@
Analysis Services
Physical Properties
Test
Ash of coals/coke
Ash of oil products
Ash in wood, pulp, paper and paperboard
Density of liquid products
Moisture of oil products
Water and Sediment in Fuel Oils
Salt in crude oil
Total acid number (TAN) of liquid
sample
Total basic number (TBN) of liquid
sample
Thermal Gravimetric Analysis (TGA)
In situ TGA-FT-IR
In situ FT-IR for both solid and liquid
sample
Attenuated total reflection infrared (ATRIR)
In situ FT-IR for solid catalyst in H2, CO,
CH4 flow (Temperature: RT to 500oC)
In situ Pyridine FT-IR
(For solid acid kinds, strength and
distribution, temperature: RT to 500oC)
NH3-TPD
(for solid acid amount, strength and
distribution, temperature: RT to 960oC)
Method or apparatus
ASTM D4422
ASTM D482
TAPPI T211 om-07
DMA 35N density meter
ASTM D4377 (KF titration)
ASTM D1796
ASTM D6470
ASTM D 644-01 (Potentiometric titration)
Price(Can $)
35
50
50
20
60
60
60
80
ASTM D2896 (Potentiometric titration)
80
Thermogravimetric Analyzer Q500 (Air, N2,
O2 flow selectable)
TGA-Q500 & Nicolet 6700 FT-IR
Spectrometer
Nicolet 6700 FT-IR Spectrometer
60
Nicolet 6700 FT-IR Spectrometer
(i solid sample; ii non-aqueous liquid)
Nicolet 6700 FT-IR Spectrometer
i
Nicolet 6700 FT-IR Spectrometer
150
Quantachrome Autosorb 1-C
160
160
65
30
50
120
ii
Elemental analysis
Test
Total sulphur and nitrogen for both liquid
and solid sample
Method or apparatus
Antek Nitrogen/Sulfur Analyzer 9000
(Nitrogen : 50 ppb to 17%;
Price(Can $)
70
Total Carbon, Hydrogen, Nitrogen, and
Sulfur for liquid and solid sample
Sulfur Analyzer: 50 ppb to 40%)
CHNS-932 (Carbon: 0.002 to 100%;
Hydrogen: 0.02 to 50%; Nitrogen: 0.02 to
50%; Sulfur: 0.04 to 65%)
120
(Available in
Jan.2011)
Gas Chromatography
Test
Gases sample analysis
(N2, O2, CO2, CO2, CH4, Paraffin gas
(C2-C6) and olefin gas (C2-C6)
Liquid sample with bp RT-350oC
(hydrocarbons, esters, organic acids)
Sulfur or Phosphorus compounds
(ppb to 30 mass%)
Sulphur compounds distribution
Nitrogen or Phosphorus compounds
(ppb to 30 mass%)
Method or apparatus
GC3400 (TCD) and GC17A(FID)
Price(Can $)
80
Varian GC 450 (FID)
80
Varian GC450 (PFPD)
100
Varian GC450 (PFPD-S)
GC-950 (NPD)
160
100
Gas Chromatography Mass Spectrometry
Test
Hydrocarbon types by GC-MS
(Non-aqueous phase sample only)
GC-MS qualitative analysis
(for major components)
GC-MS quantitative analysis
(for major n components)
Method or apparatus
SHIMADZU GC/MS 5000
Price(Can $)
180
SHIMADZU GC/MS 5000
180
SHIMADZU GC/MS 5000
&GC-450 (FID)
180+n×20
High Performance Liquid Chromatography
Test
Alkenes, aromatic and saturated
hydrocarbons in oil sample
Liquid substance sensitive to RID or
DAD analysis
Method or apparatus
Agilent HPLC 1200 (ASTM D6591, RID and
DAD)
Agilent HPLC 1200 (RID and DAD)
Price(Can $)
160
80
UV Spectrophohometer
Test
Naphthalenes in oil sample
Liquid substance sensitive to UV/V
analysis
Method or apparatus
UV/V 1800 spectrophohometer (ASTM
D1840)
UV/V 1800 spectrophohometer
Price(Can $)
60
35
Surface and Catalytic Characterization
Test
Surface area (5 points) and pore volume
