Lab L b Equipment E ipm nt Safety Goggles For the highest level of protection, safety goggles that completely cover the eye and eye socket and seal against the face are recommended. Lab Apron (folded) Beaker Beakers hold solids or liquids li id th thatt will ill nott release gases when reacted or are unlikely y to splatter if stirred or heated. Beaker Tongs Beaker tongs are used to move beakers containing hot liquids. liquids Erlenmeyer Flask Erlenmeyer flasks, sometimes called cone cone-shaped flasks, flasks hold solids or liquids that may release gases during a reaction or that are likely to splatter if stirred or heated. Volumetric m Flasks Volumetric flasks come in a variety of sizes and are used to make solutions of exact concentrations. Flask Tongs Graduated Cylinder A graduated cylinder is used to measure volumes of liquids. Always use the smallest one that accommodates the amount you need to measure and record the measurement to the first estimated digit; i.e., read between the lin f lines for th the fin finall di digit. it Funnel A f funnell iis used d to aid in the transfer of liquid q from one vessel to another or, with filter paper, paper to separate a solid from a liquid. Rubber Stoppers Rubber stoppers are used to close containers to avoid spillage or contamination. Containers should never be heated when there is a stopper in place. Test Tubes Test tubes come in a variety of sizes and are generally used as reaction vessels. They may be heated over a Bunsen burner or placed in a water bath for heating or cooling purposes. Test Tube Holder A test tube b holder h ld is useful for holding a test tube which is too hot to handle. This instrument is NOT a test tube clamp! Clamps attach h one thing hi to another thing. Test Tube Racks Test tube racks are for holding and organizing test tubes on the laboratory y counter. Plastic racks may y melt in contact with very hot test tubes. Test Tube Brushes T t tube Test t b b brushes h are used to clean test tubes and g graduated cylinders. y Bristles should not be hard enough to scratch the glass surfaces. Forcing F i a llarge b brush h into i t a small test tube will often break the tube. MicroMicro -Well Plates Micro-well plates are used Microto perform many small scale reactions at one time. The use of micromicro-well plates can reduce lab costs and is often safer (due to the smaller amounts used) than fullfull -scale experiments. experiments Glass Plates Glass plates provide a surface f f for semisemii-micro i scale experiments, such as drop p reactions and testing of acids and bases. Watch Glass W A watch glass is used to hold a small amount of liquid or solid or as a cover for a beaker. Evaporating Dish The evaporating dish is used for recovering a solid solute from a solution by evaporating off the solvent. Evaporating dishes may be heated gently. gently Crucible Crucibles are used for heating substances to very high temperatures. temperatures Crucible Tongs Crucible tongs are used with crucibles to avoid adding mass from finger oils and when handling hot crucibles. ibl They y may y also used to pick up other hot objects, but NEVER to pick up beakers! Mortar and Pestle A mortar and pestle is used to grind solids into powders. pestle mortar Spatulas / Scoopulas l Spatulas Spatulas and scoopulas are used to dispense solid chemicals from their containers. Scoopula Chemicals should NEVER be transferred with your b bare h hands. d Plastic Chemical Spoon Plastic chemical spoons are used when the metal of a regular spatula might react with i h chemicals h i l being used. Forceps Forceps are used to pick up small objects. Weigh g Boat Weigh boats are used to weigh (mass) solids that will be transferred to another th vessel. l Weighing g g paper, p p sheets of coated paper squares, may also be used to weigh (mass) solids. solids NEVER place chemicals directly on a balance!!! Analytical y Balance Analytical balances are used to find mass precisely to three or four decimal places. Glass Stir Rod A glass rod is used to manually y stir solutions. It can also be used to control the transfer of a liquid or even a single drop of a solution. Thermometers Pipets and Pipet Bulb A p pipet p measures and delivers exact volumes of liquids. Buret (on ring stand) Eudiometer Gas Collection Tube WideWide -Mouth Bottle (Gas Collecting Bottle) Wide-mouth bottles are Wideused to collect gases by the displacement of water. water Pneumatic Water Trough Water Trough g for Collecting g Gas Medicine Dropper A medicine dropper is used to transfer a small volume of liquid (less than one mL). mL). On O top of f each h medicine di i dropper d is i a “rubber “ bb bulb.” b lb ” NEVER turn the dropper upside down or