Agilent GC/MSD ChemStation and Instrument Operation

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Feb 25, 1999 Document Information: Filename FILENAME \* MERGEFORMAT USERINFO.DOC Current Owner Barney Neal Product Identifier H8720A Project Identifier Customer Training Course Update to G1701DA Current Lifecycle Phase Investigation Revision Log: Revision Date Reason For Update A.00 22 Mar 02 Initial revision. B.00 24 June 02 Added additional details C.00 1 Dec 04 Updated material to software revision G1701 DA D.01.02 Product Delivery Requirements 1. Course Description: This course is designed for those who want to enhance their skills in the use of an Agilent GC/MSD and ChemStation. 2. Course Outline with correlation to file names: NOTE: all files are available from the CAG EPI Warehouse at http://whadmin.cos.agilent.com/ MS Basics and Hardware Configuration………………………………….Chap1.ppt & Mod1.doc MS Tuning…………………………………………………….…………..Chap2.ppt & Mod2.doc Maintenance……………………………………………………………….Chap3.ppt & Mod3.doc Methods I - Data Acquisition……………………………………………...Chap4.ppt & Mod4.doc Setting Up Data Acquisition………………………………………………Chap5.ppt & Mod5.doc Qualitative Data Analysis………………………………………………….Chap6.ppt & Mod6.doc LAB EXERCISE: Qualitative Data Analysis…………………………………………….Lab6.doc Quantitative Data Analysis………………………………………………..Chap7.ppt & Mod7.doc LAB EXERCISE: Quantitation of SIM Data…………………………………...………Lab7a.doc LAB EXERCISE: Quantitation of Scan Data……………………………...…...………Lab7b.doc Sequencing, Secured Control, and RTL...………………………………...Chap8.ppt & Mod8.doc Complete Manual………………………………………………………………………h8720a.doc Student Manual (pdf)………………………………………….………………..h8720a student.pdf Instructor Manual (pdf)…………………………………….………………...h8720a instructor.pdf Additional data files……..…………………………………………………………….datafiles.exe 3. For marketing purposes of this product see the Product Release Bulletin (if available): Product Release Bulletin available? N0 4. Instructor or Delivery Agent skills required to deliver the product: A fundamental knowledge of the WinXP operating system. A detailed knowledge of the current Agilent GC/MSD operating software. Detailed knowledge of the specific MSD tune parameters and their influence on the acquired data. Detailed knowledge of the specific MSD scan acquisition parameters and their influence on the acquired data. Detailed knowledge of the specific MSD selected ion monitoring (SIM) acquisition parameters and their influence on the acquired data. Detailed knowledge of the PBM library search and Parametric Retrieval utilities. Detailed knowledge of the quantitation software and the influence of the various quantitation parameters. A fundamental knowledge of RPN commands and macro programming as related to the current Agilent operating software. 5. Equipment (Instrumentation and Software) Required for product delivery Agilent 5973N GC/MSD PC with WinXP operating system G1701DA software version D.01.02. NIST98 and NBS75K spectral libraries 6. Consumables required GC septum 10ul syringe or ALS syringe 30meter HP5MS cap column 7. Samples required Agilent GC-MS Performance Evaluation Sample (part # 05970-60045) 8. Electronic Files required All additional data files are downloadable from the data warehouse. When you unzip files, set it for the root folder (C:\ or D:\) with the "user folder names" option. This will place all method and data files in the location used in the manual. “Sequence.csv” file (downloadable from the data warehouse) will need to be placed in the "MSDchem\1\sequence" folder. 9. Tools required MSD Tool Kit (part # 05971-60561) 10. Activities required prior to product delivery Delete files created by previous class 11. Activities required during product delivery N/A 12. Activities required after product delivery Delete files created by previous class User Task Analysis The user wants to know about and how to use the new hardware and software feature(s) added with this version of the GC/MSD software. Audience Analysis GC/MSD education levels range from high school grad to Ph.D with the typical user being a college grad. Experience levels range from no experience to several years with the typical user experience about 3 – 5 years. Most students require detailed step-by-step lab instructions. Hewlett-Packard Company For Internal Use Only ! 