24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEESILC® IDD Technical Data Sheet INCI: Isododecane, Dimethicone Crosspolymer-3 CAS Numbers: 141-70-8, 541-02-6 EINECS Numbers: 205-495-9, Exempt The JEESILC® line is comprised of standard and specialty silicones. These silicones are available in the form of fluids, emulsions, compounds and lubricants, depending on the user’s desired application. This unique dispersion in Isododecane, provides a fast drying, light-silky smooth feel to Skin Care products. Additionally, JEESILC® IDD will aid in suspension properties by reducing the settling of pigments in formulations. A unique water white, clear polymer dispersion, JEESILC® IDD enhances the conditioning attributes of Hair Care formulations without leaving a greasy heavy build up. This product can provide hydrophobic conditioning to anhydrous styling products that are designed to deliver a lighter film to the hair shaft. For Sun Care formulations, JEESILC® IDD will deliver fast drying, lighter feeling benefits without the alcohol. It is especially ideal for matte finished Color Cosmetics that require a lighter feel while providing the long lasting wear of color. • • • • • Fast Drying, Smooth Feel Reduces Pigment Settlement Enhances Hair Conditioning Attributes Lighter Film Lighter Feel Properties in Hair Care Sun Care and Color Cosmetic Applications Suggested Applications: • • • • • • • • Mascara Make Up Lip Products Antiperspirant Creams/Lotions Sun Care Styling Lotions Fragrance Delivery You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Color Cosmetics: For Hair Care: For Sun Care: Between 10% and 25% with minimal energy required to process. For improved conditioning with a lighter feel to the hair, the typical usage levels are between 5% and 10%. Incorporate at levels of 10% and 15% as an alcohol replacement for anhydrous formulations. Benefits: Suggested Formulation • • • • Improved Spreadability Fast Drying Good Substantivity Lighter Feel Skin Treatment Lotion Formulation JN1-2 AP Supplier Phase A Kelco JEEN ARCH JEEN JEEN Product Specifications: Appearance @ 25°C: Ionic Characteristic: Non-Volatile Content (Wt%): Specific Gravity @ 25°C: Phase B JEEN Colorless Transparent Gel Nonionic 4 - 7.5 0.7 – 0.8 (5.8 lb/gal – 6.7/lb/gal) Viscosity: 275,000 – 700,000 cps (Brookfield LVT 0.3 rpm – spindle #4, 24 °C) Handling and Storage: • Store in Clean, Dry Area • Ambient Room Temperature • Avoid Freezing Standard Packaging: Drum: 322 Lbs. Net Wt. Pail: 33 Lbs. Net Wt. JEEN JEEN Seppic Phase C JEEN JEEN Botanicals PLUS! Phase D JEEN JEEN Product/INCI % Deionized Water Keltrol CG/Xanthan Gum Glycerin 99% Multifruit BSC JEESCREEN® B-4/ Benzophenone-4 JEECHEM GMS-165 Glyceryl Stearate (and) PEG-100 Stearate 61.70 0.20 5.00 3.00 0.10 3.00 JEESILC IDD Isododecane (and) Dimethicone Crosspolymer-3 JEESILC 211 Cyclomethicone JEESILC PDS-100 2.00 Dimethicone Simulgel NS 4.00 JEESILC 6056 Dimethicone (and) Dimethiconol (and) Laureth 4 (and ) Laureth-23 JEECIDE G-II Propylene Glycol (and) Diazolidinyl Urea (and) Methyl Paraben (and) Propyl Paraben Arnica Extract Arnica Montana Flamingo Super Red JEESORB L-20 /Polysorbate 20 Vitamin E Acetate Tocopheryl Acetate Fragrance 8.00 4.00 3.00 1.00 2.00 1.00 1.00 0.50 0.50 Procedure: 1. Heat water to 65°C. Pre-mix Keltrol and Glycerin and add to the water phase. Mix until dissolved. Add the other ingredients to Phase A one at a time and mix well. Cool to 50°C. 2. In the oil phase tank, add the JEESILC IDD, JEESILC CPS-211 and JEESILC PDS-100 and mix until uniform. Add in the Simugel and mix to 50°C. 3. Using a homogenizer, add Phase B to Phase A and mix for 10 minutes. Cool to 40°C. Switch to prop agitation. 4. Add the ingredients of Phase C one at a time into the main tank and mix well after each addition. Pre-mix Phase D in a side vessel and add to the main tank. Mix well. You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEECHEM® HPIB Technical Data Sheet INCI: Cyclomethicone, Hydrogenated Polyisobutene, Dimethicone Crosspolymer-3 CAS Numbers: 69430-24-6, 68937-10-0, 541-02-6 EINECS Numbers: 205-495-9, Exempt The JEESILC® line is comprised of standard and specialty silicones. These silicones are available in the form of fluids, emulsions, compounds and lubricants, depending on the user’s desired application. JEECHEM® HPIB is a unique dispersion of hydrogenated polyisobutene, cyclomethicone and dimethicone crosspolymer-3 that provides a long lasting, silky smooth feel to Skin Care products while giving a powder like after feel. JEECHEM® HPIB enhances the esthetic value of Creams, Lotions and Color Cosmetics and delivers a prolonged softer feel with substantivity. JEECHEM® HPIB will significantly improve the gloss of most cosmetics without leaving a greasy feel or tackiness to the skin. This product provides an especially smooth conditioning effect to most Hair Care and Styling Products without a heavy oily feel. • • • • • Improves Gloss No “Greasy” Feel Smooth Conditioning for Hair Care. No tackiness Soft Powdery Afterfeel Suggested Applications: • • • • • • Creams/Lotions Liquid Foundations Lip Products Styling Lotions Pomades Sun Care You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Creams and Lotions: Between 5% and 10% incorporated into the oil phase of the formulation. For Hair Care: For improved shine and conditioning attributes, the typical usage levels are between 3% and 5%. For Color Cosmetics: Incorporate at levels of 10% and 15% for improved long lasting wear. Benefits: • • • • Suggested Formulation Enhanced Shine Ease of Use Slick Feel Without Tack Lighter Feel Alcohol Free Sunscreen Gel This clear alcohol free sunscreen gel offers a silky smooth feel with enhanced substantivity. This unique formulation offers long lasting moisturization with SPF of 10. Supplier Product/INCI % Product Specifications: JEEN Appearance @ 25°C: Odor: Specific Gravity @ 25°C: Viscosity: Clear to Translucent Gel Odorless 0.80 – 0.94 150,000 – 600,000 cps (Brookfield LVT 0.3 rpm – spindle #4, 25 °C) JEEN JEEN JEECHEM® HPIB Dimethicone Crosspolymer -3, Cyclomethicone, Hydrogenated Polyisobutene JEESCREEN® OMC Octyl Methoxy Cinnamate JEESCREEN® OS Octyl Salicylate 86.63 7.50 5.00 Handling and Storage: • Store in Clean, Dry Area • Ambient Room Temperature • Avoid Freezing AFF Int’l Standard Packaging: Drum: 400 Lbs. Net Wt. Pail: 40 Lbs. Net Wt. Procedure: Combine the sunscreen phase with the fragrance and mix until uniform. Add this premix slowly to the JEECHEM® HPIB at room temperature and mix until uniform. Fragrance 118578 Total 0.87 100.00 You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEESILC® 3D5LV Technical Data Sheet INCI: Cyclomethicone, Dimethicone Crosspolymer-3 CAS Numbers: 69430-24-6, 541-02-6 EINECS Numbers: 205-495-9, Exempt