Agilent Technologies Classroom Series Practical Temperature Measurements 001 Agenda Background, history Mechanical sensors Electrical sensors Optical Pyrometer RTD Thermistor, IC Thermocouple Summary & Examples A1 What is Temperature? A scalar quantity that determines the direction of heat flow between two bodies A statistical measurement A difficult measurement A mostly empirical measurement 002 How is heat transferred? Conduction Metal coffee cup Convection Radiation 003 The Dewar Glass is a poor conductor Gap reduces conduction Metallization reflects radiation Vacuum reduces convection 004 Thermal Mass Don't let the measuring Sensor device change the temperature of what you're measuring. Response time = f{Thermal mass} f{Measuring device} Sensor 005 Temperature errors What is YOUR normal temperature? Thermometer accuracy, resolution Contact time Thermal mass of thermometer, tongue Human error in reading 97.6 98.6 99.6 36.5 37 37.5 006 History of temperature sensors 1600 ad 1700 12 ad 96 Fahrenheit 1 Instrument 0 Galileo: First temp. sensor pressure- sensitive not repeatable Early thermometers Not repeatable No good way to calibrate Maker 12*8=96 points Hg: Repeatable One standard scale 007 The 1700's: Standardization 1700 ad 1800 ad 0 100 Thomson effect Absolute zero 100 Celsius: Common, repeatable calibration reference points 0 "Centigrade" scale 008 1821: It was a very good year 1800 ad 1900 ad The Seebeck effect Davy: The RTD Pt 100 d @ O deg.C 009 The 1900's: Electronic sensors 1900 ad Thermistor 2000 ad 1 uA/K IC sensor IPTS 1968 IPTS 1990 "Degree Kelvin">> "kelvins" "Centigrade">> " Celsius" 010 Temperature scales Freezing point H2O Absolute zero Celsius 0 100 Kelvin 273.15 373.15 32 212 -273.15 0 Fahrenheit -459.67 0 Boiling point H O2 Rankine 427.67 671.67 "Standard" is "better": Reliable reference points Easy to understand 011 IPTS '90: More calibration points – – 273.16: TP H2O 234.3156: TP Hg Large gap – – – – – – – – – – – – 83.8058: TP Ar 54.3584: TP O2 24.5561: TP 20.3: BP Ne 17 Liq/vapor H2 13.81 TP H2 3 to 5: Vapor H2 He – – 1357.77: FP Cu 1337.33: FP Au 1234.93: FP Ag 933.473: FP Al 692.677: FP Zn 505.078: FP Sn 429.7485: FP In – 302.9146: MP Ga 012 Agenda Background, history Mechanical sensors Electrical sensors Optical Pyrometer RTD Thermistor, IC Thermocouple Summary & Examples A2 Bimetal thermometer Two dissimilar Forces due to thermal expansion metals, tightly bonded 0 Result 100 200 300 Bimetallic thermometer 400 Poor accuracy Hysteresis Thermal expansion causes big problems in other designs: IC bonds Mechanical interference 013 Liquid thermometer; Paints 100 0 Thermally-sensitive paints Liquid-filled thermometer Irreversible change Low resolution Useful in hard-to-measure area Accurate over a small range Accuracy & resolution= f(length) Range limited by liquid Fragile Large thermal mass Slow 014 Agenda Background, history Mechanical sensors Electrical sensors Optical Pyrometer RTD Thermistor, IC Thermocouple Summary & Examples A3 Optical Pyrometer Infrared Radiation-sensitive Photodiode or photoresistor Accuracy= f{emissivity} Useful @ very high temperatures Non-contacting Very expensive Not very accurate 015 Agenda Background, history Mechanical sensors Electrical sensors Optical Pyrometer RTD Thermistor, IC Thermocouple Summary & Examples A4 Resistance Temperature Detector Most accurate & stable Good to 800 degrees Celsius Resistance= f{Absolute T} Self-heating a problem Low resistance Nonlinear 016 RTD Equation R= 100 Ohms @ O C Callendar-Van Deusen Equation: For T>OC: R=Ro(1+aT) - Ro(ad(.01T)(.01T-1)) R Ro=100 @ O C a= 0.00385 / - C for Pt d= 1.49 300 200 100 0 Nonlinearity 200 400 600 800 T 017 Measuring an RTD: 2-wire method Rx 100d Pt Rlead + Rlead - V I ref= 5 mA R= Iref*(Rx + 2* Rlead) Error= 2d /.385= more than 5 degrees C for 1 ohm Rlead! Self-heating: For 0.5 V signal, I= 5mA; P=.5*.005=2.5 mwatts @ 1 mW/deg C, Error = 2.5 deg C! Moral: Minimize Iref; Use 4-wire method If you must use 2-wire, NULL out the lead resistance 018 The 4-Wire technique Rx 100d + Rlead=1d - V I ref= 5 mA R= Iref * Rx Error not a function of R in source or sense leads No error due to changes in