Laboratory Electrical Safety Section I: Principals of Electricity Statistics Ohm’s Law Alternating vs. Direct Current Effects on the Human Body Lab Safety Manual Yearly Statistics in the US involving Electrical Accidents 200,000 - Accidents 150,000 - Fires 700 - Deaths Electrical Accidents are the third leading cause of industrial deaths in the US (NIOSH Alert, December, 1986, Publication Number 87-103.) This course covers electrical safety involving household level voltages (240 and below), and is not intended to cover power line applications. Overhead lines are not insulated and carry between 7,200 and 500,000 volts. Never allow a conductor to touch an overhead power line (aluminum ladder, CB antenna, tent pole, backhoe shovel, TV antenna etc.) Ohm’s Law of Electricity V=IR V = electrical potential (volts) I = electrical current (amps) R = resistance (ohms) Voltage is almost always a constant so electrical current levels are determined by the resistance to flow. When there is a potential for electrical shock we can protect ourselves by maximizing our resistance to current flow. This is done by wearing insulating shoes and gloves, and by not making direct contact with a source of ground potential such as plumbing or other sources of ground. Our skin provides us with a natural barrier or resistance of approximately 1,000 to 100,000 ohms depending on several factors including skin thickness and surface moisture. Alternating Current (AC) + 0 Volts - Time (sec.) Direct Current (DC) + 0 Volts - Time (sec.) Alternating current or AC is what comes out of wall outlets. In the United States the direction of flow of AC changes at a rate of 60 cycles/sec (hertz). Direct current or DC flows in one direction. Properties: Shocks involving AC tend to push the recipient away while shocks involving DC tend to grab hold of the recipient making it difficult for them to get away from the shock source. Effects of Electrical Shock on the Human Body Perception Threshold Painful Shock 0.5% Painful Shock 99.5% Ventricular Fibrillation Direct Current Men Women 5.2 3.5 62 41 90 60 500 500 Alternating Men Women 1.1 0.7 9.0 6.0 23 15 675 675 All Units are in milliamps Reference: Introduction to Safety in the Chemical Laboratory, N. T. Freeman, J. Whitehead, Academic Press, New York, 1982, pg. 41. Lower levels of AC than DC will produce painful shocks in humans while lower levels of DC than AC can lead to fibrillation of the heart muscle. Women are more sensitive to the effects of both AC and DC than are men. The University of Georgia’s policies governing electrical safety can be found in the Laboratory Safety Manual (http://www.esd.uga.edu) in Section 2.X, and additional locations. Section Contents 2.X Power cords, extension cords, surge protectors 2.I.2.f Bonding and grounding of flammable liquid containers 2.IV.E Spark sources and flammable materials 2.VIII.B Explosion proof refrigerators for flammable material storage Appendix J-21 Explosion proof refrigerators for flammable material storage Section II: Common Electrical Problems Extension Cords and Power Strips Power Cords Solvents and Electricity Water and Electricity Laboratory Equipment Capacitors and Transformers Power Strips Power strips are approved for use only with computers and computerized equipment. They must be UL 1449 rated (surge suppressed). Power strips should be used sparingly. Care must be taken not to overload power strips. Extension Cord Hazards Extension cords are approved for temporary use only. If extended use is required, hard wiring such as a new outlet should be installed. Extension cords are easily frayed, a condition which may expose bare wires. If not properly placed, extension cords may also become a trip hazard. Common Power Cord Problems Exposed Wires Power cords are doubly insulated and should be replaced if the outer layer of insulation becomes frayed exposing wires. Normal Short circuit Plug V = IR As resistance decreases, current increases. Overloaded circuit A B C D Outlet or Power Strip Shorts cause a great increase in the flow of current through the cord producing heat and perhaps initiating a fire. Overloads occur when more current flows through a cord than it is rated to handle. Power strips can be overloaded if too many high current draw devices are plugged in at one time. Electrical Requirements of Common Laboratory Equipment Instrument Current (A) Balance 0.1 - 0.5 Bio. Cabinet 15 Blender 3 - 15 Centrifuge 3 - 30 Chromatograph 15 Computer (PC) 2-4 Furnace/Oven 3 - 15 Heat Gun 8 - 16 Heat Mantle 0.4 - 5 Hot Plate 4 - 12 Kjeldahl Diges. 15 - 35 Refrigerator 2 - 10 Sterilizer 12 - 50 Water Still 8 - 30 Vacuum Pump 4 - 20 Power (W) 12-60 1,800 400 - 1800 400 - 6000 1,800 400 - 600 500 -3000 1000 - 2000 50 - 600 450 - 1400 1800 - 4500 1000 - 5000 <12,000 1000 - 5000 500 - 2500 CRC Handbook of Laboratory Safety, A. Keith Furr, CRC Press, Boca Raton, Fl, 1990, pg. 331. Common laboratory equipment such as centrifuges and ovens are high current draw devices. If two or more high current draw devices are plugged into the same outlet or power strip an overloaded circuit may result. Overloaded Circuit Another common way in which power cords can be overloaded is by plugging one power strip into another. All of the current drawn by any device plugged into any of the strips must flow through a single cord Care must be taken to insure that power cords do not come in contact with hot surfaces such as the top of a