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ser- Barney Neal 12 nMicrosoft Word 9.0 a@ 4â0 @ |ÀI•e¾ @ šYƒ«øÄ h ¼ 5 A g i l e n t G C / M S D C h e m S t a t i o n a n d I n s t r u m e n t O p e r a t i o n C o n s u l t a n t + M S D T r a i n i n g C u s t o m e r , G C / M S D , C h e <?msocontentType?><FormTemplates xmlns="http://schemas.microsoft.com/sharepoint/v3/contenttype/forms"><Edi t>PublicationForm</Ed ma:default="English" ma:format="Dropdown" ma:internalName="Language" ma:readOnly="false"> <xsd:simpleType> <xsd:restriction base="dms:Choice"> <xsd:enumeration value="Chinese (Simplified)"/> <xsd:enumeration value="Chinese (Traditional)"/> <xsd:enumeration value="Danish"/> <xsd:enumeration value="Dutch"/> <xsd:enumeration value="English"/> <xsd:enumeration value="Finnish"/> <xsd:enumeration value="French"/> <xsd:enumeration value="German"/> <xsd:enumeration value="Italian"/> <xsd:enumeration value="Japanese"/> <xsd:enumeration value="Korean"/> <xsd:enumeration value="Portuguese"/> <xsd:enumeration value="Russian"/> <xsd:enumeration value="Spanish"/> <xsd:enumeration value="Swedish"/> <xsd:enumeration value="Vietnamese"/> </xsd:restriction> </xsd:simpleType> </xsd:element> </xsd:schema> <xsd:schema targetNamespace="151852f0-18c3-4ccd-adbb-656a014d69e9" elementFormDefault="qualified" xmlns:xsd="http://www.w3.org/2001/XMLSchema" xmlns:dms="http://schemas.microsoft.com/office/2006/documentManagement/ty pes"> <xsd:import namespace="http://schemas.microsoft.com/office/2006/documentManagement/ty pes"/> <xsd:element name="WHID" ma:index="2" ma:displayName="Warehouse ID" ma:description="" ma:hidden="true" ma:internalName="WHID"> <xsd:simpleType> <xsd:restriction base="dms:Text"/> </xsd:simpleType> </xsd:element> <xsd:element name="WebPageDescription" ma:index="6" ma:displayName="Web Page Description" ma:description="Description of document limited to 175 characters. 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ø ˆ d H t ¨ x 4 Ô ¼ D P # % & ' ( p ° ð Ü ) È | $ ˜ * , P Ä \ ) • 8 ! ° " ¼ R e l e a s e D a t e L i m i t e d U s e P r o d u c t L i n e L o t N u m b e r P r o d u c t G r o u p 7 d i s p l a y _ u r n : s c h e m a s - m i c r o s o f t c o m : o f f i c e : o f f i c e # E d i t o r I n d u s t P a r t N u E x t r I n d r m a u y b P s G e a t r o u p r r t N u m b e r r y A b s t r a c t L a n g u a g e G e o g r a p h y N a t i v e A p p l i c a t i o n C o n t e n t T y p e i o n D a t e P r o d u c t W H I D E x p i r a t P r o d u c t T y p e W o r k s p a c e U r l 7 d i a s - m i c r o s o f t c o m : o f f i c e : o f f i c e # A u t P a g e C o u n t I n d u s t r y T y p e S u _ C a t e g o r y C a t e g o r i e s A p p r _ C o m m e n t s - s p l a y _ u r n : s c h e m h o r b j e c t o v a l L e v e l A s s i g n e d T o _ A u t h o r ! 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<xsd:enumeration value="..."/> </xsd:restriction> </xsd:simpleType> </xsd:element> </xsd:schema> <xsd:schema targetNamespace="d60c28fc-3d14-46f3-b174-9a10a2a6c6f4" elementFormDefault="qualified" xmlns:xsd="http://www.w3.org/2001/XMLSchema" xmlns:dms="http://schemas.microsoft.com/office/2006/documentManagement/ty pes"> <xsd:import namespace="http://schemas.microsoft.com/office/2006/documentManagement/ty pes"/> <xsd:element name="Analytical_x0020_Technique" ma:index="37" nillable="true" ma:displayName="Analytical_x0020_Technique" ma:format="Dropdown" ma:internalName="Analytical_x0020_Technique" ma:readOnly="false"> <xsd:simpleType> <xsd:restriction base="dms:Choice"> <xsd:enumeration value="Atomic Absorption (AA)"/> <xsd:enumeration value="Capillary Electrophoresis (CE)"/> <xsd:enumeration value="CE/MS"/> <xsd:enumeration value="Dissolution"/> <xsd:enumeration value="Fluorescence Spectroscopy"/> <xsd:enumeration value="FTIR"/> <xsd:enumeration value="GC"/> <xsd:enumeration value="GC Analyzer"/> <xsd:enumeration value="GC QQQ"/> <xsd:enumeration value="GC Q-TOF"/> <xsd:enumeration value="GC x GC"/> <xsd:enumeration value="GC/MSD"/> <xsd:enumeration value="GC-RapidMS"/> <xsd:enumeration value="GPC/SEC"/> <xsd:enumeration