Marco Ferrero With Nicolo’ Cartiglia, Francesca Cenna, Fabio Ravera, Universita’ degli Studi di Torino & INFN 1 Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 • THEORY OF EXTRAPOLATION OF DOPING PROFILE FROM CAPACITANCE-VOLTAGE CURVES • LABORATORY SETUP • DESCRIPTION OF THE METHOD FOR DETECTORS WITHOUT GAIN • PRESENTATION OF THE RESULTS • FUTURE GOALS 2 p type Depleted Zone Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Measuring doping profile of a pn junction using the Capacitance-Voltage Curve n+ type Capacitance depends upon the area and width of depleted zone Depleted zone can be considered as a Parallel Plate Capacitor Case of NA << ND Width of depleted zone depends upon Voltage bias and doping concentration 3 Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Detector as a Trapeziodal Parallel Plate Capacitor n++ impiantation Detector CNM Run 6474 W9B6-Gain 1 Plate A Parallel plate capacitor p substrate Trapezoidal parallel plate capacitor Plate A x Plate A ≠ Plate B Plate B Plate B 4 Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Capacitance of a Trapezoidal parallel plate capacitor By the Gauss’ Theorem Plate A x Plate B parallel plate capacitor Additional contribution constant that depends upon the geometry of the detector a side of n-implantation b side of b substrate d width of detector 5 Capacitance-Voltage Curve Setup Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Laboratory PC Power supply Keithley 2410 LCR Meter Agilent E4980A Device 6 Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Setup test: measurement of a known capacitor RESONANCE CORRECT Value (~ 34pF) Verify the setup using a known capacitor 34 pF Scan in frequency from 50 Hz to 2 MHz Good frequency range of measurement [10 kHz ; 2 MHz] 7 Capacitance-Frequency curve Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 The detector is an extended network of resistors and capacitors The sensor acts as a low pass RC filter By scanning in frequency at fixed Voltage, a variation of the detector’s capacitance is observed Due to a smaller effective Area Capacitance-frequency curve shows a variation of detector’s area 8 Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Capacitance-Frequency curves at different Voltage We need to find a frequency that works well at every bias voltage. The measurements should follow the known relation between C and V. C-f (2 Volt) C-f (25 Volt) C-f (36 Volt) 9 dependency Fit Equation 7E-11 30kHz is a good frequency to work y = 9E-11x-0.518 6E-11 Capacitance [F] Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Fit to the C-V curves with the expected to select the good working frequency y = 5E-11x-0.392 5E-11 y = 3E-11x-0.276 Frequency of 30kHz 4E-11 Frequancy of 500kHz Frequancy of 1MHz 3E-11 Frequency of 30kHz Frequency of 500kHz 2E-11 Frequency of 1MHz 1E-11 0 0 20 40 60 Voltage [V] 80 10 Effect of the Trapezoidal correction 2.5E+22 Parallel plate No Cg correction Cg correction 2E+22 1/C2 [F-2] Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 For a parallel plate capacitor: 1/C2 vs Vbias should be a straight line 1.5E+22 For detector W9B6-Gain 1 Cg is about 4,69 pF 1E+22 Trapezoidal plate 5E+21 0 0 50 100 Voltage Bias [V] 150 200 11 Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Capacitance-Voltage and 1/(C2)-Voltage curve 1/(C2)-V Curve acquired at 30 kHz (Cg Corrected) Above 120 V the measurement is hard to understand 12 Width of depleted zone [um] Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Width of the depleted zone 380 330 280 Note: 360 um is too large 230 Fit Equation: 180 It’s necessary improve the absolute scale, i.e. precise knowledge of the Cg correction y = 36.924x0.5025 130 80 30 -20 0 20 40 60 80 100 120 140 Voltage Bias [V] Respected the relationship between width of depleted zone and Voltage bias 13 Extraction of the Doping profile 4.00E+12 3.50E+12 NA [cm-3] Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 To extrapolate the doping profile: calculate the derivative of 1/(C2)-V curve 3.00E+12 2.50E+12 VALUE CONSISTENT WITH EXPECTATIONS 2.00E+12 1.50E+12 1.00E+12 5.00E+11 0.00E+00 9 11 19 28 38 45 55 67 79 92 107 122 w [um] Due to the Built-in Voltage, the depth is already 9 microns at Voltage Bias=0 14 n++ p+ p 2E-10 1.8E-10 In LGAD detectors, the value of capacitance is increasing with Voltage. Why?? 1.6E-10 Capacitance [F] Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 Study of LGAD Detector 1.4E-10 It’s necessary to study and better understand the Capacitance-Voltage curve of a Detector with gain. 1.2E-10 1E-10 8E-11 6E-11 4E-11 2E-11 0 0 20 40 60 80 100 120 Voltage [V] 15 Marco Ferrero, Universita’ Di Torino, INFN, Tredi2015 The CV method illustrated allows the measurement of the doping profile in silicon sensors. The method gives the correct doping concentration for standard pin diods Application of the method on LGAD sensors under study Need to improve the Cg correction to the capacitance for a better width absolute scale 16