exact eigenstates of the HF Hamiltonian. These eigenstates of the free-field Hamiltonian are known as Volkov waves (see Appendix C), and in the length gauge, we can write the Volkov wave as q = In the above, the ket Iq q + eA(t)) exp(-iS(t)/h) (2.28) + eA(t)) represents the free electron state with momentum q + eA(t), i.e. the wavefunction of this state is exp(i(q + eA(t))x/h). Additionally, S(t) denotes the is defined as ft dt'(q + eA(t')) 2 /2m. In Figure 2-5, a length gauge Volkov wave is illustrated showing the basic mechanism of our strong-field perturbation theory calculation. Using these length gauge Volkov waves as our set of final states and inserting them into the expression for our matrix element, we find (t) / = - f dt' (" (t) UF(t, t')F(t') |#(t')) dt' K4' (t')| F(t') |#(t')) dt' (q + eA (t')I exF(t') |#(t')) exp(iS(t')/h) (2.29) (2.30) (2.31) In the above we have noted that UF is the evolution operator for the Volkov waves, and we have re-labeled our matrix element as Mq denoting emission into the Volkov state with momentum q. Unlike the photoemission case, it is not directly visible what the general form of 57 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES 12- --- -- --- -- --- -- 10 4E 0 -0.5 = 10 V/1111 -EF 0 0.5 1 1.5 2 .r (iiiii) Figure 2-5: Strong-field photoemission. The rectangular step potential is illustrated in black. We see it wiggles dramatically with the strong field E(t) with Eo = 10 V/nm (see dashed sketch). The real part of the initial wavefunction O(x) is drawn in red (numerically calculated), and the real part of a potential final state (that is a length gauge Volkov wave) is drawn in blue. This state has an energy of 3 eV above the drawn vacuum level and an additional pondermotive energy of 1.8 eV. this matrix element or the resulting emission rate I'SF will be. In the following we will calculate numerically the above matrix element and develop an analytic approximation to formulate a closed form expression for photoemission in the strong-field regime. 2.2 Strong-field photoemission Having established a basic framework and intuition for photoemission calculations, we now proceed to calculate photoemission currents in the strong-field regime. In the following, we proceed along the lines outlined above and calculate the matrix element and emission rate for strong-field photoemission assuming excitation via an ultrafast optical pulse and a continuous-wave, monochromatic excitation. However, before describing these calculations, let us first consider what we expect. We will be looking at emission current versus optical excitation field. As we have described, we expect that at some critical field strength the photoemission current will depart from the multiphoton regime and eneter the strong-field regime. We expect this critical field to be associated with a Keldysh parameter of around one. In 58 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES other words, when the tunneling time shrinks below the cycle time, that is when the optically driven tunneling current begins to dominate, we expect a departure from the multiphoton regime. Therefore, above the multiphoton regime we expect a current versus field scaling comparable to that for the field emission case. Therefore we expect the photoemission current to resemble the behavior of the Fowler-Nordheim equation. This is illustrated in Figure 2-6. 104 102 -Ivacuum 100P 10-21 4-J 10 U 10 C: iacuum 0 108 U 10~ 7F. 1012 101 100 101 Figure 2-6: Multiphoton and tunneling emission. At low fields (high -y), we expect the photoemission current to resemble the multiphoton scaling i.e. oc E02 (drawn in red). Above a critical field (-y 1) and for low -y, we expect the photoemission current scaling to resemble the Fowler-Nordheim equation (drawn in black). The parameters used above are for gold being illuminated by light with a wavelength of 1.2 4m. 2.2.1 Ultrafast optical pulse emission Let us first consider the strong-field photoemission from an ultrafast laser pulse. The laser pulse can have an arbitrary shape, E(t), as our methods will rely on numerical calculation. Let us consider the matrix element of interest 59 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES - Mq(t) ft dt'(q+eA(t')|exF(t')|#(t'))exp(iS(t')/h) = h - dx dt' exp(i(q + eA(t'))x/h)exF(t')#(x) exp(iS(t')) (2.33) dx dt'+a (exp(i(q + e A(t'))x/h)) q(x) exp(iS(t')) Where in the above we have used dence of 10(t)). (2.32) 5(I) (2.34) = (S(t) + WFi)/h to remove the time depen- Reordering the above integration and inserting the expression for Oo(x), we find Mq (t) dt' exp(i(t')) - - j t dt'exp(iS(t'))( eFt) _Q dx exp(-zx - i(q + eA(t'))x/h) (2.35) (q +eA (t')) +a) This matrix element can then be numerically calculated. Figure 2-7. 2 The results are shown in From Figure 2-7, we see that the strong-field photoemission current' closely resembles our expectations. At low fields it follows the multiphoton scaling, and at high fields it traces the tunneling emission curve. Note that additionally in Figure 2-7 we include an analytical emission rate that we will calculate in the next section for a continuous-wave excitation. The current for the ultrafast pulse very closely resembles this monochromatic calculation. 2.2.2 Continuous-wave emission For the case of continuous wave emission, an analytical emission rate can be derived as we us a far less general form of the electric field. Here we assume E(t) = Eo cos(wt) A(t) =- sin(wt) (2.36) With this simple field we can write an explicit form of the Volkov wavefunction by carrying out the integration in the S(t) term. We find 'It should be noted that in the short pulse scenario the matrix element leads directly to the actual emission rate as we assume each pulse arrives at some fixed interval, and therefore, the total integration over all time of this matrix element corresponds to the emission probability for that interval and is accordingly proportional to the actual emission current. 60 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES 10 cw (analaytical) Ac= 1.2 gm, r =9.5fs 102 10 0, 100 10 U 10- I 10 1010.1 10-12I I 10o1 10-1 100 Figure 2-7: Strong-field photoemission with an ultrafast pulse. The photoemission current is plotted for an ultrafast pulse with a central wavelength A, = 1.2 pm and a pulse duration T = 9.5 fs (WF = 5.1 eV). The pulse is of a cos 2 shape. Additionally, the photoemission rate for the continuous wave case with a wavelength A = 1.2 pm is plotted for comparison. S(t) = = dt' q2 \2m - 2m + e 2 E2 )t 4mw 2 J - sinwt') W + qeE0 mw 2 (2.37) e 2 E2 cos wt - 8mw 3 sin 2wt (2.38) We can then write the Volkov wavefunction with momentum q in the length gauge as 0"(x,t) = q exp + (i h mW 2 eEo -sinwt Cos Wt - q2 )W(772m x- 8mw 3 + e2 ES 4mw 2 t sin 2wt With this expression for the Volkov waves, we can write our matrix element as 61 (2.39) CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES Mq (t) dt' exp(iS(t')) (q + eA(t') I eEo cos wt 1#) = j = dt'exp i(t')+ _= +UP+WF h (2.40) ) x 2m L,(q~-io"'(2.41) In the above we have again used S(t) = (S(t)+WFt)/h to remove the time dependence of 1#(t)), and in the second line we have expanded the matrix element into a Fourier series with Fourier coefficients L,(q). These coefficients are defined as L,(q) 9 = 27 2ir/w dt' (q + eA(t')I exEo cos wt'|#) x 0 exp iwnt' + h- , e 2 E02 w') cos wt mrjw2 ' 8mIW3 sin 2L t , qe Eo (2.42) From the simple form of Aq(t), we can massage the total photoemission rate into the familiar form ,q |Ln(q)126 X + Up + WF - nhW (2.43) n(2 In the above, we see that to calculate the total photoemission rate, we must find Ln(q). Before proceeding to this calculation, we should briefly review the physics contained in Eq. (2.43). Firstly, the general form of this equation looks familiar. It resembles Fermi's Golden Rule. The L,(q) function resembles the perturbation matrix element in Fermi's Golden Rule, and it is followed by a delta-function enforcing energy conservation. To obtain the total emission rate, we sum over all the possible multiphoton transitions and final state momenta that conserve energy. An interesting point to note is that using the free-field, Volkov states as our final states has resulted in the ponderomotive potential appearing in the delta-function. So, to make a transition from our initial state to a final Volkov state, we must not only provide the energy to surmount the binding potential and reach the kinetic energy of the free-field state, but we also must provide the pondermotive energy of the Volkov state in the oscillating field (recall our previous discussion and Figure 2-5). We now proceed with our calculation of Ln(q) in two alternative ways. We can 62 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES take a numerical approach or we can analytically estimate these Fouriere coefficients via a saddle-point analysis. Before proceeding with both of these approaches, let us manipulate L,(q) to a slightly simpler form. First, we can use a similar trick as we used in Eq. (2.34), and we can simplify the spatial matrix element in L,(q) by re-writing it as a derivative (q + eA(t')I ex E0 coswt' \#) dx exp = J ( - i(q + eA(t'))x/h) exE0 cos(wt')#(x) dx(-ih) 0 (exp (- i(q + eA(t'))x/h))#(x) (2.44) (2.45) Inserting this new form of the spatial matrix element into our expression for Ls(q) in Eq. (2.42), we can then integrate by parts and find a simplified form for the Fourier coefficient as given by L,(q) oc dO(iq- i x exp i (n sin0 - a) +qe q+ osE0 0mhw 2 sin 2)) e2 E 2 (2.46) 8hmw 3 In the above, we have made the substitution 0 = wt', and a = V2mWF/h as before. With this simplified form, we can now easily numerically calculate L,(q) (note a similar form for L,(q) appears in Refs. [31, 32]). Summing the different L"(q) Fourier components and enforcing the energy conservation condition in the 6-function of Eq. (2.43), we can then find an expression for the total photoemission rate. This rate is plotted in Figure 2-8. In Figure 2-8, we see some interesting behavior in the total photoemission rate. Step like features emerge in the emission rate scaling. These features are 'channel closings', and they arise as a particular multiphoton channel closes. From the energy conservation condition, we know that nhw = q2 /2m+ Up + WF. As the field increases so Up increases. When n < (Up + WF)/hw an n-photon transistion can no longer provide the minimum energy to excite an electron, and this n-photon channel closes. This is the origin of these step-like features. This interplay of different n-photon channels also explains the roll-off in the emission rate current as the field increases and we move into the strong-field, tunneling regime. 63 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES 10 cw (analaytical) 102 -- cw (numerical) 100 10-2 4-J 104 U 0-6 10 channel closings 10-0 10-12 101 100 10- y Figure 2-8: Strong-field photoemission with continuous-wave excitation. The photoemission current is plotted for a continuous-wave excitation at a central wavelength of A = 1.2 pm. As before WF = 5.1 eV. The numerical calculation is plotted in pink and the analytical result is drawn in blue. Analytical emission rate We can calculate an analytical form of the total photoemission rate by approximating L,(q) via a saddle-point analysis. The general form of L,(q) can be estimated by a saddle-point analysis as follows Ln(q) = /2 g(9)eS(6 ) x g(Oi)eS) (2.47) i5"(Oi) Where in the above the Oi's are the saddle-points, and we have encapsulated the major components of Ln(q) in the functions g(9) and S(O). For reference, S(9) is S(o) = no + eq E0 2Cos 0 - 2E e2 EW sin 20 (2.48) When this term is sufficiently rapidly varying, a saddle-point analysis is reasonable. Therefore, for large fields, i.e. large E0 , we can expect our saddle-point approximation 64 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES to be valid. From the above we can calculate the saddle-points, and we find they can approximately be written as ~i sinh-'-y + VI 0- ~F + i sinh-1 + y2 (2 - 1 1/+, q + mz) + 2(1+ -i + ( 2 y2)3/2 (-y 2(1+ (2Vmowz q(2.49) nz) (2 (2.49 ( _2)3/2 (2 ( 2 .5 0 ) 0+ /m__z Note that in the calculation of the above saddle-points the Keldysh parameter, -1 w V2mWF/eEo emerges naturally. With these saddle-points we can then approximate the magnitude of our Fourier coefficients )- ' (W )WE Ln(q) (2.51) 12 ) 2 hw #++ /I+2 -1+2 Finally, using these coefficients we can estimate the sum over different multiphoton orders as an integral and calculate a complete emission rate. In other words, we can estimate (2.52) F pSF JNmi n In the above FSF is the photoemission rate associated with the n-photon transition, and Nmin gives the minimum number of photons necessary at a speficied field. Carrying out the above integration, we find -y pSF 2 1 +-y sinh-' y - 1 x exp 2 F (_hw ((I + 2 ) simh- 2-y V 2, (2.53) ( 7 exp 2n(sinh-11 - The above total photoemission rate corresponds to the curve drawn in Figures 2-7 and 2-8 (note that similar rates have been derived previously; see Refs. [18, 33]). It is interesting to note that the Keldysh parameter appears naturally in this rate as it does in the saddle-points. Additionally, from the plots in Figures 2-7 and 2-8, we see see that the above photoemission rate agrees well with the expected emission rates in the multiphoton and strong-field regimes. 65 At first glance, it might seem CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES surprising that this rate agrees with the multiphoton one as we have neglected the potential. However, when we calculate the multiphoton emission rate the excited states very closely resemble entirely free-states. In other words, the potential plays virtually no role in the multiphoton case aside from determining the initial state. Additionally, it might seem somewhat surprising that in the tunneling regime our total photoemission rate agrees asymptotically with the Fowler-Nordheim equation since here we are assuming emission from just a single level, the Fermi level, while for the Fowler-Nordheim equation we integrated over all initial energies. It is interesting that these emission rates still agree; however, it is worthwhile to note that although we only consider a single initial state in the strong-field photoemission case above, we integrate over all final momenta. This parallel between the strong-field photoemission rate and the Fowler-Nordheim equation merits further investigation. We should additionally make some mention of the characteristic roll-off we observe in the photoemission current in Figures 2-7 and 2-8. As we previously discussed, there is a channel closing phenomena occurring as we increase the field strength. As we move to higher and higher fields, higher and higher photon orders contribute and close. The contributions from each of these orders grows smaller and only the top of the transition contributes. This can be seen by looking at each of the L,(q) terms. This behavior is responsible for the characteristic current roll-off. 2.2.3 Alternative emission rate formulations In the preceding, we have discussed numerical and analytical calculations of the strong-field photoemission rate for utlrafast optical pulse excitation and continuouswave, monochromatic illumination. We have found that under both of these conditions the emission rate roughly follows a simple analytical form derived in the above and connects the multiphoton and tunneling regimes of emission. Before moving forward to discuss the time-dependence of the photoemission current in the strong-field regime. It is worth mentioning two other scenarios of relevance for strong-field photoemission calculations. The first scenario is when field penetration into the emitting metal is substantial. In this case the general behavior of the emission rate is altered. The photoemission tends to roll-off more rapidly than our derived rates. This model has been pursued previously and can be calculated numerically [31]. The second scenario worth mentioning is when there is a fixed limit to the minimum acceptable kinetic energy of the emitted electrons. This scenario might arise when image charge or space charge effects restrict the emission. To calculate the strong-field photoe- 66 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES mission rate in this case, we can use our expressions for L,(q), but only consider contributions with q > q . It can then be seen that at low fields the emission rate scales at a steeper rate and rolls-off at higher fields at a more rapid rate. The overall photoemission rate more closely resembles the tunneling emission rate. As it turns out this model seems to best agree with our experimentally measured photoemission traces; however, our development of this model is still in its early stages, so we postpone further discussion. 2.2.4 Time-dependent emission Thus far we have only considered average photoemission rates in the strong-field regime; here we consider the actual time-dependence of strong-field photoemission. We have repeatedly stressed that the strong-field photoemission regime begins when 7 - 1, and when the optically-driven tunneling current becomes substantial. reiterate, -y To 1 means that the metal surface's potential barrier is collapsed for a sufficiently long duration for a sizable amount of electrical current to be emitted via tunneling, i.e. -s < rcyc. The key point to note is that this electrical tunneling current is emitted only when the barrier is dramatically distorted, and considering that this distortion is most dramatic near the peak of the optical field, we must have electrical bursts being emitted that are sub-optical cycle in duration. In other words, in this tunneling regime, we can produce electrical bursts that are significantly shorter in duration than the optical pulse or even than an optical cycle. Considering typical optical cycle times are on the order of femtoseconds, we likely can produce attosecond bursts of electrons via strong-field photoemission. The time-dependence of strong-field photoemission and the emission of sub-optical cycle electron bursts are illustrated in Figure 2-9. Here, we show the solution to the time-dependent Schr6dinger equation' (TDSE) for our standard rectangular step potential illuminated by an oscillating light field with a wavelength of A = 1.2 /Im. The height of the step is the usual value for gold, WF= 5.1 eV. Additionally, the strength of the optical field is E0 = 30 V/nm (this field strength is typical of our experiments in Chapter 4 and leads to a Keldysh parameter value of 'y = 0.4). The TDSE solution in Figure 2-9 confirms our intuition. We see the electrical current is emitted in a sub-optical cycle burst with a full-width-at-half-maximum of ~ 860 as (optical cycle time Tcyc = 4 fs at A = 1.2 Aim). This same solution to the TDSE is 8 The TDSE was solved for here using a custom TDSE solver built to handle unbounded domains by way of discrete transparent boundary conditions (DTBCs) [34, 35]. 67 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES W--% Optical field (A = 1.2 gm) -20 0.4 - TDSE solution -- Quasi-static solution - 15 10 5 0.3 I - 0 -5 0.2- -0.5 4a, 0 x (nmii) 0.5 1 0.1 0 (13 -0.11. -4 -3 -2 -1 1 0 2 3 4 time (fs) Figure 2-9: Strong-field photoemission in the time domain. The pink shows the electric field that drives photoemission from a gold surface with WF = 5.1 eV. The field has strength Eo = 30 V/nm and wavelength A = 1.2 ym. The blue shows the probability current as found via numerical solution of the TDSE. The dashed black shows the quasi-static tunneling current. The peaks of these currents are shifted from that of the field as they are calculated a short distance from the surface. Additionally, the inset shows the potential model for the simulation (note that the potential is truncated ~ 0.5 nm from the surface for simplicity in caculation). plotted again in Figure 2-10. In Figure 2-10, however, the wavefunction amplitude is displayed against space and time. Quasi-static emission rates Another intriguing characteristic of strong-field photoemission is readily visible in Figure 2-9. In addition to the TDSE solution, we also plot the quasi-static opticallydriven tunneling current. This quasi-static current is the current given by the static field emission tunneling formula when the optical field is inserted for the static field. For example, the quasi-static optically-driven tunneling current with the Fowler- Nordheim emission current is given by J (t) = J2 exp Etun 68 - tun E(t) (2.54) CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES -3 -2- (U E 0 1 3 4 -0.5 0 0.5 1 Figure 2-10: Strong-field photoemission in space and time. The wavefunction amplitude for the simple rectangular step potential modeled in Figure 2-9 is displayed in space and time. Note the surface is located at x = 0 nm. Also, note the large current spike near t = 0 fs. Where in the above, E(t) is the field of the optical pulse, and Et, is the usual critical tunneling field'. To reiterate, the quasi-static optically-driven tunneling current follows by simply inserting the optical field into the static field emission current form and then computing the current at each time step. The quasi-static optically-driven current model assumes that the tunneling dynamics through the barrier are so fast that the oscillating optical field looks effectively static throughout. This should correspond to the regime where y << 1. Also, note the similarity between the separation of time scales here and the separation of length scales in the WKB approximation used previously. In Figure 2-9 the quasistatic current comes from calculating numerically the solution to the time-independent Schr6dinger equation when the barrier is deflected by the optical field at each time step. Inspecting the quasi-static optically-driven current, we see that it very closely resembles the TDSE solution. This implies that for this tunneling emission process, the optical field can almost be treated as a static field. Additionally, it suggests that this tunneling emission process is sensitive to the actual optical field itself. After the 9 In the calculation of this critical field the electron mass comes into play. We use here and throughout the thesis the bare electron mass because we are interested in dynamics occurring at the femtosecond level. The effective mass is an intraband effect and does not respond at this speed [36]. 69 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES preceding build-up this may seem like an obvious point, however it is an important one. Recall that in the multiphoton picture, the physical mechanism for electron emission was based on energy absorption. Therefore, the number of emitted electrons only depended on the total number of photons or the total energy of the illuminating laser or laser pulse. However, in the strong-field regime the emitted electrical current depends sensitively on the actual electric field of the light pulse. 2.3 Carrier-envelope phase effects In the final section of this chapter we discuss carrier-envelope phase effects in strongfield photoemission. In our preceding discussion, we saw that strong-field photoe- mission is a field sensitive effect. We argued that strong-field photoemission cur- rents can be accurately approximated by quasi-static tunneling models. We saw that J(t) ~ Jtia(E(t)) where J(t) is the time-dependent strong-field photoemission current, Jt,,(-) is a field emission tunneling formula that typically takes a static electric field as its argument, and E(t) is the electric field of the exciting optical pulse (see Eq. (2.53)). Now let us consider the total charge, Q, photo-emitted during illumination by this optical pulse. We can write a simple expression for Q Q( ) = = fpledt Jtun (E (V, t)) dtJo jf pulse ( - EYJ) E ( , t) ) exp (-E (E t ( , t) (2.55) In the above, we have written the total emitted charge, Q(p) and the electric field of the pulse, E(o, t), as explicit functions of the carrier-envelope phase, 0. Additionally, on the right we have replaced Jtn (') with the quasi-static Fowler-Nordheim emission formula from Eq. (2.53). Lastly, the integration label is to indicate the integration is taken over the duration of the optical pulse. Inspection of Eq. (2.54) suggests several interesting properties of Q( O). Firstly, the exponential term in the tunneling current suggests this current will be very sensitive to the height and shapes of the peaks of the electric field' . We can think of this expoentially sensitive tunneling as a threshold effect. Only when a certain field value is reached will substantial current be produced, and therefore, as illustrated 0 A clear example of this sensitivity was provided in Figure 2-9. 