Performance of a Magnetic Shape Memory Micropump 1,2 Chen , 2 Barker , 2 Müllner Yueli Sam Peter 1Department of Chemistry, CUNY Queensborough Community College, NY 11364 2Department of Material Science and Engineering, Boise State University, 83725 Introduction Objective /Design • Solid-state micropumps -a promising market for point of care diagnostics, biomedical research and lab-on-a-chip test devices. • Desirable features of micropump: free from electrical contacts, sealed within a potentially disposable lab-on-a-chip unit, pumping without ancillary mechanical devices, precise and sensitive over a wide range of volume, etc. Magnetic shape memory (MSM) alloy Ni-Mn-Ga elements: - Strain up to 6%, through twinning process, when exposed to a magnetic field. Twining boundary - Allow for a wide range of precise volumes to be C x A z delivered. C φ - Magnetic field can be c a a generated by an off-chip c source b Objective: to carry out systematic experiments measuring the pumping flow rate as a function of rotational speed of the magnet. Perpendicular Magnetic field from the diametrically magnetized cylindrical magnet. Experimental Setup b • Top view of MSMA element with twins produced by a diametrically magnetized cylindrical magnet. • MSMA micropump pumping: the magnetic field creates a cavity on the MSMA element. The cavity moves along the MSM element upon rotation of the cylindrical magnet and transports fluid. K. Ullakko, L. Wendell, A. Smith, P. Müllner, G. Hampikian. Smart Mater. Struct., 2012, 21, 115020. The magnetic shape memory micropump with Ni2MnGa element was designed at Boise State University by Kari Ullakko. The NiMn-Ga single crystal element was grown in the Magnetic Materials laboratory of Dr. Peter Müllner's group. Experimental Procedures/Results Mechanism • Schematic side view of MSMA element with twin structure of localized shrinkage. MSMA Micropump 1 mm • When moved forward to test flow rate of MSM micropump, MSM element cracked. • Multiple cracks formed indicating that the damage was not due to mechanical overload. • SEM images of fracture surface of the MSMA element exhibit ripples which may correlate with twins. • Performed experiments to test efficiency of the MSM micropump. • Diametrically magnetized cylindrical magnet was turned by a drill for approximate 4s. • Magnified view of MSM miropump moving water from left to right. • The MSM miropump successfully pumped water in both directions. 0.5 mm 0.5 mm • Constructed micropump by a single component Ni-Mn-Ga element. • MSMA micropump successfully delivered a drop of water (≈0.05ml) in both directions. • Failure of the MSMA element could be caused by following reasons: - Impurity of the MSMA element. - Turning magnet by a drill made twins move, and it also caused the MSMA micropump vibrate. Field Parallel to Face - Fatigue life of Ni-Mn-Ga is varied from 4,000 cycles u 810,000 Cycles to 800,000 cycles. After NiInitial Mn-Ga elements have been cycled many times, twinning activity would be reduced. Magnetization (Am2/kg) Procedures/Materials Conclusions/Discussion Effective Magnetic Field (MA/m) Future Work • Determine Fatigue life of Ni-Mn-Ga magnetic shape memory alloys. • Prevent any sealants (Epoxy, Silicone and Sylgard) from leaking into MSMA element to help render micropumps effective. • Fasten diametrically magnetized cylindrical magnet right under MSMA element to help increase efficiency of twins motion. • Characterize flow rate, pressure, temperature and power consumption of MSMA micrpumps. References (1) K. Ullakko, L. Wendell, A. Smith, P. Müllner, G. Hampikian. Smart Mater. Struct., 2012, 21, 115020. (2) A Smith, A. Saren, J. Jarvinen, K. Ullakko, Microfluid Nanofluid, 2015, 18, 1255-1263. (3)T. Lawrence, P. Lindquist, K. Ullakko, P. Müllner. Fatigue life and fracture mechanics of unconstrained Ni-Mn-Ga single crystals in a rotating magnetic field. Manuscript unpublished. Acknowledgements 50 µm 0.2 mm The US National Science Foundation supported this research at Boise State University through project NSFIIP-1500240.