The JEESILC® line is comprised of standard and specialty silicones. These silicones are available in the form of fluids, emulsions, compounds and lubricants, depending on the user’s desired application. JEESILC® 3D5 LV performs as a transparent, slick, tack-free lubrication silicone carrier. JEESILC® 3D5 LV is an especially useful additive in Color Cosmetics, producing a slick, fast drying film with a silky after feel. JEESILC® 3D5 LV can also be used in Sun Care formulations that require a lighter feel. JEESILC® 3D5 LV provides ease of formulating and enhanced softness in Moisturizers and Make-up applications. JEESILC® 3D5 LV may be used as is, or mixed with other silicone products under high shear, to produce a soft, slick feel that is tack free. • • • • Tack-Free Fast Drying Film Silky After-Feel Feel Modifier Suggested Applications: • • • • Creams/Lotions Make-Up Moisturizers Sun Care You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Creams and Lotions: 3–6% For Make-Up: 5 – 10% For Moisturizers: 3–6% Sun Care: 5 – 10% Suggested Formulation Silky Liquid Make-Up Foundation Formulation No. JN 1/2 Supplier Phase A Product/INCI Presperse Permethyl 99A 10.00 Isododecane JEESILC DMC 322 5.00 Cyclopentasiloxane (and)Dimethicone Copolyol Abil WE-09 4.00 Polyglyceryl-4 Isostearate (and) Cetyl Dimethicone Copolyol (and) Hexyl Laurate Bentone Gel VS-5 1.50 Cyclomethicone (and) Quaternium-18 Hectorite (and) SD Alcohol 40 JEESILC 3D5 LV 6.00 Cyclomethicone (and) Dimethicone Crosspolymer-3 Deionized Water 59.00 JEECHEM BUGL 2.50 Butylene Glycol Sodium Chloride 1.00 SP-500/Nylon 12 1.00 TIO2 SI 7.00 Titanium Dioxide (and) Silicone Yellow Iron Oxide SI 1.50 Iron Oxide (and) Silicone Red Iron Oxide SI 0.25 Iron Oxide (and) Silicone Black Iron Oxide SI 0.25 Iron Oxide (and) Silicone JEECIDE G-II 1.00 Propylene Glycol (and) Diazolidinyl Urea (and) Methyl Paraben (and) Propyl Paraben JEEN Goldschmidt Benefits: • • • RHEOX Ease of Use Slick Feel Without Tack Lighter Feel JEEN Product Specifications: Appearance @ 25°C: Odor: Specific Gravity @ 25°C: Viscosity: JEEN Water White, Clear Gel Odorless 0.80 – 0.94 700,000 cps Maximum (Brookfield LVT 0.3 rpm – spindle #4, 24 °C) Non-Volatile Content (% by Weight): Kobo Cardre Cardre Cardre 2.5 - 6.0 % Cardre (115 °C, 1 Hr) JEEN Handling and Storage: • Store in Clean, Dry Area • Ambient Room Temperature • Avoid Freezing Standard Packaging: Drum: 441 Lbs. Net Wt. Pail: 40 Lbs. Net Wt. % ________ Procedure: 1. Using a homogenizer in the main tank, combine the Permethyl 99A and JEESILC 3D5 LV and mix at moderate agitation until smooth. Add the JEESILC DMC 322, Abil WE-09 and Bentone Gel VS-5 and mix for 15 minutes. 2. In a side tank, pre-blend the Nylon 12, TiO2 and Iron Oxides. Add to the main tank, and mix for 30 minutes. Switch to prop agitation. 3. In a side tank, pre-blend the water, JEECHEM BUGL, JEECIDE G-II and Sodium Chloride. Slowly add the water phase to the oil phase. Mix for 20 – 25 minutes. You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEESILC® 35C Technical Data Sheet INCI: Dimethicone, Dimethicone Crosspolymer-3 CAS Numbers: 63148-62-9, 541-02-6 EINECS Numbers: 205-495-9, Exempt The JEESILC® line is comprised of standard and specialty silicones. These silicones are available in the form of fluids, emulsions, compounds and lubricants, depending on the user’s desired application. JEESILC® 35C performs as a transparent, slick, tack-free lubrication silicone carrier. JEESILC® 35C is an especially useful additive in cream and stick foundations, producing a slick feel, without tack. When using proper emulsifiers, stable water in oil emulsions can be obtained. JEESILC® 35C provides ease of application and enhanced softness in Moisturizers, Make-up applications and Sun Care formulations. JEESILC® 35C may be used as is, or mixed with Dimethicone under high shear, to produce a soft, slick feel that is tack free. • • • • Tack-Free Slick Feel Ease of Application Feel Modifier Suggested Applications: • • • • • Creams/Lotions Foundations Make-Up Moisturizers Sun Care You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Creams and Lotions: 2–5% For Foundations: 3–6% For Make-Up: 3–6% For Moisturizers: 2–5% Sun Care: 5 – 10% Suggested Formulation Sample Formulation The following is a starting point for utilizing JEESILC® products in formulations. Concentrations are approximate and individual components may be substituted with functional equivalents as required. Supplier • • • CRODA Good Spreadability Silky Feel Without Tack Long Lasting JEEN INT’L JEEN INT’L Product Specifications: Appearance @ 25°C: Ionic Character: Specific Gravity @ 25°C: Non-Volatile Content (% by Weight): Odor: Carrier: JEEN INT’L Clear, Transparent Gel Nonionic 0.80 – 0.94 100.00 % Odorless Low Viscosity Dimethyl Silicone (5 centistokes) Handling and Storage: • Store in Clean, Dry Area • Ambient Room Temperature • Avoid Freezing Percent (by Weight) PART A JEEN INT’L Benefits: Ingredients/INC I Jeen Shea Butter SHEA BUTTER (Butyrospermum Parkii) Crodaphos CS-20 Acid (Cetearyl Alcohol, Ceteth -20 Phosphate, Dicetyl Phosphate) Jeen Stearyl Alcohol 17.00 Jeen Cocoa ButterPPP(Theobro ma Cacao Seed Butter Jeesilc 35C Dimethicone, Dimethicone Crosspolymer-3 6.75 DI Water Glycerin 59.70 2.00 Triethanolamine 99% 0.80 Jeecide G-II Propylene Glycol, Diazolidinyl Urea, Methyl Paraben, Propyl Paraben 1.00 8.00 2.75 2.00 PART B JEEN INT’L JEEN INT’L PART C JEEN INT’L Procedure: Combine ingredients in Part A and Part B separately while mixing and heat to 75-80° C. Add Part B to Part A with mixing and cool to 45° C and add Part C. Standard Packaging: Drum: 441 Lbs. Net Wt. Pail: 40 Lbs. Net Wt. You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEESILC® UAF Technical Data Sheet INCI: Propoxytetramethyl Piperidinyl Dimethicone CAS Numbers: Mixture EINECS Numbers: Exempt The JEESILC® line is comprised of standard and specialty silicones. These silicones are available in the form of fluids, emulsions, compounds and lubricants, depending on the user’s desired application. JEESILC® UAF is a Unique silicone fluid designed to enhance the conditioning attributes of hair care formulations. The JEESILC® UAF has been developed to offer superior conditioning properties and enhanced stability in Permanent Hair Coloring products. The unique structure of the silicone fluid allows for greater stability in resisting fade, or discoloration over time…. JEESILC® UAF offers you the ability to enhance the overall hydrophobic conditioning properties of your hair care formulations, especially in Permanent Hair Color systems. The unique structure of our JEESILC® UAF will resist fading and discoloration over time when exposed to UV light. In comparison to existing silicone products the JEESILC® UAF