allow liquid to enter the bulb. Wash Bottle A wash bottle has a spout that delivers a wash solution to a specific area. Distilled water is the only liquid that should be used in a wash bottle. bottle Ringstands g and their Components p A ringstand consists of a h heavy metal t l base b and d screwscrewin metal rod to which various items may y be attached. The use of ringstands and their components (see following slides) provide a safe and convenient way to attach tt h and d supportt a wide id variety of items required in many y experimental p procedures. Ringstands and their Components Iron Rings Iron rings connect to a ringstand g and p provide a stable, elevated platform. Clay Triangle The clay triangle is used as a support for porcelain crucibles being heated over a Bunsen burner. It can also be used as a support for a funnel. funnel Ringstands and their Components Ring Utility Clamps Ring utility clamps are used to secure test tubes, flasks, burets,, distillation columns, burets etc. etc to the ringstand ringstand.. Ringstands g and their Components p Double Buret Clamps Double Buret Clamps are used to attach burets burets,, eudiometers, eudiometers or gas collection tubes to a ringstand ringstand.. Ringstands g and their Components p Wire Gauze A wire i gauze sits i on the iron ring to provide a surface on which a beaker or flask may be placed. On older wire gauze, the white material is asbestos! B Bunsen B Burner Bunsen burners are used for the heating g of nonvolatile liquids and solids. Strikers Strikers are used to light Bunsen burners. The flints on strikers are expensive. i D Do nott operate t the striker repeatedly jjust to see the sparks! p Pressed Fiber Pad A 4” 4 x 4” 4 square of ceramic fiber, it provides a surface f hot for h t beakers b k so that the beaker does not come in contact with a cold countertop and shatter. shatter Organic Lab Equipment Florence Flask The Florence Flask is used for heating substances that need to be heated evenly. evenly The bulbed bottom allows the heat to distribute through the liquid more evenly. evenly The Florence Flask is mostly used in distillation experiments. Round Bottom Flask The round bottom flask is used as: boiling flask reaction flask distilling flask collection flask Vials Vials are flat-bottomed, stoppered glass containers. containers They come in many sizes and d shapes h and d are used d to hold small amounts of liquids or solids. Vacuum Flask (Side(Side -Arm Flask or Filtering Flask) The vacuum flask Th fl k looks l k like lik an Erlenmeyer flask with a short arm coming g out of it. The "arm" is designed to connect the flask to a vacuum source. source Note the heavy the walls of f this thi flask fl k - they th are designed to withstand reduced p pressure without imploding. Buchner Funnel The Buchner funnel is a white porcelain funnel. funnel A grey or black adaptor or a stopper with a hole in it is required to connect it to a vacuum flask. fl k The Buchner is used exclusively y for vacuum filtrations. The adaptor forms a snug seal so that when reduced pressure is applied to the vacuum flask, liquid poured into the Buchner is sucked k d iinto the h flask fl k quickly. i kl Separatory Funnel The separatory funnel is used primarily in extraction procedures. The sloping sides are designed to make it easy to distinguish d h layers. l The stopcock-controlled p outlet on the bottom is designed to allow the liquid to be drained out of the funnel. A ground glass or Teflon stopper may be used to seall the h top opening. i Condenser (Condensation Tube) The condenser is used in both reflux and distillation procedures to cool and condense vapors. Y-Adaptor The Y Th Y-adaptor d t iis used d iin a distillation set-up: it holds the thermometer •it •the side-arm connects to the condenser •it connects the round bottom flask to both the therm meter and the thermometer condenser Thermometer Adaptor The thermometer adaptor consists of a standard taper joint and a rubber adaptor. The standard Th t d d ttaper jjoint i t fit fits iinto t a glassware set-up, while the rubber adaptor p holds a thermometer snugly. Claisen Adaptor The Claisen adaptor is a multi-purpose item of standard taper glassware. It is used in situations which require more than one outlet from a round bottom flask. flask Vacuum Adaptor The vacuum adaptor is used in a distillation set-up: it connects to the lower end of the condensor and serves to direct the distilled liquid into the receiving flask A "bent adaptor" would serve the same purpose in a simple or fractional distillation. A bent adaptor does o s not have ha the th connection conn ct on to a vacuum acuum sourc source,, which is on the right hand side in the above photo.