70 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES in Figure 2-11, for short pulses variation in the carrier-envelope phase can lead to dramatic differences in the total emitted charge. As written, Et IK-- u Q is a function of W. -- -t N y q =zx/2 Vr t Figure 2-11: Threshold nature of CEP sensitivity. Two short pulses and two long pulses are illustrated with carrier-envelope phases W =r and -r/2. The shifted CEP strongly affects the peak field for the short pulses (the CEP dictates whether the peak field in this case is above or below Et.,), while the CEP shift has a minimal effect on the peak field of the longer pulses. An interesting property of the strong-field emission current is that it depends on the direction of the field. Since it is a tunneling-like current the field must deflect the barrier downwards for emission, so only one field direction will emit from a surface (see for example Figure 2-9). In our experiments however, we will emit from different structures that allow for not only this one-sided emission but also two-sided emission, in which both field directions emit. We denote the charge emitted in the one-sided emission case as QT and that for the two-sided emission case as QR (the reason for this nomenclature will be clarified in Chapter 4). More specifically we define these two charges as QT&O) = Ipulse dt Jun (E - ( , t)) and 71 QR(p) = dtJtun(E(p, t)) (2.56) CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES Where in the above, E-(o, t) refers to the optical field that consists of only the negative valued part of the total optical pulse E(o, t). Similarly let us define E+(p, t) as only the positive valued part of the total optical pulse. Since E(p, t) = E(p + 27r, t), we expect QT(p) and QR(O) to be periodic with period 2-F. However, also note that QRP) = JusedtJtun(E(ot)) ju=se dt J.(E- J=use dt (Jun(E-(sp, t)) = (2.57) (p, t) + E+(so, t)) (2.58) + Jun (E+(W, t))) ulse dt (Jun(E-(o, t)) + Jtun(E- (p + 7, t))) QT((P)+QT(O+7) (2.59) (2.60) The transition from Eq. (2.56) to Eq. (2.57) follows from the behavior of the tunneling current in the general exponential form (the dominant current contributions come from field peaks and zero field produces zero current). From the above development we see then that QR(W) is in fact periodic with period r. The Fourier series expansion of QT (periodic with period 27) contains terms of the form exp(ina); however, the Fourier series expansion of QR (periodic with period r) contains terms of the form exp(i2no). In fact, we see that the expansion coefficients for QR are exactly twice those for the even harmonic of QT. This behavior and the basic model for the CEP sensitivity are demonstrated in Figure 2-12 for a 9.5 fs cos2 shaped optical pulse with a center wavelength of 1.2pm and in Figure 2-13 for the actual measured pulse used in our experiments in Chapter 4. From Figure 2-12 and 2-13, we see that our simple model predicts a carrierenvelope phase modulation depth of a few parts in a thousand. Additionally, our basic considerations of the shape and behaviors of the total emitted charge are wellfounded. We will elaborate on our model and compare it to our measurements in Chapter 4. 72 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES 1-sided 30, 30 20- 20 10, 10 'k./I A v 0 -10 A A11C.", v 0 -10 -20 -20 -30 -30 -1 5 -10 -5 A 2-sided 0 5 10 5 -1 15 -10 -5 t(fs) 0 t(fi.) 5 10 15 1 0.999 0.999 0.999 0.9 0.9985 0.9985 0.998 0.998 0.9975 0.9975 x 1000 Z- 0 0.5 1 V.Vv 1.5 0 0.5 1 ,P/7[ 1.5 1P/ 7 10 0 10* 1-sided 0 2sided ti 10 10 0 -0- - 10 2 3 4 5 fczo harmonic Figure 2-12: CEP model for a simple pulse. The top plots show a simple 9.5 fs cos 2 shaped laser pulse (red) and the resulting quasi-static emission current (Fowler-Nordheim) for the one- and two-sided emission cases. The middle plots show the emitted charge as a function of the CEP (note the two-sided charge has been magnified by a factor of 10'). The bottom plot shows the Fourier series coefficients for the emitted charge. 73 CHAPTER 2. THEORY OF PHOTOEMISSION FROM SOLID SURFACES 1-sided i 30 2-sided 30 20 20 101 10 0 S0 0 'VI -10 A I -10 -20 -20 0 -0 50 100 -5 t(fs) - 1 I 0.9995. 0.9995 0.9990 0.999 0.9985 0.9985 0.996 0.998 Z -N. 0.9975 0.997 L ) 100 50 t (fs) x 10 0.9975 0.997 . 0.9985 0 0.5 1 1.5 0 0.5 1 ,P/7 1.5 IP/7 105 * 1-sided 0 2-sided N 10 *-.--..--....- I ........... .... .......... 10 10 10 212 0 1 2 fcEO 3 4 5 harmonic Figure 2-13: CEP model for a real pulse. The top plots show the measured 9.5 fs, 1.2 pm wavelength laser pulse used in our experiments (red) and the resulting quasi-static emission current (Fowler-Nordheim) for the one- and twosided emission cases. The middle plots show the emitted charge as a function of the CEP (note the two-sided charge has been magnified by a factor of 10). The bottom plot shows the Fourier series coefficients for the emitted charge. 74 Chapter 3 Plasmonic nanoparticles and optical resonators In this chapter we discuss the fundamentals of plasmonic nanoparticle resonators. As mentioned in the previous chapter, we will be building strong-field photo-emitting devices with such plasmonic nanoparticles; so, it will be critical to have a conceptual understanding and fundamental model for the optical behaviors of these tiny nanoresonators'. Our focus in this chapter will center on constructing a simple circuit model that can accurately describe and predict the response of plasmonic nanoparticles when excited by femtosecond optical pulses. We begin with a brief, intuitive review of surface plasmons and build a conceptual physical picture of the operation of nanoparticle resonators. Next, we sketch a simple, second-order circuit model that captures the essential behaviors and optical properties of the nanoparticles. The circuit model is analyzed in the frequency and time domains, and the spectral and temporal response of our nano-resonators to femtosecond optical pulses is discussed. Lastly, we mention some details on our nanoparticle fabrication procedure, describe the overall layout of our nanoparticle emitter chips, and present fits of our nanoparticle properties to the simple, second-order circuit model. 3.1 Surface Plasmons and nanoparticle resonators Certain material surfaces can support confined electromagnetic modes; these modes are known as surface plasmon polaritons or simply surface plasmons. Over the past 'We should mention that in this chapter and the following we will interchangeably use the terms nanoparticle, nanoparticle resonator, and nano-resonator. Additionally, these terms will often be preceded by the descriptor 'plasmonic'. 75 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS decades numerous exciting applications involving these confined surface electromagnetic modes have emerged, and there are many excellent and complete references outlining their origins and behaviors [37, 38, 39]. Here, we provide just a brief, intuitive review of surface plasmons, highlighting several key properties of interest for our purposes, and we describe how nanoparticles can act as tiny optical resonators for these modes. Surface plasmons result from longitudinal oscillations in a material surface's freeelectrons. Such oscillations are illustrated in Figure 3-la. Under particular conditions, an optical wave can excite these longitudinal oscillations, and the wavelength of the oscillations, i.e. the surface plasmon polariton wavelength, Aspp, is generally in the optical domain, i.e. hundreds of nanometers. These longitudinal charge oscillations produce electric and magnetic fields as sketched in Figure 3-2b. Since the charge oscillations occur largely near the material surface, these fields are confined in near proximity to the surface. A material surface can support these charge oscillations and resulting surface plasmon modes when the real part of the dielectric function changes sign across the surface boundary. Therefore, surface plasmons commonly exist at metal-dielectric interfaces: the dielectric has a positive real part to its dielectric function, i.e. Ed > 0, and the metal has a negative real part to its dielectric function, i.e. Em < 0 (illustrated in Figure 3-la). Let us now consider a metallic, rod-shaped nanoparticle on a dielectric substrate. Since such a nanoparticle is composed of metal-dielectric interfaces on all sides, we expect the particle to support surface plasmonic, confined electromagnetic modes. These modes can propagate up and down the body of the rod. Additionally, at the truncated ends of the rod, we expect these modes will reflect back and forth. This basic picture of the optical behavior of the metallic nano-rod is analogous to that of the familiar optical cavity (see Figure 3-2). The fundamental operation of an optical cavity is reiterated in Figure 3-2a. The cavity consists of two mirrors that confine free-space electromagnetic modes to propagate in the intermediate space. These modes reflect back and forth off these mirrors and circulate in the cavity. When properly tuned, an external optical source can feed energy into these modes and buildup a tremendous amount of optical energy in the cavity (as mentioned in Chapter 1). The rod-shaped nanoparticle behaves in much the same way. An optical source can excite plasmonic modes that are confined to the nano-rod's surface (the transverse optical intensity profile for such a mode is shown in the inset of Figure 3-2b). These modes propagate up and down the body of the nano-rod, reflect from the nano-rod's end-caps, and, when fed by a properly tuned optical source, build-up a large amount 76 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS _-__-_-_-_-_- ------ AS C, < 0 - - - + - - - -+ + dielectric P metal -X b Aspp1 Figure 3-1: Surface plasmons on a metal surface. a. At a metal-dielectric interface (dielectric above the dashed line and metal below the dashed line), longitudinal surface charge oscillations can be excited. These charge oscillations are the origin of the surface plasmon polariton modes and have wavelength Aspp. b. The electric and magnetic fields produced from these longitudinal surface charge oscillations. Since the fields originate from the surface charge oscillations, they are largely confined to a region near the metal's surface (see green sketch of mode profile). (Images in a. and b. were borrowed without permission from [40]). of optical energy in such a plasmonic nanoparticle optical resonator. This analogy between the familiar optical cavity and the nanoparticle resonators is a powerful one. The optical cavity is characterized by two basic parameters: the cavity's resonant wavelength or frequency and the cavity's confinement time or quality. The resonant wavelength defines what particular wavelengths will excite the resonant modes of the cavity. The confinement time or quality define how long these modes will resonate before decaying and gives a measure of what level of optical energy can be built-up in the cavity. Similarly, we expect the nanoparticle resonators to be defined by a resonant wavelength, i.e. the wavelength at which the resonant nano-plasmonic modes will be excited, and a damping time, i.e. a timescale over which these modes will decay. 77 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS a Optical cavity b Plasmonic nanoparticle resonator Nano rods Nano-triangles Figure 3-2: Optical cavities and plasmonic nanoparticle resonators. a. The fundamental operation of a familiar optical cavity. Between the cavity mirrors an optical pulse circulates. Energy is fed into the intra-cavity pulse by an external pulse train. b. Plasmonic nanoparticle resonators, for example nanorods or nano-triangles, are analogous to the familiar optical cavity. They support surface plasmonic electromagnetic modes that can propagate up and down the nanoparticles. Inset shows the transverse intensity profile of such a mode on a nano-rod resonator with a circular cross-section and a diameter of 20 nm (image borrowed from Ref. [41] without permission). Although powerful, the nanoparticle resonator and optical cavity analogy is not exact. If we consider the confinement time of a reasonable quality enhancement cavity, we find it can take on values in the ps range. Feeding such a cavity with an optical pulse train with pulse spacing on the order of 10 ns (recall that typical repetition rates from mode-locked laser oscillators are on the order of 100 MHz), we expect hundreds of consecutive pulses to constructively interfere and add to each other inside the cavity. However, considering a nanoparticle optical resonator, as we will see, typical damping or confinement times are only on the order of 1-10 fs. Therefore the excited plasmonic mode on the nanoparticle produced by an incident laser pulse will long have damped out before the next excitation pulse arrives ~ 10 ns later. The buildup of optical energy in the nanoparticle resonator follows from a different physical picture. Energy is not built up in the plasmonic nanoparticle modes from consecutive excitation laser pulses, but from consecutive laser pulse cycles. When excited by a laser pulse, each cycle of the pulse launches a surface plasmonic electromagnetic 78 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS mode into the nanoparticle. The nanoparticle resonators are so short (lengths ~ 100 nm) that these excited modes can reflect and interfere with the modes excited by consecutive cycles of the pulse. Therefore, the nanoparticle optical resonators buildup optical energy in their surface plasmonic modes within a single optical excitation pulse2 . We expect from this process that the temporal shape of the excited field on the nanoparticle resonator will look substantially different from that of the exciting laser pulse. In the following section, we will construct a simple circuit model for these nanoparticle resonators that can accurately predict this temporal reshaping. 3.2 Circuit model for nanoparticle resonators Building on the intuitive understanding developed in the preceding section, here we seek to develop a quantitative model that can accurately predict behavior of plasmonic nanoparticles when excited by an optical pulse. Considering our preceding description of plasmonic nano-resonators, a reasonable route towards modeling these devices is to calculate the plasmonic modes supported by the nanoparticles, determine how these modes interact with the end-caps of the nano-resonators, and put these properties together to establish a model for the nano-resonator. This approach has been carried out by numerous researchers; however, it generally requires substantial numerical calculation. Additionally, numerous other approaches towards modeling plasmonic nano-resonators have been developed ranging from simple and intuitive spring-mass models [42] to sophisticated, entirely numerical approaches [41, 43]. In this section we will follow a more recent approach; we will concisely describe a simple circuit model that can accurately account for the nano-resonators spectral and temporal response to an optical pulse [40, 44, 45, 46]. We can model the plasmonic nano-resonators with a simple distributed element circuit model. For simplicity, let us consider the metallic nano-rods. Looking at a small section of the body of a nano-rod, the metallic rod and the optical excitation can be treated as an inductance in series with a resistance and an oscillating voltage source. The inductance corresponds to the Faraday and kinetic inductance of this small section; the resistance corresponds to the material and the radiation resistance of the small section; and the oscillating voltage source corresponds to the field of the 2 Note that the cartoon depiction of the circulating pulse along the nano-resonators in Figure 3-2b is actually inaccurate as it does not show this cycle to cycle interference. The cartoon in 3-2b was only to build the analogy between the familiar optical cavity and the nano-resonators; however, it fails to capture this subtlety. 79 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS optical excitation pulse on this small section of the nano-rod (here we disregard a distributive capacitance). The nano-rod is composed of many such small sections all in series. Looking at the Thevenin equivalent of this distributed element circuit, we find that we can replace this distributed model with a simple lumped element model consisting solely of an inductor in series with a resistor and an oscillating voltage source. The total inductance now corresponds to the total Faraday inductance and kinetic inductance of the metal nano-rod, the resistance to the total material and radiation resistance, and the voltage source to the total field applied across the rod. Additionally, at the end-caps of the nano-rod we place a capacitor to model charge accumulation at the nano-rod ends. The complete circuit model for the nano-rod resonator' is illustrated in Figure 3-3. a b Nano-rods Circuitmodel Vs Rrad + LK Cend Figure 3-3: Circuit model for plasmonic nanoparticle resonators. a. Image of nano-rod resonator and cartoon of basic optical cavity-like operation. b. Second-order RLC circuit model for nano-rod resonator. To extract the optical properties of the plasmonic nanoparticle from the circuit model, consider the voltage on the model's capacitor. The voltage on the capacitor is proportional to the charge on the capacitor, i.e. VC = Qend/Ced. Since the capacitor models charge accumulation at the nanoparticle's end-caps, the capacitor voltage is proportional to this end-cap charge Qend. This end-cap charge is relevant for two main reasons: firstly, the end-cap charge will dictate the dipole moment of the nanoparticle; secondly, the end-cap charge will determine the strength of the local electric field near the nano-resonator's end-caps. The importance of these two values will be illuminated as we consider our circuit model in the frequency and time domains. 3 Although we have motivated this circuit model by looking at a nano-rod resonator, we will use the same basic model for our nano-triangle resonators. 80 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS 3.2.1 Frequency domain - susceptibility and extinction Here we focus on the capacitor voltage in the frequency domain, Vc(w). This voltage is proportional to the end-cap charge, i.e. Vc(w) OC Qend. Additionally, since the nanorod is of a fixed length, 1,od, the dipole moment of the rod, prod(w), is also proportional to this end-cap charge, and accordingly, to the capacitor voltage, prod(w) Oc Vc(w). As we have mentioned, we will be fabricating arrays of nanoparticle emitters. If we consider an array of nano-rods, the polarization of the array, P(W), i.e. the dipole moment per unit volume of the array, must be proportional to prod(w). Combining all these proportionalities, we find P(w) = coX(w)E(w) cX Prod(W) Oc Vc(w) (3.1) Where in the above, X(w) is the susceptibility, and E(w) is the electric field of the optical excitation. Noting that from our model the laser voltage should be proportional to the optical excitation field, we can then note that x(w) c VC(W)/Vas(W). Solving for this transfer function from our simple second-order circuit we then find an expression for the susceptibility of the nanoparticle array x(W) C Vc(w) ZC = Vas(W) ZC+ZL +ZR 1 2 1 - W LCend + ZiwRCend 2 2 In the above, Zc, ZL, and ZR resistor respectively, and wo = w / (3.2) are the impedances for the capacitor, inductor, and 1//LCend and we have used L and R instead of the LK and T = L/R. Rrad. Note that in the above, The latter terms were used in the circuit model schematic to emphasize the dominant contributions to each circuit element. The inductance is dominantly composed of a kinetic inductance, and the resistance is primarily a radiation resistance. L and R in the above refer to the total inductance and resistance respectively; however, it is worth mentioning that since R ~ Rrad, the damping in the nano-resonators is primarily radiative. We will thus often refer to T as Trad. With a model for the susceptibility, we now will measure and fit the nanoparticle resonators extinction spectrum. The extinction spectrum is a commonly measured optical characteristic for plasmonic nanoparticle arrays and will allow us to fit the 81 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS parameters of our model. We define the optical extinction a(w) as exp(-a(w)) = T(w)/Tref(w) where T(w)/Tref(w) is the optical spectrum transmitted through the device array divided by the optical spectrum transmitted through the substrate, i.e. the reference transmission. The extinction a(w) can be related to x(w) through the imaginary part of the refractive index. From this emerges the well-known expression a(w) = CIm(X(w)). From this expression and our expression for x(w) in Eq. (3.2), we find a (W) oc w) - (W/)(3.3) w2 + (w 2 /r) The measurement of a nano-triangle array's extinction spectra along with a fit to the lineshape in Eq. (3.3) is presented in Figure 3-4. The agreement between measurement and fit is relatively good. We find for this particular nano-triangle array that the resonant wavelength is Are 1000 nm, and the damping time is rad= 5.2 fs. 1.2 Extinction -- - log T/T, f - measured model 1 0.8 ic 0.6 Ig 0.4 0.2 0 700 800 900 1000 1100 1200 1300 1400 wavelength (nm) Figure 3-4: Example extinction spectrum and fit. The blue curve represents the measured extinction spectrum for an array of nano-triangles with pitch 400 nm, altitude 200 nm and base 150 nm. The dashed red curve shows the fit via Eq. (3.3). 3.2.2 Time-domain ultrashort pulse broadening Here we will concentrate on the capacitor voltage in the time domain, Vc(t). This voltage is proportional to the end-cap charge, i.e. Vc(t) OC Qend(t). From our preceding discussions, we have seen that these nano-resonators resemble tiny optical 82 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS dipoles. We therefore expect the peak fields near our nano-resonators to occur right near the end-caps and for this peak field to be directly related to the end cap charge, i.e. Epl(t) OC Qend(t) oc Vc(t), where Ep,(t) refers to the peak nano-plasmonic optical field. Therefore, we expect that the time-domain behavior of the nano-plasmonic field will follow that of the capacitor voltage. Returning to our circuit model, the capacitor voltage obeys the familiar, second-order differential equation d2 Vc(t) 2 dt 1 dVc(t) + r dt +w!Vc(t) = W0Vias(t) OC E(t) (3.4) where E(t) in the above is the field of optical excitation pulse. Therefore, by solving the above equation with a specified optical driving pulse, we can estimate the temporal behavior of the localized plasmonic field around our nanoparticle resonators. An example of such a solution is provided in Figure 3-5. In this example an excitation laser pulse with the black envelope 4 and a central wavelength of 1.2 pm is input for Vlas. The blue pulse is the resulting envelope of the response Epi(t) Oc Vc(t). The . nanoparticle used in this example has a resonant wavelength of Ares = 1256 nm and a damping time of Trad = 7.4 fs 5 1 I AR,, = 125 6 nm 0.8 0.6 Trad I 14 . - 0.41 Excita tion pulse - Nano -res. pulse 0.2 I a -40 -30 -20 0 -10 10 20 30 40 time (fs) Figure 3-5: Ultrafast optical pulse broadening in a nanoparticle resonator. The resonator used has a resonant wavelength of 1256 nm and a damping time of 7.4 fs. The black trace shows the excitation pulse envelope (central wavelength of 1.2 pm). The blue trace shows the envelope of the response on the nanoparticle resonator. 