1 Quickly Erupted Volcanic Sections of the Steens Basalt, Columbia River Basalt 2 Group: Secular Variation, Tectonic Rotation, and the Steens Mountain Reversal 3 4 Nicholas A. Jarboe 5 University of California, Department of Earth and Planetary Sciences, 6 1156 High St., Santa Cruz, CA 95064 USA (njarboe@pmc.ucsc.edu) 7 8 Robert S. Coe 9 University of California, Department of Earth and Planetary Sciences, 10 1156 High St., Santa Cruz, CA 95064 USA 11 12 Paul R. Renne 13 1) Berkeley Geochronology Center, 2455 Ridge Road, Berkeley, CA 94709 USA 14 2) University of California, Department of Earth and Planetary Science, Berkeley, CA 15 94720 USA 16 17 Jonathan M.G. Glen 18 U.S. Geological Survey, MS989, 345 Middlefield Road, Menlo Park, CA 94025 USA 19 20 Edward A. Mankinen 21 U.S. Geological Survey, MS937, 345 Middlefield Road, Menlo Park, CA 94025 USA 22 23 24 Abstract 25 The Steens Basalt, now considered part of the Columbia River Basalt Group (CRBG), 26 contains the earliest eruptions of this magmatic episode. Lava flows of the Steens Basalt 27 cover about 50,000 km2 of the Oregon Plateau in sections up to 1000 m thick. The large 28 number of continuously-exposed, quickly-erupted lava flows (some sections contain over 29 200 flows) allows for small loops in the magnetic field direction paths to be detected. For 30 volcanic rocks, this detail and fidelity are rarely found outside of the Holocene and yield 31 estimates of eruption durations at our four sections of ~2.5 ka for 260 m at Pueblo 32 Mountains, 0.5 to 1.5 ka for 190 m at Summit Springs, 1-3 ka for 170 m at North Mickey, 33 and ~3 ka for 160 m at Guano Rim. That only one reversal of the geomagnetic field 34 occurred during the eruption of the Steens Basalt (the Steens reversal at ca. 16.6 Ma) is 35 supported by comparing 40Ar/39Ar ages and magnetic polarities to the geomagnetic 36 polarity time scale. At Summit Springs two 40Ar/39Ar ages from normal polarity flows 37 [16.72 ±± 0.29 Ma (16.61) and 16.92 ±± 0.52 Ma (16.82); ±± equals 2σ error] place their 38 eruptions after the Steens reversal, while at Pueblo Mountains an 40Ar/39Ar age of 16.72 39 ±± 0.21 Ma (16.61) from a reverse polarity flow places its eruption before the Steens 40 reversal. Paleomagnetic field directions yielded 50 non-transitional directional-group 41 poles which, combined with 26 from Steens Mountain, provide a paleomagnetic pole for 42 the Oregon Plateau of 85.7°N, 318.4°E, K = 15.1, A95 = 4.3. Comparison of this new pole 43 with a reference pole derived from CRBG flows from eastern Washington and a synthetic 44 reference pole for North America derived from global data implies relative clockwise 45 rotation of the Oregon Plateau of 7.4 ± 5.0° or 14.5 ± 5.4°, respectively, probably due to 46 northward-decreasing extension of the Basin-and-Range. 47 Introduction 48 The Steens Basalt of the Oregon Plateau may cover as much as 50,000 km2 (Mankinen et 49 al., 1987; Carlson and Hart, 1987) of southeastern Oregon, northwestern Nevada, and 50 northeasternmost California. Its extent, eruptive timing, and relationship to the Columbia 51 River Basalts (CRB) have undergone continued debate. Geochemical and field studies 52 have expanded the traditional Columbia River Basalt Group (CRBG) to include the 53 Steens Basalt (Hooper et al., 2002; Camp et al., 2003; Camp and Ross, 2004; Brueseke et 54 al., 2007) at its base. The relative stratigraphy of the Steens Basalt and the CRBG has 55 been traced over 150 km with relationships determined by an intermediate formation, the 56 basalt of Malheur Gorge (Camp et al., 2003; Brueseke et al., 2007). The reverse-to- 57 normal (R-N) polarity change as recorded at Steens Mountain (Steens reversal) is 58 believed to be the only reversal to have occurred during the eruption of the Steens Basalt 59 (Mankinen et al., 1987; Camp and Ross, 2004). 60 61 We are studying the location, age, and transitional field behavior of the Steens reversal 62 recorded throughout the Oregon Plateau (Figure 1). 40Ar/39Ar age determinations from 63 lavas erupted during the transition (Jarboe et al., 2006; Jarboe et al., in preparation) place 64 the reversal at 16.69 ±± 0.14 Ma (16.58). See next section “Age Data Presentation” for 65 age presentation conventions. Due to Basin-and-Range faulting and little vegetative 66 cover, many thick (>500 m) sections of Steens basalt or their possible equivalents are 67 well exposed and have been studied by others (Watkins, 1963; Mankinen et al., 1987 and 68 references therein; Brueseke et al., 2007). So far over a dozen locations have been 69 sampled for paleomagnetic and geochronologic study (Figure 1). A forthcoming paper 70 will report on sections studied that record transitional field behavior (Jarboe et al., in 71 preparation). In this paper we discuss the paleomagnetic and geochronologic results from 72 four sections that record stable polarity secular variation: Summit Springs (60 km 73 northeast of Steens Mountain), Pueblo Mountains (65 km south of Steens Mountain), 74 North Mickey (25 km east of Steens Mountain) and Guano Rim (95 km southwest of 75 Steens Mountain). Except for one lava at Summit Springs, each section erupted during a 76 single geomagnetic polarity chron, and 40Ar/39Ar data, stratigraphy, and petrological 77 considerations place their eruptions in chrons just before or after the Steens reversal. 