Emre 3-16_Layout 1 2/11/16 4:01 PM Page 77 WELDING RESEARCH SUPPLEMENT TO THE WELDING JOURNAL, MARCH 2016 Sponsored by the American Welding Society and the Welding Research Council Resistance Spot Weldability of Deformed TRIP800 Steel Various parameters were investigated for obtaining optimum tensile shear strength, weld button geometry, and electrode indentation BY H. E. EMRE AND R. KAÇAR ABSTRACT In order to simulate automotive manufacturing conditions, the spot weldability of cold­deformed, in tension by 10%, TRIP800 steels was investigated in this study. Tensile shear strength and failure mode associated with button geometry and electrode indenta­ tions were also evaluated, and weld lobe was drawn for resistance spot­welded de­ formed TRIP800 steel. The microstructure of the weldment was evaluated and the hard­ ness profile of the weldment was also determined. It was found that the properties of the weldment are directly related to parameters used for the process and deformation of base metal prior to welding. It was found that the button diameter and button size ratio of deformed TRIP800 steel spot welds should be at least 4√t and 0.14–0.30, respectively, for pullout failure mode, acceptable shear strength, and surface quality. KEYWORDS • Resistance Spot Weld • Cold Deformation • Welding Parameters • Weld Lobe Diagram Introduction Transformation-induced plasticity steel (TRIP) is an advanced highstrength steel (AHSS). It has been applied widely in the automotive industry to reduce weight and improve vehicle safety (Refs. 1–3). Its structure usually consists of bainite, martensite, and retained austenite embedded in a continuous soft ferrite matrix (Refs. 4–8). Decomposition of the austenite phase into martensite during plastic deformation improves ductility (Refs. 3, 8–11). This phenomenon involves formation of strain-induced martensite by deformation of metastable austenite and leads to an increase of strength, ductility, and toughness of the steel (Refs. 12, 13). Among the welding methods used in the automotive industry, resistance spot welding is the most widely used joining technology for manufacturing auto body structures. In practical applications, steels are frequently subjected to deformation prior to welding. As mentioned earlier, during plastic deformation and straining, the retained austenite phase is also transformed into martensite in TRIP steel. High elongation values of the TRIP steels are explained by the interactions of the deformation and phase transformation mechanisms during straining of the material (Ref. 4). The effectiveness of the deformation can be reduced significantly during welding in the heat-affected zone (HAZ), where the peak temperatures are too low to cause melting but high enough to cause a change in the microstructure and properties of the materials (Ref. 14). The mechanical properties of the cold-deformed TRIP steels can be also affected by the phase transformations associated with the thermal cycle during welding. An extensive literature survey found no study about spot weldability of colddeformed TRIP steel. In order to simulate automotive manufacturing conditions, the spot weldability of deformed TRIP800 steel was investigated in detail. For this purpose, the tensile shear strength, weld button geometry, and electrode indentation were determined for a quality assessment of the weldment and obtained weld lobe diagram. The results were compared with the weldability of as-received welded TRIP800 samples that were published elsewhere (Ref. 15). The hardness profile and structure of the weldment were also evaluated for optimization of the welding parameters. Experimental Method Materials and Welding Processes The chemical composition of TRIP800 steel sheet in 1.5 mm thickness is given in Table 1. The deformation in tension by 10% was carried out by using a Shimadzu-type tensile test machine with a cross-head speed of 5 mm/min. Test samples were spot welded in a pneumatic, phase-shift controlled AC spot welding machine with 60 kVA capacity in 50 Hz electrical circuit. Spherical tip electrodes (CuCrZr) having 5.5 mm diameter were used. The welding schedule applied in the experiment is H. E. EMRE (hayriyeertek@karabuk.edu.tr) and R. KAÇAR are with the Department of Manufacturing Engineering, Karabük University, Karabük, Turkey. MARCH 2016 / WELDING JOURNAL 77-s Emre 3-16_Layout 1 