Data Sheet MEPGGPENd Gas Purification Assemblies PG Series Gaskleen® Purifier Assemblies and Manifolds Description Pall’s Gaskleen® PG purifier assemblies have been designed to handle process flow rates up to 1,000 slpm. • An optional bypass manifold is available complete with isolation valves and backplate for easy mounting. • Pall’s purification materials are available in every standard configuration. • All purifier assemblies contain an integral 316L stainless steel particle filter. • 100% helium leak and pressure tested. • No detectable metal contribution above background in HCl gas with HCLP material • No detectable metal contribution above background in HBr gas with HBRP material Specifications Assembly Flow Rates • PG550: 75 slpm • PG2400: 500 slpm • PG11000: 1,000 slpm Particle Filter Options • PG550/PG2400: 0.4 µm or 0.003 µm • PG11000: 0.4 µm Connections • 1⁄4 in or 1⁄2 in gasket seal (VCR1 or compatible) male/male • Inlet/outlet isolation valves (for PG11000) Assembly Material • Electropolished 316L SS • <0.25 µm/<10 µin Ra internal surface finish Operating Conditions • Maximum operating pressure PG550/PG2400: 3.45 MPa/500 psig PG11000: 1.72 MPa/250 psig • Maximum operating temperature: 100˚C/212˚F (INP, SIP, FCP, SF6P), 40˚C/104˚F (NH3P, GEH4P, OXP, CLXP, HCLP, HBRP, CDAP) • EU Pressure Equipment Directive: Assemblies have been evaluated for compliance with the European Union’s Pressure Equipment Directive 97/23/EC and are CE-marked. 1 VCR is a trademark of Swagelok Co. List of Purifiable Gases Gas Family Material Effluent Specification2 Nitrogen, argon, helium, xenon, krypton, neon INP <1 ppb H2O, O2, CO2 and CO Silane, hydrogen, methane, cyclopropane, propane, dimethyl ether SIP <1 ppb H2O, O2, CO2 and CO Carbon monoxide SIP <1 ppb H2O, O2, CO2, Ni(CO)4, and Fe(CO)5 Fluoromethane, difluoromethane, trifluorine, tetrafluoroethane, pentafluoroethane, heptafluoropropane, carbon tetrafluoride, perfluoropropane, perfluorocyclobutane, hexafluoroethane FCP <1 ppb H2O, O2, CO2 and CO Ammonia NH3P <1 ppb H2O, O2, CO2 and CO Germane GEH4P <1 ppb H2O, O2, CO2 and CO Sulfur hexafluoride SF6P <1 ppb H2O, O2, CO2 and CO Air, carbon dioxide, oxygen, nitrous oxide OXP <10 ppb H2O Boron trichloride, chlorine, trichlorosilane, dichlorosilane CLXP <100 ppb H2O Hydrogen chloride HCLP <15 ppb H2O Hydrogen bromide HBRP < 50 ppb H2O Photolithography clean dry air CDAP < 1 ppb H2O, < 300 ppt organics (as C4), < 10 ppt acid gases (as SO2), < 15 ppt basic gases (as NH3), < 1 ppt refractory compounds (as HMDSO) 2 As tested in inert gas. Pressure Drop vs. Gas Flow Rate Nitrogen flow rate (in scfm @ 68˚F and 1 atm) Nitrogen flow rate (in scfm @ 68˚F and 1 atm) 2.50 2.00 1.50 0.00 10.0 7 103 kPa/15 psig inlet 6 3 207 kPa/30 psig inlet 2 552 kPa/80 psig inlet 37.5 25.0 50.0 62.5 75.0 0 0.0 552 kPa/80 psig inlet 40.0 6 4 20.0 2 100 150 200 250 300 350 400 450 500 0 Pressure drop (kPa) 8 Pressure drop (psid) Pressure drop (kPa) 60.0 25.0 37.5 50.0 62.5 8 40.0 6 30.0 4 20.0 552 kPa/80 psig inlet 10.0 0.0 0 50 100 150 200 250 300 350 400 450 500 70.0 2 10.0 100 150 200 250 300 350 400 450 500 0 Nitrogen flow rate (in slpm @ 20˚C and 1 atm) Pressure drop (kPa) 4 552 kPa/80 psig Inlet Pressure drop (psid) 40.0 103 kPa/15 psig inlet 60.0 8 6 30.0 207 kPa/30 psig inlet 20.0 10.0 0.0 552 kPa/80 psig inlet 0 50 100 150 200 250 300 350 400 450 500 PG2400___VMM8 with 0.4 µm filter 30.0 35.0 50.0 Note: For pressure drop information for a specific application, please contact Pall Microelectronics. 