has demonstrated superior performance against fading, while enhancing the overall conditioning and detangling. Our JEESILC® UAF improves hair color depth, longevity while reducing color fade in formulations. • • • • Superior Conditioning Enhanced Stability UV Stable Detangler Suggested Applications: • • • Hair Care Lotions Hair Care Conditioners Permanent and Semi-Permanent Hair Color Products You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Hair Care Lotions: 1–3% For Hair Coloring Formulas: 2- 5% Color Fade Study Whiteness of 3%of Emulsion in the Bath (30%Solids Microemulsion) 100%Cotton Fabric - Dried @120'C Benefits: 72 • • • • Provides a Soft Silky Feel to the Hair Enhances Shine and Hair Depth Resistance to UV Discoloration Provides Web Comb and Reduces Fly Away 70 68 66 64 62 60 58 Product Specifications: 56 54 Appearance @ 25°C: Specific Gravity @ 25°C: Clear to Slightly Hazy Liquid 0.94 – 0.97 Viscosity @ 25°C: 10,000 – 60,000 52 50 Di Amino Di Amino MonoAmino UAF Untreated Ganz Whiteness Readings (Brookfield, #4 @ 30 rpm) Handling and Storage: • Store in Clean, Dry Area • Ambient Room Temperature • Avoid Freezing Standard Packaging: Drum: 430 Lbs. Net Wt. Pail: 40 Lbs. Net Wt. You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEESILC® 6056 Technical Data Sheet INCI: Dimethicone, Dimethiconol, Laureth 4, Laureth-23 CAS Numbers: 63148-62-9, 70131-67-8, 5274-68-0, 68551-12-2 EINECS Numbers: Exempt, Exempt, 226-097-1, Exempt A silicone emulsion that allows for ease of incorporating silicone function into oil-in-water emulsions. This nonionic emulsion contains on average 55 percent of a high molecular weight dimethicone having a particle size range of 0.1 to 0.2 micros, allowing for improved feel, moisturization and film properties. JEESILC®6056 offers you the ability to easily incorporate a soft silky feel to your current oil-in water formulations. Our nonionic emulsion can be added directly into the water phase of the formula at room temperature using a low degree of mixing. In addition to enhance the feel, JEESILC® 6056 will also offer good water resistance properties for Liquid Foundations and Sunscreen systems. The small particle size distribution will allow for high concentrations without impacting the formulations final viscosity. • • • • Improved Feel Soft Silky Feel Ease of Use in Oil/Water Emulsions Enhanced Film Formation Suggested Applications: • • • • Liquid Foundations Sun Screen Lotions, Creams and Sprays Moisturizing Creams and Lotions Hair Care Lotions and Conditioners You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Liquid Foundations: 2–4% For Sunscreen Formulas: 4–8% Water Resistant Sunscreen Spray SPF 30 For Moisturizing Creams & Lotions: 2–4% 1–3% Benefits: • Provide a soft, silky feel. Enhance Film Formation for Color Retention and Water Resistance. Provide Wet Comb and Conditioning. Product Specifications: Appearance @ 25°C: pH (as is) @ 20°C: % Solids (2g/1hr/150 °C): Viscosity: Particle Size (nm): Milk White Emulsion 4.5 – 8.0 64.0 – 66.5 700,000 cps Maximum 600 – 1,000 Handling and Storage: • Store in Clean, Dry Area • Ambient Room Temperature • Avoid Freezing Standard Packaging: Drum: 440 Lbs. Net Wt. Pail: 40 Lbs. Net Wt. Supplier Product/INCI % Phase A JEEN For Hair Care Lotions & Conditioners: • • Suggested Formulation JEECHEM TN 5.00 C12-15 Alkyl Benzoate JEEN JEESCREEN® OS 5.00 Octyl Salicylate ® JEEN JEESCREEN OMC 7.50 Octyl Methoxy Cinnamate ® JEEN JEESCREEN B-3 4.00 Benzophenone-3 Roche Parsol 1789 1.60 Butyl Methoxydibenzolmethane {avobenzone} Goldschmidt Tego Care 450 3.00 Polyglyceryl-3 Methylglucose Distearate Croda Syncrowax ERL-C 0.60 C18-36 Acid Glycol Ester JEEN JEESILC® PDS-100 4.00 Dimethicone JEEN Vitamin E Acetate 0.10 Tocopheryl Acetate Phase B DI Water 65.14 Noveon Carbopol® EDT 2020 0.18 Acrylates/C10-30 Alkyl Acrylate Crosspolymer Phase C JEEN Triethanolamine 0.08 Phase D JEEN JEECIDE P 0.80 JEEN JEESILC® 6056 3.00 Dimethicone (and) Dimethiconol (and) Laureth-4 (and) Laureth 23 Procedure: Phase A: Combine first 3 ingredients of Phase A; mix well. Add JEESCREEN Benzophenone 3; mix at room temperature for 10 minutes. Heat to 80°C while mixing. Add Parsol 1789; mix for 4 more minutes while keeping temperature at 80°C. Add Tego Care 450; mix 2 – 3 minutes. Add Syncrowax ERL-C; mix for 2 – 3 minutes. Add remaining ingredients of Phase A; mix. Keep temperature of Phase A at 80°C. Phase B: In separate vessel sift Carbopol® EDT 2020 to room temperature deionzed water. Mix while heat to 75 – 80 C. Slowly add Phase A to Phase B. Add TEA (Phase C) to Phase AB to pH 5.4 – 5.5. Mix well. Apply high shear mixing. Add Phase D below 55°C, then slowly add Phase E (JEESILC 6056). Apply moderate mixing while cooling to 30°C. Homogenize at 30°C (~9,000 rpm) for 3 – 5 minutes. ® Carbopol is a registered trademark of Noveon You Can Count On Us! We’re clearly your choice for Specialty Polymers…. 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEESPERSE® HD Technical Data Sheet INCI: Isododecane, Dimethicone Crosspolymer-3, Laureth-4, Ceteth-10 CAS Numbers: 13475-82-6, 541-02-6, 5274-68-0, 9004-95-9 EINECS Numbers: 236-757-0, Exempt, 226-097-1, 500-014-1 A volatile hydrocarbon dispersion that allows for ease of incorporating Isododecane into water based formulations. This nonionic dispersion contains on average 80 percent of a volatile hydrocarbon, 4 percent silicone polymer, non-ionic surfactant and water. The Isododecane dispersion is designed to offer a user friendly, cold process feel modifier, that possesses a volatile profile. In addition to offering superior feel, the hydrophobic nature of the Dimethicone Crosspolymer-3 will enhance the overall film properties while delivering a soft dry after-feel. JEESPERSE® HD offers you the ability to easily incorporate a dry , soft silky feel to your water based formulations by incorporating it directly into the water phase of the formula at room temperature. Suggested Applications: • Matte Foundations • Sun Screen Lotions, Creams and Sprays • Moisturizing Creams and Lotions • Hair Care Lotions You Can Count On Us! 