2/11/16 4:01 PM Page 78 WELDING RESEARCH Table 1 — Chemical Composition of TRIP800 Steel (wt­%) Elements C Si Mn P S Cr Mo Al Fe TRIP800 0.2 1.66 1.69 0.015 0.0002 0.006 0.011 0.43 Balance Table 2 — Welding Parameters Welding Current (kA) Welding Time (cycles) Force (kN) Squeeze Time (cycles) Hold Time (cycles) 1 3 5 6 7 8 9 10 5 10 15 20 25 6 15 15 ton diameter (dn), button height (hn), and electrode indentation depth (ei) — was measured on the metallographic cross section of the weldment. The common criterion for the average weld button diameter should be equal to or larger than 4√t (t: material thickness in mm) for desired pullout failure (PF) mode for steels. However, there is no information on average weld button diameter, weld button height, and weld button size ratio (hn/dn) for colddeformed and welded samples for producing the desired PF mode. Note: 1 cycle = 0.02 s Results A B Effect of Deformation on the Structure of Weldment C D E Fig. 1 — Microstructure of TRIP800 steel. A — As­received base metal; B — cold­ deformed base metal; C — SEM microstructure of as­received TRIP800 steel; D — SEM microstructure of cold­deformed base metal; E — SEM microstructure of cold­deformed base metal at high magnification (M: martensite, A: austenite, : ferrite, b: bainite). given in Table 2. Mechanical Test and Metallographic Evaluation All the welded joints were exposed to a tensile-shear test for determining joint strength. For this purpose, five test samples were prepared for each weld variable. Samples were tested with a crosshead speed of 10 mm/min. A sample was cross sectioned through the center of the button, mounted, ground, polished, and then etched for 5 s with 2% nital. The weldment structure was evaluated by optical and scanning electron microscope (SEM). The hardness measurements were carried out by using a Shimadzu microhardness tester with a load of 500 g. Weld Button Geometry Evaluation The weld button geometry — but- 78-s WELDING JOURNAL / MARCH 2016, VOL. 95 The microstructure of the asreceived TRIP800 steel contains bainite, martensite, and retained austenite phases embedded in a continuous ferrite matrix, as seen in Fig. 1A and C. The microstructure of the asreceived samples was taken from the vertical cross section in the rolling direction. However, the cold-deformed samples exhibited elongated grains along the strain direction, as seen in Fig. 1B. Most of the retained austenite in the structure was transformed into martensite (Fig. 1D) due to cold deformation process. A small amount of retained austenite grains were observed in the structure, only under high magnification — Fig. 1E. The as-received and cold-deformed TRIP steels were also analyzed by using x-ray diffractometer (XRD) to clarify the present phases in the structure — Fig. 2. As-received TRIP800 steel analysis revealed peaks for austenite, ferrite, and martensite, which are the main constituents also observed using metallographic examinations. However, deformed sample analysis revealed peaks for ferrite and martensite. The XRD result for cold-deformed TRIP800 steel indicated no evidence of austenite peaks, hence, it is thought that the majority of retained austenite Emre 3-16_Layout 1 2/11/16 4:01 PM Page 79 WELDING RESEARCH A A B C Fig. 3 — Microstructure across the resistance spot weld of 10% cold­deformed TRIP800 steel. A — Weld nugget; B — HAZ; C — grain growth in HAZ. ments within the fusion zone produces a sharp gradient in the B composition distribution through microsegregation (Ref. 16). In TRIP steels, due to the strong affinity for oxygen, the added Al and Si readily form oxides during welding, while leaving the weld pool depleted of these elements (Refs. 17, 18). It is also known that the reaction between the dissolved alloying elements in the weld pool with the available oxygen, nitrogen, and carbon forms nonmetallic inclusions (Ref. 18). Inclusions were observed in the weld nugget and HAZ. The energy-dispersive spectroscopy (EDS) analysis of incluFig. 