hot plate where they may melt exposing bare wires. Frayed or melted cords should be replaced immediately before bare wires are exposed. Solvents and Electricity Common household refrigerators employed in laboratories must have a “LABORATORY USE ONLY” sticker. Household refrigerators should never be used for the storage of flammable liquids due to the many spark sources that are present. NFPA Rating System Flammability 3 Health 1 0 W Special Reactivity The NFPA (National Fire Protection Association) diamond provides a quick visual indication of the hazardous properties of a substance. A rating a rating of 3 or 4 indicates a severe hazard. Flammable liquids (NFPA flammability rating of 3 or 4) that require refrigeration must be kept in either an explosion proof or a flammable storage refrigerator. Explosion proof and flammable storage refrigerators are specially designed for flammable liquid storage. The interior of these two types of refrigerators do not contain any potential spark sources such as lights and switches. Mantle Heater Variac Flammable solvents must never be heated with an open flame or other potential ignition source. When solvent heating is required, mantles or other spark free sources must be employed. Mantle heaters must be plugged into a control device such as the Variac pictured in the lower right hand corner of the illustration. Mantles must never be plugged directly into a wall outlet. Variacs and other spark sources such as power strips must be located outside of any fume hood where flammable vapors are present. Bonding Strap Grounding Strap Dispensing Container greater than 5 gallons Earth Ground When dispensing flammable liquids from containers larger than 5 gallons, the containers must be bonded and grounded to prevent build up of static electricity. Bonding is achieved by making a conducting connection between both containers using grounding straps or thick copper wire. Grounding is achieved by making a conducting connection between the larger vessel from which liquids are dispensed, and earth ground. When non metal containers are employed, bonding and grounding is performed by making direct contact with the liquid. Many plastics such as those found in truck bed liners readily hold static charge. Explosions can occur when gas cans are placed on a bed liner before they are filled. The build up of static electricity is most likely to be a problem on cold dry days. Water and Electricity Outlet without GFCI Eyewashes should be located away from electrical devices and outlets. Outlets within six feet of a sink or other source of plumbing must be GFCI protected in order to minimize shock hazards. An unprotected outlet (non-GFCI) is illustrated above. Safety showers must not be located directly over switches, outlets, equipment, or other sources of electrical energy such as those shown in the picture to the left. Exposed Wiring Oil immersion bath Oil immersion baths are often employed to control the temperature of a reaction. The wire coil that comprises the heating element must be hard wired (soldered to a plug and insulated). Oil immersion baths should never be connected to a source of electrical power by the use of banana clips or other temporary connections. Power supplies represent a potentially lethal source of electrical energy. Exposed connectors such as banana clips (alligator clips) should never be attached to a power supply or any other high voltage, high current producing device. Cable Connectors BNC Signal lead or feed-through Recessed lead MHV BNC connectors are used with standard (household) very low voltage devices such as cable TV boxes. BNC connectors should never be used for high voltage applications. MHV Additional connectors are often used to shielding connect equipment to high voltage sources such as power supplies. MHVs have recessed signal leads or feed-throughs, and have additional shielding at the end of the connector Capacitors are located inside of all laboratory equipment. They come in many different shapes and sizes. Capacitors can remain energized and produce harmful shocks long after a piece of equipment has been unplugged. A discharge delivering 10 joules of energy can be lethal. Ten joules of energy can be delivered by the discharge of even small highly energized capacitors (0.2 microfarads charged to 10 KV etc.). Capacitance (mF) 0.2 20 80 320 3000 Charge (KV) 10 1 0.5 0.25 0.1 Note that 320 microfarad (and larger) capacitors can deliver lethal shocks when charged to household voltage levels (250 V). Capacitors may also contain PCBs or polychlorinated biphenyls. Capacitors which contain PCBs must be disposed of properly in accordance with regulations governing PCBs. Typical Transformer Transformers are potential sources of high voltage and may also contain polychlorinated biphenyls. Electrophoretic equipment containing high voltage power supplies and signal leads are found in many laboratories. Care must be taken to use only approved equipment. Electrophoretic setups should never be homemade or modified. Leads should be checked periodically for frays. Section III: Working Safely with Electricity Grounds and Wires Circuit Testers Surge Suppressors and GFCIs Lock Out/Tag Out Safety Rules First Aid Fire Fighting Three types of Ground Connections Earth Equipment Virtual Three types of ground connections are commonly found. Virtual (also know as floating) grounds are not true grounds and may be energized. If a connection