78 Although some others believe that the Steens Basalt gradually erupted over millions of 79 years (Brueseke et al., 2007), we will show that magnetic field behavior, field polarity, 80 and geochronology of these sections are consistent with rapid local emplacement (1-3 ka) 81 within ~300 ka of the Steens reversal. 82 83 Age Data Presentation 84 Ages in early literature were usually reported with one sigma uncertainty, while two 85 sigma is commonly reported today. We suggest (and herein adopt) using ± to represent 86 exclusively one sigma, ±± to indicate two sigma and ±x to indicate an x% confidence 87 interval. For example ±95 would represent an uncertainty at the 95% confidence interval. 88 This convention is used for ages throughout this paper, with standard paleomagnetic 89 conventions used elsewhere. When citing values with uncertainties from other work, we 90 prefer to present the uncertainty given in the original and convert to other uncertainties if 91 needed for clarity. 92 93 We present ages here using the Fish Canyon sanidine (FCs) age of 28.201 ±± 0.214 Ma 94 determined by astronomical calibration (Kuiper et al., 2008) and the 40K decay constant 95 of 5.463 ±± 0.107 × 10-10/a (Steiger and Jager, 1977; updated by Min et al., 2000). To 96 ease comparison to other 40Ar/39Ar ages in the literature, the 40Ar/39Ar ages determined 97 using the Earthtime (An NSF supported international scientific initiative; 98 http://www.earth-time.org) conventions of 28.02 Ma for the FCs (Renne et al., 1998) and 99 5.543 ±95 0.089 × 10-10/a for the 40K decay constant (Steiger and Jager, 1977) are 100 included in parenthesis after each age. 101 102 Paleomagnetic Procedures 103 All paleomagnetic procedures and analyses were performed at the University of 104 California, Santa Cruz unless otherwise noted. Paleomagnetic cores were sampled with a 105 2.5 cm diameter, water-cooled, diamond-studded, hollow core bit using a hand-held 106 gasoline powered drill. The cores were drilled 5-10 cm deep, oriented to an accuracy of 107 1º-2º while still attached to the outcrop using an orienting stage and a Brunton compass. 108 Sun sites, sun shadows, and site points of known direction were used to correct for local 109 magnetic anomalies. Flow bottoms were generally drilled to minimize the chance of 110 remagnetization by overlying flows. The orientation angles were recorded to the nearest 111 degree and time to the nearest minute. Cores were later cut into 2.5 cm long specimens 112 back at the laboratory. In general the deepest, least weathered specimens from each core 113 were used when determining the paleomagnetic field directions. 114 The natural remanent magnetization (NRM) of the specimens was stepwise- 115 demagnetized in a decaying alternating field (AF) of up to 200 mT and magnetizations 116 were measured in a 2G superconducting magnetometer. Twelve-position measurements 117 were made using custom built hardware and software. An Agico JR-5 calibration sample 118 was measured at least daily and kept within 1.2º of the expected direction with an 119 estimated error no greater than 1.2º. The characteristic remanent magnetization (ChRM) 120 direction of each specimen was determined with straight-line-to-the-origin fits 121 (Kirschvink, 1980) and occasional great circles (McFadden and McElhinny, 1988) using 122 PMGSC42 software (Enkin, 2005). Most specimens were well-behaved upon stepwise 123 AF-demagnetization (Figure 2a). Any viscous component was typically removed by 2 to 124 15 mT (Figure 2b). A few specimens taken from near lightning strikes required greater 125 demagnetization fields to reveal the ChRM, but in most cases a well defined direction 126 was determined (Figures 2c,d). In areas of unusually strong lightning remagnetization, 127 some specimens were overprinted with magnetizations that were not removed even at the 128 highest (~200 mT) demagnetization steps (Figure 2e). In such cases the magnetic 129 direction during AF-demagnetization usually followed a great circle toward the ChRM 130 direction (Figure 2e). 