value="ICP-MS"/> <xsd:enumeration value="ICP-OES"/> <xsd:enumeration value="LC"/> <xsd:enumeration value="LC QQQ"/> <xsd:enumeration value="LC Q-TOF"/> <xsd:enumeration value="LC TOF"/> <xsd:enumeration value="LC/MS"/> <xsd:enumeration value="Micro GC"/> <xsd:enumeration value="MP-AES"/> <xsd:enumeration value="MS"/> <xsd:enumeration value="NMR"/> <xsd:enumeration value="PCR / qPCR"/> <xsd:enumeration value="Rapid-MS"/> <xsd:enumeration value="Thin Layer Chromatography"/> <xsd:enumeration value="UHPLC"/> <xsd:enumeration value="UV-Vis-NIR Spectroscopy"/> <xsd:enumeration value="X-ray Crystallography"/> </xsd:restriction> </xsd:simpleType> </xsd:element> <xsd:element name="Matrix" ma:index="38" nillable="true" ma:displayName="Matrix" ma:format="Dropdown" ma:internalName="Matrix" ma:readOnly="false"> <xsd:simpleType> <xsd:restriction base="dms:Choice"> <xsd:enumeration value="Biodiesel/Biogas"n i n g M a t e r i a l L i b r a r y 7 4 <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration /> value="Biofuel(s)"/> value="Biological Mass"/> value="Biologics"/> value="Blood"/> value="Bone"/> value="Breast Milk"/> value="Cell culture"/> <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration <xsd:enumeration value="Cereals"/> value="Coffee"/> value="Composites"/> value="Cosmetics"/> value="Dairy"/> value="Designer Drugs"/> value="Drinking Water"/> value="Drugs of Abuse"/> value="Edible Oils"/> value="Ethanol"/> value="Feces"/> value="Flavors"/> value="Food - Other"/> value="Fragrances"/> value="Fruits"/> value="Gas Fuel"/> value="Glass"/> value="Grains"/> value="Human Tissue"/> value="Juice"/> value="Legumes"/> value="Liquid Fuel"/> value="Meat"/> value="Metals"/> value="Minerals"/> value="Natural Gas"/> value="Nutraceutical(s)"/> value="Nuts"/> value="Oil"/> value="Optical Coatings"/> value="Optical 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xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:dcterms="http://purl.org/dc/terms/" xmlns:odoc="http://schemas.microsoft.com/office/internal/2005/internalDoc umentation"> <xsd:import namespace="http://purl.org/dc/elements/1.1/" schemaLocation="http://dublincore.org/schemas/xmls/qdc/2003/04/02/dc.xsd" /> <xsd:import namespace="http://purl.org/dc/terms/" schemaLocation="http://dublincore.org/schemas/xmls/qdc/2003/04/02/dcterms .xsd"/> <xsd:element name="coreProperties" type="CT_coreProperties"/> <xsd:complexType name="CT_coreProperties"> <xsd:all> <xsd:element ref="dc:creator" maxOccurs="1" ma:index="9" ma:displayName="Author"/> <xsd:element ref="dcterms:created" minOccurs="0" maxOccurs="1"/> <xsd:element ref="dc:identifier" minOccurs="0" maxOccurs="1"/> <xsd:element name="contentType" minOccurs="0" maxOccurs="1" type="xsd:string" ma:index="35" ma:displayName="Content Type"/> <xsd:element ref="dc:title" maxOccurs="1" ma:index="1" ma:displayName="Title"/> <xsd:element ref="dc:subject" minOccurs="0" maxOccurs="1"/> <xsd:element ref="dc:description" minOccurs="0" maxOccurs="1"/> <xsd:element name="keywords" maxOccurs="1" ma:index="7" ma:displayName="Keywords"> <xsd:simpleType> <xsd:restriction base="xsd:string"> <xsd:minLength value="1"/> </xsd:restriction> </xsd:simpleType> </xsd:element> <xsd:element ref="dc:language" minOccurs="0" maxOccurs="1"/> <xsd:element name="category" minOccurs="0" maxOccurs="1" type="xsd:string"/> <xsd:element name="version" minOccurs="0" maxOccurs="1" type="xsd:string"/> <xsd:element name="revision" minOccurs="0" maxOccurs="1" type="xsd:string"> <xsd:annotation> <xsd:documentation> This value indicates the number of saves or revisions. The application is responsible for updating this value after each revision. </xsd:documentation> </xsd:annotation> </xsd:element> <xsd:element name="lastModifiedBy" minOccurs="0" maxOccurs="1" type="xsd:string"/> <xsd:element ref="dcterms:modified" minOccurs="0" maxOccurs="1"/> <xsd:element name="lastPrinted" minOccurs="0" maxOccurs="1" type="xsd:dateTime"/> <xsd:element name="contentStatus" minOccurs="0" maxOccurs="1" type="xsd:string"/> </xsd:all> </xsd:complexType> </xsd:schema> </ct:contentTypeSchema>

Agilent GC/MSD ChemStation and Instrument Operation

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