'The black excitation pulse used here is an actually measured laser pulse that will be described in greater detail in Chapter 4. It is the pulse displayed in Figure 2-13. 'These numbers are from an actual fabricated nano-triangle array. 83 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS 3.3 Nanoparticle fabrication and characterization For the experiments that will be described in the following chapter, we fabricate a collection of different nanoparticle resonators. As described, the nanoparticles take on two main shapes: nano-rods and nano-triangles. The nanoparticles are fabricated on a 1 cm2 sapphire chip. The sapphire is coated in a 50 nm layer of indium tin oxide (ITO) that is patterned to separate the chip into emitters and collectors (to be discussed in Chapter 4). An overview of the chip architecture is shown in Figure 3-6. A total of eighteen different device arrays were fabricated. Of these arrays there were seven different nano-rod size arrays and nine different nano-triangle arrays. Extinction spectra for all the nano-rods are shown in Figure 3-7. Extinction spectra for all the nano-triangles are shown in Figure 3-8. Finally, a microscope image of the chip layout as well as a sketch of all the different resonances for the arrays is included in Figure 3-9. 500 nm Figure 3-6: Chip overview. a. Picture of the actual chip. b. Zoomed in microscope image of the arrays of devices. c. Zoom in of the purple region outlined in part b. d., and e. electron micrographs of the blue and red regions outlined in part c. 84 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS model - - - - measured 1 0.8 C S0.6 o.4 0.2 0 700 800 900 1000 1100 1200 1300 1400 wavelength (nm) Figure 3-7: Extinction spectra for the nano-rod devices. The blue traces are measurement and the red dashed traces are model fits according to Eq. (3.3). The dark blue trace is for the nano-rod with resonant wavelength 1041 nm. - model - - - measured 1 0.8 S0.6 0.4 0.2 700 800 900 1000 1100 1200 1300 wavelength (nm) Figure 3-8: Extinction spectra for the nano-triangle devices. The blue traces are measurement and the red dashed traces are model fits according to Eq. (3.3). The dark blue trace is for the nano-triangle with resonant wavelength 1059 nm. 85 1400 CHAPTER 3. PLASMONIC NANOPARTICLES AND OPTICAL RESONATORS Figure 3-9: Image and sketch of chip layout. a. Microscope image of set of eighteen fabricated device arrays. b. Sketch showing the resonant wavelengths of each array. The R and T labels indicate whether the array is a nano-rod array or a nano-triangle device array. 86 Chapter 4 Photoemission from plasmonic nanoparticles In the previous two chapters we discussed the theory behind photoemission in the multiphoton and strong-field regimes, and we described the basic properties and behaviors of plasmonic nanoparticles. In this chapter we put these ideas together and describe photoemission from plasmonic nanoparticle resonators. We begin by discussing the motivation for investigations into photoemission near nanostructures and by providing an overview of past as well as on-going work in this area. We next briefly describe our early experiments and sketch the experimental approach we follow in this work. Next, we provide some details regarding the various components of our experimental system: we discuss the femtosecond laser source, the laser pulse measurement system, the carrier-envelope phase stabilization technique, and the device alignment microscope. We then proceed to present our experimental results. First, we investigate basic scaling properties of the photoemission signal and demonstrate signatures of the strong-field regime. Next, we use the strong-field photoemission current to perform interferometric autocorrelations and characterize the nano-plasmonic, ultrafast optical field excited by the femtosecond laser pulse on the nanoparticles. Lastly, we demonstrate the carrier-envelope phase sensitivity of the photoemission signal and develop a simple model for predicting this carrier-envelope phase response. 4.1 Strong-fields near nanostructures As discussed in Chapter 1, over the past decade, photoemission, in particular strongfield photoemission, from nanostructures has garnered tremendous interest for its po87 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES tential scientific and technological impact. From a scientific perspective, the prospect of generating sub-optical cycle electron bursts or even attosecond electron packets (as we discussed in Chapter 2) suggests exciting possibilities in probing ultrafast phenomena near solid-surfaces at unprecedented temporal resolutions. For example, such ultrashort electron bursts might allow the probing of electron motion in solid-state surfaces and nanostructures as well as the probing of the ultrafast fields or plasmons excited near such surfaces [47]. From a technological standpoint, the prospect of switching electrical currents with the optical field of light might offer opportunities for novel opto-electronics or detectors such as on-chip carrier-envelope phase detectors [10, 12, 48, 49, 50]. Additionally, as we will discuss, there are exciting applications for strong-field photo-emitting nanostructures in electron-beam technologies as novel photo-cathodes. Central to the applications for strong-field photoemission outlined above are two fundamental optical properties of nanostructures: field-enhancement and localization. Nanostructures can offer field enhancement to an incident optical wave. This field enhancement generally arises from two phenomena: geometric focusing and resonance. The geometric focusing or geometric enhancement emerges from the nanostructure's lightning-rod-like behavior when illuminated with optical fields. Intuitively, at sharp corners and tips with nanometer-scale radii of curvature electric field lines will become very crowded as the field attempts to bend around the corner all the while remaining normal to the surface. This 'field-line crowding' results in a concentration of the optical energy and a resulting electric-field enhancement [51]. The physics is conceptually the same to the behavior of a lightning-rod. Additionally, this geometric enhancement is the same process that leads to localization. As described, the electric field-lines crowd at sharp corners and tips, and the optical energy becomes concentrated or localized. This localization or this concentrated spot of high electric-field can result in highly-localized photoemission. This highly-localized electron emission from the geometrically enhanced field near a sharp tip or corner of a nanostructure is of great technological interest for future photocathode technologies as it might serve as a very low-emittance virtual point-source of electrons [52, 53]. The second source of field-enhancement is resonance. As discussed in the previous chapter certain material surfaces can support confined electromagnetic modes that result from oscillations of the material's electrons and are seemingly bound to the material surface. As we discussed, metallic nanoparticles can act as resonators for these surface-plasmonic modes, and when fed by a properly tuned optical source, they can build up a tremendous optical energy and field. 88 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES In the following, we leverage the field-enhancement properties of nanostructrues, in particular plasmonic nanoparticle resonators, to achieve the necessary field strengths to explore some of the interesting strong-field photoemission phenomena described above. Before discussing our particular approach and results however, let us review some of the major results to date and some of the on-going work in the study of strong-field photoemission near nanostructures. 4.1.1 Previous results and ongoing work In studies of strong-field photoemission near nanostructures, there have been two major classes of nanostructures that have been used: nano-tips and plasmonic nanoparticles. These two basic geometries nicely follow the division laid out previously in our field-enhancement discussion, i.e. nano-tips are devices largely dominated by geo- metric enhancement effects and plasmonic nanoparticles are largely resonant devices. The big-picture approaches to strong-field photoemission experiments with these two device types are illustrated in Figure 4-la and b. The essential experimental concept is similar for both device types: a nano-tip or an array of plasmonic nanoparticles is mounted in a vacuum setting. The nano-tip or array is then illuminated with a femtosecond laser pulse, and the photo-emitted electrons are collected and analyzed. In the following, we will briefly describe some of the prior results and on-going work with each of these device types. Nano-tip emitters comprise sharp metallic nano-tapers with radii of curvature at the very tip of only a few nanometers. Coated atomic-force microscopy tips or other similarly sharp tips, commonly composed of tungsten or gold, are used in these experiments. As mentioned, these nano-tips show primarily a geometric, lightning-rod-like field-enhancement effect at the tip, and when illuminated by femtosecond laser pulses, photo-emit large, short bursts of electrons. Since the first experiments demonstrating femtosecond-laser triggered photoemission from nano-tips [54, 55, 56], there has been an explosion of experimental works in this area, with most investigations targeting the strong-field regime. Thus far there have been demonstrations of the roll-off in the current yield as the strong-field regime is approached [31, 12, 57] (discussed previously in Chapter 2); there have been measurements of the electron energy spectra of the emitted electrons showing re-scattering behavior[10, 11, 12, 23, 57, 58, 59, 60] 1; 'This electron re-scattering phenomena is a classic signature of the strong-field regime [7]. The essential concept is sub-optical cycle electrons are emitted from the metal surface, and after emission, wiggle in the nearby laser field. Some of these electrons will be redirected back towards the metal surface and scatter off the surface. These re-scatter electrons can pick up large amounts of energy 89 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES Single nano-tip emitters a Nanoparticle emitter arrays b fslaser pulse eectrons electron pulse d c 10 . -rod red 20 25 10 .2 1 - 0 5 Energ (W) 10 0 Cu-ff posat~on 5 10 15 Enwxy(ov) 4 10 16 0 10 Noemaked Nomtnakod co t rate (au.) cont rate (a.u.) Figure 4-1: Strong-field physics with nanostructures. a. Schematic of nanotip emitter operation. b. Basic layout for nanoparticle emitter experiments. c. Example data set showing carrier-envelope phase effects in the emitted electron's energy spectra from nano-tip emitters. d. Energy spectra showing large rescattered plateau of emitted electrons from nanoparticles. (illustrations and pictures in a-d borrowed from Refs. [10, 22] without permission). and there have been a number of works exploring carrier-envelope phase sensitivity in the emission process [10, 121. As discussed in Chapter 2, the field-sensitive nature of the strong-field emission process has excited researchers about the prospect of being able to detect carrier-envelope phase effects in strong-field photoemission currents. Detection of the carrier-envelope phase of ultrafast laser pulses (see discussion in Appendix A) is a classic problem in ultrafast optics, and a compact, chip-scale detector could be revolutionary. Additionally, carrier-envelope phase effects are of interest from a purely scientific perspective as such effects are a hallmark of true optical field-sensitivity. So far, carrier-envelope phase signatures have appeared in the energy spectra of electrons emitted from nano-tips [10] and more recently have been shown in the total emission current as well [12]; however although scientifically intriguing, thus far the overall strength of these effects has been relatively weak and not suitable for an effective carrier-envelope phase detector (see Figure 4-1c). from the laser field and have particular signatures in the emitted electron energy spectra. 90 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES Although also of great interest for strong-field photoemission, plasmonic nanoparticle emitters have received much less attention to date. These emitters frequently are composed of arrays of gold nanoparticles of spatial dimensions on the order of ten to a hundred nanometers patterned on a transparent substrate. These nanoparticles experience both resonant and geometric enhancement effects and, like nano-tips, photoemit large electrical currents when illuminated by femtosecond laser pulses. Although there have been fewer experimental investigations into these emitters, the emitted electron energy spectra has been studied and shown to demonstrate re-scattering effects characteristic of the strong-field regime [22] (see Figure 4-1d). Additionally, these emitters have attracted particular attention for futuristic photocathode applications as discussed previously [52, 53]. 4.2 Strong-fields on a chip Our approach to strong-field photoemission involves moving the experiments to a chip. As discussed in Chapter 1, strong-field physics generally involves complex laser amplifiers, large vacuum setups, and generally complex experimental machinery. Strongfield experiments with nanostructures are frequently simpler than other strong-field science investigations; the field-enhancement provided by the nanostructures often means complex laser amplifiers are unnecessary. The field from tightly focused laser pulses directly from an ultrafast, mode-locked oscillator are often sufficient to reach the strong-field regime. However, although simpler in this regard, strong-field experiments with nanostructures do require much of the other large, expensive experimental machinery of traditional strong-field physics, in particular vacuum setups. Our general concept at the start of this work was to remove the cost and complexity of these experimental setups by putting our nanostructure, our detectors, and our entire experiments on the surface of a micro-scale chip. With collecting electrodes and detectors only nanometers to tens of microns from our emitting nanostructures vacuum might not be required, and strong-field science experiments can be carried out under ambient conditions with tightly focused laser pulses directly from a modelocked, ultrafast laser oscillator. Such on-chip strong-field experiments are not only interesting from the perspective of a simplified experimental platform but also could provide the opportunity to make compact, novel opto-electronic devices and detectors that operate in the strong-field regime. In the following, we discuss some of our early attempts towards on-chip strongfield physics. Next, we extract valuable lessons from this early work and outline the 91 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES essential approach and device design we use in our on-chip strong-field experiments presented in the remainder of this chapter. Flattened nano-tips on a chip 4.2.1 Our initial work towards on-chip strong-field physics involved moving nano-tip emitters to a chip. The basic approach to these on-chip nano-tip emitters was to flatten to make a two-dimensional nano-tip emitter, on a chip with a of an nearby collector electrode. An illustration of the basic concept and an image the nano-tip, i.e. early device geometry are provided in Figure 4-2. Our flattened, two-dimensional tips were composed of a 30 nm thick layer of gold and showed a small ~ 10 nm radius of curvature near the tip apex. They were estimated to show similar geometric optical field-enhancements to the free-standing, three-dimensional nano-emitter tips used in many previous experiments [61]. Additionally, the collector electrodes were placed only around a hundred nanometers from the flattened nano-tips and small bias voltages were applied to them (on the order of a few volts). Although small, these bias voltages led to tremendous bias fields due to the small emitter-collector gap distance so close ~ 1 V/(100 nm) = 10 MV/m). The collector electrodes were placed to the emitters, only on the order of a hundred nanometers, because the devices were operated under ambient conditions. The mean-free path of a low-energy, few eV, electron in air is typically mf ~ 200-300 nm [62]. In order to ensure the ambient conditions would not affect our ability to collect the emitted electrons, the collector (EBIAs was placed within this mean-free path. a b v's TiS e Figure 4-2: Nano-tip emitter experiments on a chip. a. Conventional nano-tip emitter experimental arrangement (illustration borrowed from Ref. [10] without permission). b. Basic layout of one of our flattened on-chip nano-emitting tips. 92 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES The preliminary photoemission results from these flattened nano-tips showed only miniscule currents. The tips were illuminated with tightly-focused a 6 fs laser pulses with a central wavelength of A ~ 800 nm emerging from a home-built Ti:sapphire mode-locked oscillator 2 . The laser pulse were scanned in energy up to 5 nJ; however, only near negligible currents were observed, and these currents fluctuated and were unreliable. Additionally, at the higher pulse energies device damage was consistently an issue. The exact issues and reasons for this poor performance are not entirely understood; possible explanations include fabrication and electrical contact issues with the flattened nano-tips, backwards emission from the edges on the collector, among other effects. Investigating a set of these flattened nano-tip emitters, an interesting observation was made. The fabrication of the flattened nano-tips involved an initial electron beam lithography process to pattern the gold nano-tips which was subsequently followed by an optical lithography process to create large gold pads to electrically connect to the flattened nano-tips (see Figure 4-3a). When the edge of one of the large connecting gold pads was illuminated, we measured a relatively large photoemission current at the collector (see Figure 4-3a). Looking at the SEM image in Figure 4-3a, we see that the photolithographically defined pads have very rough edges. The photolithography was done hastily, and imperfect resist sidewalls coupled with the lift-off process led to the formation of the apparent roughness. This roughness takes the form of thin gold whiskers at the edges of these large gold pads. When illuminated with the femtosecond Ti:sapphire laser pulse, these whiskers show the same geometric field-enhancement that the nano-tips demonstrate, and accordingly they photo-emit electrons. The remarkable fact here is that the emitting whisker was tens of microns away from the collector electrode, yet despite this gap, many mean-free-paths in length, the electrons still reliably traversed the ambient conditions from the emitter to the collector (see Figure 4-3b). This observation fundamentally changed a crucial element of our on-chip flattened nano-tip emitter design. The collector electrodes had all been placed only around a hundred nanometers from the nano-tip emitters and mostly only single emitters had been used because the assumption was the emitted electrons would not effectively traverse distances much greater than a mean-free-path, mf ~ 200-300 nm, under ambient conditions. However, the above experiment revealed that this was false. The length scale of interest is not the electron's mean-free-path, but the 'capture-free' 2 This home-built laser operates at 84 MHz and makes use of a similar layout and design as Refs. [63, 64]. 93 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES path, i.e. the mean distance the electron can travel before being captured. For our initial experiments, we are only concerned with the total emitted electrical current. Therefore, for our purposes it is irrelevant whether the emitted electrons scatter in air; it only matters that the electrons can travel from emitter to collector before being captured by a volatile organic, electronegative species, or something else in the intermittent air. Additionally, this capture-free path is far greater for low-energy electrons in ambient conditions than the mean-free path. Low-energy electrons have been demonstrated to have nanosecond lifetimes in ambient conditions which for a 1 eV electron could translate into a path length approaching the mm-scale [65, 661. This revelation of the importance of the capture-free-path versus the mean-free path lifted a critical restriction in our on-chip strong-field emitter design and, as we will now discuss, pushed us towards plasmonic nanoparticle emitters. b TiS o emitter current (4) 2 - @ collector current (Jd 0 s-Jc 'Eand Ic measured consecutively -os 1 2 3 4 S a 7 8 - a 0 10 Time (s) Figure 4-3: Electrical currents across large gaps under ambient conditions. a. Basic experimental arrangement. Electrical emission from gold whisker on photo-lithographically defined pad. b. Measured electrical currents: emitter current, collector current, and current difference. All currents were measured sequentially, i.e. one after the other. 