131 132 Generally, at least eight samples were taken from each flow and the mean flow directions 133 were determined using Fisher (1953) or McFadden and McElhinny (1995) statistics 134 (Figure 3). Directions, virtual geomagnetic poles (VGPs), and other data for the flows are 135 shown in Table 1. Three flows at Summit Springs yielded too few ChRMs or great circle 136 fits to determine mean flow directions. In the remaining flows 658 cores were measured, 137 and of these 570 had resolvable characteristic directions, 72 yielded acceptable great 138 circle fits, and 16 directions were rejected. Of the rejected directions 8 had lightning 139 overprints so strong as to completely overwhelm the ChRM, 1 had an unstable 140 demagnetization path, and 7 had resolvable characteristic directions but with outlying 141 directions far (> 40°) from the flow mean direction. These rare outlying directions are 142 likely due to mis-orientation of the core, undetected post-eruptive movement of the 143 sampled outcrop, or complete overprinting. 144 145 Sampling Strategy and Grouping Flow Directions 146 The volcanic sections presented here were sampled as part of our search for lava flows 147 erupted during the Steens reversal to shed light on transitional field behavior. For this 148 reason we chose flow-on-flow sections, where exposure is high, stratigraphy is 149 straightforward, and cover between flows that might conceal a long eruption hiatus or 150 other geological complexity is minimal (see Appendix A1.1 and A1.2 for photos). If 151 measurements in the field with a hand held-fluxgate magnetometer suggested lava flows 152 with intermediate polarity, then we sampled almost every flow unit. If not, we still 153 sampled the section in case overprints obscured a transition zone, usually skipping some 154 lava flows that could be aquired on a return visit if a transition were found, so that we 155 could cover a greater interval. For studies of secular variation in flow-on-flow sections 156 such as these, skipping some flows is common practice because the episodic nature of 157 volcanism results in packets of successive lavas that span little time and have directions 158 that are the same or very similar. To test that this is the cause rather than extended 159 intervals of unchanging field direction, geochemical analyses of some of these packets 160 are being performed under the assumption that little magma differentiation occurs during 161 a burst of frequent eruptions. 162 163 Nonetheless, we still encountered some repetitions of the same or very similar directions 164 in stratigraphically ordered flows. Following the practice of earlier studies at Steens 165 Mountain, these flow packet directions are combined into directional groups (DGs) by 166 the method described by Mankinen et al., (1985). Specifically, lava-flow mean directions 167 that are in sequence and whose α95’s overlap are combined unless they trend in a 168 consistent direction, in which case the flows are not grouped. After this procedure there 169 are 50 remaining directions, of which 13 represent averages of more than one flow and 37 170 that are individual flow directions. All the directions for individual lava flows, as well as 171 the grouped-flow directions, are given in Table 1. The mean direction for each of the four 172 sections do not differ significantly whether computed from the directional groups or from 173 the individual flows, but the confidence circles are a little larger when flows are grouped 174 because N is smaller. In general, we expect that the grouped data provide a more 175 representative sampling of secular variation, and thus the directions and VGPs shown in 176 the figures are for the DGs unless otherwise noted. 177 178 40Ar/39Ar Geochronology Procedures 179 All sample preparation and analyses for 40Ar/39Ar geochronology were done at the 180 Berkeley Geochronology Center (BGC). Plagioclase, sanidine, or groundmass aliquots 181 were prepared from either alteration-trimmed rocks from the same flows as the 182 paleomagnetic cores or the paleomagnetic cores themselves. These samples were 183 crushed, washed, and sieved into size fractions. Each size fraction used was magnetically 184 separated with a Frantz Isodynamic Separator, washed ultrasonically in a dilute (3-4%) 185 HF solution for 3-5 minutes, and rinsed in a purified-water sonic-bath for 20-40 minutes. 