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: Liquid Foundations: Sunscreen Formulations: Moisturizing Creams and Lotions: Hair Care Lotions and Conditioners: 25 – 35% 10 – 15.0% 10.0 – 15.0% 15.0 – 20.0% Matte Foundation Formulation No. 40020120-1 Benefits: Ingredient JEESPERSE HD • Provide a soft, dry silky feel. • Enhance film formation for color retention and water resistance. Bentone Gel VS-5 Product Specifications: Appearance @ 25 °C: % Solids Milk White Emulsion (0.5 – 1.0g/35 min-1hr/105 °C): 7.5 – 9.5 % Viscosity (Brookfield, Spindle 4.1.5 rpm): Particle Size, nm: 30,000 – 200,000 300 - 1000 • DI Water JEECHEM BUGL Sodium Chloride SP-500 TIO2 SI Yellow Iron Oxide SI Red Iron Oxide SI Black Iron Oxide SI JEECIDE G-II Supplier % JEEN International 25.0 JEEN International Goldschmidt 5.0 Rheox 1.50 JEEN International Sodium Chloride 4.0 50.0 2.5 1.0 Nylon 12 Titanium Dioxide and Silicone Iron Oxide and Silicone Kobo Cardre Inc. 1.0 7.0 Cardre hic 1.5 Iron Oxide and Silicone Cardre Inc. 0.25 Iron Oxide and Silicone Cardre Inc. 0.25 Propylene Glycol (and) Diazolidinyl Urea (and) Methylparaben (and) Propylparaben JEEN International 1.00 Procedure: 1. Using a homogenizer in the main tank, combine the JEESPERSE HD and the JEESILC DMC 322, WE-09 and Bentone Gel VS-5 and mix for 15 minutes. Handling and Storage: • JEESILC DMC 322 Abil WE-09 INCI Nomenclature Isododecane and Dimethicone Crosspolymer-3 and Laureth-4 and Ceteth-10 Cyclopentasiloxane and Dimethicone Copolyol Polyglyceryl-4 Isostearate and Cetyl Dimethicone Copolyol and Hexyl Laurate Cyclomethicone and Quaternium-18 Hectorite and SD Alcohol 40 Water Butylene Glycol Store in Clean, Flame Proof, Well Ventilated Area 2. Follow Good Manufacturing Practices 3. In a side tank, pre-blend the Nylon 12, Ti02 and Iron Oxides. Add to the main tank, and mix for 30 minutes. Switch to prop agitation. In a side tank, pre-blend the water, JEECHEM BUGL, JEECIDE G-II and Sodium Chloride. Slowly add the water phase to the oil phase. Mix for 20-25 minutes. Standard Packaging: Drum: Pail: 325 Lbs. Net Wt. 32 Lbs. Net Wt. You Can Count On Us! 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEESPERSE® HP-60 Technical Data Sheet INCI: Cyclomethicone, Hydrogenated Polyisobutene, Dimethicone Crosspolymer-3, Laureth-4, Laureth-23 CAS Numbers: 69430-24-6, 68937-10-0, 541-02-6, 5274-68-0, 68551-12-2 EINECS Numbers: Exempt, Exempt, Exempt, 226-097-1, Exempt JEESPERSE® HP-60 is a fine particle size emulsion that contains gelled cyclomethicone and hydrogenated polyisobutene using our new silicone polymer Dimethicone Crosspolymer-3. This unique system has a very small particle size distribution in the range of 500 – 700 nanometers. The principal benefits are: ease of formulation, enhanced spreadability and improved emulsion stability while effectively delivering a soft powder like after feel. JEESPERSE® HP-60 offers you the ability to easily incorporate a soft silky feel to your current oil-in-water formulations. Our nonionic emulsion can be added directly into the water phase of the formula at a temperature range of 45 – 50 degrees Celsius using a low degree of mixing. In addition to the enhanced after feel the JEESPERSE® HP-60 will provide great emolliency and stability to your Liquid Foundations, Sunscreens, Creams and Lotions. Suggested Applications: • Liquid Foundations • Sunscreen Lotions, Creams and Sprays • Moisturizing Creams and Lotions • Hair Care Lotions and Conditioners You Can Count On Us! 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: Liquid Foundations: Sunscreen Lotions, Creams and Sprays: Moisturizing Creams and Lotions: Hair Care Lotions and Conditioners: 2.0 – 4.0% 4.0 – 8.0% 2.0 – 4.0% 1.0 – 3.0% Benefits: Silky Night Cream Supplier Phase A JEEN • Provides a Soft Silky Feel • Aids in Stabilizing Emulsions • Provides Moisturization and Conditioning JEEN JEEN Product Specifications: Phase B JEEN JEEN JEEN Appearance @ 25 °C: pH (“As Is”): % Solids (2g/1hr/150 °C: Viscosity (Brookfield): Particle Size: Milk White Emulsion 4.50 – 8.00 64.0 – 66.5 500 - 2000 600 - 1000 Handling and Storage: • • • Keep Container Closed Ambient Room Temperature Store in Clean, Dry Area Standard Packaging: Drum: Pail: 400 Lbs. Net Wt. 35 Lbs. Net Wt. Product/INCI JEEN JEEN JEEN Phase C JEEN Phase D JEEN Deionized Water JEECIDE G-II Propylene Glycol, Diazolidinyl Urea, Methyl Paraben, Propyl Paraben Propylene Glycol USP Glycerin 99% Hampene NA-4 Tetrasodium EDTA JEEMATE 2000-DPS PEG-40 Stearate JEECHEM GMS-D Glyceryl Stearate SE JEECHEM CTG Caprylic/capric triglyceride Stearyl Alcohol NF Mineral Oil USP JEESILC PDS-200 Dimethicone Vitamin E Acetate Tocopheryl Acetate % _ _ 61.20 0.75 2.25 2.00 0.10 _ 2.00 4.80 5.00 3.00 10.00 0.30 0.10 _ Deionized Water Sodium Citrate 2.00 0.50 _ JEESPERSE HP-60 6.00 Hydrogenated Polyisobutene, Cyclomethicone, Dimethicone Crosspolymer-3, Laureth-23, Laureth-4 Procedure: Combine ingredients of Phase A and heat to 80°C. Mix on lightning mixer with medium speed. In a separate vessel, combine ingredients of Phase B and heat to 80°C. Slowly add Phase B to Phase A under lightning mixer. Start cooling to 40°C and add Phase C, then the JEESPERSE HP-60 into the batch. Mix well to uniformity. Continue cooling to room temperature. You Can Count On Us! 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEENATE® 3H Technical Data Sheet INCI: POLYETHYLENE CAS Numbers: 9002-88-4 EINECS Numbers: Exempt JEENATE® 3H is a polyethylene wax that contains a unique hydrocarbon distribution that is predominantly linear with a very low concentration of branched Polyethylene. The JEENATE® 3H Polyethylene is predominantly C-30 or greater with low levers of C-26 hydrocarbon function. This unique carbon distribution allows the formulators to increase the overall crystalline structure of oils with a melting point of less than 70 °C. JEENATE® 3H is ideal for improving the overall hardness, and crystalline structure of most traditional cosmetic oils, namely volatile silicones in stick formulations. In addition, because of the linear nature of the polyethylene, JEENATE® 3H is very effective at increasing the viscosity of oils to aid in emulsion stabilization. The ® hydrophobic nature of the JEENATE 3H will aid in film integrity, substantivity and conditioning. Suggested Applications: • • • • • • • Lipsticks Foundation Make-Up Sticks Liquid Foundations Mascara Sunscreen Lotions and Creams Moisturizing Creams and Lotions Hair Care Lotions and Conditioners You Can Count On Us! 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Lipsticks: For Foundation Make Up Sticks: For Liquid Foundations: For Sunscreen Formulations: For Moisturizing Creams and Lotions: For Hair Care Lotions and Conditioners: 8.0 10.0 2.0 4.0 2.0 1.0 Suggested Formulation Cream to Powder No. 40020-2 Benefits: • • • • – 12.0 % – 15.0 % – 4.0 % – 8.0 % – 4.0 % – 3.0 % Ingredients Improve Oil Hardness and Crystal Structure. Reduce Oil Bleed. Enhance Film Formation for Color Retention. Improve Emulsion Stability. Product Specifications: Appearance @ 25°C: Melting Point Range °C: Typical Penetration @ 25°C:: Specific Gravity @ 25 C: Odor: White Flake 62 - 68 15.5 0.83 Slight Handling and Storage: • Store in Clean, Dry Area • Ambient Room Temperature • Avoid Freezing Phase A JEESILC PTM Phase B JEENATE 3H Microcrystalline Wax Phase C JEECHEM OP Panalane LE -14 JEECHEM ISP Propyl Paraben Phase D Light Brown Iron Oxide Titanium Dioxide Talc INCI Nomenclature Supplier % WT Phenyl Trimethicone JEEN Int’l 16.00 Polyethylene JEEN Int’l 13.00 9.00 Octyl Palmitate Hydrogenated Polyisobutene Isostearyl Palmitate Propylparaben JEEN Int’l 15.00 13.00 JEEN Int’l 10.00 JEEN Int’l 0.15 3.00 11.00 9.85 PROCEDURE: Heat Phase B and C to 95 °C and mix until uniform. Once uniform cool Phase B/C to 80 degrees °C and slowly add Phase A and Phase D mix until uniform. Pour product into desired package and cool to room temperature. Standard Packaging: Drum: Box: Pail: 330 Lbs. Net Wt. 45 Lbs. Net Wt. 40 Lbs. Net Wt. You Can Count On Us! 