Lab Packet Handout

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Name: ______________________________________________
Date: Sep. 5/8, 2014
Labs & Activities
Portfolio Project – Chemistry I
Identity by Density Lab
Important Dates:
A Day Dates
September 5
September 9
September 11
September 15
September 17
B Day Dates
September 8
September 10
September 12
September 16
September 18
In Class…
Lab explained and assigned
Do the lab, explore the criteria, turnitin.com sign-up
Writing time in class
Writing time in class
Writing time in class
DUE by 11:59 PM on turnitin.com
Late lab reports will be penalized 5% each day late
Sections of Lab Report: Use this to ensure that you have included all required
pieces. Find the template on the class website!
1. Title page (on its own page – use Resource packet for proper formatting)
2. Purpose (1 complete sentence)
3. Materials (includes a bulleted list of all materials including all chemicals used in the lab)
4. Procedure (copied from the procedure on the class website, you DO NOT write this)
5. Lab Safety (is a bulleted list that is specific to the lab)
6. Data (this is a table)
7. Analysis (using Microsoft Equation Editor – use Resource packet for directions)
8. Conclusion (typed in paragraph form)
9. Application (typed in paragraph form)
10. Works Cited (on its own page – use Resource packet for proper formatting)
See rubric for grading criteria
of each part
Introduction:
Because density is an intensive property, any element should be able to be identified through
a series of density measurements and calculations. The purpose of the lab is to identify the
unknown element by determining its density. To do this, you will be measuring the density of your
unknown element three times, from which you will calculate the average density of that element.
You will then be able to compare your average density to the known density values of several
different elements and calculate your percent yield to determine how accurate the experiment was.
Key Terms:
Intensive Property:
Density =
Percent Yield:
Purpose: What is the purpose of this lab? Write ONE sentence only.
The purpose of this lab is _____________________________________________________________________________________
__________________________________________________________________________________________________________________
__________________________________________________________________________________________________________________
Re-Phrase of Purpose: Write the purpose in a different way. Write ONE sentence only. Use this in conclusion.
__________________________________________________________________________________________________________________
__________________________________________________________________________________________________________________
__________________________________________________________________________________________________________________
__________________________________________________________________________________________________________________
2
Materials: This should be a bulleted list of
your materials so that they are properly included in your lab report.
They should include all chemicals as well.
Don’t forget to include your unknown element NUMBER and DESCRIPTION of the element using
observations.
Element # _________ (description: ____________________________________________________________________________)
Procedure: The procedure is provided for you but must still be included in your lab report. This procedure will be
uploaded to the class website so that you can copy and paste it into your report.
1. Unequally separate the element into three mass boats.
2. Mass the three element samples on the balance. Record in data table.
3. Fill the graduated cylinder with between 20-30 mL of water. Record the exact initial volume
in data table.
4. Put all of the contents of the first mass boat into the graduated cylinder with the water.
Record the final volume in the data table.
5. Pour out the water and retrieve and dry the element sample.
6. Repeat steps 3-5 with the remaining two samples of the element.
Lab Safety: This should be a bulleted comprehensive so that a scientist can safely repeat your experiment.
3
Data: Includes a data table. This table should be in your lab report.
Measurement
m
a
b
v=a–b
m/v
Mass (g)
Initial Volume
of Water (mL)
Final Volume
of Water (mL)
Volume of
Unknown (mL)
Density
(g/mL)
1
2
3
Analysis: This includes all the work needed to calculate density (see bullet list). In your lab report, this should be
included typed using Microsoft Equation Editor. See example on the next page.

Density calculation for one of the measurements.

Average calculation for the three density measurements.
Average =

Determine the identity of the unknown element. Your element is aluminum (Al), copper (Cu)
or zinc (Zn). First, research the known densities of these elements and record them here.
Element
Density (g/mL)
Aluminum (Al)
Copper (Cu)
Zinc (Zn)
**Source of information: write down the MLA citation here, to use in your Works Cited page.
Based on the research, what was the unknown element? Compare the average density
calculated above to the known densities of the elements in the table. Use the density that is
closest to the average density that was calculated. This should be written in sentence form.

