The Decatur High School Science Lab

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The Klein High School

Science Lab

Chemistry Laboratory Safety

Lab Safety: Everyone is

Responsible!

• " I didn't mean to" and " It wasn't my fault " are two statements that have no place in the lab.

• Horse-play will not be tolerated.

• Lack of pre-lab preparation is the biggest threat to lab safety.

• Read lab instructions prior to coming to lab. If you do not understand any procedure, ask your instructor for explanation.

• Never perform unauthorized or unsupervised experiments.

Safety Glasses and a lab apron must be worn any time you are in the lab area.

– Safety glasses are stored in the goggle cabinet at the front of the room, lab aprons are on the hooks at the front of the room

– Contact lenses increase the potential damage to the eye in a chemical accident, please wear your glasses for lab

Long hair and bulky clothing are dangerous in the lab area .

– There is a danger of catching fire, as well as being soaked in chemicals.

– Wear appropriate clothing.

– Tie back long hair.

Rings, watches, and dangling jewelry are dangerous in the lab area.

– Corrosive or irritating liquids may get underneath a ring or watch and produce irritation.

– Dangling jewelry may catch on a piece of labware and cause an accident.

• Always pay attention to verbal instructions given by your teacher.

Prevention = Smartest Move

• Before beginning work in lab, clean the lab bench top and your glassware

• Direct contact with chemicals should be kept to a minimum

• Never taste any chemicals or substances produced by a chemical reaction

• Eating or drinking in lab is never permitted

Fume hood should be used when burning chemicals and when a chemical reaction gives off noxious gases

Heating Precautions

• Do not heat heavy or thick glassware, such as graduated cylinder or reagent bottles.

• Avoid heating any apparatus too suddenly

• When heating a substance in a test tube, be careful not to point tube at another person or yourself

• Do not hold tip of test tube directly in the flame

Accidents Can Happen

• Remain calm! A minor problem can quickly become a major one if you overreact.

• Report all accidents to your teacher immediately, no matter how small.

• Types of accidents and how to handle them:

Broken Glass:

• The most common accident in the lab , even with the best of care.

• If you are using the equipment properly, you will not get into trouble for breaking a piece of glassware, but you will still be required to pay for the broken glassware.

• If you are not using the equipment properly, or if horse-play is involved, you will be required to pay for the broken glassware and disciplinary action may be taken.

• Report any breakage to your teacher immediately.

• Do not move until your teacher says it is safe to do so.

• If anyone is cut, report it immediately.

• Chemical spills are often involved with glass breakage. When that occurs, follow those safety precautions too.

Cuts and Scrapes:

• Report the situation and let your teacher help the injured person.

• There is always a possibility of infection , even with the most minor injury. For this reason you should report any cut or scrape, even if there is no visible blood.

• Do not come into contact with another person's blood , either directly or indirectly.

Chemical Spills:

• Chemical Safety Warning Signs - NFPA, ANSI, OSHA

• Depending on the chemical spilled the procedure can vary; for most of the chemicals we will use, water is the best treatment – flush the affected area with water for up to 15 minutes (20 minutes for eyes)

• The most potentially dangerous chemicals used in our lab are corrosive acids and bases. Always treat acids and bases with care even if you are using dilute solutions.

• You are to treat all spills as DANGEROUS.

• Stop where you are and let your teacher advise you about what to do.

• Always consult the proper Safety Data Sheet before doing anything. Sometimes adding water is not the proper step – know those exceptions

• Kitty litter and baking soda are located in the hood for large spills.

Fire:

• Lab burners are the source of most problems:

– Bunsen burners have very few malfunctions. If a malfunction occurs, turn off the gas and notify your teacher- end of problem.

– Be aware when a burner is in use at your lab station. Never leave a flame unattended

– When you are not actively heating something - turn the burner off .

• Clothing or Hair is the most dangerous type of fire in the lab.

– Don't panic!

– If you are the one involved in a fire stay where you are - help is coming .

– If your partner is involved in a fire get the fire blanket . Your teacher will be racing you to the blanket and both of you will help your partner smother the fire.

– If the fire is not at your lab station stay away !

• The science teacher is the only person authorized to use the fire extinguisher

Lab Safety Equipment

Eye Wash/Shower Station:

– Eye wash station is located on the right side of the lab.

It should only be used if chemicals come in contact with the eyes

– Flood eyes and eyelids with water for a minimum of 20 minutes .

– Shower in the event that large amounts of chemicals are spilled or splashed onto the skin or clothing

Fire Safety Blanket:

– The fire safety blanket is located at the front of the science lab.

– Fire blankets are not the best means to extinguish a fire. They may be used to extinguish clothing that is burning, but should never be used on any other type of fire.

– Fire blankets are a good means to keep shock victims warm.

Fire Extinguisher:

– The fire extinguisher is located on the lab wall.

– Only the science facilitator is authorized to use the fire extinguisher.

– Fire extinguishers are classified according to a particular fire type and are given the same letter and symbol classification as that of the fire.

– Types of extinguishers:

• TYPE A -- Combustibles wood, cloth, paper, rubber and plastics.

• TYPE B -- Flammable liquids, oil, grease and paint thinners.

• TYPE C -- Energized electrical equipment

• TYPE D -- Combustible metals (magnesium, titanium, sodium, lithium, potassium).

• Multipurpose Extinguishers are an effective agent against Types A, B, and C fires.

Our laboratory fire extinguisher is Type ABC.

– To effectively operate an extinguisher, think P-A-S-S.

• P -- pull the pin

A -- aim the hose at the base of the fire

S -- squeeze the handle

S -- sweep the hose back and forth

Protect others

• Clean-up is important for the safety of others and for the preservation of equipment.

• Your lab station and equipment should be cleaned before you worry about the lab report.

• What clean-up should be done after each lab?

– Dispose of chemicals as directed by your teacher

– NEVER put unused chemicals back into their original container.

– Return chemical containers to the chemical table.

– Wash and dry all glassware, then store properly.

– Clean hardware, but DO NOT wash. If any hardware is wet, dry completely before storing. This is to prevent rusting.

– Clean and dry your lab table.

What is SDS ?

• S afety D ata S heet

• A “non-standard” form required of all chemical distributors

• Must contain all relevant information on a chemical including but not limited to:

– health, fire, poison, & causticity hazards

– first aid

– controls/special protections

– carcinogens

– physical/chemical characteristics

– spill/leak procedures

Where Do We Find the SDS?

SDS sheets are maintained in each:

– chemical storeroom

– preparation room

Ask your instructor if you wish to see one.

You are expected to check SDS online for every lab.

(http://avogadro.chem.iastate.edu/msds/M

SDS_S.html)These sheets can be found on flinnsci.com. You should note storage, safety precautions, and skin damage.

The NFPA Diamond

• N ational F ire P rotection A ssociation

• “Standardized” labeling system for chemical hazards

• Includes four color codes red (flammability) blue (health) yellow (reactivity)

• Numerical Ratings o= no hazard white (special warnings)

1= slight 2= moderate

3= severe 4= extreme

• Used by KHS Science Department

Flammability

Health

NFPA Hazard

Label

Reactivity

• Required on all chemical labels

• Scale value from 0-4

Special Notice

3

4

OXY

2

NFPA Hazard

Label

1 What is the greatest safety hazard for the chemical illustrated to the left?

2 What is the reactivity value of the chemical?

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