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEENATE® 4H Technical Data Sheet INCI: POLYETHYLENE CAS Numbers: 9002-88-4 EINECS Numbers: Exempt A unique linear Polyethylene that will improve the overall product hardness of cosmetic stick formulations. The crystalline nature of JEENATE® 4H, will enhance the high temperature stability of cosmetic stick formulations, while providing a smooth lubricous hydrophobic film. In addition, the JEENATE® 4H will also increase the oil phase viscosity in emulsions to improve high temperature stability and aid in the overall product substantivity. JEENATE® 4H is ideal for improving the overall hardness, and crystalline structure of most traditional cosmetic oils, namely volatile silicones in stick applications. The hydrophobic nature of the JEENATE® 4H will aid in film integrity, substantivity and conditioning properties. Combinations of the JEENATE® 4H, along with JEENATE® 3H will provide an optimum integration of melting point and hardness. Suggested Applications: • • • • • • • Lipsticks Foundation Make Up Sticks Liquid Foundations Mascara Sun Screen Lotions and , Creams Moisturizing Creams and Lotions Hair Care Lotions and Conditioners You Can Count On Us! 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: Lipsticks: 8.0 – 12.0 % Foundation Make Up Sticks: 10.0 – 15.0 % Liquid Foundations: 2.0 – 4.0 % Sunscreen Formulations: 4.0 – 8.0% Moisturizing Creams and Lotions: 2.0 – 4.0% Hair Care Lotions and Conditioners: 1.0 – 3.0% Benefits: Improve Oil hardness and crystal structure. • Reduce oil bleed • Enhance film formation for color retention. • Improve emulsion stability. Mineral Oil C Product Specifications: Castor Oil C • Test Method Appearance @ 25°C: Melting Point °F: Viscosity @ 210°F:: Penetration @ 77 F: Color (Saybolt): Pastille 158 - 175 1 – 10 cps 13 – 22 dmm 15 – 40 ASTM D 127 ASTM D 3236 ASTM D 1321 ASTM D 156 Handling and Storage: • • • • Compatibility Chart JEENATE® 4H 5% Addition Cyclomethicone C Phenyl Trimethicone C Isododecane C Octyl Palmitate C C = Compatibility Store in Clean, Dry Area Ambient Room Temperature Avoid Extreme Temperature Follow GMP Procedures Standard Packaging: Bag: 55 Lbs. Net Wt. Pail: 20 Lbs. Net Wt. You Can Count On Us! 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEENATE® 5H Technical Data Sheet INCI: POLYETHYLENE CAS Numbers: 9002-88-4 EINECS Numbers: Exempt A unique linear Polyethylene that will improve the overall product hardness of cosmetic stick formulations. The crystalline nature of JEENATE® 5H will enhance the high temperature stability of cosmetic stick formulations while providing a smooth lubricous hydrophobic film. In addition the JEENATE® 5H will also increase the viscosity of the oil phase to improve high temperature stability and aid in the overall product substantivity. JEENATE® 5H is ideal for improving the overall hardness, and crystalline structure of most traditional cosmetic oils, namely volatile silicones in stick formulations. The hydrophobic nature of the JEENATE® 5H will aid in film integrity, substantivity and conditioning properties. Combinations of the JEENATE® 4H, along with JEENATE® 5H will provide an optimum combination for all your stick applications. Suggested Applications: • Lipsticks • Foundation Make Up Sticks • Liquid Foundations • Mascara • Hair Care Lotions You Can Count On Us! 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Lipsticks: 8.0 – 12.0% For Foundation Make Up Sticks: 10.0 – 15.0% Liquid Foundations: 2.0 – 4.0% Hair Care Lotions: 1.0 – 3.0% Benefits: • Improve Oil hardness and crystal structure. • Reduce oil bleed Compatibility Chart JEENATE® 5H 5% Addition • Enhance film formation for color retention. Mineral Oil C Castor Oil C Cyclomethicone C Product Specifications: Test Method Appearance @ 25°C: Pastille Visual Melting Point °F: 181- 194 ASTM D 127 Viscosity @ 210°F:: 5 – 15 cps ASTM D 3236 Penetration @ 77 F: 3 – 8 dmm ASTM D 1321 Color (Saybolt): 12 – 25 ASTM D 156 Handling and Storage: • • • • Phenyl Trimethicone C Isododecane C Octyl Palmitate Store in Clean, Dry Area Ambient Room Temperature Avoid Extreme Temperature Follow GMP Procedures C C = Compatibility Standard Packaging: Bag: 50 Lbs. Net Wt. Bag: 55 Lbs. Net Wt. You Can Count On Us! 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEENATE® SP Technical Data Sheet INCI: Polyethylene, Stearoxy Dimethicone CAS Numbers: 9002-88-4, 68554-53-0 EINECS Numbers: Exempt, Exempt A unique silicone modified Polyethylene that will improve the overall structure and feel of the oil phase in emulsion and anhydrous formulations. The crystalline nature of JEENATE® SP will enhance viscosity of most cosmetic oils which will results in improved high temperature stability of emulsions and anhydrous products, while providing a smooth lubricous hydrophobic film. Additionally the JEENATE® SP also acts as a dispersing agent for inorganic materials , allowing for a smooth uniform payout and spreadability of colors and sunscreens. JEENATE® SP, is ideal for improving organic sunscreen performance, film properties resulting in a softer feel for your applications. The hydrophobic nature of the JEENATE® SP will aid in film integrity, substantivity and conditioning properties. Suggested Applications: • Lipsticks • Foundation Make Up Sticks • Liquid Foundations • Mascara • Sun Screen Lotions and , Creams • Moisturizing Creams and Lotions • Hair Care Lotions and Conditioners You Can Count On Us! 