(1 point)
Surface area (11 points),pore volume (1
point) and pore size distribution
(micro or meso-pores analysis, up to 40
adsorption/desorption points)
Chemisorption analysis
(H2, CO, O2, CH4, CO2, NH3)
Chemisorption analysis with pulse
titration
(H2, CO, O2, CH4, CO2, NH3)
Temperature program reduction,
oxidation and desorption
(H2-TPR, CO-TPR; O2-TPD; TPD, H2TPD, CO-TPD, CH4-TPD, CO2-TPD,
NH3-TPD)
Method or apparatus
Quantachrome Autosorb 1-C (N2 adsorption)
Price(Can $)
70
Quantachrome Autosorb 1-C (N2 adsorption)
160
Quantachrome Autosorb 1-C
120
Quantachrome Autosorb 1-C
160
Quantachrome Autosorb 1-C & GC-3400
160
240 (with
quantitative
analysis)
Particle Size Distribution
Test
Laser particle size range and distribution
analyzer (0.3-300 um)
Method or apparatus
Analysette 22
Price(Can $)
45
Hydro-processing Service
Test
Hydro-treating of oil sample in fixed bed
( low viscous liquid sample, temperature:
up to 400°C, pressure: up to 1450 psi,
capacity: max. catalyst loading of 20ml,
liquid flow 10ml/min )
Hydro-treating of oil sample in batch
reactor with stirring
(viscous liquid available, temperature: up
to 500°C, pressure: up to 4500 psi,
capacity: max. filling volume: 600ml)
Method or apparatus
Autoclave Engineers BTRS-Jr-PC Micr –
reactor system with computer controller
Price(Can $)
70 (per hour)
Autoclave Engineers
High Temperature, Bolted Closure Laboratory
Batch Reactors (SUS reactor and Hastelloy C
reactor)
Hydrothermal or solvent (supercritical
fluid) treatment in batch reactor with
stirring
Autoclave Engineers
High Temperature, Bolted Closure Laboratory
Batch Reactors (Hastelloy C reactor)
70 (per hour)
70+n×10
(Continuous
sampling
available, n
sampling
times)
70 (per hour)
(temperature: up to 450°C, pressure: up
to 4500 psi)
Supercritical CO2 extraction
(temperature: up to 120°C, pressure up to
12000psi)
Supercritical solvent fluid extraction
(temperature: up to 350°C, pressure up to
1500psi, solvent: water, methanol,
ethanol, hexane or acetone )
Supercritical Fluid SFT-100
70 (per hour)
Supercritical Fluid reactor
70 (per hour)
Vacuum and Atmosphere Treatment
Test
Vacuum calcination (min. 0.1mmHg,
max. 1000°C)
Atmosphere calcination (normal pressure,
H2, N2, O2, air, He, CO or Ar flow
controllable, max. 1000°C )
Method or apparatus
Vacuum tubular oven
Price(Can $)
60 (per hour)
Vacuum tubular oven
60 (per hour)
Super Speed Centrifuge
Test
Separation by high speed centrifuge
(max. speed: 25000 rpm, controllable
temperature range:-16 to 40°C)
Method or apparatus
Du Pont Sorvall RC-5B Refrigerated
superspeed centrifuge
Price(Can $)
50
Please be informed:
1.
Customers have to provide the special gas standard samples except for O2, N2, CO2, CH4, CO, H2, and
hydrocarbon gas of C<6 standards.
2.
Quotation is available upon request on customized analytical services or lab services.
Contact:
Prof. Ying Zheng
Tel: 1-506-447-3329
Email: yzheng@unb.ca
Address: Department of Chemical Engineering, University of New Brunswick
P.O. Box 4400, 15 Dineen Dr. Head Hall,
Fredericton, N.B., E3B 5A3, Canada