4.2.2 On-chip nanoparticle emitter arrays Without the mean-free path length scale restriction, we shifted our device design towards nanoparticle emitters. With the nanoparticle emitters, we could place many 94 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES emitters in the focused laser spot, and without the mean-free path restriction, we could place the collector electrode microns away from the emitters and the laser illumination. The basic layout of our modified on-chip strong-field emitter devices is illustrated in Figure 4-4. The chips are composed of a sapphire substrate coated in a 50 nm thick layer of the transparent conductor indium tin oxide (ITO). The nanoparticle emitters are patterned on the ITO layer via electron-beam lithography. The nanoparticles are composed of 20 nm thick layer of gold with no adhesion layer to the ITO. As we described in the previous chapter, several different nanoparticle shapes and sizes are fabricated on the chips. Nanoparticle emitter arrays substrate (sapphire) Emitter (ITO) Collector (ITO) electrode gap (3 pm) Figure 4-4: Nanoparticle emitter device layout (optical microscope image). The substrate is composed of a sapphire chip coated in indium tin oxide (ITO). An array of nanoparticle emitters is fabricated on the ITO layer (enclosed by the red box in the image and an example show in the inset). The ITO is patterned into two regions: an emitter that connects to the nanoparticles and a collector. The collector is separated from the emitter by a few micron gap. The essential surrounding experimental components along with the basic layout of our strong-field emitter chips are illustrated in Figure 4-5. Figure 4-5 shows the same optical microscope image Figure 4-4 from a section of one of our chips (for a largerscale view of the chip see Figures 3-6 and 3-9). Femtosecond excitation laser pulses are tightly focused through an objective and illuminate these nanoparticle arrays. Under 95 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES 2. Nanoparticle emitter arrays Emitter SF phenomena on a chip under ambient conditions I Collector Figure 4-5: Nanoparticle emitter device layout (optical microscope image) and basic experimental setup. Femtosecond laser pulses are focused by an objective (Obj.) to a small spot-size on the nanoparticle array. The excitation laser pulses result in strong-field photoemission from the devices, and the photoemitted electrons jump from emitter to collector. The three main elements of the following few chapters are numbered. this intense optical illumination, the nanoparticles emit electrons in the strong-field regime. These emitted electrons jump across the small (~z3 pm) gap from the emitter to the collector. In Chapter 3 we analyzed the plasmonic nanoparticle emitter arrays and characterized our fabricated arrays (i.e. we discussed item 2 from Figure 4-5). In the following sections we will provide details on the femtosecond laser source (item 1 in Figure 4-5) and will present our experimental observations of strong-field phenomena on our chips under ambient conditions (item 3 in Figure 4-5). Our main objectives in these experiments will be to observe novel strong-field photoemission phenomena from our plasmonic nanoparticle emitters under ambient conditions. As we discussed in Chapter 2, there are several intriguing effects that emerge from photoemission in the strong-field regime. Most notably, in the strongfield regime, sub-optical cycle electron bursts can be produced and these brief electrical currents can be switched on and off with each optical cycle of a laser pulse. This electric field, or optical waveform, production and control of electrical currents near nanostructures has been intensely pursued by researchers. As described, our experimental arrangement, or on-chip strong-field laboratory, is only capable of mea96 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES suring total currents; however, we can look for signatures of this waveform control by looking for carrier-envelope phase sensitivity of the total photoemitted current. This will be the main thrust of our experiments: the exploration of optical waveform controlled electrical currents from plasmonic nanoparticles in the form of carrier-envelope phase (CEP) sensitivity. Along the way we will also demonstrate other signatures of strong-field photoemission and use the strong-field photoemission signal to precisely characterize the temporal behavior of the plasmonic field near the nanostructures. 4.3 Experimental details In this section we present some details on the various components of the experimental setup. We first mention some details regarding the femotsecond laser source. Next, we discuss the measurement and characterization of the ultrashort, femtosecond laser pulses emerging from this source and used in the experiments. We move on to describe the carrier-envelope phase stabilization procedure. Finally, we mention some details regarding the device alignment microscope. This section is intended to provide a large-scale overview of the different elements that go into the experiment. 4.3.1 Few-cycle Er:fiber based laser source The femtosecond laser source consists of two main parts: an Er:fiber oscillator and a supercontinuum generation stage. An overview of the basic system is sketched in Figure 4-6 (similar systems have been described in Refs. [67, 68, 69, 70, 711). The Er:fiber laser produces optical pulses at fR = 78.4 MHz with approximately Ep = 0.375 pJ. The emitted pulse train then passes through an acousto-optic frequency shifter (AOFS), and the first diffracted order is sent into an Er:doped fiber amplifier (EDFA). As we will describe in greater detail in the following, the AOFS tunes the carrier-envelope offset frequency of pulse-train. a pulse energy Ep 1 The pulses out of the EDFA have 4.5 nJ and are compressed in a silicon prism compressor to a duration of - 90 fs. These pulses are then focused into a specially designed highly nonlinear fiber 3 (HNF). In the HNF the interplay of various non-linear optical processes lead to supercontinuum generation. In particular a two-part spectrum is generated; a Raman-shifted soliton is produced near a wavelength of 1.9 pm, and a dispersive wave spectrum is also generated with a center wavelength near 1.2 Am. The dispersive wave 3 This fiber consists of a germanium-doped highly non-linear segment and several other different fiber stretches that have been spliced together. The fibers are designed by the group of Prof. A. Leitenstorfer [68, 70]. 97 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES spectrum is relatively flat from 1-1.4 pm and illustrated in Figure 4-6. The dispersive wave will be used for our experiments and is compressed post-HNF in an SF10 prism compressor. The SF10 prism compressor also contains a spatial filter that picks off the Raman-shifted soliton so that at the output of the entire laser system we are left with just the dispersive wave spectrum with a pulse energy of around Ep = 0.3 nJ, a repetion rate of the Er:fiber oscillator seed at fR = 78.4 MHz, and a relatively flat spectrum spanning the wavelength range of 1-1.4 pm. Erfiber oscillator Supercontinuum Gen. si pc HNF Optical Spectrum 0. 40.1 nEp= 0.3 nJ f.=75. MHz 02 AOSISpIO9PC 01 9 AV 3 1000 1100 1200 1300 1400 1500 wavelength (nm) Pulse measurement CEP stabilization Experiments Figure 4-6: Femtosecond laser system overview. Schematics and pictures of the Er:fiber oscillator and the supercontinuum generation stages are shown. At the output of the femtosecond laser system is the dispersive wave spectrum spanning 1-1.4 pm as shown. The dispersive wave pulses are sent from the laser system output to the pulse measurement setup, the carrier-envelope phase stabilization/characterization setup, and the actual strong-field experiments. 4.3.2 Pulse measurement The dispersive wave pulses out of the femtosecond laser system are measured with a two-dimensional spectral shearing interferometer (2DSI)'. The results of the pulse measurement are shown in Figure 4-7. Figure 4-7a shows a repeat of the dispersive 4Two-dimesional spectral shearing interferometry is a spectral-shearing pulse measurement technique similar to SPIDER but with simpler and less-sensitive calibration requirements. For further information see Ref. [72]. 98 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES wave spectrum, and Figure 4-7b shows the measured pulse shape (blue) and the transform-limited pulse (red-dashed). The central spike of the measured pulse has a full-width-at-half-maximum of r ~ 9.6 fs, close to that of the ideal transform-limited pulse. a b Optical Spectrum Retrieved Pulse I 0.8 0.8 0.6 0.6 -Measured =9.6fs . 1 C 0.4 0.4 0.2 , = 0.3 M fR =78.4MHz 0.2 a 900 1000 C 0 1400 1100 1200 1300 wavelength (nm) 1500 -40 -20 0 time (fS) 20 40 d InterferometricAutocorrelation Predicted -FnL *Measured .4 0 -40 -30 -20 -10 0 delay (f6) 10 20 30 40 Figure 4-7: Dispersive wave pulse measurement. a. Spectrum of the dispersive wave pulse used in the experiments. b. Measured optical pulse shape from the 2DSI (blue) and the ideal transform-limited pulse (dashed-red). c. Interferometric autocorrelation measurements (note the early delay data is poor due to an error in the calibration at the start of this trace). d. Image of the 2DSI setup. To confirm the measured pulse shape, interferometric autocorrelation (IAC) measurements were additionally performed. The IACs were taken by focusing two pulses,temporally spaced by a carefully calibrated delay, into a 40 pm thick Beta barium borate (BBO) crystal and recording the produced second-harmonic generation signal 5 . The IAC measurement for the optical pulse displayed in Figure 4-7b is given in Figure 4-7c. 'We should additionally mention that in the interferometer that composes the IAC specially designed group-delay dispersion matched beamsplitters are used. These beamsplitters show a group delay equivalent to 0.75 mm of fused silica (up to an arbitrary constant) on both reflection and transmission. The effect of these beamsplitters is incorporated in the calculations of the expected IAC traces provided in Figure 4-7c. 99 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES In Figure 4-7c the measured IAC data is displayed (red dots); the expected IAC for an ideal transform limited pulse is shown (light blue); and the expected IAC for the measured pulse given in Figure 4-7 is displayed (dark blue). The expected IAC for our measured pulse fits the measurement reasonably well, so we have some confidence in our measured pulse shape and characteristics. Carrier-envelope phase stabilization 4.3.3 As we have mentioned one of our primary goals will be to detect carrier-envelope phase sensitivity in our photoemission experiments. Therefore, it is critical to stabilize the carrier-envelope phase of our femtosecond laser pulses. The CEP of the laser pulse train emitted by our femtosecond laser system is illustrated in Figure 4-8a. Ideally, from pulse to pulse the CEP shifts by some specific amount A&p (as mentioned in Chapter 1, this shift is due to a mismatch the between group velocity and phase velocity in the laser cavity). However, with noise and other perturbations this progression of the CEP can be irregular; therefore, we need to actively control the CEP to ensure we have reproducible and predictable electric field shapes from pulse to pulse. To stabilize the CEP of our laser pulse train we must first detect the CEP of the pulse train and then feedback the detected signal to an actuator that can tune the CEP to the desired value. In our setup, the CEP is detected in the conventional way with an f - 2f interferometer. The basic layout of our f - 2f interferometer is shown in Figure 4-8a. The long-wavelength Raman-shifted soliton and a very small portion of the shortest wavelength light from the dispersive wave are picked off in the SF10 prism compressor. These two optical signals are sent to the f - 2f. The output of the interferometer is then sent to the AOFS which tunes the CEP of the laser pulse train. The AOFS uses acoustic waves to Doppler shift the pulse train and accordingly tune the CEP of the laser pulse train [67, 73]. The results of the CEP lock are presented in Figure 4-8b. These results come from an out-of-loop f - 2f interferometer and show good fringe stability and a relatively low rms drift in the CEP of only 167 mrad. f We should mention that our in-loop - 2f interferometer contains an additional acousto-optic modulator in one arm to allow for locking of the carrier-envelope offset phase down to 0 Hz. 100 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES a VCZ- A ) V quLo A 9CEO b Out-of4aopyf-2 C mrad V 6rm,=167 0 - 1.5L 0 10 20 30 40 50 60 time (s) Figure 4-8: Carrier-envelope phase stabilization and characterization. a. Overview of the modifications to the femtosecond laser system to allow carrierenvelope phase locking. The physical meaning of the CEP is also illustrated to the right. b. Results from the out-of-loop f - 2f interferometer when the carrier-envelope offset frequency is locked to 0 Hz. 4.3.4 Device alignment The final component of the experimental setup is the device alignment microscope. In our experiments, we illuminate a 20 pm x 20 pm array of plasmonic nanoparticles with focused femtosecond laser pulses that have a beam diameter of only around 4 pm. To reliably and consistently place this tiny laser spot on our emitter array, we build a simple confocal microscope. The microscope is illustrated in Figure 4-9a. A reflecting objective (Obj. 1 at the top of the picture in Figure 4-9a) focuses the laser light onto our devices (device mount image included to the right). The laser light is then collected by a second objective (Obj. 2 at the bottom of the picture in Figure 4-9a) and imaged onto 101 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES a b fs-source Fit (Gaussi.n) 0 Meuremert - 2. 0.53 W,=1.9 -10 White Pm -5 foci 0 5 10 podtrn (-) light Figure 4-9: Alignment microscope setup and focused spot characterization. a. Picture of the confocal alignment microscope and the device mount (right). b. Knife-edge measurements of the focused laser spot in both transverse planes (measurement made by scanning a 10 pm wide gold wire across the laser spot). c. Example microscope image recorded on the CCD. Old devices are shown with very high spatial resolution. a CCD. Additionally, a white light source illuminates our mounted device through the collecting objective (Obj. 2). This light reflects from our devices and is also imaged on the CCD. This simple confocal microscope allows us to simultaneously image our devices and the position of our focused laser spot. An example image of an early set of our devices is included in Figure 4-9c. From the scale bar, we see that our confocal microscope can accurately image fine features of our devices and enable precise alignment of our focused laser spot. The confocal microscope setup offers the additional opportunity to characterize the focused laser spot. Gold alignment pads or wires can be swept across the focused laser spot to record knife-edge traces of the focused spot. Such knife-edge measurements for both transverse directions are included in Figure 4-9b. In these measurements a 10 prm wide gold wire was scanned across the focused laser spot, and the laser spot is found to have beam waists in the two transverse directions of w, = 3.5 tm and wy = 1.9 Pm. 102 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES 4.4 Photoemission measurements In this section we present measurements of photoemission currents from our plasmonic nanoparticle devices. First, to confirm our fundamental picture of the device operation, we make simultaneous measurements of the current leaving the emitter electrode and the current arriving at the collector electrode and compare the relative phases of these currents. Next, we will analyze how the photoemission current varies as the excitation pulse intensity is increased. Finally, we will discuss degradation and changes to our devices through use. Collector and emitter currents 4.4.1 First and foremost, we want to confirm the basic picture of our device operation. We want to be sure that our devices are emitting electrons and that these electrons are reliably crossing the few micron gap from emitter to collector. To this end, we illuminate our nanoparticle emitters and simultaneously measure the current at the collector electrode, JC (the collector current), and the current at the emitter electrode, JE (the emitter current). The results of this first measurement are shown in Figure 4-10. In the top panel of Figure 4-10, we see that Jc and JE match extremely well, and both currents are relatively stable over the approximately three and a half minute measurement period. These measurements are made via lock-in detection6 , so we can additionally compare the relative phase of the emitter and collector currents. This relative phase is shown in the lower panel of Figure 4-10. We see that the relative phase of the currents is almost exactly 180'. Therefore, Jc and JE must have opposite signs. Additionally, we observe that a current is only produced when the laser illuminates the device array and when there is a positive bias on the collector electrode relative to the emitter (for the experiment shown in Figure 4-10 this bias was VBIAS = 10 V). When the laser illuminates other regions of the chip or when the laser is turned off there is no current. Additionally, when the bias between on the collector is increased relative to the emitter the current is increased, while when this bias is decreased or made negative, the current can be decreased dramatically. From these results, we can conclude that electron are being emitted from our plasmonic nanoparticle devices, traveling across the few micron gap between the emitter and the collector, and reliably arriving at the collector. Lastly, we should mention that the data presented in Figure 4-10 was recorded from a nano'The illuminating laser beam is chopped at fchp = 200 Hz, and the collector and emitter currents are independently measured on two different lock-in amplifiers. 103 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES triangle array with ARes = 1059 nm and TRad = 5.8 fs. Similar behavior was observed for all the emitter arrays. Collector current (d 6 J Emitter current (Ji) .2c 12n z C Emitter VBWs = 0 10 V 50 100 150 20 Time (s) V a 181. Am=1059 nm X = 5.8 fs O= 179.9' 0.2IJC'- 5I 4.2 8.5 pA 1C - 18(1 1 79 0 50 100 150 200 Time(s) Figure 4-10: Collector and emitter currents from a nano-triangle array. The upper plot shows the simultaneous measurement of the collector and emitter currents and the stability of these currents. The bottom plot shows the relative phase between the collector and emitter currents. The right image shows a reminder of our basic experimental arrangement. The nano-triangle array has ARes = 1059 nm and rad = 5.8 fs. 4.4.2 Photoemission current versus pulse energy Here we sweep the excitation laser pulse intensity and observe the photoemission current yield for different biases and different device types. Starting at the laser's full pulse energy and slowly decreasing it with a neutral density filter, we measure the collector current. We find that at low pulse energies the photoemission current follows a power-law scaling of - I where I is the excitation pulse intensity (I oc Ep where Ep is the pulse energy). At higher pulse energies, the photoemission current rollsoff from this scaling and, for a range of pulse energies, scales like J2. An example of this behavior is plotted in Figure 4-11 and Figure 4-12. Figure 4-11 shows the photoemission current at the collector versus pulse energy for a nano-triangle array with ARes = 1105 nm and rad = 6.4 fs. Data for four different collector bias voltages: 5 V, 10 V, 20 V, and 30 V are displayed. Figure 4-8 shows a similar presentation of data but for nano-rod devices with ARes = 1041 nm and rad = 4.8 fs. The data displayed in Figure 4-11 and Figure 4-12 is representative of similar 104 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES 5. 5I A,=1105nm -cd =6.4fs 101 10 C CP - 40 VBus= 30 V = 20V V 0 2= 1042.6 nA 0.0125 0.025 37 e- pulse /emitter 0.05 0.1 0.2 Pulse energy (ni) Figure 4-11: Photoemission current versus pulse energy for a nano-triangle array. The array has ARes = 1105 nm and Tra = 6.4 fs. The current scaling is measured for four different collector biases. At low pulse energies the current scales as ~ 1 5, while at higher pulse energies this scaling falls off to - I2. The blue dot at the top right of the graph labels a data point that shows 42.6 nA of current which corresponds to approximately 37 electrons per pulse per emitter. photoemission current scaling measurements performed on our other devices. There are several important trends to mention. Firstly, the I5 5 scaling at low pulse energies agrees with our expectation for multiphoton photoemission. The central wavelength of our excitation laser is 1.2 pm, and, as mentioned, the work function of gold is around 5.1 eV, so we expect to need 5 - 6 photons to surmount this barrier. We therefore expect the multiphoton photoemission current to follow an P scaling with n = 5 - 6. This is exactly what we observe at low pulse energies. At higher pulse energies and intensities, we expect that the photoemission mechanism will shift from multiphoton to strong-field photoemission. As discussed in Chapter 2, we expect a resulting roll-off of the current scaling. This is again what we observe. The turning point for this current roll-off occurs near Ep ~~25 pJ, which implies at Ep ~ 25 pJ the Keldysh parameter is close to unity. With our focal conditions and wavelength, 105 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES this implies a field enhancement of ~ 20 for our devices, which is typical of what has been measured for similar plasmonic nanoparticles [22]. Another observation is that all of the current scaling curves at the different biases share very similar shapes. They all have similar turning points and scaling behavior. An initial thought may have been that the current roll-off at higher pulse energies is due to a space-charge effect which, at high photoemission current yields, begins to limit the scaling; however, the fact that these curves are independent of bias indicates otherwise. This suggests that strong-field effects are indeed responsible for the current roll-off behavior. 15.5 Aae, =1041 nm t, = 4.8 fs ,' , 101 I C 100 - 110 C 101 .J2 -0oo 0040 0 VBs= 10-2 I = 20 V = 10 V = 5V U 10~ 30 V if = 34.3 nA = 21 e- / pulse / e mitter 0.0125 0.025 0.05 0.1 0.2 Pulse energy (ni) Figure 4-12: Photoemission current versus pulse energy for a nano-rod array. The array has ARe, = 1041 nm and rad = 4.8 fs. The current scaling is measured for four different collector biases. At low pulse energies the current scales as ~ I 5, while at higher pulse energies this scaling falls off to ~ 12. The blue dot at the top right of the graph labels a data point that shows 34.3 nA of current which corresponds to approximately 21 electrons per pulse per emitter. In the preceding measurements we looked at photoemission current scaling behavior from nano-rod and the nano-triangle emitters under different bias conditions. Now, let us consider the photoemission current scaling for emitters with different sizes 106 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES and resonant behaviors. In Figure 4-13 and Figure 4-14, we show currents scaling data for four different nano-triangle arrays and four different nano-rod arrays (all measured at a 30 V bias). In Figure 4-13 we see that for three of the four different nano-rod arrays, the current scaling curves take on a very similar shape. This again implies that the field-enhancement for these arrays is comparable. This is reasonable as these three arrays all have their resonant wavelengths in the bandwidth of the excitation laser pulse (AR, = 1256 nm, 1158 nm, and 1059 nm). The off-resonant array takes on a very different current scaling shape and emits far fewer electrons. In Figure 4-14 we see similar behavior for nano-rods. The on-resonant arrays show similar current scaling behaviors, while the off-resonant array shows slightly different behavior. 101 ARes = 1256 nm 100 = 951 nm J5.5 = 1158 nm = 1059 nm 4.. C I.-1 a 0 10-1 0 0 = 10' 0.0125 0.025 0.05 0.1 0.2 Pulse energy (ni) Figure 4-13: Photoemission current versus pulse energy for four different nano-triangle arrays. The four arrays have ARe, = 951, 1059, 1185, and 1256 nm. The measurements were made at 30 V bias. 107 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES 10 AR= 1238 nm = 1177 nm 15.51' = 1041 nm = < 968nm 4 10 5 10 %=0 10 0.0125 0.025 0.05 0.1 0.2 Pulse energy (ni) Figure 4-14: Photoemission current versus pulse energy for four different nano-rod arrays. The four arrays have Ages = 968, 1041, 1177, and 1238 nm. The measurements were made at 30 V bias. 4.4.3 Device degradation . The final photoemission measurements we present in this section concern stability and degradation. One possible issue with our on-chip emitters operating under ambient condition could be stability. Considering the extremely dirty, out-of-vacuum operating environment, we first look at how repeatable our photoemission measurements are.In Figure 4-15 two measurements are shown of the current scaling behavior for a nano-triangle array. The first measurement (red) shows the same data displayed in Figure 4-11 (30 V collector bias). The second measurement (blue) was made by increasing the optical intensity. The sweep direction of the neutral density filter was reversed and the photoemission current was measured. This measurement was taken several minutes after the first. Over this time window the current scaling measurements are clearly very stable and repeatable 7 7 We should also note that our emitter arrays are used many times over month long periods and continue to show good, consistent performance. 