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: Lipsticks: Foundation Make Up Sticks: Liquid Foundations: Sunscreen Formulations: Moisturizing Creams and Lotions: Hair Care Lotions and Conditioners: 8.0 – 12.0% 5.0 – 10.0% 2.0 – 4.0% 4.0 – 8.0% 2.0 – 4.0% 1.0 – 3.0% Extended Wear Lipstick Formulation JN111104EU Benefits: • • • • Improve Oil hardness and crystal structure. Improve oil thickness of organic sunscreens Enhance film formation for color retention. Improve emulsion stability. Product Specifications: Phase Ingredients A Behenyl Alcohol S75 A A Kester Wax EM Siliconyl Candelilla JEENATE SP A JEENATE 4H A Polybutene H300 Pigment Base A A Appearance @ 25°C: Congealing Point °C: Absorptivity : Heavy Metals: Oil Content: White to Off White Wax 65 – 75 ASTM D 938 < 0.01 USP 851 < 0.002 % USP 231 0.75 Maximum ASTM D 7212-68 A A Siliconyl Candelilla Siliconyl Polyethylene Polyethylene Polybutene Supplier % Koster Keunen 8.00 Koster Keunen Koster Keunen JEEN Int’l. 5.00 JEEN Int’l. 2.00 BP Chemical 2.00 Red Iron Oxide53 % Dimethicone Titanium Dioxide - 17.8% Kester Wax K-24 -28.6% Cyclomethicone Isodeodecane 5.00 9.00 15.00 JEEN Int’l. 44.00 Presperse 10.00 Total Handling and Storage: • • • JEESILC CPS-312 Permethyl® 99A INCI Nomenclature Behenyl Alcohol 100.00 Procedure: Store in Cool, Dry, Well Ventilated Area Store away from Oxidizing Agents Store away from Strong Acids 1. Melt & mix all components @ 80° C, excluding JEESILC CPS-312 and Permethyl 99A. 2. Once fully melted and mixed, add Pigment Base. ® 3. Add JEESILC CPS-312 and Permethyl 99A. Allow temperature to cool to 65° C. 4. Pour into molds. You Can Count On Us! Standard Packaging: Box: This information is furnished without warranty, expressed or implied, except that it is accurate to the best knowledge of JEEN International Corporation. The data on this sheet relates only to the specific material designated herein. JEEN International Corporation assumes no legal responsibility for use or reliance upon these data. 55 Lbs. Net Weight You Can Count On Us! 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEECIDE CAP-2 Technical Data Sheet INCI Name: Caprylyl Glycol, Phenoxyethanol, Hexylene Glycol CAS Numbers: 1117-86-8, 122-99-6, 107-41-5 EINECS Numbers: 214-252-7, 204-589-7, 203-489-0 JEEN International has recognized the need for a synergistic blend of conventional and nonconventional preservative ingredients that inhibit microbial growth. JEECIDE CAP-2 is a unique easyto-use clear liquid preservative that is: • • • • • • • • • Paraben-free Formaldehyde-free Broad spectrum activity – effective against bacteria, yeast and mold Active over a wide pH range (3-10) Compatible with anionic, cationic and non-ionic surfactants and emulsifiers Toxicologically safe for use Equally suitable for use in both rinse-off and leave-on products Effective in difficult to preserve Water/Silicone emulsions Approved for Global use. pH Stability: Stable in the usual operating range of 3-10 which is typical for most personal care products. Light Stability: JEECIDE CAP-2 is light sensitive and should always be stored in an opaque container. Recommended Use Level: JEECIDE CAP-2 can be added at 0.5 – 1.5% for effective anti-microbial efficacy. However, it is important that every formulation be challenge-tested to determine the correct level of JEECIDE CAP2 to ensure proper preservation. Method of Addition: It is suggested not to add this blend to a product at a temperature exceeding 70 - 75ºC for extended time periods. For emulsion products, because of the excellent compatibility of this blend with most ingredients, incorporation of it during the cool-down phase of processing is preferred. . It is soluble or dispersible in most non-polar materials. JEECIDE CAP-2 is not water soluble however for highly aqueous systems, the addition of a co-solvent, coupling agent or surfactant (eg. Polysorbate 20) in a 1:1 ratio will make it water soluble to obtain a clear system. Page 1 of 3 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Technical Data Sheet continued….JEECIDE CAP-2 Solubility Data: Ingredient Mineral Oil Cyclomethicone Dimethicone 200/100 cst. Caprylic/Capric Triglycerides Water Propylene Glycol Ethanol 190 Proof Isododecane C12-15 Alkyl Benzoate Isopropyl Myristate Butylene Glycol Phenyltrimethicone Compatibility D IS D S D S S S S S S S D: Dispersible IS: Insoluble S: Soluble Recommended Use Level: JEECIDE CAP-2 can be added at 0.5 – 1.5% for effective anti-microbial efficacy. However, it is important that every formulation be challenge-tested to determine the correct level of JEECIDE CAP2 to ensure proper preservation. Microbiological Activity: JEECIDE CAP-2 is effective against both gram-positive and gram-negative bacteria, yeast and molds. Page 2 of 3 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Technical Data Sheet continued….JEECIDE CAP-2 Minimum Inhibitory Concentration (MIC) Objective: Determine activity of JEECIDE CAP-2 to Minimum Inhibitory Concentration (MIC) broth tests. Procedure: A standard microtiter plate MIC test was conducted in Tryptic Soy Broth (bacteria) Sabouraud Dextrose Broth (yeast and molds). Results: As shown in Table 1, JEECIDE CAP-2 is very effective at low concentrations against gram negative and positive bacteria and effective against yeasts and molds. Table 1. Minimum Inhibitory Concentrations Organism Gram-Negative bacteria Burkholderia cepacia Escherichia coli Enterobacter gergoviae Enterobacter aerogenes Flavobacterium odoratum Klebsiella pneumoniae Proteus mirabilis Pseudomonas aeruginosa Gram-positive bacteria Staphylococcus aureus Staphylococcus epidermidis Yeast Candida albicans Saccharomyces cerevisiae Mold Aspergillus niger Pencillium sp. Product Specifications: Appearance: Odor: Specific Gravity: % Water (KF): ATCC # JEECIDE CAP-2 25416 8739 33028 13048 NCIB 13294 4352 9240 9027 1250 625-1250 5000 1250-2500 1250 625 1250 2500-5000 6538 12228 625 625 10231 7752 313 <78 9642 Cosmetic isolate <78 <78 Clear liquid Slight, characteristic 0.967 – 1.016 1 MAX Preservative Compositional Breakdown: Phenoxyethanol: 30.0 – 40.0 % Regulatory: Product approved for Global Use. You Can Count On Us! Revision Date: 3/16/2005 Page 3 of 3 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Kill Test Data JEECIDE CAP-2 has been tested using the tube testing method. Below are the results: JEECIDE CAP-2 @ 1% Bacteria Yeast Mold Pool 1 Results 3 Pool 2 3 Pool 3 3 Pool 4 Pool 5 3 3 Scale: 0 = No Kill 1 = Slight 2 = Moderate 3 = Kill You Can Count On Us! All suggestions and data in this bulletin are based on information we believe to be reliable. They are offered in good faith. However, no guarantee is made or implied as conditions and methods of use of our products are beyond our control. We recommend that the prospective user determine the suitability of our materials and suggestions on an experimental basis before adopting them on a commercial scale. Statements as to the use of our products are not to be construed as recommendations for their use in the infringement of any patents. 