2 — XRD results. A — As­received; B — cold­ sions is presented in Fig. 4. The deformed TRIP800 steel. result indicates that inclusions could be a mixture of aluminum and silicon oxide — Fig. 4A and transformed into martensite. B. Similar oxide inclusions were obThe microstructure of the weldment served in GTA welded high-Al and was also evaluated and results are high-Si TRIP steels (Ref. 18). shown in Fig. 3. The structure of the weld button contains the martensite phase due to its high cooling rate — Fig. Effect of Deformation and 3A. The structure of the HAZ transWelding Parameters on formed to predominantly martensite Properties and Failure Mode with small areas of ferrite, lath bainite, and retained austenite, depending on The macrographs of the failure the ultimate temperature reached and mode of the tested samples are shown cooling rate — Fig. 3B and C. in Fig. 5. Three distinct failure modes Results imply that an increase in were observed (Refs. 19–21). welding current and time increases heat 1) Interfacial failure (IF), in which input, which leads to expansion of the fracture propagating through the fuHAZ region. Since the deformation desion zone was observed for all welding creases the recrystalization temperature currents at 5 cycles and for all welding of the steel, grain growth proceeds more times at 1 kA. rapidly. Briefly, the deformation process 2) Pullout failure (PF), in which failalso extends to the HAZ. ure occurs by the effect of the withIn the case of a very rapid cooling of drawal of the weld button from a sinthe spot weldment, an insufficient difgle sheet, was observed from 3 to 9 kA fusion occurs in the precipitated solid welding currents, at 15 to 25 cycles crystals and the remaining liquid, so welding time. The fracture of the weld the inhomogeneity of the alloying ele- made with high expulsion current is through the full thickness of the base metal. The nugget diameter exceeds the electrode diameter and the fracture occurs outside the indented area (PF mode) (Ref. 22). 3) Partial interfacial failure (PIF), in which the fracture first propagates in the fusion zone, was observed for 5 cycles from 5 to 10 kA and 10 kA at all welding times. With higher welding times at higher welding currents, such as 10 kA, the amount of molten metal increases and fused metal ejects and the weld nugget diameter starts to decrease, so the fracture occurs at the edge of the button through the fusion zone and causes IF or PIF modes. No satisfactory joint is expected due to excessive heat input over 11 kA. The strength of the weldment varies with failure types. It increases in the order of IF, PIF, and PF modes. In determining the effect of welding parameters on the strength of deformed steel, all welded samples were tensile shear tested in order to evaluate the weld quality. Test results are shown in Fig. 6A and B. As seen in Fig. 6A and B, the maximum strength is obtained for 9 kA welding current at 20 cycles welding time. It was found that the strength increased with increasing welding time and current up to maximum level, then it gradually decreased due to increased molten metal and spreading of fused metal as well as uneven electrode indentation. The desired button diameter can only be obtained by proper adjustment of welding current vs. welding time. When time is short, the button diameter decreases. On the contrary, when it is long, the amount of molten metal increases and fused metal spreads out and as a result the strength of the welding joint decreases (Ref. 25). Kimchi also reports that exMARCH 2016 / WELDING JOURNAL 79-s Emre 3-16_Layout 1 2/11/16 4:01 PM Page 80 WELDING RESEARCH tic deformation. This is consistent with the results obtained from the tensile shear test. It is believed that increased hardness in the weld button increases the strength of the weldments. However, the hardness of the cold-deformed sample decreased in the HAZ. The HAZ of the as-received samples (450–500 HV0.5) had slightly higher hardness than the cold-deformed samples (424–475 HV0.5) for the same welding parameters, as seen in Fig. 7. It may be attributed to the severe deformation that decreases the recrystalization temperature; this, in turn, leads to the coarsening of grain in the HAZ during welding. In other words, work hardening is mostly wasted in the HAZ during recrystallization and grain growth. A B Effect of Deformation and Welding Parameters on the Weld Button Geometry Fig. 4 — EDS analysis of nonmetallic inclusions. A — 8 kA and 20 cycles; B — 9 kA and 25 cycles parameters in the fusion zone. A B C Fig. 5 — Failure mode of welded samples. A — IF; B — PIF; C — PF. pulsion due to high heat input causes loss of surface quality as well as strength in the resistance spot weldment (Ref. 22). Hardness