lead R Twice as much wire Twice as many scanner channels Usually slower than 2-wire 019 Offset compensation Voffset + 100d - V I ref (switched) Eliminates thermal voltages Measure V without I applied Measure V With I applied R= V I 020 Bridge method 100 d d 1000 V d 1000 100d High resolution (DMM stays on most sensitive range) Nonlinear output Bridge resistors too close to heat source 021 3-Wire bridge 100d 1000d Rlead 1 V 1000d Sense wire 3-Wire PRTD Rlead 2 Keeps bridge away from heat source Break DMM lead (dashed line); connect to 100d RTD through 3rd "sense" wire If Rlead 1= Rlead 2, sense wire makes error small Series resistance of sense wire causes no error 022 Agenda Background, history Mechanical sensors Electrical sensors Optical Pyrometer RTD Thermistor, IC Thermocouple Summary & Examples A5 Electrical sensors: Thermistor Rlead=1 5k d d Rlead=1d + - Hi-Z; Sensitive: 5 k V d I= 0.1 mA @ 25C; R = 4%/deg C Limited range 2-Wire method: R= I * (Rthmr + 2*Rlead) Lead R Error= 2 d /400= 0.005 degrees C Low thermal mass: High self-heating Very nonlinear 023 I.C. Sensor I= 1 uA/K + 5V - 100 d V = 1mV/K 960d High output Very linear Accurate @ room ambient Limited range Cheap 024 Summary: Absolute T devices RTD Thermistor I.C. Most accurate Most stable Fairly linear High output Fast 2-wire meas. High output Most linear Inexpensive Expensive Slow Needs I source Self-heating 4-wire meas. Very nonlinear Limited range Needs I source Self-heating Fragile Limited variety Limited range Needs V source Self-heating 025 Agenda Background, history Mechanical sensors Electrical sensors Optical Pyrometer RTD Thermistor, IC Thermocouple Summary & Examples A6 Thermocouples The Gradient Theory Ta Tx The WIRE is the V= V sensor, not the junction Tx The Seebeck e(T) dT Ta coefficient (e) is a function of temperature 026 Making a thermocouple Ta Tx B V Two wires make a A Ta thermocouple V= e Ta A Voltage output is Ta Tx dT + e B dT nonzero if metals are not the same Tx 027 Gradient theory also says... Ta Tx A V If wires are the A Ta Ta Tx e dT + A V= Ta e A dT = 0 same type, or if there is one wire, and both ends are at the same temperature, output= Zero. Tx 028 Now try to measure it: a Fe b Tx Theoretically, Vab= f{Tx-Tab} Con But, try to measure it with a DMM: Cu Tx V Cu Cu Fe Con = Fe V Tx Con Cu Result: 3 unequal junctions, all at unknown temperatures 029 Solution: Reference Thermocouple Problems: a) 3 different thermocouples, b) 3 unknown temperatures Solutions: a) Add an opposing thermocouple b) Use a known reference temp. Isothermal block Fe Cu Cu Fe Tx Add Tx Con V V Con Tref Tref = 0 oC Cu Fe Cu Fe 030 The Classical Method Cu Fe Tx V Con Tref o =0C Cu Fe If both Cu junctions are at same T, the two "batteries" cancel Tref is an ice bath (sometimes an electronic ice bath) All T/C tables are referenced to an ice bath V= f{Tx-Tref} Question: How can we eliminate the ice bath? 031 Eliminating the ice bath Don't force Tref to icepoint, just Cu V Fe Con Cu Fe measure it Compensate for Tref Tx mathematically: V=f{ Tx - Tref } Tice Tref Tice If we know Tref , we can Tice compute Tx. 032 Eliminating the second T/C Cu Fe Tx V Extend the isothermal block If isothermal, V1-V2=0 2 Con Cu Fe Tref Cu Fe 1 Tx V Tref 2 Con Cu 1 033 The Algorithm for one T/C Cu V Tref Cu Fe IC or thermistor Tx Measure Tref: RTD, o Tref ==> Vref @ O C for Type J(FeCon C) Know V, Know Vref: Compute Vx Solve for Tx using Vx Compute Vx=V+Vref Vx Vref 0 o Tref V Tx 034 V Linearization Small sectors 0 o Tref Tx T 2 3 V +.... a9 V Polynomial: T=a +a V +a V +a 0 1 2 3 9 Nested (faster): T=a 0 +V(a 1 +V(a 2 +V(a 3 2 +.......))))))))) 0 Small sectors (faster): T=T +bV+cV Lookup table: Fastest, most memory 035 Common Thermocouples mV E 60 Platinum T/Cs Base Metal T/Cs K J N 40 20 T 0 500 RS 1000 2000 deg C All have Seebeck coefficients in MICROvolts/deg.C 036 Common Thermocouples Type J K T S E N Metals Seebeck Coeff: uV/C Fe-Con Ni-Cr Cu-Con Pt/Rh-Pt Ni/Cr-Con Ni/Cr/Si-Ni/Si 50 40 38 10 59 39 Microvolt output is a tough measurement Type "N" is fairly new.. more rugged and higher temp. than type K, but still cheap 037 Extension Wires Possible problem here Large extension wires Small diameter measurement wires Extension wires are cheaper, more rugged, but not exactly the same characteristic curve as the T/C. Keep extension/TC junction near room temperature Where is most of the signal generated in this circuit? 