186 The samples were then hand-picked under a microscope. For plagioclase and sanidine 187 aliquots, clear grains were selected and any grains with visible inclusions or surface 188 alteration were discarded. Individual groundmass grains were selected to exclude any 189 containing phenocryst fragments. These aliquots and Fish Canyon sanidine (FCs) grains 190 were then placed into separate pits in aluminum disks, wrapped tightly in aluminum foil, 191 and irradiated for 5 hours in the CLICIT facility of the TRIGA reactor at Oregon State 192 University. The neutron fluence (J-parameter) experienced by each aliquot was calculated 193 using an age of 28.02 Ma (Renne et al., 1998) from the FCs standards which had been 194 placed in the center and around the edge of the disk. After waiting typically 4-6 months 195 for 37Ar to decay to optimal measurement levels, samples were degassed with a CO2 laser 196 and the argon isotopes were analyzed with an online MAP 215C mass spectrometer. 197 Samples were then heated in steps for plagioclase and groundmass samples and to total 198 fusion or in steps for single grains of sanidine. Analysis of the empty chamber and 199 atmospheric argon were run often to determine the blank correction and the 200 spectrometer’s mass discrimination, respectively. Parabolic or linear curves were fit to 201 the individual ion beam intensity versus time data to determine the relative abundances of 202 the 40Ar, 39Ar, 38Ar, 37Ar, and 36Ar isotopes found in the sample. The plateau ages were 203 then determined with the program Mass Spec version 7.621 (Deino, 2001) using 95% 204 indistinguishability confidence criterion applied to at least 50% of the 39Ar released 205 comprising at least three contiguous steps unless otherwise stated. Weighted (by inverse 206 variance) mean ages from multiple single-grain plateau ages were determined with 207 Isoplot 3.66 (Ludwig, 2003). 208 209 Volcanic Sections: Geology and Paleomagnetism 210 Pueblo Mountains 211 The reverse polarity Steens-like Pueblo Mountains section (42.1ºN, 118.7ºW) is 60 km 212 south of Steens Mountain at the southern end of the Steens Mountain escarpment (Figure 213 4; photos and larger scale map in Appendix A1.1). The Steens Basalts were first 214 described at the type section at Steens Mountain by Fuller (1931): “The rock is distinctive 215 in the field both from a peculiar porous texture, which is quite characteristic, and from its 216 local content both of labradorite phenocrysts ranging from 1 to 4 cm. in length, and of 217 olivine grains, which are predominantly under 2 mm. in diameter.” (photos Appendix 218 A1.3) Unlike the Steens type section, which is underlain by mid-Miocene volcanics, the 219 Pueblo Mountains section is unconformably underlain by crystalline Middle Cretaceous 220 intrusive and metamorphic basement (Hart et al., 1989). We sampled 11 of about 20 221 flow-on-flow lavas from a continuous section extending across 2.3 km and spanning 260 222 m of elevation. Four other flows located to the south of the main section were also 223 sampled in an unsuccessful attempt to find normal polarity lava flows from the overlying 224 normal polarity chron. Flows in the Pueblo Mountains are tilted 20ºW about a strike of 225 180º and our paleomagnetic field directions have been corrected accordingly. The attitude 226 of the beds was determined by field measurements and are in good agreement with 227 1:24,000 scale mapping of the area by Rowe (1971). 228 229 The mean direction for each flow at Pueblo Mountains is given in Table 1. To estimate 230 how long the changes in magnetic directions took, we compare the record of the 231 continuous section to a high resolution historical record from Germany (Schnepp and 232 Lanos, 2005). Their record encompasses the last 2600 years from sites with similar 233 latitudes and geographical extent as our study area (Figure 5a). The directions span about 234 30º east-to-west and 15º north-to-south with the whole area traversed in about 2000 years. 235 Smaller loops of the field are also made during the main traverse. The lower resolution 236 record at Pueblo Mountains is comparable (Figure 5b). It makes a little over one large 237 loop with some internal complexity that is suggestive of a small loop. The secular 238 variation behavior of the field is similar to that observed in other high-resolution records 239 (Ohno and Hamano, 1992; Hagstrum and Champion, 2002). Assuming that the 240 geomagnetic field at 16.6 Ma behaved similarly to the modern field, the record suggests 241 that the Pueblo Mountains section erupted in about 2500 years. Also supporting a short 242 eruption duration is the low dispersion of VGPs (14.6°), which is significantly less than 243 the 21.2° estimated for full secular variation during this period of geologic time 244 (McFadden et al., 1991). Thus we conclude that the upper ~250 m of the section of 245 Steens-like lavas at Pueblo Mountains erupted in about 2.5 ka. 246 247 Summit Springs 248 The section at Summit Springs (43.1ºN, 118.3ºW) is 60 km northeast of Steens Mountain 249 at the northern end of the Steens Mountain escarpment (Figure 4, photos Appendix A1.2). 