measurements of samples were also performed and results are shown in Fig. 7A–D. It was found that deformed TRIP800 base metal hardness values were ap- proximately 100 HV0.5 higher than those of the as-received sample due to transformation of retained austenite into martensite during plastic deformation. The weld button hardness of colddeformed samples increased as compared to as-received samples due to increasing volume of martensite phase and grain refining with much more plas- 80-s WELDING JOURNAL / MARCH 2016, VOL. 95 The quality and strength of the weldment can be estimated by measuring its button diameter (Ref. 23). Sun et al. (Ref. 12) reports that AHSS spot welds with a fusion zone size of 4√t (t = thickness of sheet, mm) cannot produce a button with a desired pullout failure mode for both DP800 and TRIP800 spot welds under lap shear loading. Kumar-Pal and Bhowmick (Ref. 24) claim that the average button diameter should be equal to or larger than 4√t for button pull out failure mode in dualphase steels for a sheet thickness less than 1.5 mm. The relationship between button size and welding parameters was determined and results are shown in Fig. 8. Figure 9 clearly shows that it is possible to achieve a desired PF mode through a constant button diameter of 4√t by using welding parameters of more than 10 cycles welding time and 3 kA welding current. The button diameter of the spot weld increased with increasing welding currents up to maximum level (i.e., 7 kA for 10 cycles), then it gradually decreased. This phenomenon may be attributed to high heat input resulting in undesired expulsion, which results in the loss of liquid metal from the button. It was also found that the button diameter increased while the button height decreased. Because a higher heat input produces a larger fused vol- Emre 3-16_Layout 1 2/11/16 4:01 PM Page 81 WELDING RESEARCH A B Fig. 6 — Tensile shear load bearing capacity of weldment. A — Effect of welding current; B — effect of welding time. ume, the size of the button naturally increases with increasing electrode indentation; therefore, the button height decreases. The button diameter, or button height, is not enough to determine the strength of spot welded joints. However, the button size ratio can be used for this purpose (Ref. 25). Therefore, the relationship between button geometry and welding parameters was determined for all the weldments, as shown in Figs. 9–11. It was found that the button height of the welded specimen decreased with increasing welding parameters, except for a welding time of 5 cycles — Fig. 9. Meanwhile, the electrode indentation depth appeared to increase with increased heat input — Fig. 10. The button size ratio diagram associated with the welding parameters was evaluated from Fig. 11. The (0.14–0.3) button size ratio was found to be sufficient to achieve the desired PF mode. The PIF mode observed when the ratio was lower than 0.14 appears to be associated with the expulsion of molten metal from the weld area resulting from the high heat input, while the IF and PIF modes associated with a ratio higher than 0.3 could be the result of low heat input that is not sufficient enough to create the required button and button size ratio. Effect of Button Geometry on the Tensile Shear Strength of Samples The strength associated with button geometry and electrode indenta- tion depth was also determined and results are shown in Figs. 12–15, respectively. As a result of an increase in button diameter, the strength of the deformed samples increased. However, the strength began to decrease after a critical button diameter (i.e., 8-mm weld button for 20 cycles) — Fig. 12. By increasing welding current and welding time, the amount of the fused metal increased, so the button diameter increased, and the button height nearly reached the sheet thickness but then decreased with increasing electrode indentation. The strength also increased up to a limited value by decreasing button height and increasing electrode indentation depth, and then it started to decrease due to thinning of the cross section of the button as a result of high heat input — Figs. 13 and 14. When the button size ratio vs. tensile shear strength diagram was investigated, it was seen that with increasing button size ratio, strength of the deformed samples decreased — Fig. 15. Determining the Weld Lobe A graphical