038 Noise: DMM Glossary Normal Mode ac NOISE DMM Input Resistance HI LO Normal Mode dc SIGNAL Normal Mode: In series with input Common Mode: Both HI and LO HI DMM Input Resistance terminals driven equally LO Common Mode ac NOISE 039 Generating noise Electrostatic Noise DMM Input Resistance Magnetic Noise HI Normal Mode LO dc SIGNAL Large surface area, high Rlead: Max. static DMM Input Resistance R leak coupling HILarge loop area: Max. magnetic coupling Large R lead, small R leak: R lead Max. LO common mode noise Common Mode Current Common Mode ac source 040 Eliminating noise Electrostati c Noise DM M Inpu tR Magneti c Noise HI Normal Mode dc SIGNAL L O Filter, shielding, small loop area (Caution: filter slows down the measurement) HI DM M Input R R leak Make R leak close to L O - + Common Mode Current Common Mode ac source 041 Magnetic Noise Magnetic coupling DMM Input Resistance Induced I Minimize area Twist leads Move away from strong fields 042 Reducing Magnetic Noise Equal and opposite induced currents DMM Input Resistance Even with twisted pair: Minimize area Move away from strong fields 043 Electrostatic noise AC Noise source Stray capacitances DMM Input Resistance Inoise Stray resistances Stray capacitance causes I noise DMM resistance to ground is important 044 Reducing Electrostatic AC Noise source Coupling DMM Input Resistance HI LO Rleak Shield shunts stray current For noise coupled to the tip, Rleak is still important 045 A scanning system for T/Cs One thermistor, multiple T/C channels Noise reduction CPU linearizes T/C DMM must be very high quality OHMs Conv. Isolators HI uP LO Integrating A/D Floating Circuitry ROM Lookup uP I/O (HP-IB, RS-232) To Computer Grounded Circuitry 046 Errors in the system Ref. Block Thermal gradient T/C Calibration & Wire errors Thermal emf Ref. Thermistor cal, linearity OHMs Conv. Reference Thermistor Ohms measurement Linearization algorithm Isolators HI uP LO Integrating A/D Floating Circuitry ROM Lookup DMM offset, linearity, thermal emf, noise uP Extension wire junction error I/O (HP-IB, RS-232) Grounded Circuitry 047 Physical errors Shorts, shunt impedance Galvanic action Decalibration Sensor accuracy Thermal contact Thermal shunting 048 Physical Errors Water droplets cause galvanic action; huge offsets Hot spot causes shunt Z, mete shows the WRONG temperatur Exceeding the T/C's range can cause permanent offset Real T/C's have absolute accuracy of 1 deg C @ 25C: Calibrate often and take care 049 Physical error: Thermal contact Surface probe Make sure thermal mass is much smaller than that of object being measured 050 Physical errors: Decalibration 350 C 300 C 200 C 100 C 975 C 1000 C This section Don't exceed Tmax of T/C produces the Temp. cycling causes work-hardening, ENTIRE signal decalibration Replace the GRADIENT section 051 Agenda Background, history Mechanical sensors Electrical sensors Optical Pyrometer RTD Thermistor, IC Thermocouple Summary & Examples A7 The basic 4 temperature sensors RTD Thermistor Most accurate High output Fast Most stable 2-wire meas. Fairly linear Expensive Very nonlinear Slow Limited range Needs I source Needs I source Self-heating Self-heating 4-wire meas. Fragile I.C. Thermocouple High output Most linear Cheap Limited variety Limited range Needs V source Self-heating Wide variety Cheap Wide T. range No self-heating Hard to measure Relative T. only Nonlinear Special connectors Absolute temperature sensors 052 Summary Innovation by itself is not enough... you must develop standards Temperature is a very difficult, mostly empirical measurement Careful attention to detail is required 053 Examples Measurement Photochemical process Sensor RTD (most accurate) control: Thermistor Flower petal: Molten glass: Induction furnace: 100 degree Heat aging oven: (lowest thermal mass) Optical pyrometer (hi temp, no contact) RTD (if <800C); or T/C (Beware magnetic I noise) Any of the 4 sensors 054