Lab Final Review Spring 2012 Chem 1111 Format • Definitions, calculations, short answer, True/false • Questions from all labs – Know terms and calculations associated with each experiment; Safety precautions – Know glassware and equipment used throughout semester. • Parts of a Scientific Report: Writing Lab Reports and Scientific Papers - Know what goes into each part • Safety Rules • MSDS What is it and what info is in it • Techniques and procedures • Plotting Data and the meaning of a graph Exp 1C –Some Measurements of Mass and Volume • Know how to correctly measure volume, mass – Uncertain digits!!! • Calculate density • Use correct sigfigs • How to use standard deviation on a set of data Math for Chemistry: Dimensional Analysis • Know how to perform all calculations – Density, mols, molecular weight, concentration, % water, % yield, hydrates, titrations Exp 1A – Identification of An Unknown Compound • Physical vs. chemical properties • How density and boiling point are useful in identifying unknown liquids • How to use critical thinking and the process of elimination to identify unknowns from sets of reactions Exp 3A – The Empirical Formula of an Oxide • Know the difference between mixtures, elements, pure substances. • Heating, Combustion/ignition techniques • Know the sequence of calculations: – Stoichiometry – Mass and % Exp 3B – Hydrates and their Thermal Decompositions • Calculate % water • Calculate formula of hydrate Exp 4A – Conductivity of Aqueous Solutions • • • • • Indications of a reaction Types of reactions observed Balance chemical equations Write Ionic Equations Know the effects of adding two solutions of ionic compounds, additivity principle, solutions of an acid and a base Exp 4B – Ionic Reactions in Aqueous Solutions • Write and Balance Ionic Equations, net ionic equations • Use solubility tables to predict formation of precipitates • Compare results to identify an unknown Exp 4C – How Much Acetic Acid is in Vinegar? • Know what a titration is and why we do them. • Macid Vacid = Mbase Vbase for a mole ratio of 1:1 • Macid Vacid x b moles = Mbase Vbase for a mole ratio other than 1:1 • Difference between endpoint and equivalence point • Role of indicator and pH in titration • Calculations for % acid • Study the links on titration technique Exp.9 – Analysis of KClO3 – KCl mixture • Molar ratio concept – Calculate moles of product from moles of reactant and balanced equation. Exp 7 – The Absorption Spectrum of CoCl2 • • • • Beer’s Law – in words and as an equation The meaning of a standard curve How to use linear regression How to find standard deviation and use it in reporting experimental values • How a spectrophotometer works Exp 9A – The Identity of an Insoluble Precipitate • Know how to use stoichiometry to calculate limiting reagents • Use ratios to identify the product • Draw Lewis structures of related ions Exp 6 – Thermochemistry and Hess’s Law • • • • Exothermic vs. endothermic Basis for calorimetry Free energy, entropy, enthalpy (temp change) Draw a cooling/heating curve and extrapolate values Exp 19A – Oxidation – Reduction Reactions • Identify: • Substance oxidized, reduced • Reducing agent, oxidizing agent • Make inferences from observed changes