explanation of the ranges of welding parameters over which acceptable spot welds are formed at a constant electrode force is known as a “spot weld lobe curve” (Ref. 26). The spot welds defining the lower limit of the lobe curve are undersize, resulting in weaker nuggets. On the other hand, the spot welds at the upper limit of the lobe curve are large, resulting in severe expulsion, which decreases the weld strength. The selection of the lower limit of the weld lobe is determined by the specific demand of automakers. The weld lobe diagram generally is developed with regard to the welding parameters vs. button size. However, some researchers developed a weld lobe diagram based on electrode indentation depth and strength in resistance spot welded steels (Refs. 25, 27). In the present study, weld strength was used as a criterion to assess the weld quality. It can be seen from the left limit of the diagram, when indentation is small, low strength and button size were achieved. High welding current and weld time increase electrode indentation, which may exceed an acceptable limit, causing severe expulsion (Ref. 27). Weld strength reduces due to expulsion. The right limit of weld lobe was drawn according to 80% and 100% of maximum strength, while the left limit of the weld lobe was established according to indentation depth equal to about 25% of sheet thickness. The weld lobe of deformed TRIP800 steel based on welding parameters is shown in Fig. 16. If higher strength (100%) is desired, 9 kA welding current and 15 cycles welding time should be applied. However, 7 kA welding current and 25 or 20 cycles welding times are advised. The 25% sheet thickness limit is exceeded in these conditions. When a high surface quality rather than strength is desired, the welding current range of 3 to 4 kA and 20 to 25 cycles welding times should be applied. When the 80% of strength and acceptable surface quality are desired, the welding current range of 5–6 kA MARCH 2016 / WELDING JOURNAL 81-s Emre 3-16_Layout 1 2/11/16 4:01 PM Page 82 WELDING RESEARCH increasing density of the dislocations in the deformation and the formation of Cottrell atmosphere on the HAZ–base metal interface during welding. Khodabakhshi et al. (Ref. 29) reported that different rates of deformation applied to low-carbon steel used in the automobile industry caused an increase in electrical resistance. The strength of the colddeformed samples was determined to be higher than the as-received ones using the same welding parameters. More heat input raises the temperature at the electrode-sheet interface, and more plastic deformaD C tion is generated even under a constant electrode force (Refs. 29, 30), and for this reason the electrode indentation depth is found to be higher in the cold-deformed TRIP800 steel weldment. It is believed that an increase in electrode indentation caused much more contact surface between the watercooled electrode and weld button so the cooling rate increased in the colddeformed weldment. This caused the weld button to have more fine-grained microstructure and a higher Fig. 7 — Hardness profiles. A — As­received samples produced by using 8 kA welding current; B — hardness. The grain refining cold­deformed samples by using 3 kA; C — 8 kA; D — 10 kA welding current. increased the strength of the weldment. The width of the weld lobe and 20–25 cycles welding times should austenite transforms into a much gives an indication of good welding pabe applied. harder martensite phase and dislocarameters and the tolerance of the weld tion density is increased. Therefore, schedule in a production environment. electron flow is prevented due to high Discussion Compared to the as-received welded dislocation density and disordered samples, weld lobe diagram in previcrystal structure, thus electrical resisWeld button diameter and weld ous work (Ref. 15), the cold-deformed tivity is increased. So, heat generation button size ratio are the most critical and then welded samples, weld lobe diin prestrained TRIP800 spot welds (Q factors in weld quality in terms of 2 agram became narrow. The weld lobe = I R ) increased with the same weldpeak tensile shear load and failure t curves set back to lower welding curing parameters as compared with the mode for TRIP800 spot welds. As comrents with the same welding time. as-received ones, and more heat generpared to the as-received