10 103 kPa/15 psig Inlet 60.0 Pressure drop (kPa) 25.0 207 kPa/30 psig Inlet 8 40.0 6 30.0 4 20.0 552 kPa/80 psig Inlet 10.0 0.0 0 2 0 100 200 300 400 500 600 700 800 900 1000 Nitrogen flow rate (in slpm @ 20˚C and 1 atm) PG11000 Series assembly Pressure drop (psid) 70.0 20.0 10 6 40.0 Nitrogen flow rate (in scfm @ 68˚F and 1 atm) 15.0 0 8 50.0 Nitrogen flow fate (in slpm @ 20˚C and 1 atm) PG2400___VMM8 with 0.003 µm filter 10.0 2 Nitrogen flow rate (in scfm @ 68˚F and 1 atm) 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 207 kPa/30 psig Inlet 20.0 10 0.0 80.0 10 30.0 103 kPa/15 psig inlet PG2400___VMM4 with 0.4 µm filter Nitrogen flow rate (in scfm @ 68˚F and 1 atm) 8.0 10.0 12.0 14.0 16.0 5.0 0.00 Nitrogen flow rate (in slpm @ 20˚C and 1 atm) 0.0 2.0 4.0 6.0 80.0 103 kPa/15 psig Inlet 70.0 0.0 80.0 75.0 207 kPa/30 psig inlet 50.0 Nitrogen flow rate (in slpm @ 20˚C and 1 atm) PG2400___VMM4 with 0.003 µm filter Pressure drop (kPa) 12.5 70.0 12 10 50 0 0.50 0.25 552 kPa/80 psig inlet 0.0 80.0 14 60.0 50.0 207 kPa/30 psig inlet 2.0 Nitrogen flow rate (in scfm @ 68˚F and 1 atm) 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 207 kPa/30 psig inlet 60.0 0.75 4.0 PG550 with 0.4 µm filter 80.0 50 1.00 6.0 Nitrogen flow rate (in slpm @ 20˚C and 1 atm) Nitrogen flow rate (in scfm @ 68˚F and 1 atm) 8.0 10.0 12.0 14.0 16.0 0 1.25 103 kPa/15 psig inlet Pressure drop (psid) 12.5 1 Pressure drop (kPa) 4 0.0 2.0 4.0 6.0 100.0 103 kPa/15 psig inlet 0.0 2.50 2.00 1.50 5 PG550 with 0.003 µm filter 0 1.00 8.0 Nitrogen flow rate (in slpm @ 20˚C and 1 atm) 0.0 0.50 Pressure drop (psid) 1.00 4 2 0 Pressure drop (psid) 0.50 Pressure drop (psid) Pressure drop (kPa) 0.00 50.0 45.0 40.0 35.0 30.0 25.0 20.0 15.0 10.0 5.0 0.0 0 Lifetime Calculations 75.0 62.5 37.5 2 ppm 25.0 5 ppm 12.5 0.0 1 ppm 10 ppm 0 2,000 4,000 6,000 8,000 10,000 Flow rate (slpm) Flow rate (slpm) 50.0 Service life (hrs) Pall AresKleenTM purification material: inert gas service Gaskleen® PG550 purifier assembly, part # GLP9INPVMM4 500 450 400 350 1 ppm 300 250 2 ppm 200 150 5 ppm 100 50 10 ppm 0 0 2,000 4,000 Service life (hrs) 6,000 8,000 Pall AresKleenTM purification material: inert gas service Gaskleen® PG2400 purifier assembly, part # GLP24INPVMM4/VMM8 Inlet pressure: 207 kPa (30 psig) contaminant challenge as H2O Flow rate (slpm) Inlet pressure: 207 kPa (30 psig) contaminant challenge as H2O 1000 900 800 1 ppm 700 600 2 ppm 500 400 5 ppm 300 200 10 ppm 100 0 0 2,000 4,000 6,000 Service life (hrs) Note: For lifetime calculations in a specific application, please contact Pall Microelectronics. 8,000 10,000 Pall AresKleenTM purification material: inert gas service Gaskleen® PG11000 purifier assembly, part # GLP110INPVFM8 Inlet pressure: 207 kPa (30 psig) contaminant challenge as H2O Nominal Assembly Dimensions 1041.4 mm 41.0 in 990.6 mm 39.0 in 201.7 mm 7.94 in 439.4 mm 17.30 in ø76.2 mm ø3.00 in PG550 ø152.4 mm ø6.0 in Note: For manifold dimensions, please contact Pall Corporation. 10,000 ø101.6 mm ø4.00 in 254.0 mm 10.0 in PG2400 PG11000 Technical Information Impurity Removal as Tested in Specific Gases Specific Gas Impurity Removal Efficiency Inert gases: nitrogen, argon, helium, xenon, krypton, neon <1 ppb H2O, CO2, O2, and CO, as tested in argon and nitrogen using APIMS analyzer Flammable gases: silane, hydrogen, methane, ethane, cyclopropane, propane, dimethyl ether <1 ppb H2O, CO2, O2, and CO, as tested in argon, nitrogen and hydrogen using APIMS analyzer <1 ppb H2O, as tested in carbon monoxide using trace moisture analyzer H2O and siloxanes removed to trace levels, as tested in silane using APIMS Carbon monoxide <1 ppb Ni(CO)4, and < 1 ppb Fe(CO)5, as tested in carbon monoxide using GC-ECD analyzer Ammonia <1 ppb H2O, CO2, and O2, as tested in argon using APIMS <12 ppb H2O, as tested in ammonia using NIR-TDLAS Removal of O2 and CO2 to trace levels, as tested in ammonia using GC-DID Fluorocarbons: fluoromethane, difluoromethane, trifluoromethane, tetrafluoroethane, pentafluoroethane, heptafluoropropane, carbon tetrafluoride, perfluoropropane, perfluorocyclobutane, hexafluoroethane <1 ppb H2O, CO2, O2, and CO, as tested in argon and nitrogen using