is made from an energized virtual ground to either an equipment or an earth ground, current will flow (shock potential). Outlet Wire Color Conventions Several different outlet wiring color conventions exist, but don’t take anything for granted. It is always best to check rather than to assume that a wire is hot or neutral based upon the wire color. Typically the hot wire is black, the neutral or return wire is white, and the ground wire is green. Circuit Analyzer Light Configuration Condition Open (unconnected) ground Open neutral Open hot Hot and ground reversed Hot and neutral reversed Correct wiring Inexpensive circuit analyzers can be used to determine if an outlet is wired correctly. Open ground means that the receptacle is not connected to earth ground. The term hot and neutral reversed is also called reversed polarity. Connection Tester Fuse Multimeter Range Selector V/ohms common amps To Outlet Connection testers are use to determine if a circuit is energized. Multimeters are used to measure the voltage, resistance, or current flow of a circuit or resistor. Both devices should only be used by trained personnel. Function of a Typical Surge Suppressor Spike Input wave form Output wave form Surge suppressors reduce voltage spikes and transients (surges). All surge suppressors and/or power strips used on campus must be UL (Underwriters Laboratories) 1449 rated. Check the back of your power strip/suppressor for a UL sticker. Function of a Typical GFCI Switches Hot Line In GFCI Receptacle Current Sensor Load Neutral Line In A GFCI or ground fault circuit interrupter shuts off the flow of current upon sensing a fault condition such as an electrical shock. Switches quickly open in the GFCI device in order to prevent the shock victim from receiving a lethal amount of electricity. GFCI Use Any outlet within 6 feet of a sink or other source of plumbing should be equipped with a GFCI. Recalling Ohm’s law, V=IR, very low resistances such as an earth ground (plumbing etc.) allow for very high levels of current flow. Typical GFCI Outlet Receptacles containing a GFCI are noted by the test and reset buttons, and should be tested monthly to insure proper operation. GFCI device may be located at a circuit breaker instead of an outlet. This arrangement allows several outlets to be protected with a single GFCI device. Breaker locked in off position Lock out/Tag out To insure the safety of repair personnel, electrical panels and equipment with electrical panels must be locked out and equipment tagged out of service before any repairs are performed. The lock must never be removed from an electrical panel until repairs have been completed, and only then by an individual with the appropriate authority. Repairs must only be performed by trained professionals. Common Lock-out Signage Common Tag-out Signage Locked out and tagged out equipment must be clearly labeled so that no unauthorized personnel turn on the power or try to use equipment that is under repair. Rules for Working Safely with Electricity 1. Don’t attempt any work that you feel uncomfortable performing. 2. Wear proper insulating boots and gloves as necessary. 3. Follow Lock-out Tag-out procedures as required. 4. For higher voltage applications, keep one hand in your back pocket to keep a circuit from being completed across your heart. 5. Know the location of any kill switches and cut off switches. 6. Before working near capacitors, allow them to fully discharge. 7. Post emergency numbers by the telephone. 8. Never touch an energized person with your bare hands but rather use a wooden broom or other non-conductor to push them away from a source of current. First Aid for Electrical Shock Victims The most common symptom of electrical shock is physical shock. Signs of physical shock include: 1) Cold, clammy skin 2) Pale face 3) Chilled feeling or patient is physically shaking 4) Nausea or vomiting 5) Shallow breathing. Approved Treatment for Physical Shock Patients 1) Keep patient lying down 2) Keep airway open 3) Elevate patients’ legs if no bones are broken 4) Keep patient warm if conditions are cool or damp 5) Give fluids if patient is able to swallow 6) Never give alcohol to patient 7) REASSURE the patient Test tag should be current Electrical Fires Small Nozzle Dry chemical extinguishers (also know as ABC extinguishers) are approved for fighting electrical fires. The label indicates the type of extinguisher that is present. Electrical fires should only be fought if the situation is well in hand. If you feel uncomfortable fighting a fire, pull the alarm and exit the building. ABC indicated on label Pressure Gauge Label indicates type A Type A fire extinguishers use water to put out fires. They are not approved for use on electrical fires. Type A extinguishers are denoted by a pressure gauge at the top of the unit that indicates whether or not the extinguisher is fully charged. All type A extinguishers have been removed from service on the UGA main campus. Type B or carbon dioxide (CO2) fire extinguishers should also not be used to fight electrical fires due to the possibility of moisture condensing on electrical circuits. Carbon dioxide extinguishers are denoted by the large funnel nozzle. Funnel Nozzle This training was developed by Wes Kolar of the UGA Environmental Safety Division. Please direct any questions or comments to ESD at the following number: (706 5425801), or contact us through our web site (www.esd.uga.edu).