welded ation leads to the formation of a larger TRIP800 samples in previous work weld area in the weldment. Conclusions (Ref. 15), the critical button diameter Mukhopadhyay et al. (Ref. 28) invessize (4√t) for desired strength of 10% From the results given above, the tigated as-received resistance spot welds for cold-deformed TRIP800 samples following conclusions can be drawn: and 5% prestrained BH (bake hardenwas found to be lower than as-received 1) The tensile shear strength of ing) steels. They reported that prestrain samples’ button diameter size (4.5√t). the samples increased with heat input samples’ strength was higher than the It could be attributed to the plastic dedue to increased welding time and as-received samples depending on the formation of TRIP800 steels in which A 82-s WELDING JOURNAL / MARCH 2016, VOL. 95 B Emre 3-16_Layout 1 2/11/16 4:01 PM Page 83 WELDING RESEARCH Fig. 8 — An effect of welding parameters on weld nugget diameter. Fig. 9 — An effect of welding parameters on the weld nugget height. Fig. 10 — An effect of welding parameters on the electrode inden­ tation depth. Fig. 11 — An effect of welding parameters on the weld nugget size ratio. current. However, after the critical welding parameters, the strength starts to decrease because of the excessive heat input and expulsion. Cold deformation before welding increases the strength of the resistance spot welded TRIP800 steels. 2) The button diameter and button size ratio of welds for producing PF mode that results in acceptable strength and good surface quality should be at least 4√t and 0.14–0.30, respectively, in cold-deformed TRIP800 weldments. 3) The strength increases with an increase in electrode indentation depth and button diameter before severe expulsion occurs. 4) Cold deformation of TRIP800 steels increases the hardness and the strength of the weldment. 5) Three distinct failure modes were observed and the strength of the weldment increase in the order of IF, PIF, and PF modes. 6) Deformed TRIP800 steel hardness is found approximately 100 HV0.5 higher than those of the as-received sample. The button hardness increases with increasing heat input due to martensite transformation. 7) The weld lobe was produced to determine the acceptable strength and desired surface quality associated with welding parameters. Cold deformation of TRIP800 steel shrinks the weld lobe area and sets back the weld lobe curves for lower welding currents at the same welding times. Acknowledgment The authors thank the Karabük University project office for its kind support. References 1. Krizan, D., and De Cooman, B. C. 2008. Analysis of the strain-induced martensitic transformation of retained austenite in cold rolled micro-alloyed TRIP steel. Steel Res Int. 79(7): 513-s to 522-s. 2. Wiewiorowska, S. 2010. Determination of content of retained austenite in steels with trip effect deformed at different strain rates. Steel Res. Int. 81: 262-s to 265-s. 3. Khan, M. I., Kuntz, M. 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Mechanical properties and microstructure of resistance spot welded severely deformed low carbon steel. Materials Science and Engineering A 529(25): 237-s to 245-s. 30. Pouranvari, M., Abedi, A., Marashi, P., and Goodarzi, M. 2008. Effect of expulsion on peak load and energy absorption of low carbon steel resistance spot welds. Science and Technology of Welding & Joining 13(1): 39-s to 43-s. Authors: Submit Research Papers Online Peer review of research papers is now managed through an online system using Editorial Manager software. Papers can be submitted into the system directly from the Welding Journal page on the AWS website (aws.org) by clicking on “submit papers.” You can also access the new site directly at editorialmanager.com/wj/. Follow the instructions to register or log in. This online system streamlines the review process, and makes it easier to submit papers and track their progress. By publishing in the Welding Journal, more than 70,000 members will receive the results of your research. Additionally, your full paper is posted on the American Welding Society Web site for FREE access around the globe. There are no page charges, and articles are published in full color. By far, the most people, at the least cost, will recognize your research when you publish in the world-respected Welding Journal. MARCH 2016 / WELDING JOURNAL 85-s