108 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES As=1105nm 101 xm =6.4fs 100 0 am a 10-2 10' 9 Vus= 30 V 10 42.6 nA = 37 e- / pulse 0.0125 0.025 0.05 I emitter 0.1 0.2 Pulse energy (ni) Figure 4-15: Repeatable photoemission current scalings. The measurement was made at 30 V from a nano-triangle array with Ages = 1105 nm and TRad = 6.4 fs. The red trace is the same measurement as shown from Figure 4-7. The blue trace is measured by sweeping the intensity in the opposite direction several minutes later. The second concern when it comes to device repeatability is degradation. Under the ambient conditions the devices might degrade due to the dirty environment, ion bombardment, etc. Figure 4-16 shows a microscope image and an SEM image of the devices after fairly extensive use8 . From the microscope image the devices do not seem to change their optical properties. They appear identical under the optical microscope; however, near the edge a light colored layer is appearing on the collector side. Looking at the SEM, this light colored layer seems to be due to a de-lamination of the ITO layer from the collector. Additionally, looking at the SEM, the device quality on the emitter side does not seem to have degraded at all. This degradation 8For our purposes, extensive use means many experimental runs, but likely only on the order of tens of minutes of continuous exposure to the laser at the highest pulse energy. 109 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES of the ITO does not have a tremendous effect on the emission (the ARe, = 1158 nm trace from Figure 4-13 was measured with the labeled array). The only effect of this degradation seems to be to lower the effective bias field; as the ITO de-laminates, the high-quality ITO pushes further from the emitter or, effectively, the collector is pushed further from the emitter. The origin of this degradation is unclear, but likely relates to technical details associated with the ITO deposition process or possibly the ITO etch process. a b Figure 4-16: Emitter array degradation. a. Microscope image of extensively used device arrays (the labeled array was used in this condition to measure the ARe, = 1158 nm trace from Figure 4-13). The light colored strip near the collector edge forms during device operation. b. SEM image of the labeled device array. The light colored strip from the microscope image appears to be ITO de-lamination. 4.5 Probing the plasmonic field via IAC In this section we describe interferometric autocorrelation (IAC) experiments performed with our devices. In our preceding discussion we saw that for a range of pulse energies, as the current scaling begins to roll-off into the strong-field regime, the photoemission current scales as 1'. We can use this second-order non-linearity to carry out second-order IACs with our plasmonic nanoparticle devices'. These autocorrelation measurements allow us to characterize the temporal shape of the plasmonic field around the or nanoparticles and may validate the time-domain predictions from our 'Similar measurements have been performed using the non-linear light produced when plasmonic nanoparticles are illuminated by femtosecond excitation pulses. However, these studies have been restricted to third-order IACs [30, 74, 751. 110 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES simple nano-resonator circuit model. The results from three such IAC measurements are given in Figure 4-17, Figure 4-18, and Figure 4-19. AR, = 1256 nm . T,.d= 7A fs - -40 -30 -20 -10 0 Measured IAC expected IAC SHG IAC 10 20 30 40 10 20 30 40 delay (fs) 0. 8 - Excitation pulse Nano-res. pulse 0.6 EU 0.4 0.2 -40 -30 -20 -10 0 time (fs) Figure 4-17: Interferometric autocorrelation measurement performed with the strong-field photoemission current. The device used in this measurement is a nano-triangle array with ARe, = 1256 nm and Trad = 7.4 fs. The top trace shows the measured autocorrelation (red), the expected autocorrelation from our time-domain model (blue), and the second-harmonic generation (SHG) autocorrelation measured previously. The bottom panel shows the measured pulse (black) that excites the nano-resonator array and the expected pulse from our time-domain model (blue). The results in Figure 4-17 agree extremely well with the time-domain predictions of our simple circuit model. Note the data shows a dramatically broadened autocorrelation compared to what was measured in section 4.3.2 from the excitation laser pulse directly out of the femtosecond laser system. When the pulse excites the plasmonic mode on the nanoparticle resonator, it broadens as the resonator filters the pulse. The excellent agreement between the predicted autocorrelation, derived from the time-domain response of our simple circuit model, and the measured result give confidence in the validity of our simple frequency and time-domain model for the 111 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES nano-resonators as well as our measured pulse shape. 8 AR. =1105 nm = 6.4 fs T 7 6 _____ * expected IAC - ______ Measured IAC - SHG IAC 5 4 3 1 -40 -30 -20 -10 0 10 20 30 40 10 20 30 40 delay (fs) - 0.8 - Excitation pulse Nano-res. pulse 0.6 0.4 0.2 0 -40 -30 -20 0 -10 time (fs) Figure 4-18: Interferometric autocorrelation measurement performed with the strong-field photoemission current. The device used in this measurement is a nano-triangle array with ARes = 1105 nm and Trad = 6.4 fs. The top trace shows the measured autocorrelation (red), the expected autocorrelation from our time-domain model (blue), and the second-harmonic generation (SHG) autocorrelation measured previously. The bottom panel shows the measured pulse (black) that excites the nano-resonator array and the expected pulse from our time-domain model (blue). The results in Figure 4-18 show the data for a second autocorrelation on a nanoresonator array shifted slightly off-resonance. Again, there is excellent agreement between our predicted autocorrelation and the measurement. Note, that for this array the pulse broadening is less significant as the resonance is slightly off the central wavelength of the excitation pulse. Finally, in Figure 4-19, we present one last autocorrelation measurement that further corroborates the accuracy of our circuit model. This trace shows a pulse that is barely broadened by a nearly off-resonant nanoparticle resonator. Lastly, we should mention that similar results have been found for autocorrelations from all of our device arrays, and such that overall, we have high112 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES confidence in the predictive abilities of our simple circuit model for our plasmonic nano-resonators and in our measured pulse shape. 8 7 6 AR,, = 1041 n ,,d = 4.8 fs I Measured HAC - -SHG 5 EU expected IAC IAC 4 11 -40 -30 -20 -10 0 10 20 30 40 10 20 30 40 delay (fs) 1 0.8 - Excitation pulse Nano-res. pulse 0.6 Ed 0.4 0.2 0 -40 -30 -20 -10 0 time (fs) Figure 4-19: Interferometric autocorrelation measurement performed with the strong-field photoemission current. The device used in this measurement is a nano-triangle array with ARes = 1041 nm and Trad = 4.8 fs. The top trace shows the measured autocorrelation (red), the expected autocorrelation from our time-domain model (blue), and the second-harmonic generation (SHG) autocorrelation measured previously. The bottom panel shows the measured pulse (black) that excites the nano-resonator array and the expected pulse from our time-domain model (blue). 4.6 Carrier-envelope phase sensitivity The final set of experiments we will carry out with our nano-emitter devices will be targeted at looking for carrier-envelope phase effects in the photoemission current. As discussed, carrier-envelope phase effects are a signature of optical waveform control, and this area has been one of the more hotly targeted measurements researchers have sought to perform with strong-field photo-emitting nanostructures. In the following 113 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES section, we will describe preliminary carrier-envelope phase sensitivity measurements, and we will discuss modeling the CEP effect. First, recall our simple model for CEP sensitivity from Chapter 2, and let us consider the more specific form of Q(p) for our nano-triangle and nano-rod devices. The electric field sensitive strong-field photoemission from our two device types is illustrated in Figure 4-20. An interesting property of the strong-field emission current that we noted in Chapter 2, is that it depends on the direction of the field. Since it is a tunneling-like current the field must deflect the barrier downwards for emission, so only one field direction will emit from a surface. With an optical pulse as illustrated in Figure 4-20, our nano-rods will emit during every half-cycle of the optical pulse and will emit from both ends (two-sided emission), while our nano-triangles, which experience significant field enhancement only at their sharp apex1 0 , will only emit from their apex and, therefore, will only emit for half of the optical cycles (onesided emission). We can then use the results from Chapter 2 regarding one- and two-sided emitters to model the charge emitted by the nano-rods, QR(p), and the nano-triangles, QT (W). F+() F(t) F-() Figure 4-20: Geometry of strong-field emission. Nano-triangles and nanorods are illuminated by femtosecond laser pulses (here labeled F(t)). The Nanotriangles will only emit from their apex and therefore only emit for half of the pulse's optical cycles, while the nano-rods emit from every cycle. As described, we expect for our pulses the carrier-envelope phase sensitive current to be relatively small. For the measurement, we therefore stabilize the carrier-envelope offset frequency, i.e. fCEO = 2 kHz, and look at the radiofrequency (RF) spectrum of the emitted current with a narrow resolution bandwidth near this frequency. The results from an initial measurement are shown in Figure 4-21. In the top panel of Figure 4-21, we see the RF spectrum at 1 Hz resolution bandwidth of the emitter '0 This is the sharp apex that is aligned with the polarization direction of the field. 114 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES current from the nano-triangles (blue). We see a strong ~ 23 dB component at the fCEO. This component disappears when the fCEO is unlocked (red). In the bottom panel of Figure 4-21, we see the same plot for the nano-rods. Since we expect no odd-harmonics of fCEo in the current from the nano-rods, it is no surprise that no peaks are visible. 10 A for triangles 0 J.ne 10RBW CL. ~23 dB = 1 Hz 1.9 _1 -A 20 1.95 2 Frequency (kHz) 2.05 2.1 2 2.05 2.1 Ifia 0 to go -10 JE for rods JEfnoise RBW = 1 Hz -20 1.9 1.95 Frequency (kHz) Figure 4-21: Initial CEP sensitivity measurement. The top trace shows the RF spectrum of the emitter current for a nano-triangle array and the bottom trace for a nano-rod array with the fCEO locked to 2 kHz. The noise data corresponds to when the fCEO is unlocked. The units dBpA are equivalent to 20loglo(JE/1 pA). We next confirm the CEP sensitivity of the current by carrying out a simple phasestepping experiment. In this experiment a barium fluoride wedge is progressively slid through the exciting laser pulse. The mismatch between the group velocity and phase velocity in the wedge will lead to a shift in the absolute CEP of the laser pulse train as it passes through the wedge. In this experiment we again lock the fCEo to a 2 kHz local oscillator. We then use the signal from this local oscillator as the reference to a lock-in amplifier. The lock-in amplifier measures the carrier-envelope phase sensitive 115 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES component of the emitter current from a nano-triangle device (same device used in the data from Figure 4-21). The relative phase measurement on the lock-in should give us the phase difference between the local oscillator and the CEP of the pulse train. Therefore, we expect that if the response on the lock-in is actually due to a CEP sensitive effect, then sliding the wedge through the pulse train will step this relative phase. In our experiment we shift the wedge 2.5 mm with a translation stage every 10 s. From the expected group and phase velocity mismatch at the central wavelength of our pulses i.e. 1.2 ptm, we expect this phase to step by ~ 560. This is almost exactly what we observe. The deviations from this behavior are explained by the warm-up or settling time of the lock-in and the 167 mrad rms deviations expected in the stabilized carrier-envelope phase (see Figure 4-8). 7 450 400 BaF wedge "0 350 . 300 250 200, Insert .75* B F 2 wedge 2.5 mm every 10 s 100 50 56 qCEP shift 10 20 30 40 time (s) 50 60 70 80 Figure 4-22: Absolute phase stepping measurement. A barium fluoride wedge is stepped through the excitation pulse train shifting the absolute CEP of the pulse train. The response is measured via lock-in detection. Thus far we have seen convincing evidence that our strong-field nano-devices show carrier-envelope phase sensitive properties in their photoemission currents. Here we would like to see if our simple model can accurately predict this sensitivity. To this end let us define the carrier-envelope phase sensitivity. This sensitivity, S, will be defined as the CEP sensitive current divided by the average current. 116 The CEP sensitive CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES current JCEP is the magnitude of the first harmonic of fCEO in the photoemission current spectrum. The average current is just the mean photoemission current, i.e. JE. If we calculate the sensitivity for our measured pulse shape (see Figure 4-7b or the field in Figure 2-13 and the model in Chapter 2), we find that S ~1-4. Now if we input our measured pulse shape into our time domain circuit model for our plasmonic nanoparticles and use the resulting pulse to calculate the sensitivity, then we find a different sensitivity for each nanoparticle type. These different sensitivities are plotted in Figure 4-23b. We refer to this model as the 'super-simple model' for the CEP sensitivity or the SSM model. In a next experiment we measure the carrier-envelope phase sensitive current from seven different nano-triangle devices. Five of these traces are shown in Figure 7-23a. From Figure 7-23, note that the magnitude of the CEP sensitive current varies as we shift the resonant wavelength of the device. The off-resonant devices show relatively little CEP sensitive current, the CEP sensitive current is maximized just as the resonant wavelength of the devices begins to approach the excitation spectrum, and then the CEP sensitive current falls off as the devices move on resonance. We then translate these measurements of is then plotted in Figure 7-23b. JCEP to CEP sensitivity numbers. This data From Figure 7-23b, we see that remarkably our extremely simple model for the CEP sensitivity very accurately predicts the measured sensitivity. This is a very initial result, and it still needs to be seen how reproducible this agreement is as the pulse shape shifts or more nanoparticle arrays are used. 117 CHAPTER 4. PHOTOEMISSION FROM PLASMONIC NANOPARTICLES a A,= 951 nm A4= 1000 nm Af = 1059 nm AR.= 1105 nm A= I I * Salft * CL - ... * 1.95 2 2.05 I * I I I I I I I I I I I I I I I I I I I I I I 2 I I I I I * I I I I I I I I I I I I I I I I 2.05 2.05 2 Frequency (kHz) 2 2.05 2 2.05 b ----------------------------- ----------------o 0 08 -. 8 * 0 600 SSM 0 8 model 850 900 950 1000 1050 1100 1150 1200 1250 1300 AR. (nm) Figure 4-23: CEP sensitivity versus ARes. a. RF traces of the emitter currents from five different nano-triangle arrays are displayed (note each trace is measured from 1.94 - 2.06 kHz). b. The corresponding sensitivity is plotted for these five devices and two additional ones. 118 Chapter 5 Enhancement cavities for high-harmonic generation In this chapter and the following ones, we depart from strong-field physics at the nanoscale and move to discuss cavity-enhanced high-harmonic generation (HHG)1. We will outline the basics of cavity-enhanced HHG. The essential motivation for enhancement cavities for strong-field physics will be described, and the concept of passive amplification inside an ultrafast, femtosecond enhancement cavity will be reviewed. Next, we will discuss the requirements for an effective enhancement cavity for HHG and the challenges associated with designing such a cavity. Finally, previous and ongoing work in this area will be discussed, and we will outline our novel approach to designing enhancement cavities for strong-field physics. 5.1 Enhancement cavities for strong-field physics Interest in strong-field physics has exploded over the past several decades. HHG has provided a route to compact, coherent sources of short-wavelength light in the extreme-ultraviolet (EUV) and soft x-ray regime, attosecond science is pushing temporal resolution to the atomic scale, and new applications are constantly appearing. However, as mentioned in Chapter 1, to reach the necessary intensities for strong-field physics, complex amplifier systems are generally required. As we have discussed, such amplifiers can readily produce millijoule pulses of tens of femtoseconds in duration, however only after reducing the seed oscillator's repetition rate from near 100 MHz down to the kHz regime. In recent years femtosecond enhancement cavities have 'We should note that much of the following chapters parallels previous published work by the author. See Refs. [76, 77]. 119 CHAPTER 5. ENHANCEMENT CAVITIES FOR HIGH-HARMONIC GENERATION emerged as an alternative route to achieving the high-intensities necessary for strongfield physics with the additional advantage of maintaining the driving oscillator's high repetition rate [26, 78, 79, 80, 81, 821. The coupling of an ultra-short pulse train from a mode-locked laser to a femtosecond enhancement cavity is sketched in Figure 5-1. Inside the femtosecond enhancement cavity, pulses are enhanced through constructive interference. After a single round-trip through the cavity, a pulse constructively interferes, adds to, the next pulse in the optical pulse train (see Figure 5-1a). When the cavity/mode-locked laser system is appropriately stabilized such that each mode in the frequency comb overlaps with a cavity resonance, then each comb mode experiences the natural enhancement inside the cavity and, accordingly, the entire pulse is amplified (see Figure 5-1b). a. Time Domain b. Frequency Domain ci ii *1 Resomwe Frquency *~ComibMode Frequency Figure 5-1: Operation of a femtosecond enhancement-cavity. a. In the time domain, small portions of the incident pulse train are transmitted into the cavity and add to the circulating intra-cavity pulse. If the cavity parameters are properly tuned, these transmitted pulses will constructively add and build-up the energy of the intra-cavity pulse. b. In the frequency domain, the cavity has a comb of resonances spaced by the free-spectral range of the cavity. If each spectral mode of the incident optical pulse train overlaps a cavity resonance, the pulse train will be enhanced. The utility of this intra-cavity pulse enhancement for HHG can be understood in two-ways. First, the cavity can be interpreted as a passive amplifier that increases the power of the incident pulse train to levels suitable for HHG. Since the intensity enhancement in a cavity is ~ 1/loss, the intra-cavity loss must be low for significant amplification. Accordingly, the loss associated with the HHG process or the HHG conversion efficiency must be low; however, since HHG energy conversion efficiencies 2 2 Although conversion efficiencies for HHG are typically < 10- 5 losses may be much higher due 120 CHAPTER 5. ENHANCEMENT CAVITIES FOR HIGH-HARMONIC GENERATION are typically < 10-5 one expects suitable amplification [83]. This interpretation of the cavity operation is generally adopted by the cavity-enhanced HHG community; however, an alternative interpretation is to consider HHG as a general non-linear process with some conversion efficiency as L. i] and some total loss which we will now define Considering the cavity enhancement of a 1/L, the effective HHG efficiency becomes ~ 7/L (>> 7). In this interpretation the cavity's function is to increase the efficiency of HHG production from the high-repetition rate, un-amplified pulse-train coupled into the cavity by recycling the un-converted portion of each pulse for further HHG generation. Given the preceding discussion, high-intensity femtosecond enhancement cavities are of great interest for strong-field physics. Recently, femtosecond enhancement cavities have been demonstrated with intra-cavity average powers of kilowatts, and intra-cavity peak intensities > 10" W/cm2 have been achieved in such cavities operating at typical megahertz oscillator repetition rates [26, 80, 84]. Intra-cavity HHG (i.e. cavity-enhanced HHG) has been demonstrated with tens of microwatts of average power per harmonic in the extreme-ultraviolet [26, 80]. These sources have allowed for novel EUV spectroscopic studies [80] and may make way for higher flux sources of EUV and soft x-ray light in years to come. 5.2 Enhancement cavity design for HHG Although tremendous progress has been made with high-intensity femtosecond enhancement cavity technology, many strong-field physics applications demand higher intra-cavity peak intensities than have been achieved. Intra-cavity peak intensity is in part limited by the damage threshold of the cavity mirrors and the achievable mode waist on the cavity mirrors (~ 1 mm for high-intensity bow-tie cavities) [78, 79, 26, 80]. Additionally, the next generation of high-intensity femtosecond enhancement cavities for HHG require higher harmonic yields. Harmonic yields in cavity-enhanced HHG are largely limited by the out-coupling optics. Sapphire plates [78, 79, 26], EUV gratings [81, 80], and small apertures in the cavity mirrors [82, 85, 86] have been used for coupling high-harmonics out of enhancement cavities, but the best demonstrated out-coupling efficiencies remain relatively low (a 10%). Considering the above requirements, the ideal enhancement cavity for HHG must possess three main characteristics: to ionization that does not contribute to the HHG output. This is an ongoing area of study. 121 CHAPTER 5. ENHANCEMENT CAVITIES FOR HIGH-HARMONIC GENERATION 1. Significant intensity gain from the mirror surfaces to the focus. In the following, we will use the term intensity gain to refer to the ratio of the optical intensity at the intra-cavity focus to the intensity at the cavity mirrors. Dielectric mirrors can only withstand intensities of around 1010 - 1011 W/cm 2 without damage. Additionally, since phase-matching considerations limit the minimum spot-size of the driving laser pulse to be = 30 pm, significant intensity gain means a large spot-size on the cavity mirrors. 