250 It consists of approximately 50 normally magnetized flow-on-flow lavas in a well- 251 exposed 190 m thick section. Many of these Steens Basalts are plagioclase-rich with 252 plate-like crystals up to 3 cm in length. The section is covered at the bottom by the much 253 younger Devine Canyon Tuff, which flowed south out of the Harney Basin over some 254 existing topography (Vic Camp, pers. comm., 2005). Under the tuff, 1 km east of the 255 bottom of the section, a reverse polarity flow is exposed in a road cut adjacent to State 256 Highway 78. This basalt is not Steens-like in appearance and does not contain the large 257 plagioclase crystals found in many Steens basalt flows, setting it apart from the other 258 flows at Summit Springs. Given its uncertain stratigraphic relationship with the main 259 section and its problematic 40Ar/39Ar age determination, this flow could have erupted 260 before or after the Steens reversal. Even with this stratigraphic uncertainty, we include its 261 magnetic direction in the mean pole calculation as it almost certainly erupted within 1 Ma 262 of the Steens reversal. 263 264 Eighteen horizontal flows were sampled, fifteen of which gave directions consistent 265 enough to calculate flow mean directions (Table 1). Flow ss17 is the younger Divine 266 Canyon Tuff and is not discussed further. Comparison of the Summit Springs directional 267 path to that of Steens Mountain is done without correcting for latitude because the 268 geocentric axial dipole (GAD) field inclination differs by less than half a degree between 269 the two sites. This is much less than other errors such as those related to bedding 270 corrections or core orientation. 271 272 The beginning and end of the directional path as recorded at Summit Springs (Figure 273 6a,b) has some similarities to the path at the end of the reversal at Steens Mountain 274 (Figure 6c,d) (Mankinen et al., 1985), but the sense of movement in the middle of the two 275 records is different. The first five field directions (DGs 1-5) from the bottom of the 276 section at Summit Springs span a large angle representing an unknown amount of time. 277 In the upper part of the section (DGs 5-10) a small loop of the field suggests an eruption 278 duration of about 500-1500 years when compared to Holocene records. In conclusion, 279 based on 40Ar/39Ar ages and paleomagnetic arguments, the upper 150 m of lavas at 280 Summit Springs is likely to have erupted over 500-1500 years, possibly immediately after 281 the Steens reversal. 282 283 North Mickey 284 The section at North Mickey (42.8ºN, 118.3ºW) is 25 km east of Steens Mountain at the 285 north end of the Mickey Basin (Figure 4). The section is on a down-dropped block of 286 Steens Basalt as mapped by Hook (1981) and “correlation is established on the basis of a 287 paleomagnetic reversal observed in the two areas, and supported by petrologic 288 observations and chemical analysis.”(Hook, p.2). He found two reverse polarity flows 289 below seven normal polarity flows at Mickey Butte 7.5 km southwest of the North 290 Mickey section. Two 40Ar/39Ar dates from groundmass separates [a reverse lava 16.69 ±± 291 0.18 Ma (16.58), a normal lava 16.59 ±± 0.30 Ma (16.48)] by Brueseke et al. (2007) 292 suggest the reversal at Mickey Butte is the Steens reversal. On inspection the Mickey 293 Butte section has extensive cover between outcropping flows. Only a few flows are 294 exposed in the 60 m section between the reverse polarity flow at 1470 m and the normal 295 polarity flow at 1530 m. Looking for transitional lavas erupted during the Steens reversal, 296 the better exposed flow-on-flow section at North Mickey was drilled. While only normal 297 polarity lavas were found at the North Mickey location, stratigraphic continuity and the 298 Steens-like character (large 2-4 cm plagioclase crystals) of the lower flows suggest that 299 these lavas erupted soon after the Steens reversal. 300 301 The 320 m North Mickey section consists of approximately 35 normal polarity flow-on- 302 flow lavas in a well-exposed section. Every flow of the first 16 from the bottom was 303 sampled for paleomagnetic analysis. Some flows at the top of the section were skipped as 304 we believed to have already sampled through any potential reversal. The last two flows 305 near the top were not Steens-like: aphyrhic, fine grained, and weathering to a reddish 306 brown color. The AF-demagnetization data for all samples from this section were very 307 well-behaved (Fig 2a). Only 8 great circle fits were used from a total of 128 samples and 308 only one sample direction was discarded. Paleomagnetic directions are given in Table 1. 