APIMS analyzer <1 ppb O2, as tested in trifluoromethane using trace oxygen analyzer <10 ppb H2O, as tested in trifluoromethane using trace moisture analyzer and FTIR Germane <1 ppb H2O, CO2, O2, and CO, as tested in argon and nitrogen using APIMS analyzer Sulfur hexafluoride <1 ppb H2O, CO2, and O2, as tested in argon using APIMS Oxygenated gases: carbon dioxide, oxygen, nitrous oxide, clean dry air <10 ppb H2O <1 ppb H2O, and CO2, as tested in argon using APIMS analyzer Chlorinated gases: boron trichloride, chlorine, trichlorosilane, dichlorosilane <100 ppb H2O <1 ppb H2O, and CO2, as tested in argon using APIMS analyzer Halogenated gases: hydrogen chloride, hydrogen bromide < 15 ppb H2O as tested in hydrogen chloride using CRDS < 50 ppb H2O as tested in hydrogen bromide using CRDS < 1 ppb H2O as tested in argon using APIMS analyzer Photolithography clean dry air < 1 ppb H2O as tested in argon using APIMS analyzer < 300 ppt C4H8 as tested in argon using APIMS Analyzer < 10 ppt SO2 as tested in nitrogen using ion chromatograph < 15 ppt NH3 as tested in nitrogen using ion chromatograph < 1 ppt HMDSO as tested in argon using APIMS analyzer and baseline subtraction Unit conversion: 1 bar = 100 kilopascals Part Numbers / Ordering Information Series Part Number3 PG550 GLP9xxxxFVMM4 Description Purifier assembly, 75 slpm, 0.003 µm filter, ⁄4 in gasket seal (VCR or compatible) male/male 1 GLP9xxxxFMAN Bypass manifold with GLP9xxxFVMM4 assembly GLP9xxxxFVMM4GCMAN Gas cabinet manifold with GLP9xxxFVMM4 assembly GLP9xxxxVMM4 Purifier assembly, 75 slpm, 0.4 µm filter, ⁄4 in gasket seal (VCR or compatible) male/male 1 PG2400 GLP9xxxxMAN Bypass manifold with GLP9xxxVMM4 assembly GLP9xxxxVMM4GCMAN Gas cabinet manifold with GLP9xxxVMM4 assembly GLP24xxxxFVMM4 Purifier assembly, 300 slpm, 0.003 µm filter, ⁄4 in gasket seal (VCR or compatible) male/male 1 GLP24xxxxFVMM8 Purifier assembly, 300 slpm, 0.003 µm filter, ⁄2 in gasket seal (VCR or compatible) male/male 1 GLP24xxxxFMAN Bypass manifold with GLP24xxxxFVMM8 assembly GLP24xxxxVMM4 Purifier assembly, 500 slpm, 0.4 µm filter, ⁄4 in gasket seal (VCR or compatible) male/male 1 GLP24xxxxVMM8 Purifier assembly, 500 slpm, 0.4 µm filter, ⁄2 in gasket seal (VCR or compatible) male/male 1 GLP24xxxxMAN PG11000 Bypass manifold with GLP24xxxxVMM8 assembly 4 GLP110xxxxVFM8 Purifier assembly, 1,000 slpm, 0.4 µm filter, 1 ⁄2 in gasket seal (VCR or compatible) female inlet/male outlet GLP110xxxxMAN4 Bypass manifold with GLP110xxxVMM8 assembly 3 See list of purifiable gases on page 1. Example: GLP9INPFVMM4. 4 The PG11000 stainless steel assembly (used with all GLP110 part numbers) is fabricated in accordance with the ASME BPVC Section VIII, Division 1, and has a U-stamp. If the user determines that an L-stamp is required for a lethal service application, please contact Pall Microelectronics for cost and availability. 25 Harbor Park Drive Port Washington, New York 11050 USA +1.800.360.7255 toll free (toll free in USA only) +1.516.484.3600 phone +1.516.625.3610 fax microelectronics@pall.com Visit us on the Web at www.pall.com/micro Pall Corporation has offices and plants throughout the world. For Pall representatives in your area, please go to www.pall.com/contact.asp Because of technological developments related to the products, systems, and/or services described herein, the data and procedures are subject to change without notice. Please consult your Pall representative or visit www.pall.com to verify that this information remains valid. Products in this document may be covered by the following patent number: US 7,465,692 © Copyright 2007, 2011, 2014 Pall Corporation. Pall, , and Gaskleen are trademarks of Pall Corporation. ® Indicates a Pall trademark registered in the USA. Filtration. Separation. Solution.SM is a service mark of Pall Corporation. MEPGGPENd December 2014