2. A method to couple the HHG beam out of the enhancement cavity. Due to momentum conservation, the HHG beam is generated collinearly to the driving beam. Since EUV/soft x-ray light is strongly absorbed by virtually all materials, out-coupling the HHG is a non-trivial task. 3. A desirable intra-cavity beam for phase-matching the HHG process. For brevity, this last requirement will not be discussed here; it suffices to say that phase-matching HHG is a complicated, still-debated subject, and for our purposes this requirement translates simply to a beam with a spot size > 30 pm. The bow-tie ring cavity has been the workhorse of previous studies on cavityenhanced HHG. A sketch of two bow-tie ring cavities is presented in Figure 5-2. The modes of these resonators are the conventional Hermite-Gaussian beams. These resonators allow spot sizes of several mm 2 on the cavity mirrors while having focused waists of e 30 pm. Such intensity gain is suitable for HHG at the lower end of the intensity range = 10 W/cm 2 , but scaling intensities to > 1014 W/cm 2 pushes the required intensity on the cavity mirrors beyond the damage threshold. An additional challenge with the bow-tie cavity geometry has been out-coupling the harmonics. As mentioned, a popular out-coupling method has been to use an intra-cavity sapphire plate (see Figure 5-2a) oriented at Brewster's angle for the driving laser light. The plate then presents virtually no loss for the pump light while giving a small Fresnel reflection to the EUV. The disadvantages of this technique are: the Fresnel reflection is relatively small for the EUV giving an out-coupling efficiency of < 10%; and, for high-intensities, non-linearities in the plate [87] are unavoidable, and these non-linearities limit the in-coupling to the cavity. An alternative out- coupling method uses an EUV grating etched onto a highly-reflecting cavity mirror (see Figure 5-2b) [81, 80]. The small pitch of the grating does not affect the driving 122 CHAPTER 5. ENHANCEMENT CAVITIES FOR HIGH-HARMONIC GENERATION Out-coupled High Harmonics a. Brewster Plate arculating Driving Ught b. Diffracted High Harmonics Circulating Driving Ught EUVGrating/High Reflector Figure 5-2: Bow-tie ring cavities and popular out-coupling schemes for intracavity HHG. a. A sapphire plate is placed in the cavity and Brewster's angle to couple out the generated HHG beam. b. An EUV grating is etched on to a highly reflecting cavity mirror to diffract out the generated high harmonics. light, but diffracts the generated harmonics out of the cavity. This technique avoids the non-linearities of the sapphire plate, but still presents an out-coupling efficiency of only ~ 10%. Finally, some additional work has been done recently using higherorder Hermite-Gaussian modes in bow-tie cavities to allow for small apertures in the cavity mirrors [82, 85, 861. These studies have been restricted to using only several Hermite-Gaussian modes however and have had limited success primarily due to the very small apertures < 100 tm they allow. In the coming chapters, we will describe high-intensity cavities based on BesselGauss beams. We will design and prototype such cavities, and as we will see, Bessel- Gauss intra-cavity modes might allow us to bypass the major hurdles and challenges of cavity-enhanced strong-field physics [76, 77]. These cavities allow for large (> 1 123 CHAPTER 5. ENHANCEMENT CAVITIES FOR HIGH-HARMONIC GENERATION mm) diameter holes in the cavity mirrors as well as centimeter size effective mode diameters on the cavity mirrors. These Bessel-Gauss type cavities might allow for efficient out-coupling as well as increased intensity gain for future cavity-enhanced, high-intensity physics. In the following two chapters, we will first derive the basic properties of Bessel-Gauss beams and develop the tools to work with these beams (Chapter 6). We next will put these developments to use and design Bessel-Gauss cavities for high-intensity applications (Chapter 7). Additionally, we will describe preliminary demonstrations of these cavities as well as highlight the new challenges these Bessel-Gauss designs present (Chapter 7). 124 Chapter 6 Bessel-Gauss beams In this chapter we introduce Bessel-Gauss beams. We begin by deriving the somewhat more familiar Bessel beam and show how the Bessel-Gauss beam-type emerges as a paraxial and physically-realizable approximation to the Bessel beam. Next, we construct Bessel-Gauss beam solutions by superposing familiar Gaussian-like beams. We then describe the focal and far-field properties of Bessel-Gauss beams and illustrate their advantages for strong-field enhancement cavities. Lastly, in preparation for design of such cavities with Bessel-Gauss modes, we analyze how Bessel-Gauss beams transform as they traverse simple optical elements. 6.1 Bessel beams to Bessel-Gauss beams In deriving the Bessel beam, or any optical beam-type, the starting point is the Helmholtz equation (6.1) (V 2 +k 2 ) U(, z) =zO where U(', z) is the usual complex scalar amplitude of the optical beam, and the equation is written in cylindrical coordinates (j', z) = (r, 0, z). Let us look for beamlike solutions to Eq. (6.1) with planar wavefronts, i.e. let us look for solutions of the form UB(-, z) = A (r)eikzz (6.2) Inserting this ansatz into Eq. (6.1), we find that A(f) must satisfy the two-dimensional Helmholtz equation (6.3) (V2 + 2 ) A(-) = 0 where VT = r + + 12 is the Laplacian in polar coordinates, and 125 = k2 - kz. CHAPTER 6. BESSEL-GAUSS BEAMS Eq. (6.3) is of a very familiar form and can readily be solved by separation of variables. The solution takes on the well-known form A = AmJm(/3r)eimO, m = 0, 2, ... 1, (6.4) where Jm(-) is the Bessel function of the first kind and of mth order, and Am is a constant. Considering m = 0, our complex scalar wave amplitude is then UB(r-, Our solution UB(', z) z) (6.5) A 0 J 0 (,8r)eikzz is the well-known Bessel beam [88, 89]. Note that the trans- verse amplitude of the beam takes the form of a familiar Bessel function while the wavefronts of the beam are planar. In other words, the beam does not diffract. This seemingly remarkable result has contributed to the tremendous interest in Besseltype beams. r(, ) However, considering the behavior of IUB AJ2(r) 2 ~ A0/r x cos (8r - 7r/4). So, (, z) 2 for large r, we find UB(rz)I 2 decays for large r like l/r. Therefore, the energy in the Bessel beam, i.e. E - f0 rdrIUB (, z)1 2 , must be infinite. This divergent behavior is readily visible in the k-space distribution of the Besselbeam. In Figure 6-la we have plotted the two-dimensional Fourier transform of UB(', z) = AoJo(Or). In k-space, the Bessel beam corresponds to a singular ring This singular ring implies that the Bessel beam is composed of a superposition of plane-waves with each plane-wave component having its central wavevector directed along the surface of a cone. This plane-wave picture not only suggests the infinite energy content of the Bessel beam, but it also hints at a construction for a physically-realizable Bessel-like beam. Since it is the singular nature of the k-space that leads to the infinite energy demands, let us add some width to the Bessel beam's singular k-space ring. Mathematically, we can convolve a smooth function with the singular ring to provide this width. Convolving with a Gaussian function, we obtain a k-space distribution as illustrated in Figure 6-1b. Convolving with a Gaussian in k-space translates to multiplying by a Gaussian in real space. Therefore the real-space beam corresponding to the 'physical' k-space 'This Fourier transform result follows directly from the integral representation of Jo(r), Jo(r) ~ J0 exp(-irsinO)dO (see Ref. [901 pp. 140). 126 i.e. CHAPTER 6. BESSEL-GAUSS BEAMS distribution illustrated in Figure 6-1b, takes on the following form at the focal plane UBG(iz=O) = UB(F,z = 0) x exp(-r2 /w2) = AoJo(#r) x exp(-r2 /w ) (6.6) where in the above we have used a real-space Gaussian with width wo. This beam type is known as the Bessel-Gauss beam, and it turns out that it is an exact solution to the paraxial Helmholtz equation [91]. The Gaussian windowing function provides for a beam with finite energy that is a physically-realizable approximation to the Bessel beam. Figure 6-1: k-space distribution for a Bessel and a Bessel-Gauss beam. a. The k-space distribution for a Bessel beam at the focal plane z = 0. b. The k-space distribution for a Bessel-Gauss beam at the focal plane z = 0. Unlike the Bessel beam, we expect the Bessel-Gauss beam to diffract. From Eq. (6.6), we see that near the focal plane at z = 0, the optical wave amplitude is peaked near r = 0, i.e. the z-axis or the optical axis. As the beam diffracts, we expect it to spread, and somewhere in the far-field we expect the amplitude will resemble the spatial Fourier transform of the amplitude at the focus. In other words, we expect somewhere in the far-field, for the beam to resemble the k-space distribution near the focus. Since the k-space distribution near the focus takes on the annular shape illustrated in Figure 6-1b, we expect the Bessel-Gauss beam will go from a tightly focused spot to a large annular beam. From this simple analysis we already can see the advantages of Bessel-Gauss beams 127 CHAPTER 6. BESSEL-GAUSS BEAMS for cavity-enhanced high-harmonic generation (HHG). Recall from Chapter 5 that the main requirements for enhancement cavities for HHG were 1. Large mode areas on the cavity mirrors (hence high intensity gains or intensity ratios from cavity focus to mirror surface) and 2. A means to out-couple the collinearly generated high-harmonics. The Bessel-Gauss beam diffracts from a tightly focused spot to a large annulus. As we will see in the coming sections, the area of the annulus is large enough to allow for significant improvement in intensity gain compared to the conventional Gaussian modes of bow-tie enhancement cavities. Additionally, the out-coupling advantages of the Bessel-Gauss beam are obvious; in the far-field the Bessel-Gauss beam will have very little on-axis amplitude, and a large hole could be placed in the cavity mirrors for out-coupling the generated harmonics while not perturbing the intra-cavity Bessel-Gauss mode. 6.2 Constructing Bessel-Gauss beams In the following section we will provide a more rigorous derivation of Bessel-Gauss beams. We will take a constructive approach and build up Bessel-Gauss beams by superposing Gaussian-like beams 2 . The Gaussian-like beams we will superpose are called 'decentered' Gaussian beams, and as we will see, they share many familiar attributes with the Gaussian beam and will provide valuable intuition for BesselGauss-type beams [93]. In the following, we first introduce these decentered Gaussian beams and then use them to construct Bessel-Gauss beams. Decentered Gaussian beams The decentered Gaussian beam is an intuitive generalization of the Gaussian beam. The basic decentered Gaussian beam is illustrated in Figure 6-2. At the focal plane, z = 0, the decentered Gaussian beam in a cylindrical coordinate system (r, z) = (r, 0, z), takes on the form, UdG(', z = 0) a0 exp(-( i?- id1/wo) 2 ) x exp(i/r cos(O - -y)) (6.7) where a 0 is a constant, ia describes the off-center position of the focus, and the modulating plane wave with wavevector of magnitude /3 and direction parallel to Fd provides some tilt to the beam. Note, referencing Figure 6-2, that Td = (rd, Y). In 2 The approach in this section is similar to that followed in prior work. In particular see Refs. [76, 92]. 128 CHAPTER 6. BESSEL-GAUSS BEAMS other words the angle -y in Eq. (6.7) defines the inclination angle of the focal center position with respect to the x-axis (this angle is not labeled in Figure 6-2). 0 Op z I Figure 6-2: Decentered Gaussian beam. At the focal plane z = 0 (shaded), the beam has a Gaussian distribution that is displaced from the origin by r'd = (rd, -y). Away from the focal plane the beam resembles a tilted Gaussian beam, propagating at an angle p to the optical axis, i.e. the z-axis. As illustrated in Figure 6-2, at the focal plane the decentered Gaussian beam, UdG(T, 0, z = 0), resembles a Gaussian beam of waist wo whose central wavevector has a component of magnitude in the transverse plane. Intuitively, it seems that this beam might resemble a Gaussian beam that simply has a displaced focal spot and a tilted direction of propagation. In fact this is exactly correct! If the decentered Gaussian beam of the form above is propagated by means of a Fresnel diffraction integral, we find the following Gaussian-like beam 129 CHAPTER 6. BESSEL-GAUSS BEAMS 2 O exp (_j k(r q(z) 2q(z) udG(r, 0, z) = + 2rrc(z) cos(O rc(z)2 - i - -)) \(6.8) x exp(i3r cos(O - q(z) = qo + z y)) rc(z) = rd + z sin p ; (6.9) In the above, the qo and q(z) terms correspond to the q parameter of the beam decentered Gaussian beam. This parameter transforms just like that of the conventional Gaussian beam. Also, note the parameter rc(z) describes the 'center of mass' of the beam or, essentially, the beam center position as a function of z. Although, Eq. (6.8) can see opaque at first glance, closer inspection reveals that the decentered Gaussian beam very closely resembles a conventional Gaussian beam that propagates with at an angle r to the optical axis. Finally, note that in the above we neglect exclusively z-dependent phase terms; in the following, we will adhere to this convention for simplicity. Bessel-Gauss beams Let us now consider the different decentered Gaussian beams produced as we let -, the inclination angle of r' and # with respect to the x-axis, vary (see Figure 6-3a). In particular, let us first consider these beams to have rd = 0. In this case, we see the central wavevectors of the different decentered Gaussian beams trace out the surface of a cone with semi-aperture angle o. Superposing these different decentered Gaussian beams with variable -y, we obtain dyudG(r, = Ao qoexp q(z) 0, z) r2 ~_kr (z)( 6.10_ i k k(r 2 + r2 (Z)) _ _ _ ) UBG(r, z) = jr CZq 2q(z) q(z) = qo + z ; x JO 8r - rc(z) = z sin o (z) r (6.11) In the above we have used the integral representation of Jo, the zeroth order Bessel function of the first kind (see pp. 140 of Ref. [90]), Ao is a constant, and q(z) and rc(z) are given by the same expressions as before with rd = 0 (Eq. (6.9) and Eq. (6.11) are identical with rd = 0). Looking closely at the form of Eq. (6.10), we see 130 CHAPTER 6. BESSEL-GAUSS BEAMS that we have a beam that at the focus (z = 0) resembles a Gaussian modulating a Bessel function. This is the Bessel-Gauss beam (abbreviated as BG beam from here on). b TY ) ) a V Z Z * I! ~*1~ Figure 6-3: Constructing Bessel-Gauss beams. a. We superpose many decentered Gaussian beams with differing -y. This amounts in superposing many decentered Gaussian beams along the surface of a cone (rd = 0) or a frustum (rd = 0). b. An overlay of the transverse intensity profile after the superposition. Note the annular form of the generalize Bessel-Gauss beam. We can generalize the BG beam by letting rd take on a non-zero value. We now superpose many decentered Gaussian beams with centers lying on a circle of radius rd. This superposition is again schematically illustrated in Figure 6-3a, and a sketch of the resulting transverse intensity profile is overlaid in Figure 6-3b. The central wavevectors of these decentered Gaussians make up the surface of a frustum (i.e. a truncated cone) with semi-aperture angle p. This form of beam is known as the generalized Bessel-Gauss beam (called the gBG beam from here on): (2 + rT2z) X Jo (3 C q(z) = qo + z r (z) Note that Eq. (6.12) is of the form of Eq. (6.10). 131 = Td + z sin p k3r q (z) ) = Ao q) exp (2 q(z) (2q(z) (6.12) ) UgBG(T, z) (6.13) CHAPTER 6. BESSEL-GAUSS BEAMS Although the expressions for UBG and UgBG(r, z), with a Bessel functions of a complex argument, may not easily reveal their essential properties and behaviors, theses beam can intuitively be understood by recalling that they are superpositions of physically-intuitive decentered Gaussian beams. The r - z plane cross-section of a gBG beam, consisting of intersecting decentered Gaussian beams, is illustrated in Figure 6-4a, and the amplitude is plotted for a specific gBG beam in Figure 6-4d. Similarily, the r - z plane cross-section of a BG beam, consisting of intersecting decentered Gaussian beams with rd = 0, is illustrated in Figure 6-4b, and the amplitude is plotted for a specific gBG beam in Figure 6-4e. Note that the BG beam is a special case of the gBG beam. The BG beams is the gBG beam with rd = 0. There is another special case of the gBG beam that is of interest. Consider a gBG beam built with decentered Gaussian components that have $ 0 and o = 0. This is the modified Bessel-Gauss beam (mBG beam from here on) and is a superposition of decentered Gaussian beams lying along the surface of a cylinder with radius rd. The r - Z plane cross-section of a mBG beam is illustrated rd in Figure 6-4c, and the amplitude is plotted for a specific mBG beam in Figure 6-4f. a b Generaized Besse-auis a d Modified Bessel-Gauss C Bessel-Giuss f 2 2 2 1 1 1 2=0 E20 E20 -20 -1--m. -1 -1 5 10 15 20 25 30 z (CM) 35 40 05 10 15 20 z (cm) 25 30 35 40 0 . 5 10 15 20 .- 25 30 35 40 z(cM) Figure 6-4: Types of Bessel-Gauss beams. a.-c. Illustrations of r - z plane cross-sections of gBG, BG, and mBG beams respectively. d.-f. Plots of the amplitude in the r - z plane for gBG (A = 1 pm, wo = 200 pm, W = 0.210, rd = 0.25 mm), BG (A = 1 pm, wo = 200 pm, W = 0.290), and mBG (A = 1 pm, wo = 200 pm, rd = 1 mm) beams respectively. 132 CHAPTER 6. BESSEL-GAUSS BEAMS 6.3 Focal properties of Bessel-Gauss beams Having established some basic intuition for Bessel-Gauss type beams, we now quickly summarize the focal properties of BG beams essential for our purposes. Here we discuss only BG beams as our initial cavity designs in Chapter 7 will consist of BG beams at the foci, and BG beams are sufficient to illustrate our main results. As already described, at the focal plane the BG beam takes the form of a Gaussian component modulating a Bessel function. Looking at the focal plane, from Eq. (6.10), UBG(r, z = 0) = AO exp(-r/w')Jo(3r). An r -0 plane cross-section of the amplitude of a BG beam at its focus is plotted in Figure 6-5a. The peak intensity of a BG beam at its focus, I' can then readily be found3 from Eq. (6.10) with z = 0 2P Ifoc (6.14) In this form the peak intensity of a BG beam resembles the general form of that for a Gaussian beam with effective waist defined as Wfoc = wo exp In the above P is the beam power, of the first kind, and WB I1 1 (6.15) OWB o is the zeroth order modified Bessel function = 2.4/3 is the approximate waist of the Bessel component (i.e. the first zero of Jo(#3r), illustrated in Figure 6-5a). The approximate form of wffl given in Eq. (6.15) follows from inspecting the argument of the Bessel function in Eq. (6.15). Looking at this argument, we see that /32 W2 /4 = /svG) 2 where o //k is the semi-aperture angle of the BG beam (as already described) and OG 27kwo is the divergence angle of the component decentered Gaussian beams. Since we are interested in BG beams that result in an annular (i.e. donut) shape far from the focus, we must have LPG << o, i.e the Gaussian components must diverge slower than their peak intensity axes spread apart. So, for the regime of interest 3 2 W2/4 = ( O/G) 2 >> 1, and the asymptotic expansion of Io (pp. 116 of Ref. [901) yields the approximate form of. As mentioned, far from the focus, the BG beams of interest resemble an annular shape. The amplitude of a BG beam far from the focus is plotted in Figure 6c. The amplitude of the BG beam far from the focus can be approximated as an annulus with Gaussian cross-section, i.e. UBG(r, z) (Bo/Vr~) exp(-(r -- r(z)) 2 /w(z) 2 ) where 3In the following we make use of the integral in Eq. (2.3) of Ref. [91]. 133 CHAPTER 6. BESSEL-GAUSS BEAMS w(z) = N1 + (z/zo) 2 , z >> zo, and Bo is a constant [94]. Using this expression, the peak-intensity of the BG beam far from the focus at position z can be approximated 2P P Z r=7(W 11(Z)) 2 Again, in this form the peak intensity of a BG beam resembles that of a Gaussian beam with effective waist defined as )(z) 2 2- x w(z) x rc(z) (6.17) where rc(z) is as in Eq. (6.11), i.e. the peak-intensity axes of the component decentered Gaussian beams (illustrated in Figure 6-5c), and w(z) is as defined above, i.e. the waist of the component decentered Gaussian beams at z (illustrated in Figure 6-5c). We can now put together a simple expression for the intensity gain of a BG beam. In line with our earlier definitions, we here define the intensity gain of a beam at a position z as the ratio of the peak intensity at the focus to the peak intensity at the position z, so Ig(z) = IOC/IFF(z) where Ig(z) is the intensity gain. As we have emphasized, intensity gain is a parameter of great relevance for highintensity enhancement cavities. For a Gaussian beam, we easily see that IG(z) (z/zo) 2 when z >> zo. Combining Eq. (6.14) and Eq. (6.16) we find '7rw(z)2 /7rw the intensity gain for a BG beam 2 (G where C = 12 2 (6.18) zo 2w/2.4 is a constant. For comparison, we repeat the intensity gain of a Gaussian beam Ig() Recall that for the beams of interest zo >> OG (6.19) since we want annular shapes in the far-field. Comparing the intensity gain expressions in Eq. (6.18) and Eq. (6.19), we see that the BG beam's intensity gain can exceed that of the Gaussian beam by orders of magnitude. In Figure 6-5b, the intensity gain of a Gaussian beam with wo = 30 pm is compared to that of BG beams with Gaussian component wo = 30 pm and semiaperture angles o of 1', 2', 30, and 4'. In Figure 6-5b, the green curves represent exact numerical calculations and the orange curves are based on the approximate 134 CHAPTER 6. BESSEL-GAUSS BEAMS b a 0.5 BG: wo 200 pn, p =.29* =40 10 0.25106 1'1,2wI E 0 -- 30 Exact (Numerical) Approximate (Analytical) V =20 1* 10 -0.25 SC -0.5 0.5 103 (U -A 2 10 - C -0.5 0 0.25 -0.25 x(mm) 10 10 10-1 -21 -2 -1 0 x(mm) 1 10 2 1 0 10 10 2 Z/z7 -- Figure 6-5: BG beam focal properties and intensity gain. a. Plot of amplitude cross-section in the z = 0 plane of a BG beam with A = 1 pim, wo = 200 pm, and semi-aperture angle o = 0.29' (same parameters from BG beam plotted in Figure 6-4e). Cross-section of the focus in the y-direction is on the right with 2 WB labeled. b. Plot of approximate (orange dashed) and exact (solid green) intensity gain of BG beams with A = 1 pm, wo = 30 pm, and semi-aperture angles o of 1', 20, 30, and 40 at distance z. The intensity gain of a Gaussian beam with A = 1 ym and wo = 30 pm (blue curve) is also included. c. Plot of the amplitude cross-section in the z = 20 cm plane of the BG beam from plot a. Cross-section in the y-direction is included on the right with w and r, labeled. form in Eq. (6.17). From Figure 6-5b we see that our approximate expression is very accurate far from the focus (z >> zo). Additionally, we see that for the reasonable parameters plotted, the intensity gain of a BG beam may far exceed that of a normal Gaussian, and therefore, the BG beam may allow cavity geometries with intensity gains far exceeding those of bow-tie Gaussian cavities. 6.4 Bessel-Gauss beams and simple optical elements With some intuition with regards to Bessel-Gauss beams and with a feel for the basic focal properties of these beams, we now move on to consider the transformation of Bessel-Gauss beams by spherical and conical optical elements. Spherical optical 135 CHAPTER 6. BESSEL-GAUSS BEAMS elements are those that impart a quadratic spatial phase to a wavefront e.g. a thin lens or a spherical mirror. Conical optical elements give a linear (i.e. ~ exp(icakr)) spatial phase to wavefronts e.g. transmitting or reflecting axicons. In the following, the importance of these elements in manipulating gBG beams will be discussed. Consider the spatial phase, i.e. the r-dependent phase, of a gBG beam at plane z = L. Denoting this phase by $gBG(r) = #gBG(r) we find (from Eq. (6.12)) ik r 2 + i arg (JO (3r 2R(L) - k (L) rc Y) q(L) (6.20) where we have expanded the Gaussian term in the conventional way so that R(L) L + z2/L. The Gaussian part of the gBG beam gives a quadratic phase while the Bessel part contributes the last-term in Eq. (6.20). For a large class of gBG beams, we can accurately approximate (as shown and discussed in Appendix D and in Ref. [95]) the last term in Eq. (6.20) as OgBG ik 2R(L) T2 + (Lro 2 z # k ik Z=I 1 + (L/zo) 2 r (6.21) Therefore, the spatial phase of the gBG beam is well-approximated as the sum of a quadratic part and a linear part. #con(r) A conical optical element, with spatial phase = -iozkr at z = L, changes the linear part of an incident gBG beam's spatial phase. The overall functional form of this phase remains unchanged however, and to account for the new linear part of the spatial phase, the gBG beam transforms to a new gBG beam with altered parameters (q6, r, /'). From a straightforward calculation we determine these altered parameters; they are included in Eq. (6.22). A spherical element, with spatial phase q5ph(r) = -ikr 2 /2f at z = L, changes the quadratic part of the gBG beam's spatial phase while leaving the overall functional form unchanged. Similarly, a gBG beam transforms after a spherical element into another gBG beam with new parameters (q', r', 0'). This transformation has been previously described in detail [96]. Collecting our results, we find that after conical or spherical optical elements the gBG beam parameters transform as: Conical (Ocon(r) qO = q(L) = -iekr) ; ro = rc(L) 136 ; -k& a= (6.22) CHAPTER 6. BESSEL-GAUSS BEAMS -ikr 2 /2f) Spherical (Obph(r) qO = _ q(L) kreL_ ; -q(L)/f + 1 ) (Lro =rc (L) ; #= L (6.23) The gBG beam, after a conical or spherical element, can then be written (up to a constant phase factor [96]) in the standard form of Eq. (6.12) and Eq. (6.13) with the substitutions qo -* q, ro -- r', # - 13', and where z' = z - L, i.e. z' is the distance to the optical element at z = L. Considering the gBG transformation properties in Eq. (6.22) and Eq. (6.23), we can formulate an intuitive picture of gBG beam propagation through conical and spherical optical elements. Propagation through such elements can be compactly summarized as follows: 1. Through conical optical elements, (a) the Gaussian component i.e. the q parameter of a gBG beam is unaffected; and (b) the peak- intensity axes of the decentered component beams follow the trajectories of meridional rays through the element. 