309 310 Once again movement of the magnetic field during the eruption of the section suggests 311 that the flows were erupted over a short period of time. The first 7 directions (DGs 1-7) 312 make one counter-clockwise loop of the magnetic field, which represents an estimated 313 500-1500 years based on modern analogues (Figure 7a). The youngest flows at Steens 314 (Figure 7b) also loop in this way (DGs 10-16), suggesting that the North Mickey flows 315 may have erupted during the same period of time as the uppermost flows found at Steens 316 Mountain. Provided this correlation is correct, the North Mickey section preserves flows 317 younger than the youngest flows found at Steens Mountain. From near the last directions 318 recorded at Steens, the directions at North Mickey move to the northwest (DGs 7-12) 319 (Figure 7c). This could imply about half the previous loop duration of about 750 years. 320 The last four directions (DGs 13-16) record a movement back to slightly east of the GAD 321 field direction before returning to the northwest (Figure 7d). Because this behavior 322 appears less continuous, the eruption rate may have been much lower for this upper part 323 of the section. The number of skipped flows and the change in petrology for the upper 324 two flows precludes estimating the duration of eruption for this part of the section based 325 on secular variation. In conclusion the bottom 17 flows (170 m) at the North Mickey 326 location erupted in about 1000-3000 years and may overlap in time with the end of the 327 Steens record. The next two flows are Steens-like and probably erupted within a few tens 328 of thousands of years after the Steens reversal. The top two flows are not Steens-like and 329 probably erupted within 1 My of the Steens reversal based on mapping by Hook (1981) 330 and lava ages from Brueseke et al. (2007). 331 332 Guano Rim 333 The section at Guano Rim (42.1ºN, 119.5ºW) is 95 km southwest of Steens Mountain in 334 the middle of a 20 km long escarpment. It consists of about 50 flow-on-flow reverse 335 polarity lavas sampled 160 m up a small canyon (Figure 4). These samples were taken 336 much earlier than the other sections, in 1986 and 1988, and their paleomagnetic 337 directions determined at the U.S. Geological Survey (Menlo Park, California). Test 338 samples were progressively AF-demagnetized in peak fields up to 80 mT. Each flow was 339 magnetically cleaned at a peak alternating field chosen on the basis of behavior during 340 the progressive demagnetization experiments (the stable endpoint method) to remove 341 viscous and lightning strike overprints. Directions for each flow are given in Table 1. The 342 samples are very well-behaved with k values for the flows varying from 103 to 1900 and 343 only three flows with k < 200. 344 345 Once again based on secular variation considerations these Steens-like lavas seem to have 346 erupted over a short period of time. The first six directions (DGs 1-6) make one small 347 loop to the west of the expected GAD field direction, suggesting 500-1500 year duration 348 (Figure 8a). Then the field moved to a southwest and shallower direction before returning 349 to another tight group (DGs 8-12) in a similar direction to the first (Figure 8b). This 350 second movement suggests a duration of about 1000-2000 years, so the duration of the 351 eruptions at Guano Rim may be ~3000 years. 352 353 Locality Means, Stability Tests, and Averaging of Secular Variation 354 Table 2 contains mean directions and VGPs for the four localities. Both polarities are 355 well-represented, and the directions pass reversal tests. At the two northern localities the 356 flows are all normal polarity except for one stratigraphically isolated flow (ss18, Table 1) 357 at Summit Springs discussed earlier, whereas at the two southern localities the flows are 358 entirely reverse. The means of the opposite polarity flows differ from antiparallel by 5.4°, 359 well under the critical value of 8.4° for distinguishability at 95% confidence (McFadden 360 and McElhinny, 1990). Because only one-fifth of the flows required tilt correction (the 361 Pueblo Mountains section, dipping only 20°), a strong fold test is precluded, but even so 362 the improvement in clustering upon untilting (k1/k2=1.19) is significant at 76% 363 confidence. In light of these stability tests and the straightforward behavior of the great 364 majority of samples during progressive demagnetization, these lava flows have almost 365 certainly preserved reliable directions of the geomagnetic field at the times they cooled. 