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEECIDE CAP-4 Technical Data Sheet INCI Name: Caprylyl Glycol, Phenoxyethanol CAS Numbers: 1117-86-8, 122-99-6 JEECIDE CAP-4 attributes include the following: • • • • • • • • • • Paraben-free Formaldehyde-free Highly effective anti-microbial Active over a wide pH range (3-10) Compatible with anionic, cationic and non-ionic surfactants and emulsifiers Toxicologically safe for use Equally suitable for use in both rinse-off and leave-on products Effective in difficult to preserve Water/Silicone emulsions Globally approved: US, EU and Japan. Can be used alone or in combination with other preservatives pH Stability: Stable in the usual operating range of 3 – 10 which is typical for most personal care products Recommended Use Level: JEECIDE CAP-4 can be added at 0.5 – 1.5% for effective anti-microbial efficacy. However, it is import that every formulation be challenge-tested to determine the correct level of JEECIDE CAP-4 to ensure proper preservation. Method of Addition: For emulsion products, JEECIDE CAP-4 can be added directly to the water phase during pre or postemulsification at or below 80 °C. It is soluble or dispersible in most non-polar materials. JEECIDE CAP-4 is not water soluble however for highly aqueous systems, the addition of a co-solvent, coupling agent or surfactant (eg. Polysorbate 20) in a 1:1 ratio will make it water soluble to obtain a clear system. Page 1 of 3 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Technical Data Sheet continued…. Solubility Data: Ingredient Water Mineral Oil Apricot Kernel Oil Jojoba Oil Cyclomethicone PEG-8 Dimethicone 200/100 cst Phenyltrimethicone Glycerin Propylene Glycol Ethanol 190 Proof C12-15 Alkyl Benzoate Butylene Glycol Polysorbate – 20 Polysorbate – 80 PEG-40 Hydrogenated Castor Oil Compatibility IS D S S IS S D D S S S S S S S S D: Dispersible IS: Insoluble S: Soluble Recommended Use Level: 0.5 – 1.5% Microbiological Activity: JEECIDE CAP-4 is effective against both gram-positive and gram-negative bacteria, yeast and molds. In difficult to preserve systems, JEECIDE CAP-4 can be used in combination with other preservative agents. Examples of this are: • 0.5 – 1.0% JEECIDE CAP-4 and 0.20% Potassium Sorbate or Sorbic Acid • 0.5 – 1.0% JEECIDE CAP-4 and 0.05% Iodopropynyl Butylcarbamate • 0.5 – 1.0% JEECIDE CAP-4 and 0.20% DMDM Hydantoin • 0.5 – 1.0% JEECIDE CAP-4 and 0.10% Sodium Benzoate Page 2 of 3 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Product Specifications: Test Appeearance Odor Specific Gravity % Moisture (KF) % Phenoxyethanol (HPLC) % Caprylyl Glycol Specifications Clear Liquid Characteristic 1.0126 – 1.0217 1 % Maximum 53 – 58 42 - 47 Regulatory: Approved for global use. Storage Conditions: JEECIDE CAP-4 can be stored in the original, unopened containers at ambient temperature for at least one year. When exposed to freezing temperatures, JEECIDE CAP-4 may cloud and slightly separate. The product should be mixed and gently warmed to 45 – 50 °C to obtain a clear mixture. You Can Count On Us! All suggestions and data in this bulletin are based on information we believe to be reliable. They are offered in good faith. However, no guarantee is made or implied as conditions and methods of use of our products are beyond our control. We recommend that the prospective user determine the suitability of our materials and suggestions on an experimental basis before adopting them on a commercial scale. Statements as to the use of our products are not to be construed as recommendations for their use in the infringement of any patents Page 3 of 3 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEECIDE CAP- 5 Technical Data Sheet INCI Name: Phenoxyethanol & Caprylyl Glycol & Potassium Sorbate & Water & Hexylene Glycol CAS Numbers: 1117-86-8, 122-99-6, 590-00-1, 7732-18-5, 107-41-5 EINECS Numbers: 214-254-7, 204-589-7, 246-376-1, 231-791-2, 203-489-0 JEEN International has recognized the need for a synergistic blend of conventional and nonconventional preservative ingredients that inhibit microbial growth. JEECIDE CAP-5 is a unique easyto-use clear liquid preservative that is: • • • • • • • • • Paraben-free Formaldehyde-free Broad spectrum – effective against bacteria with enhanced protection against yeast and mold for difficult to preserve fomulations. Active over an acidic pH range 3.0 – 6.5 Compatible with anionic, cationic and non-ionic surfactants and emulsifiers Toxicologically safe for use Equally suitable for use in both rinse-off and leave-on products Effective in difficult to preserve Water/Silicone emulsions Approved for Global use. pH Stability: Stable in the operating range of 3.0 – 6.5. Recommended Use Level: JEECIDE CAP-5 can be added at 0.5 – 1.5% for effective anti-microbial efficacy. However, it is important that every formulation be challenge-tested to determine the correct level of JEECIDE CAP-5 to ensure proper preservation. Method of Addition: It is suggested not to add this blend to a product at a temperature exceeding 70 - 75°C for extended time periods. For emulsion products, because of the excellent compatibility of this blend with most ingredients, incorporation of it during the cool-down phase of processing is preferred. It is soluble or dispersible in most non-polar materials. JEECIDE CAP-5 is not water soluble however for highly aqueous systems, the addition of a co-solvent, coupling agent or surfactant (eg. Polysorbate 20) in a 1:1 ratio will make it water soluble to obtain a clear system. 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Technical Data Sheet continued…. Solubility Data: Ingredient Mineral Oil Cyclomethicone Dimethicone 200/100 cst. Caprylic/Capric Triglycerides Water Propylene Glycol Ethanol 190 Proof Isododecane C12-15 Alkyl Benzoate Isopropyl Myristate Butylene Glycol Phenyltrimethicone Compatibility D IS D S D S S S S S S S D: Dispersible IS: Insoluble S: Soluble Microbiological Activity: JEECIDE CAP-5 is very effective against both gram-positive and gram-negative bacteria; and very effective against yeast and molds. 2 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Microbiological Challenge Studies: A study was conducted using 2 formulations: an oil-in-water emulsion and a water-in-oil emulsion using 0.5% and 1.0% JEECIDE CAP-5. The protocol used was a modification of the CTFA Challenge Test using a 3 week re-challenge time period instead of a 4 week period. All samples were inoculated at the start of the study and sampled at 24 hours, 48 hours, 7 days, 14 days and 21 days. After 21 days, all samples were re-inoculated and subjected to a second challenge. Oil-in-Water Emulsion Ingredients Water Glycerin Apricot Kernel Oil Cetearyl Alcohol & Ceteareth-20 Glyceryl Stearate & PEG-100 Stearate JEECIDE CAP-5 Test Organism Control 0.5% JEECIDE CAP-5 1.0% JEECIDE CAP-5 70.50 4.00 17.00 4.50 70.00 4.00 17.00 4.50 69.50 4.00 17.00 4.50 4.00 4.00 4.00 X 0.50 1.00 Unpreserved Control Initial Challenge 24 hrs. 7 days 21 days S. aureus ATCC 6538 7.4 x 10 4 <10 3 P. aeruginosa ATCC 9027 2.5 x 10 4 1.6 x 10 7 1.9 x 10 K. pneumoniae ATCC 4352 1.6 x 10 5 7.6 x 10 4 C. albicans ATCC 10231 4.1 x 10 4 8.3 x 10 A. niger ATCC 9642 + Penicillium sp. isolate 3.4 x 10 4 2.5 x 10 Unpreserved Control Re-challenge 24 hrs. 7 days 21 days 1.4 x 10 6 4.3 x 10 2 <10 7 1.5 x 10 7 2.0 x 10 7 1.9 x 10 7 4.0 x 10 3 1.1 x 10 6 1.6 x 10 6 4.0 x 10 5 4 5.3 x 10 4 4.0 x 10 5 4.4 x 10 5 8.0 x 10 5 4 1.4 x 10 4 5.1 x 10 4 3.0 x 10 4 2.9 x 10 4 <10 3 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com 0.5% JEECIDE CAP-5 Initial Challenge Test Organism 0.5% JEECIDE CAP-5 Re-challenge 24 hrs. 7 days 21 days 24 hrs. 7 days 21 days S. aureus ATCC 6538 <10 <10 <10 <10 <10 <10 P. aeruginosa ATCC 9027 <10 <10 <10 <10 <10 <10 K. pneumoniae ATCC 4352 <10 <10 <10 <10 <10 <10 C. albicans ATCC 10231 1.2 x 10 4 <10 <10 <10 <10 <10 A. niger ATCC 9642 + Penicillium sp. isolate 2.3 x 10 3 <10 <10 <10 <10 <10 1% JEECIDE CAP-5 Initial Challenge 24 hrs. 7 days 21 days 24 hrs. S. aureus ATCC 6538 <10 <10 <10 <10 <10 <10 P. aeruginosa ATCC 9027 <10 <10 <10 <10 <10 <10 K. pneumoniae ATCC 4352 <10 <10 <10 <10 <10 <10 C. albicans ATCC 10231 <10 <10 <10 <10 <10 <10 A. niger ATCC 9642 + Penicillium sp. isolate <10 <10 <10 <10 <10 <10 Test Organism 1% JEECIDE CAP-5 Re-challenge 7 days 21 days 4 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Water-In-Oil Emulsion Control Ingredients Water Glycerin Butylene Glycol Sodium Chloride Cyclomethicone Dimethicone Isostearyl Palmitate Isododecane & Dimethicone Crosspolymer-3 Cyclomethicone & PEG/PPG-18/18 Dimethicone JEECIDE CAP-5 Test Organism 0.5% JEECIDE CAP-5 1.0% JEECIDE CAP-5 59.70 4.00 3.00 0.30 7.00 2.00 4.00 10.00 59.20 4.00 3.00 0.30 7.00 2.00 4.00 10.00 59.20 4.00 3.00 0.30 7.00 2.00 4.00 10.00 10.00 10.00 10.00 X 0.50 1.00 Unpreserved Control Initial Challenge 24 hrs. 7 days 21 days 4 S. aureus ATCC 6538 2.0 x 10 P. aeruginosa ATCC 9027 4.4 x 10 K. pneumoniae ATCC 4352 1.1 x 10 C. albicans ATCC 10231 1.1 x 10 4 A. niger ATCC 9642 + Penicillium sp. isolate 2.0 x 10 3 4 5 4.0 x 10 7.1 x 10 1.1 x 10 8.5 x 10 1.2 x 10 3 4 5 3 4 Unpreserved Control Re-challenge 24 hrs. 7 days 21 days <10 7.2 x 10 9.5 x 10 3 <10 8.7 x 10 2.2 x 10 3.6 x 10 8.0 x 10 3 3 1.5 x 10 2.0 x 10 2 4 3 3 3 <10 3.5 x 10 3.4 x 10 4.8 x 10 1.7 x 10 <10 4 3 3 3 1.1 x 10 5 <10 1.7 x 10 2.2 x 10 3 3 5 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Test Organism 0.5% JEECIDE CAP-5 Initial Challenge 24 hrs. 7 days 21 days 0.5% JEECIDE CAP-5 Re-challenge 24 hrs. 7 days 21 days S. aureus ATCC 6538 <10 <10 <10 <10 <10 <10 P. aeruginosa ATCC 9027 <10 <10 <10 <10 <10 <10 K. pneumoniae ATCC 4352 <10 <10 <10 <10 <10 <10 C. albicans ATCC 10231 1.1 x 10 2 <10 <10 <10 <10 <10 A. niger ATCC 9642 + Penicillium sp. isolate 3.0 x 10 1 <10 <10 <10 <10 <10 1% JEECIDE CAP-5 Initial Challenge Test Organism 1% JEECIDE CAP-5 Re-challenge 24 hrs. 7 days 21 days 24 hrs. 7 days 21 days S. aureus ATCC 6538 <10 <10 <10 <10 <10 <10 P. aeruginosa ATCC 9027 <10 <10 <10 <10 <10 <10 K. pneumoniae ATCC 4352 <10 <10 <10 <10 <10 <10 C. albicans ATCC 10231 <10 <10 <10 <10 <10 <10 A. niger ATCC 9642 + Penicillium sp. isolate 2.0 x 10 <10 <10 <10 <10 <10 1 6 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Results: Oil-in-Water The JEECIDE CAP-5 at 1.0% killed all the challenge organisms within 24 hours after each challenge. At 0.5%, activity was slower versus yeast and mold than against bacteria after the first challenge, but molds were reduced to less than 10 per gram within 48 hours (results not shown). After the second challenge, 0.5% was effective against all organisms within 24 hours. Water-in-Oil The JEECIDE CAP-5 was effective against bacteria within 24 hours after each challenge. At 1.0%, the JEECIDE CAP-5 was faster against yeast and mold than at 0.5% after the first challenge but no organisms were detected 24 hours after the second challenge in the presence of 0.5% or 1.0% JEECIDE CAP-5. Product Specifications: Appearance @ 25 °C: Odor: Specific Gravity: % Water (KF): Clear to slightly hazy liquid* Slight, Characteristic 1.015 – 1.065 12 Maximum *Caution: Product may separate upon standing. Mix before use. Preservative Compositional Breakdown: % Phenoxyethanol: 35 – 45% % Potassium Sorbate: 8 – 15% Regulatory: Product approved for Global Use. You Can Count On Us! 7 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Kill Test Data JEECIDE CAP-5 has been tested using the tube testing method. Below are the results: JEECIDE CAP-5 @ 1% Bacteria Yeast Mold Pool 1 Results 3 Pool 2 3 Pool 3 3 Pool 4 Pool 5 3 3 Scale: 0 = No Kill 1 = Slight 2 = Moderate 3 = Kill You Can Count On Us! All suggestions and data in this bulletin are based on information we believe to be reliable. They are offered in good faith. However, no guarantee is made or implied as conditions and methods of use of our products are beyond our control. We recommend that the prospective user determine the suitability of our materials and suggestions on an experimental basis before adopting them on a commercial scale. Statements as to the use of our products are not to be construed as recommendations for their use in the infringement of any patents. 8 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com JEECHEM® FS-102 Technical Data Sheet INCI: Hexylene Glycol, PEG-25 Hydrogenated Castor Oil, PEG-40 Hydrogenated Castor Oil CAS Numbers: 107-41-5, 61788-85-0, 61788-85-0 EINECS Numbers: 203-489-0, Exempt, Exempt JEECHEM® FS-102 is a low-odor, high performance solubilizing agent. JEECHEM® FS-102 has great solvent power that is useful for solubilizing fragrances, essential oils, active ingredients, vitamins and other hydrophobic substances into aqueous-based systems. In some formulations, it can replace alcohol to allow the claim of “alcohol-free”. • Solubilizer • Alcohol Replacement Suggested Applications: • Body Washes • Shampoos • Facial Cleansers • Perfumes & Colognes • Toners You Can Count On Us! 1 24 Madison Road, Fairfield, New Jersey 07004, USA Tel: 800-771-JEEN (5336), Tel: 973-439-1401, Fax: 973-439-1402, email: info@jeen.com , Website: www.jeen.com Recommended Use Levels: For Body Wash: For Shampoo: For Perfumes & Colognes: Toners: 0.75 – 1.5% 0.75 – 1.5% 0.75 – 1.5% 0.75 – 1.5% Benefits: Aids in maintaining clarity • Freeze Thaw Stability • Non-Tacky • Excellent skin feel • Solubility Data Usage: Product Specifications: Appearance @ 25°C: Color (Gardner): pH% 5%: Moisture, %: Iodine Value: Acid Value: Viscous Liquid 4 Maximum 5.0 – 7.50 1.0 Maximum 1.0 Maximum 2.0 Maximum Handling and Storage: • Store in Clean, Dry Area • Ambient Room Temperature • Follow GMP procedures To solubilize hydrophobic substances into aqueous systems, it is recommended the substance be pre-mixed with JEECHEM® FS-102 in a 1:1 ratio to obtain complete solubility and clarity of the substance in the finished product. Standard Packaging: Drum: 450 Lbs. Net Wt. Pail: 40 Lbs. Net Wt. You Can Count On Us! 2