2. Through spherical optical elements, (a) the Gaussian component i.e. the q parameter transforms like that of an on-axis Gaussian beam; and (b) the peak-intensity axes of the decentered Gaussian component beams follow the trajectories of meridional rays. These basic propagation rules are demonstrated and tested through three examples illustrated in Figure 6-6. In the first example (illustrated in Figure 6-6a, b, and c), consider a spherical mirror with radius of curvature R = 20 cm at position z = R = 20 cm and an incident mBG beam of wavelength A = 1 pm, Gaussian component waist wo = 300 pm, and ro = 1 mm (the focal plane is z = R/2 = 10 cm as shown in Figure 6-6b). The mBG beam propagates, reflects from the mirror, and transforms to a new gBG type beam. From Eq. (6.23) and the above discussion, we expect (a) the Gaussian component waist of the new gBG beam to be w' = Af/ rwo = 106 pm (as for an on-axis Gaussian) and (b) the mBG beam to transform into a BG beam with its focus at z = R/2 (meridional rays parallel to the optical axis transform to meridional rays intersecting the optical axis at the focus). In Figure 6-6b we plot an r - z plane cross-section of the numerically simulated amplitude in this scenario and observe the expected behavior. In Figure 6-6c we plot cross-sections in the r direction of the spatial amplitude and phase of the field at the end of propagation and see our numerical (blue) simulation agrees to a high degree of accuracy with our analytical prediction from Eq. (6.12) and Eq. (6.23) (red-dashed). 137 The wave-propagation CHAPTER 6. BESSEL-GAUSS BEAMS software used for numerical simulation will be discussed in the next section. b a C 1 15 0 .8 10 ~0.6 V 5 .4 L0 0 .2 -5 - E C 0 z (cm) d 1 r(mm) r(mm) 30 - .8 0 .6 .-g 2 Numerical Analytilca 20 810 E .4 0 0 .2 0 g Numerical Analtca 1 2-10 1 f -- h 5 10 15 20 z(cm) 15 10 5 0 0 04-10 0 .A0 2 4 01 r (mm) 0 2 r(mm) 4 1 0 1 25 .8 20 - - Numerical Analytical C0 .6 Er-= 810 .4 .2 0 0 zICM) 0 1 r(mm) 2 -5 0 1 r(mm) 2 Figure 6-6: gBG beam transformations. a. Example 1 geometry: an mBG beam reflecting from a curved mirror. b. r - z plane cross-section of numerically simulated amplitude for example 1 (note z-axis corresponds to reflecting geometry). c. r-direction cross-sections of field's spatial amplitude and phase at the end of propagation (numerically simulated (blue) and analytical (red-dashed)). d. Example 2 geometry: an mBG beam reflecting from a reflecting axicon. e and f are as b and c but for example 2. g Example 3 geometry: an mBG beam reflecting from a toroidal optic. h and i are as b and c) but for example 3. For the second example (illustrated in Figure 6-6d, e, and f), the same mBG beam from above propagates through the same geometry and reflects from a reflecting axicon of apex angle a = 0.570. In this example we expect the mBG beam to become a gBG beam (we do not expect the Gaussian waist of the component decentered beams to occur at their intersection point). In Figure 6-6e an r - z plane cross- section of a numerical simulation of the amplitude is plotted, and we observe the 138 CHAPTER 6. BESSEL-GAUSS BEAMS expected behavior. In Figure 6-6f an r direction cross-section of the field's spatial amplitude and phase at the end of propagation are plotted, and our numerical (blue) simulation agrees well with our analytical prediction from Eq. (6.12) and Eq. (6.22) (red-dashed). Finally, the third example (illustrated in Figure 6-6g, h, i) contains a hybrid conical-spherical optic. The optic is a general toroidal optical element i.e. a spherical and a conical element separated by zero distance. The same mBG beam from the prior two examples propagates through the same geometry and reflects from this toroidal element. Recall that a conical optical element adjusts the tilt parameters of a gBG beam while leaving the Gaussian parameters alone (i.e. the conical element affects only the peak-intensity axes of the decentered component beams), and a spherical optical element adjusts all the parameters of a gBG beam. Therefore, by combining a conical and spherical element into a general toroidal optic, the tilt parameters (i.e. ro and /) and Gaussian parameter (i.e. q parameter) of a gBG beam can be independently adjusted by one optical element. Our final example illustrates this as the toroidal element consists of a spherical part of radius of curvature R = 20 cm and a conical part with tilt such that the focus (i.e. the point of intersection for the decentered component beams) will lie at exactly z = 2R/3. In Figure 6-6h an r - z plane cross-section of a numerical simulation of the amplitude is plotted, and again, we observe the expected behavior. Figure 6-6i shows an r direction cross-section of the field's spatial amplitude and phase at the end of propagation, and our numerical (blue) simulation agrees well with our analytical prediction from Eq. (6.22), and Eq. (6.23) (red-dashed). 139 (6.12), Eq. CHAPTER 6. BESSEL-GAUSS BEAMS 140 Chapter 7 Bessel-Gauss beam enhancement cavities In this chapter we build upon the properties of Bessel-Gauss beams derived and discussed in the previous section to analyze Bessel-Gauss beam enhancement cavities. We begin our discussion by considering the overall design principles of Bessel-Gauss beam cavities and how to build such cavities from fundamental Gaussian designs. We then specifically discuss the design of the confocal Bessel-Gauss cavity and possible arrangements for high-harmonic generation applications. Next, we discuss a continuous-wave experimental demonstration of the confocal Bessel-Gauss cavity and highlight the limitations of Bessel-Gauss modes illuminated by this demonstration. Finally, we conclude this chapter with a summary of the work pursued on BesselGauss beams and the outlook for this nascent research field. 7.1 Bessel-Gauss beam cavity design Prior work has explored Bessel-Gauss beam cavities with axicons and flat mirrors [98], axicons and curved mirrors [95, 99], and general phase-conjugating optics [100]; however, this past work has focused on Bessel-Gauss cavities for use as laser resonators. In the following section, we extend this body of work on Bessel-Gauss cavities to enhancement cavities. We outline a different general approach to designing gBG beam cavities, discuss in detail a particular novel gBG cavity i.e. the confocal BG cavity, and comment on future challenges in realizing high-intensity gBG cavities. Consider an enhancement cavity composed of two spherical and two flat mirrors supporting a Gaussian beam solution as illustrated in Figure 7-la. The Gaussian 141 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES beam is re-imaged as it traverses the cavity i.e. q(z + 2L) = q(z) where 2L is the round-trip cavity length. Additionally, for small-angles, the Gaussian beam's peak intensity axis follows that of a ray through the system. a Gaussian Cavity C Bessel-Gauss Cavity Figure 7-1: Gaussian cavities and Bessel-Gauss cavities. a. Illustration of a Gaussian beam enhancement cavity. Note that the harmonics (purple pulse) are generated collinearly with the driving beam. b. The intra-cavity Gaussian mode intensity on the cavity mirrors in the x - y plane. The dashed white circles indicate roughly where two of the cavity mirrors lie. c. Illustration of a BesselGauss enhancement cavity. This cavity is rotationally symmetric about the z-axis (as indicated by the red circle). Also, note that the harmonics propagate along the z-axis. d. Intra-cavity Bessel-Gauss mode intensity on the segmented cavity mirror in the x - y plane. The dashed white circles roughly show the boundaries between the different sections of the segmented mirror. For an enhancement cavity to support a gBG mode, the intra-cavity gBG beam's Gaussian parameter (i.e. q parameter) and tilt parameters (i.e. ro and 3) must repeat after every round-trip. (Recall that the gBG beam's q parameter is associated with the Gaussian properties (e.g. waist) of the component decentered Gaussian beams, and the tilt parameters are associated with the peak-intensity axes of the component decentered beams.) Consider the r - z plane cross-section of our conventional Gaussian cavity. If we revolve this cross-section about its central axis (as illustrated in Figure 7-1b), the tilted flat mirrors become conical optical elements, 142 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES and the spherical mirrors become toroidal optical elements (these elements can be imagined as different sections of one complex, segmented mirror structure as illustrated in Figure 7-1b). Recalling the transformation properties of gBG beams, we see this cylindrically symmetric cavity structure supports a gBG mode that is composed of decentered component beams that closely resemble the Gaussian mode of the conventional Gaussian cavity. This link between conventional Gaussian cavities and Bessel-Gauss cavities is a powerful one. It allows us to directly generate gBG cavity designs from well-known Gaussian ones (albeit the gBG cavities may demand sophisticated mirror structures that are non-trivial to fabricate). In this initial discussion, we restrict our focus to gBG cavities that require only spherical mirrors (in particular, the confocal BG cavity). Before embarking on this discussion, we should mention that a brief description of the cavity mode-solver we will use in the following is included at the end of this chapter. 7.1.1 Confocal Bessel-Gauss cavity In the following we will discuss the confocal cavity and show it supports BG type modes. The confocal cavity is degenerate i.e. every other Hermite-Gaussian mode of the confocal cavity shares the same resonance frequency. These modes can then simultaneously resonate in the cavity and superpose to form different field profiles. To restrict the cavity to operate only in a single BG type mode, we consider patterning the cavity mirrors in an annular (i.e. donut) shape. The annulus is highly reflective (reflectivity RH) and has average radius ravg and thickness Ar (illustrated in Figure 7-2a); the rest of the mirror surface has a low reflectivity (RL). The highly reflective annular pattern yields low-loss to only a single BG mode: the BG mode composed of minimally-divergent decentered Gaussian beams (illustrated in Figure 7-2b). From the cavity center to the mirror surface (a distance of R/2) there exist minimally divergent decentered Gaussian beams. These beams have a waist wo,min = AR/2ir at the cavity center, and Wmin = V/2wo,min at the mirror surfaces. All other decentered Gaussians and higher-order decentered Hermite-Gaussians have a larger waist at the mirror surface. Therefore, if the width of the patterned annulus is chosen to be small enough (i.e. Ar ~ 3w), then only the BG mode composed of decentered Gaussians with waist wo,min will have low-loss. This method of single-mode selection is analogous to inserting an iris in a laser resonator to restrict the output to the fundamental Gaussian mode. The average radius of the annulus determines the tilt angle of each decentered component beam, so for the BG mode, p = tan'(2ravg/R). 143 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES b a Ar least divergent mode RL, low-reflectivity RH, high-reflectivity Figure 7-2: Single-mode selection in the confocal BG cavity. a. Cavity mirror with patterned annular (donut-shaped) region of high-reflectivity. b. Cross-section of patterned cavity mirror with incident beams. Using our cavity mode-solver, we simulate an example patterned-mirror confocal cavity (shown in Figure 7-3). This cavity's patterned mirrors have parameters: ravg = 8 mm, Ar = 3 .1wmin = 1.2 mm, RH = 1, and RL = 0.1. The mirror radius of curvature is R = 50 cm and spacing is L = 49.97 cm. The cavity is simulated at wavelength A = 1 Am. From the r - z plane cross-section plot of the mode amplitude in Figure 4-3a, we see, as expected, the cavity mode resembles a BG beam through one pass of the cavity (through the focus) and transforms at the cavity mirror to a mBG beam for the return trip. In Figure 7-3b and Figure 7-3c, we plot the intensity in the radial direction at the cavity mirror and at the focus, respectively (labeled in Figure 7-3a). From these plots we see our numerical simulation (blue) agrees well with the analytically expected mode (red-dashed). Additionally, normalizing the peak intensity at the cavity mirror, we see the peak intensity at the focus is I = 1.5 x 104 (this is the intensity gain). We also see the effective waist at the focus is we! f = 33 lim. From our mode-solver, we find the loss of the fundamental mode plotted in Figure 7-3 is < 0.0011%, and the loss of the next higher-order mode is > 2.5% (note this is exclusively diffraction-loss as RH = 1). These losses can be fine tuned by adjusting Ar. Additionally, we note that although we simulate a continuous-wave cavity, the patterned mirror confocal cavity supports a wide bandwidth. Simulating the example cavity above at A = 950 nm and A = 1050 nm, we find the fundamental mode has < 0.0015% loss and the next higher-order mode has > 1.7% loss. Finally, we should note for our example cavity L = R; this is due to a non-paraxial propagation effect. For even modest tilt angles (for this cavity, o = tan- 1 (2rag/R)), non-paraxial propagation leads to small spatial phase shifts, and to maintain low-loss modes we must have L = R cos V. 144 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES aM a -10 - Nurnerical - C Analytical Numerical -Analytical 16000 1 14000 12000 ~0.6 E-2 8000 0~ W 0.4 10 20004 010 0.2! 2 100~~ 4C 6 8 0 w6000 4000 . E 2000 10100 20 z (cm) 30 40 6 C r (mm) CLM -0.2 0 0.2 r (mm) Figure 7-3: Patterned-mirror confocal BG cavity simulation. a. r - z plane cross-section of fundamental BG mode amplitude. b. Normalized mode intensity at mirror surface plotted against r (as labeled in a). c. Mode intensity at focus plotted against r (same normalization as b and labeled in a). The example cavity above shows virtually no intensity on the optical axis at the cavity mirrors. With millimeter-sized holes at the centers of the cavity mirrors, the modes are unaffected. The above cavity, which corresponds to a repetition rate of = 300 MHz, provides near-perfect out-coupling for intra-cavity HHG. Additionally, with its high-intensity gain, this cavity may support peak intensities at the focus fR approaching 10" W/cm2 without damage to the cavity mirrors. We can use our ana- lytical understanding of the example cavity above and our mode-solver to see how the properties of the patterned mirror confocal cavity scale as we shift the cavity's geometry. In particular, we are interested in how the intensity gain, Ig, and effective waist, weff, scale with varying repetition rate and ravg. The results of an analytical and numerical scaling are given in Figure 7-4 where we plot I and weff of the simulated example cavity above (red dot) and other numerically simulated cavity geometries (black dots) and the analytical scaling results for I and weff using numerical integration (green) and the approximate expressions from section 2.2 (orange-dashed). From the scaling results, we see that the approximate and exact analytical expressions agree well with each other and with the numerically simulated cavities. All numerically simulated modes have fundamental mode loss < 0.0016% and higherorder mode loss > 2.5%. A limitation of the patterned-mirror confocal BG cavity is also apparent. As the repetition rate grows so does the intensity gain, and so shrinks the effective waist. This is due to the connection between the Gaussian component AR/2ir). For of the BG mode and the repetition rate (connected through wo,min = lower repetition rates, the Gaussian component is large. The intensity gain can still 145 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES a 4b _ 100 o Simulation points 5 - - _ _ __ 120 x 10 o 300 MHz, I = 1.5x10 4 Analytical (Exact) - Analytical (Approx.) o 300 MHz, wr = 33 Am o Simulation points - 80 - Analytical (Exact) Analytical (Approx.) 60 f3 C4 40 2 20 1~ _ 400 200 300 Repetition Rate (MHz) YO 4mm20 00 500 r., 2rm 400 200 300 Repetition Rate (MHz) 500 Figure 7-4: Patterned mirror confocal cavity scaling. a. Intensity gain, Ig, scaling with repetition rate (i.e. cavity length and mirror radius of curvature). b. Effective waist, weff, scaling with repetition rate (i.e. cavity length and mirror radius of curvature). For all cavities in these plots Ar = 3.1Wmin. be made high and the effective waist small by making a very tight Bessel focus (i.e. small WB) by increasing ra,; however non-paraxial effects ultimately limit rayg, and the patterned-mirror confocal BG cavity is likely best suited for higher repetition rates. There are two clear possible future challenges of gBG cavities: stability and mirror surface variations. When considering cavities with only spherical mirrors, the requirements to support a gBG type mode lead directly to the confocal and concentric cavity (both of which, as conventional Gaussian cavities, lie on the stability boundary). Performing a stability analysis with our cavity mode-solver on the example cavity discussed previously, we find that for a range of AL = 50 Am about the cavity length L = 49.97 cm, the fundamental mode loss can be kept < 0.002% while the next higher-order mode loss > 2.4%. This relatively narrow stability regime may make realization of the patterned-mirror confocal cavity challenging. However, we note that gBG type cavities with more sophisticated mirror structures (not restricted to only spherical mirrors) can easily avoid these stability regime boundary issues. The challenges associated with mirror surface variations may prove more difficult to remedy. Consider a cavity geometry supporting a gBG type mode; the mode is composed of decentered Gaussian component beams. The cavity mirrors have some surface variations associated with the manufacturing process. If one localized region of the mirror surface varies e.g. the local radius of curvature, designed to be R, is actually R + AR, then the decentered Gaussian component beam situated in this 146 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES region may not be resonant in the cavity. Across the entire mirror, depending on surface variations, only a subset of the entire family of decentered component beams may resonate and, accordingly, the entire gBG beam may not resonate. This problem is associated with azimuthal degeneracy. Returning to our derivation of gBG beams in Chapter 6, if we vary the amplitudes of the component decentered Gaussian beams as we superpose them, we can produce azimuthal modulation in the final gBG beam and a higher-order (azimuthal) gBG beam [94]. Returning to our general Bessel- Gauss cavity design strategy, we see that such higher-order azimuthal gBG beams are also modes of gBG cavities. Therefore, mirror surface variations in a gBG cavity may prefer a particular higher-order azimuthalgBG beam (or superposition of such beams) over the fundamental mode. Issues and restrictions associated with mirror surface variations will be exposed in the subsequent section. 