366 367 Figure 9 shows the grouped flow directions that constitute the means in Table 2 for the 368 four new localities and also Steens Mountain. For reverse directions the antipodes are 369 plotted and all the directions have been rotated so that the mean of the entire distribution 370 is at the center of the equal area projection. Although secular variation is not well 371 averaged at any one of the four localities, due to rapid eruption rates, a compilation of all 372 four sections should do a much better job. The total eruptive time for the continuous parts 373 of the four sections is probably 6-10 ka, distributed on both sides of a polarity transition 374 estimated to have taken 4400 900 years (Mankinen et al., 1985). In addition, directions 375 are included from the nine flows that are not demonstrably part of the ‘continuously’ 376 emplaced sections, but for which age and polarity indicate that they were erupted within a 377 million years of the transition, most of them probably much closer. The shape of the 378 distribution, which does not depart greatly from circular symmetry, resembles that 379 expected for the time-averaged field at the latitude (43°N) of Steens Mountain (e.g., 380 Tauxe and Kent, 2004, Fig. 5). This is true for our four new localities combined, for the 381 Steens Mountain locality itself, and for all of them together (Figure 9). Moreover, the 382 angular dispersions of VGPs for all three data sets (Table 2) agree well with the expected 383 range of 20.0-22.6° from analyses of 5-22.5 Ma global lava-flow data (McFadden et al., 384 1991). 385 386 These VGPs, corresponding to the directions in Figure 9, are plotted in Figure 10. Note 387 that the transformation to VGPs maps the approximately circular distribution of 388 directions into a distribution that is distinctly elongated. Although differing amounts of 389 tectonic rotation about a vertical axis could also produce elongation in this same 390 orientation, the agreement with expected shape and amount of secular variation of 391 directions described above suggests that little or no such movement has occurred between 392 the localities. Even stronger testimony against substantial differential tectonic rotation is 393 the comparable elongation in VGP distribution of the pre- and post-transitional flows of 394 Steens Mountain itself (Figure 10), which are from a single structural block. In 395 conclusion, all evidence indicates that the distribution of directions and associated VGPs 396 provides a representative time-average of middle Miocene secular variation sufficient to 397 yield a good estimate of the geocentric axial dipole field for the region. 398 399 Mid-Miocene Pole and Rotation of the Oregon Plateau 400 Our new data from the four localities invite a reexamination of the question whether the 401 Oregon Plateau has rotated relative to cratonic North America. The mean paleomagnetic 402 pole for our 50 directional groups and the 26 non-transitional directional groups at Steens 403 Mountain defines a high-quality paleomagnetic pole (Table 2) that represents a large 404 portion of the central Oregon Plateau (Figure 1). Omitted are several much older, smaller 405 scale studies that likely were not performed to the same standards. This Oregon Plateau 406 paleomagnetic pole is 5.1° from the High Plains pole used by Mankinen et al. (1987), 407 which consists almost entirely of VGPs from Steens Mountain and is very close to the 408 Steens pole in Table 2. Those authors also compiled results from studies published in the 409 nineteen sixties and seventies for 59 presumably unrotated flows of the Columbia River 410 Basalt Group (CRBG pole in Table 2). These flows are on average only one-million years 411 younger than the Steens Basalt and lie farther north in Washington and northernmost 412 Oregon. The CRBG and High Plains poles are almost identical, and so they concluded 413 that no significant rotation (0.4° 7.6°) occurred between the south-central Oregon 414 Plateau and the CRBG block of southeast Washington since mid-Miocene time. Our new 415 Oregon Plateau pole, however, implies clockwise rotation of 7.5° 5.9° relative to the 416 CRBG. 417 418 In addition, the paleomagnetic pole for the CRBG block might not be strictly 419 representative for the North American craton. There is a paucity of other useful data of 420 appropriate age from North America itself, but by reconstructing the relative positions of 421 the plates using sea-floor magnetic anomalies, mid-Miocene data from other continents 422 become available. Using this method, Besse and Courtillot (2002) provide a 15 Ma 423 synthetic pole for the North American plate (Table 2). Relative to it the Oregon Plateau 424 pole is rotated 14.5° 5.4° clockwise. 