Percent yield calculation using the actual density average (from your data) and the expected
density (from the table of known densities you researched).
4
Example of what using Equation Editor should look like:
Using Microsoft Equation Editor allows you to set up your analysis like this! (Note that the
numbers here are just an example and not the same as the ones expected in your report. The
setup should look just like this, except for the notes in white.) For directions on how to
use Equation Editor, look at your resource packet.
Density of Measurement 1:
11.2g
= 2.01 g mL
5.57mL
Notice the UNITS!
Average Density:
2.01+1.85 +1.92 5.78
=
= 1.93 g mL
3
3
Based on the average density of 1.93g/mL, the element in this experiment was magnesium
because it had the closest known density of 1.74g/mL.1
Percent Yield:
1.93
´100 = 111%
1.74
A percent yield of 111% means that the density calculated in
the lab was 11% above the actual density of the element.
Conclusion: Includes the following criteria in complete PARAGRAPH form:
Paragraph #1:
 Concise summary of the lab:
o Rephrase of the purpose (use the second re-phrased one from pg. 2)
o Define key terms from lab (pg. 2)
o Briefly describe what you did in the lab (in 1 or 2 sentences) – How did you
measure density? This should not be a step-by-step procedure.
Paragraph #2:
 Summary of the results and analysis. This should include:
o The three density measurements (from Data)
o The average density calculated (from Analysis)
o The identity of the element
 Sentence Starter: The identity of the unknown element is _______ because…
o The percent yield of the actual density compared to the theoretical density of the
element.
o What does this percent yield mean? (look at 2nd white box on Equation editor
sample above)
 Sentence Starter: A percent yield of ______% means that …
5
A
Application: This will be written in complete PARAGRAPH form:
This is a completely different scenario from the lab you completed. It has nothing to do with the same
element.
You have a new sample of an element, which is a yellow colored solid. Unfortunately, you do
not have the appropriate materials to determine its density. You do, however, have the materials to
measure its melting point. You follow a very similar procedure – you split your element into three
smaller samples. You then carefully melt each sample using a Bunsen burner and a thermometer.
The results of your melting point experiments are below:
Measurement
Melting Point
(oC)
1
105
2
122
3
110
Calculate the average melting point of this element:
Use the physical description of the element along with the average melting point calculated to
research what element you have in this scenario. Use the source provided on the class website.
In your paragraph include:
 What was the average melting point of the element?
 What is the identity of this element? How do you know? (use in-text citations based
on your research)
 Both melting point and the physical description are intensive properties. Why can
these be used to identify an unknown element?
 Why was more than the melting point needed to identify the element? Hint: if I had
just given you melting point, you likely would have misidentified the element…
6
B
Application: This will be written in complete PARAGRAPH form:
This is a completely different scenario from the lab you completed. It has nothing to do with the same
element.
You have a new sample of an element, which is a silver colored solid. Unfortunately, you do
not have the appropriate materials to determine its density. You do, however, have the materials to
measure its melting point. You follow a very similar procedure – you split your element into three
smaller samples. You then carefully melt each sample using a Bunsen burner and a thermometer.
The results of your melting point experiments are below:
Measurement
Melting Point
(oC)
1
38
2
43
3
40
Calculate the average melting point of this element:
Use the physical description of the element along with the average melting point calculated to
research what element you have in this scenario. Use the source provided on the class website.
In your paragraph include:
 What was the average melting point of the element?
 What is the identity of this element? How do you know? (use in-text citations based
on your research)
 Both melting point and the physical description are intensive properties. Why can
these be used to identify an unknown element?
 Why was more than the melting point needed to identify the element? Hint: if I had
just given you melting point, you likely would have misidentified the element…
76
C
Application: This will be written in complete PARAGRAPH form:
This is a completely different scenario from the lab you completed. It has nothing to do with the same
element.
You have a new sample of an element, which is a silver colored liquid. Unfortunately, you do
not have the appropriate materials to determine its density. You do, however, have the materials to
measure its boiling point. You follow a very similar procedure – you split your element into three
smaller samples. You then carefully boil each sample using a Bunsen burner and a thermometer.
The results of your boiling point experiments are below:
Measurement
Boiling Point
(oC)
1
345
2
340
3
341
Calculate the average boiling point of this element:
Use the physical description of the element along with the average boiling point calculated to
research what element you have in this scenario. Use the source provided on the class website.
In your paragraph include:
 What was the average boiling point of the element?
 What is the identity of this element? How do you know? (use in-text citations based
on your research)
 Both melting point and the physical description are intensive properties. Why can
these be used to identify an unknown element?
 Why was more than the boiling point needed to identify the element? Hint: if I had
just given you boiling point, you likely would have misidentified the element…
68
D
Application: This will be written in complete PARAGRAPH form:
This is a completely different scenario from the lab you completed. It has nothing to do with the same
element.
You have a new sample of an element, which is a bluish-white colored solid. Unfortunately,
you do not have the appropriate materials to determine its density. You do, however, have the
materials to measure its boiling point. You follow a very similar procedure – you split your element
into three smaller samples. You then carefully boil each sample using a Bunsen burner and a
thermometer. The results of your boiling point experiments are below:
Measurement
Boiling Point
(oC)
1
1744
2
1740
3
1732
Calculate the average boiling point of this element:
Use the physical description of the element along with the average boiling point calculated to
research what element you have in this scenario. Use the source provided on the class website.
In your paragraph include:
 What was the average boiling point of the element?
 What is the identity of this element? How do you know? (use in-text citations based
on your research)
 Both melting point and the physical description are intensive properties. Why can
these be used to identify an unknown element?
 Why was more than the boiling point needed to identify the element? Hint: if I had
just given you boiling point, you likely would have misidentified the element…
69
E
Application: This will be written in complete PARAGRAPH form:
This is a completely different scenario from the lab you completed. It has nothing to do with the same
element.
You have a new sample of an element, which is a silvery-gold colored solid. Unfortunately,
you do not have the appropriate materials to determine its density. You do, however, have the
materials to measure its boiling point. You follow a very similar procedure – you split your element
into three smaller samples. You then carefully boil each sample using a Bunsen burner and a
thermometer. The results of your boiling point experiments are below:
Measurement
Boiling Point
(oC)
1
680
2
681
3
671
Calculate the average boiling point of this element:
Use the physical description of the element along with the average boiling point calculated to
research what element you have in this scenario. Use the source provided on the class website.
In your paragraph include:
 What was the average boiling point of the element?
 What is the identity of this element? How do you know? (use in-text citations based
on your research)
 Both melting point and the physical description are intensive properties. Why can
these be used to identify an unknown element?
 Why was more than the boiling point needed to identify the element? Hint: if I had
just given you boiling point, you likely would have misidentified the element…
10
6
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