7.2 Confocal Bessel-Gauss cavity demonstration As described in the previous section, the confocal Bessel-Gauss cavity consists of two mirrors with radii of curvature R, separated by a distance L = R. We outlined a procedure to isolate a single radial cavity mode in the previous section by patterning the cavity mirrors to consist of a highly reflective ring-shaped pattern (reflectance RH) and a low reflectivity (reflectance RL) background region (see Figure 7-2a and 7-5a). To reiterate, the ring-shaped patterns act as effective apertures and provide low-loss to only a single, fundamental cavity mode. This fundamental mode of the cavity resembles a BG beam as it traverses the focus and a mBG beam on its return trip (see Figure 7-3a). Our confocal Bessel-Gauss demonstration cavity operates at A = 633 nm, and the cavity mirrors have a radius of curvature R = 15 cm. The patterned rings have average radius ravg 1.3 mm and thickness Aric = 534 um (input coupler mirror) and Arc = 440 pm (output coupler mirror). The cavity mirrors were fabricated via a photolithography/lift-off process in which a 15 nm thick Cr layer was deposited on the surface of a dielectric mirror with reflectance RH = 99.1%. The Cr layer coats the entire mirror surface except for the desired ring-shaped pattern; the pattern edge roughness is < 1 pm. The thin Cr layer interrupts the operation of the dielectric mirror such that the reflectance outside the ring patterns is RL ~ 30%. Simulations of the cavity geometry predict a finesse of ~ 288 for the fundamental BG/mBG mode. Coupling to the cavity is performed via an axicon-based imaging system (see Figure 7-6). The output of a HeNe laser is transformed through an axicon into a 147 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES a RL, low-reflectivity RH, high-reflectivity Figure 7-5: Confocal Bessel-Gauss cavity mirrors a. Illustration of patterned cavity mirror with intra-cavity mode intensity overlaid (not to scale). Inset is a microscope image of a section of a patterned mirror used in the experiment. b. Photograph of actual patterned cavity mirror in the experimental setup. BG-like beam. This beam is imaged through a 4f imaging system and sent into the confocal Bessel-Gauss cavity. Behind the cavity back mirror, the cavity outputcoupling mirror, a pellicle is placed to sample the transmitted intra-cavity mode. The transmitted mode sampled by the pellicle is imaged on a CCD camera. The main results of this imaging are included in Figure 7-7. The fraction of the mode that is not sampled by the pellicle is focused onto a photodiode and used for observing the cavity transmission peaks and locking the cavity via a dither lock. In Figure 7-7a, we see that when the cavity is slightly misaligned and the cavity length is swept back and forth over the main resonance, i.e. the main transmission peak, the cavity mode takes on an odd shape and the measured finesse is ~ 300, near the expected finesse of the cavity. Recalling that a BG/mBG beam is a superposition of decentered Gaussian (dG) beams, the odd mode shape corresponds to only a subset of the dG component beams being well-aligned and resonant. We should also note that we only coarsely measure the finesse as the ratio of the free-spectral range to the full-width at half maximum of the transmission peak recorded on the photodiode. As the cavity is tuned to an aligned state (Figure 7-7b), more dG component beams become aligned, and the fundamental mode appears; however, the transmission peak is broadened (and takes on a multi-peaked structure), and the finesse drops to 40. When the cavity is then locked (Figure 7-7c), the mode profile changes from the fundamental BG/mBG mode to a ring-shaped mode with some azimuthal variation. These experimental results can be explained by small surface variations in the cavity mirrors. Consider a region of the mirror surface in which the local radius of curvature, Riocai, is perturbed, Riocal = R + JR. The dG component occupying this 148 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES a Locking Electronics HeNe source 4f imaging 0 b i- 21A cm - 20.7 cm----- 40 cm- 13.6 i Patterned mirror confocal cavity E %E 2 4 0 80 60 40 20 100 z(cm) Figure 7-6: Confocal Bessel-Gauss prototype cavity. a. Experimental arrangement (sampling pellicle and CCD not shown). The photodiode signal is used to lock the cavity (input-coupling mirror is actuated with a piezo). b. Simulated field (r - z plane cross-section) traversing the coupling optics/cavity system. region will have a slightly shifted resonant frequency. With many perturbed regions, we expect the transmission peak to broaden and take on a multi-peaked structure, as observed. Additionally, when locked, we expect the cavity mode to no longer resemble the fundamental BG/mBG mode, but to include some azimuthal variation as only a subset of the dG component beams will be resonant at the lock point. Quantitatively, we can estimate the impact of mirror surface variations by a simple analysis. The resonant frequency, v, of the TEMmn mode, i.e. the m, n HermiteGaussian mode, of a two mirror symmetric cavity with mirror curvature R and spacing L can be written (pp. 762 of Ref. [971) v=ovF q M COs'(1 - LIR) (7.1) where vF is the free-spectral range of the cavity and q is the longitudinal mode number. Evaluating the derivative of Eq. (7.1) with respect to R at the confocal spacing L = R, we find _-L/F (mrn r1) 7r 149 ( __R R )=x-- (7.2) CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES Figure 7-7: Images of the transmitted cavity mode. Images are normalized and taken when the cavity is a. misaligned and the cavity length is swept (the dashed ring is added for ease of illustration), b. well-aligned and the cavity length is swept c. locked from a well-aligned state. where we have used the notation 6v (6R) to refer to the infinitesimal variation in v (R). This expression gives an estimate for the shift in the resonant frequency of the TEMmn mode when there is a small shift in the cavity mirror curvature. Now consider the intra-cavity BG/mBG mode of the confocal Bessel-Gauss cavity as a superposition of TEM,,. modes. At the mirror surfaces, the radial extent of the intra-cavity BG/mBG mode is ~~ravg; the radial extent of a TEMmn mode is w V/m + n where w is the Gaussian spot-size of the mode (pp. 691 of Ref. [97]). We therefore expect the largest value of m + n in the superposition to be ~ (rav,/w)2 (note that here w is also the spot-size of the intra-cavity BG/mBG mode's component dG beams and is directly related to Ar). In the presence of a small shift in the mode composing the superposed intra- cavity mirror curvature, 6r, each TEM.U cavity BG/mBG mode suffers a different resonant frequency shift with the maximum shift given by S6lV m ax I= $ Wr W x (-) R (7.3) We thus expect the resonance peak of the intra-cavity BG/mBG mode to broaden, and we can identify the quantity Feff = vF/2IvimaxI as the effective finesse of this new resonance, broadened due to curvature variations throughout the mirror surface. We can then write a simple expression for the effective finesse Feff ~ 2 ((raVg/w) 2 x (6R/R)) 150 (7.4) CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES The validity of Eq. (7.4) is demonstrated numerically in Figure 7-8. The simulated points in Figure 7-8 follow from numerically solving for the cavity mode of our cavity geometry with mirrors of curvature R + SR and differing values of rav,/w. The simulations agree very well with our simple analysis. We can also compare this simple model to our experimental results. The mirrors used in the experiment were specified to have A/10 surface quality, so the height difference from the center of the mirror to the mirror edge, h, should not vary around the mirror's edge by more than ~ A/10 ~ 63 nm. Letting h' = h + Jh with Jh = 63 nm (Figure 7-8), and finding the radius of curvature R' = R+JR, associated with this height difference from the mirror center to the mirror edge, we see that for our mirrors we can roughly estimate 6R/R ~ 0.05%. These curvature variations predict a finesse in our cavity of ~ 55.7, relatively close to the value of ~ 40 that we experimentally observe. 4 10 - LA Analytical Result 0 Simulation Points rIW-R=7.47(exp.) ...... S10 h+6h > 10 o 0.0's Finesse=.5S.7 .2 10 1 101 w lr Figure 7-8: Effective finesse in the presence of curvature variations. The solid line (green) is the analytical model i.e. Eq. (7.4). The dots (black) represent simulation results. The dashed line (red) shows the value of r,,,g/w used in the experiment. The inset illustrates the simple model for estimating curvature variations. In the preceding analysis and discussion, we have seen that cavity mirror surface variations can dramatically affect the finesse of the confocal Bessel-Gauss cavity. Returning to the decentered Gaussian beam picture, in order to maintain the fundamental BG/mBG mode, we must ensure that the resonance frequency shifts of 151 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES the differing dG component beams are small compared to the width of the cavity's natural resonance. In other words, the broadening of the cavity resonance associated with losses due to the imperfect mirror reflectivity should far exceed any broadening associated with mirror surface variations i.e. the reflectivity-limited finesse must be much less than the surface-variation-limited effective finesse. This criterion was not met for our experiment: the reflectivity-limited finesse is - 300 while the surface- variation-limited effective finesse is ~ 40; and clearly, the fundamental BG/mBG mode was not maintained. Referring to Figure 7-8, we see this criterion may pose a strict requirement on high-intensity Bessel-Gauss enhancement cavities as small fractional curvature variations and relatively small values of ravg/w yield low effective finesses i.e. significantly broadened resonances. For future applications involving high-intensity Bessel-Gauss cavities, extremely precise mirror surfaces may be necessary. Additionally, cavity designs beyond the confocal Bessel-Gauss cavity that may be less sensitive to curvature variation issues are a possibility. As a final note, we mention that although we have primarily used the dG beam picture to understand the confocal Bessel-Gauss cavity, an equivalent picture can be formulated in terms of higher-order azimuthal Bessel-Gauss beams [92]. The challenges associated with mirror surface variations can then be connected to azimuthal mode degeneracy in the confocal Bessel-Gauss cavity. In conclusion, we have reported an experimental demonstration of a continuouswave confocal Bessel-Gauss cavity. We have highlighted mirror surface variations as the major challenge associated with scaling the confocal Bessel-Gauss cavity to highintensity applications and provided a simple analytical model for understanding this effect. Cavity mode-solver Our cavity mode solver is based on the scattering matrix method for optical systems and is designed for cylindrically symmetric cavity geometries [104]. Cylindrically symmetric cavity modes are represented as N-dimensional column vectors (the radial coordinate is discretized into N points). Each optical element composing the cavity, including lengths of dielectric or vacuum, is described by a 2N x 2N scattering matrix. (Scattering matrices for optical systems are generally 2 x 2 matrices relating incoming waves to outgoing ones [104, 103]; here, each radial point has its own scattering matrix and lumping all the points together, we represent each element as a 2N x 2N scattering matrix). Lengths of dielectric or vacuum have block diagonal scattering 152 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES matrices where each block is a matrix describing propagation. Using the exact matrix representation of the quasi-discrete Hankel transform (denoted here as F) [102, 101], each propagation block can be written as where A is the wavelength, k is the wavevector, v is the spatial frequency, and z is the propagation length. Propagation amounts to transforming the wavefront to the spatial frequency domain, weighting each spatial frequency by the correct phase factor for propagation, and transforming back to the spatial domain (the matrices PA, were used for propagation in the simulations). After forming scattering matrices for each individual cavity component, these matrices can be composed to form a scattering matrix of the complete cavity system [1041. The entire cavity can then be represented by a single 2N x 2N dimensional matrix. The cavity modes correspond to the eigenvectors of this matrix and can be found by any standard numerical eigenvalue solver. An obvious advantage of our mode solver is the ability to immediately solve for all the higher order modes of a cavity system. This does come with the disadvantage of having to store and manipulate a possibly large 2N x 2N matrix; for all simulations in this thesis however, the modes were solved for on a desktop computer with a radial step-size of < 1 pm in a matter of minutes. 153 CHAPTER 7. BESSEL-GAUSS BEAM ENHANCEMENT CAVITIES 154 Appendix A Pulse trains in the time and frequency domains In this appendix we review some of the basic properties of optical pulse trains in In particular, we focus on the properties of the the time and frequency domains. carrier-envelope offset phase (CEP) and the carrier-envelope offset phase frequency fCEO- In Chapter 1, we defined the CEP of an optical pulse as the phase offset between the carrier wave maximum and the optical pulse envelope. We described how the CEP of consecutive pulses in a pulse train shift by some fixed amount Ap (in the absence of noise). We defined the carrier-envelope phase offset frequency, fCEO, as the rate at which the CEP changed. More specifically JCEO = As in Chapter 1, in the above, fR 27 (A.1) X fR is the pulse repetition rate. Recalling that our optical pulse train can be described as a train of pulse envelopes multiplying a carrier wave, we can think of the CEP as arising from the mismatch between the carrier wave frequency, f, fe, and the repetition rate frequency, fR (think of the scenario when = nfR; in this case o = 0). In this picture we can then write Ap = (TR In the above, TR TR = mod Tc) x 1/fR and T, = 1/f,. Note that we can write (A.2) TR - nTc where n is the integer value such that nT is closest to TR. consider f, mod fR. We can write f, mod 155 fR mod T= Now let us = (TR - nTc)(TRTc) with n defined APPENDIX A. PULSE TRAINS IN THE TIME AND FREQUENCY DOMAINS as above. Therefore, we must have f, mod fR = (TR mod Tc) x fR/T. Plugging this into Eq. (A.2) and subsequently plugging into Eq. (A.1), we find fCEO = f, mod (A.3) fR With this simple development, we see a direct relationship between the fCEO and the frequency domain picture of the pulse train. This relationship is emphasized in Figure A-1 in which we sketch the connection between the time and frequency domain pictures of an optical pulse train. F I Optical pulse train - Time domain TA 1. In the time domain, the optical pulse train resembles an array of regularly spaced pulses where each pulse can be described as a carrier-wave modulated by a pulse envelope. 2. We can decompose the pulse train into a train of pulse envelopes (black) x multiplied by a carrier wave (orange). II 3. P(t) decomposed into a pulse envelope function P(t) convolved with a train of delta functions (green). X A* 1 The pulse envelope train can be further t Time domain ............ .... ------------.. .... ------------------------------... Frequency domain f -0 |ll & IA ~ spacing 1/T = fR). The carrier wave becomes a delta function at carrier frequency f, and the multiplications and convolutions exchange places. f ) XI 5. Optical pulse train - Frequency domain . nf+fcro .. fi.t Moving to the frequency domain, P(t) transforms to a broad spectrum P(q) (blue). The delta-function train transforms into another delta function train (with * (P 4. --------. ------------- f Carrying out the above operations, we find that the frequency domain representation of the optical pulse train is a broad spectrum modulating a delta function comb. The center of the spectrum is f, the comb spacing isfa, and each line in the frequency comb can be represented as nfR + fao where fco= f, modfR. Figure A-1: An optical pulse train in the time and frequency domains. In the above, we proceed step by step from the time domain to the frequency domain. As we mentioned, in the absence of noise, A& is constant, and so fCEO is fixed. 156 APPENDIX A. PULSE TRAINS IN THE TIME AND FREQUENCY DOMAINS However, for any real ultrafast laser system perturbations will lead to drifts in Ap and fCEO. For many applications, our experiments included, it is important to have a fixed, measurable fCEO. The most common method to measure the fCEO for feedback stabilization is via f-2f interferometery. The basic operation of an f-2f interferometer is illustrated in Figure A-2. The basic concept is to frequency double a low frequency component of the optical pulse train and mix this with a high frequency component. This frequency doubling and mixing ultimately produces a beat note at the fCEO. Note that a critical requirement of an f-2f interferometer is for at least an octave of optical bandwidth (that is an f and 2f component must be present in the spectrum). fR nflR+fCEO SHG 2nfA+ 2 fCEo -- +fCEO Figure A-2: The basic f-2f interferometer. In the basic f-2f interferometer a low frequency component from the spectrum is frequency doubled via secondharmonic generation (SHG) and mixed with a high frequency component. The mixing process yields a beat-note at the fCEo- 157 APPENDIX A. PULSE TRAINS IN THE TIME AND FREQUENCY DOMAINS 158 Appendix B Evolution operator basics In this appendix we review the basics of the evolution operator in non-relativistic quantum mechanics. We formulate a perturbative expansion for the evolution op- erator and discuss this operator in the interaction picture. We define the evolution operator U(t, to) as an operator that evolves an initial state at time t o to its form at time t. ) = U(t, to) 0(to)) (B.1) Considering the above definition, the evolution operator has several immediately obvious properties U(t, to) = 1 (for t = to) (B.2) = U(tt1)U(ti, to) (B.3) = U-I(to, t) = Ut (to, t) (B.4) The last property (unitarity) follows from conservation of probability. Inserting Eq. (B.1) into the time-dependent Schr6dinger equation with Hamiltonian H(t), we find ih U(t, to) = H(t)U(t, to) (B.5) Integrating this equation, we can move to an integral equation for the evolution operator U(t, to) = 1 - dt'H(t')U(t', to) 159 (B.6) APPENDIX B. EVOLUTION OPERATOR BASICS U(t, o) = 1 - - dt'U(t, t')H(t') (B.7) The second equation above follows from taking the Hermitian conjugate of the first, applying the properties in Eq. (B.4), and swapping t and to. Repeatedly substituting U(t', to) on the right-hand side of Eq. (B.6) with the full form of Eq. (B.6), we can find an iterative expression for the evolution operator U(t, to) = 1 - i ] t 2 ( dt'H(t') + )dt' t dt"H(t')H(t") + (B.8) The above perturbative expansion for the evolution operator U(t, to) is the well-known Dyson series. In this thesis we work with Hamiltonians that can be separated into well-understood constant portions and time-varying parts. We can write the general form of these Hamiltonians as H = HO + Hint(t) We work with these Hamiltonians in the 'interaction picture'. (B.9) In the interaction picture, we separate the influence of Ho and Hint on the initial state. We define the interaction picture state as 1|1,(0)) = Uo (tI to) 10(M))(.) = exp (iHo(t - to)/h) 4'(t)) (B.11) In the above, we make use of Uo, the evolution operator for the time-independent - portion of the Hamiltonian, Ho. It can easily be seen that Uo(t, to) = exp (iHo(t to)/h). Now plugging Eq. (B.11) into the time-dependent Schr6dinger equation, we find (t) (t) wh iIwuse (B. 12) In the above, we have made use of Hi'nt(t) which we define as 160 APPENDIX B. EVOLUTION OPERATOR BASICS Hit(t) = exp (iHo(t = Uot(t, to)Hint(t)Uo(t, to) - to)/h)Hint(t) exp (- iHo(t - to)/h) (B.13) (B.14) In a parallel with our earlier developments, we can also define a time evolution operator in the interaction picture. We define this operator as (B.15) ) =U 1J 1(t, to) [|41 (to)) Similar to the normal evolution operator, this operator evolves interaction picture states from time t Inserting the definition in Eq. o to time t. (B.15) into the Schr6dinger equation, we find a at ih U(t, to) = Hit(t)U1 (t, to) (B.16) As before, we can integrate this differential equation and convert it into integral form -t U,(t, to) 1 - U1 (t, to) 1- i - I dt'Hit(t')U1 (t' to) (B.17) j dt'U1 (t, t')Hit (t') (B.18) hto hto Again, the second equation above follows from taking the Hermitian conjugate of the first, applying the properties in Eq. (B.4), and swapping the t and to variables. Let us now express the total evolution operator, U(t, to), in terms of the interaction picture evolution operator, U1 (t, to), and the evolution operator for the timeindependent part of the Hamiltonian, Uo(t, to). First, note that 110,(W) = Uil (t0t) |10A(0)) = U(t, to) '?7(to)) (B. 19) (B.20) The second equation above follows since |@b(to)) = JV(to)) from Eq. (B.10). Additionally, note that from the definition of the interaction picture state, we also have 161 APPENDIX B. EVOLUTION OPERATOR BASICS I () =U0t (t, to) 0(t)) (B.21) - = U1(t, to)U(t, to) 4(to)) (B.22) Combining Eq. (B.20) and Eq. (B.22), we then find that U(t, to) = Uo(t, to)U, (t, to) (B.23) With this relationship between the different evolution operators and with Eq. (B. 17) and Eq. (B.18), we can obtain two integral expressions for the total time-evolution operator U(tto) = Uo (t, to) - dt'U(tt')Hint(t')U(t' to) (B.24) U(t,to) = Uo(t, to) - i dt'U(t, t')IHint(t')Uo(t', to) (B.25) Now let us consider a situation in which a system starts in state 16). Under the action of the time-independent part of the Hamiltonian, Ho, this initial state evolves to 10(t). However, under the action of the complete Hamiltonian (including Ho and Hint), this state evolves to 1,0(t)). For this general system, we can write an expression for |/(t)) from Eq. (B.25). We find - t We make use of this expression in Chapter 2 (also note an complimentary expression can be found from Eq. (B.24)). Lastly, we should note that if we iteratively solve Eq. (B.17), we can generate a perturbative expansion for the evolution operator in the interaction picture (this directly parallels our development of Eq. (B.8)). If we employ the relations (B.14) and (B.23), we then find 0 U(t, t1) - ftdt'U0 (t, t')Hint W) ht + = " U (t, t') tdtl 2 I t'dt" Uo (t, t')H in (t') UO (t', t") H in(t") -+ 162 . (B. 27) APPENDIX B. EVOLUTION OPERATOR BASICS This perturbative expansion for the total evolution operator is used extensively in our calculations in Chapter 2. 163 APPENDIX B. EVOLUTION OPERATOR BASICS 164 Appendix C Volkov waves a at i'h/, = F ) In the following we derive the Volkov wave solutions to the Schr6dinger equation with the 'free-field' Hamiltonian, HF. Recall that HF consists only of the kinetic part of the Hamiltonian and the potential associated with an electromagnetic field. We look for solutions to this equation then with the Hamiltonian (f + eA (t)) 21) = (C.1) In the above, as usual, A(t) is the vector potential. Not that we have written HF in the velocity gauge i.e. with the electrostatic potential equal to zero, (p = 0. In this gauge we can solve Eq. (C.1) with a wavefunction of the form 79/L(x, t) = exp(iqx/h)#(t) (C.2) Inserting Ov"(x, t) into Eq. (C.1), we find do S = 1 2m diet (q + eA(t))2 #(t) (C.3) This equation can then be directly integrated, and we find qvi(x, t) = exp ((iqx - iS(t)) /h) (C.4) In the above, we have used the quantity S(t) which we define as S(t) = J (q + eA(t')) 2 dt' 165 (C.5) APPENDIX C. VOLKOV WAVES Note that in the above S(t) closely resembles the action of the electron wiggling in the laser field. Additionally, in the above we have used the superscript V to denote that this is a 'Volkov' wave solution, and we have used the superscript V to denote that we are working in the velocity gauge. Additionally, the subscript q denotes the momentum of the wave. In our calculations we make use of, not the velocity gauge Volkov wave, but the length gauge version. We now convert ov(x, t) to its length gauge counterpart 2bv(x, t). Recall the gauge transformation rules for electromagnetic potentials = '= A' - VA(x, t) (C.6) + -tA(x, t) (C.7) In the above p denotes the electrostatic potential. To transform from the velocity gauge (o = 0) to the length gauge (A = 0), the function A = - A is required. For our simple one-dimensional case, this function takes the form A(x, t) = xA(t) (C.8) Now let us consider the transformation of a wavefunction under a gauge transformation. Considering the Hamiltonian for an electron in an electromagnetic field given with potentials (p, A), we find that when the potentials transform to (p', A') as given by Eq. (C.6) and Eq. (C.7), the wavefunction transforms as <'(x, t) = exp (ieA(x, t)/h) >'(x, t) (C.9) This can easily be confirmed via direct substitution. Using this result, we can transform 04v(x, [) to the length gauge. We find that the length gauge form of the Volkov wave of momentum q is given by 04(x, t) = exp (ieA(x, t)/h)/'(x, t) (C.10) = exp (iexA(t))44'"(x, t) (C.11) - exp (i((q+eA(t))x - S(t))/h) (C.12) Lastly we should note that we can rewrite the length gauge Volkov wave in ket 166 APPENDIX C. VOLKOV WAVES notation as q q + eA(t)) exp (- iS(t)/h) (C.13) Where in the above Iq + eA(t)) is the momentum eigenstate with eigenvalue q +-eA(t). In other words, (xIq + eA(t)) = exp (i(q + eA(t))x/h). 167 APPENDIX C. VOLKOV WAVES 168 Appendix D Bessel-Gauss beam spatial phase In this short appendix, we show that the spatial phase of a large class of generalized Bessel-Gauss (gBG) beams can accurately be represented as the sum of a quadratic component and a linear component. More specifically, we show that the approximate form of Eq. (6.20) provided in Eq. (6.21) is reasonable. We should note that a similar approximation has previously been used for Bessel-Gauss (BG) beams [95]. First, we write the second term in Eq. (6.20) as arg (JO ( arg(Jo(u + iv)) -_k-rc( ) (D.1) where u and v are given by kr 3r = 1 + (L/zo) 2 1 + (L/zo) or 1 + (L /zo) (L 2 2 L zo ) zo + (D.2) ZO kr I (rd) (rd'\ (L/zo) 2 zo (D.3) The relation rc(L) = rd+ L sin p = rd + (t/k)L has been used in the above (from Eq. (6.13)). Returning to Eq. (6.23), with Iu + ivl >> 1, we can use the asymptotic form of the Bessel function (pp. 114 of Ref. [90]), and we find arg(Jo(u + iv)) arg(cos(u+ iv -7r/4) - tan-- (tan(u - 7r/4) tanh v) -u+7r/4 1/k zo 169 1 + (L/zo) 2 +4 (D.4) APPENDIX D. BESSEL-GAUSS BEAM SPATIAL PHASE The last approximation is very accurate when jvj > 3 (tanh(3) ~ .995). Therefore, when jvt >> 1, Eq. (6.27) is an accurate approximation. Inspecting Eq. 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