425 426 These new estimates for Oregon Plateau rotation reopen an early suggestion by Magill 427 and Cox (1980 and 1981) that south-central Oregon rotated about 10° clockwise relative 428 to southeast Washington since 20 Ma because of E-W extension of the Basin-and-Range 429 that decreases to zero northward. The High Plains result of Mankinen et al. (1987) 430 appeared to rule out that hypothesis. Nonetheless, several later studies revived the idea of 431 a Basin-and-Range-extension contribution to clockwise rotation of the Oregon Coast 432 Range and pushed the boundary of the rotated block to western Oregon so as to respect 433 the conclusion that Steens Mountain had not rotated (e.g., Wells and Heller, 1988). Our 434 new pole for the Oregon Plateau, however, indicates 7.5 degrees clockwise rotation 435 relative to the CRBG pole of southeast Washington and 14.5 degrees relative to the 436 synthetic pole for North America. It is derived from almost three times the number of 437 directional groups, including those for Steens Mountain, and represents a much larger 438 area of the Oregon Plateau. Northward decreasing Basin-and-Range extension still 439 appears to be the most likely mechanism for explaining such clockwise rotation. The 440 opening of the Oregon-Idaho graben is one well-studied example, its extension dated 441 between 15.3 Ma and 10.5 Ma and dying out to the north in central Oregon (Cummings et 442 al., 2000). 443 40K 444 Decay Constant and FCs Age Discussion 445 The conventional age of the Fish Canyon sanidine (FCs) agreed upon by the Earthtime 446 community is 28.02 ± 0.28 Ma (1σ as per the uncertainty convention used in this paper, 447 including the uncertainty in the decay constant; Renne et al, 1998). A more precise age 448 for the FCs (28.201 ±± 0.046 Ma, decay constant uncertainties included) has been 449 determined by intercalibration with the astronomical timescale (Kuiper et al., 2008). The 450 determination of this age is insensitive to the 40K decay constant value and any more 451 accurate age of the FCs determined in the future is unlikely to fall outside of the above 452 uncertainties. Other uncertainties in determining an 40Ar/39Ar age are now likely to 453 dominate. This FCs age is also in close agreement with an independent determination of 454 the FCs age of 28.28 ±± 0.06 Ma (Mundil et al., 2006) by intercalibration with the U/Pb 455 dating system. 456 457 The conventional 40K decay constant value of 5.543 × 10-10/a (sum of λβ- and λЕ ) stated 458 in Steiger and Jager, (1977) is from Beckinsale and Gale (1969) with a 40K half-life(T1/2) 459 of 1.265 ±95 0.0020 for “young” ages ( Beckinsale and Gale state “.. the error in T as a 460 result of errors in λЕ and λβ- is never greater than about ± 1.6% at the 95% confidence 461 level.”) adjusted for 40K abundance in Garner et al., (1976). Using the 1.6% uncertainty, 462 we get a decay constant of 5.543 ±95 0.089 × 10-10/a. This decay constant was updated to 463 5.463 ±± 0.107 × 10-10/a by Min et al., (2000) using new values for various physical 464 constants and a statistically rigorous analysis of the underlying activity data. This 40K 465 decay constant has much higher uncertainties than the reproducibility afforded by current 466 analytical techniques and methods. Motivated in part by the geochronological 467 community, two experiments to directly measure the 40K half-life by liquid scintillation 468 counting (LSC) techniques give T1/2= 1.248 ±95 0.004 × 109 a (Malonda and Carles, 469 2002) and T1/2= 1.248 ±95 0.003 × 109 a (Kossert and Gunther, 2004). Converting these 470 half-lives to decay constants and taking the weighted mean (although the two 471 experiments have some correlated error), we calculate a 40K decay constant of 5.5541 ±± 472 0.010 × 10-10/a. This value is in agreement with the geologically determined value of 473 5.530 ±± (7%) × 10-10/a (Mundil et al., 2006). 474 475 Nominal ages in this study were determined using 28.02 Ma (Renne et al., 1998) for FCs 476 and the Steiger and Jager (1977) decay constant. A more accurate representation of our 477 results, we believe, is given by the astronomically-calibrated age of Kuiper et al. (2008) 478 for FCs and the Steiger and Jager updated by Min et al., (2000) value for the 40K decay 479 constant. These preferred ages are most appropriate for comparison with the GTS2004 480 time scale, as discussed below. For a summary of the ages using different 40K decay 481 constants and FCs ages, see Table 3. See Appendix A2 for additional plateau and 482 isochron plots (A2.1-3), an isotopic data summary table (A2.4), an age adjustment 483 calculation spreadsheet (A2.5), and a spreadsheet with extended isotopic data and plots 484 (A2.6). 485 40Ar/39Ar 486 Results 487 Summit Springs 488 The second lava flow from the top of the section (ss02, Figure 4) has a normal polarity 489 and an 40Ar/39Ar plateau age of 16.72 ±± 0.28 Ma (16.61) from a plagioclase separate 490 (Figure 11a). The 15-step plateau encompasses all of the degassing steps and is well- 491 behaved. Inverse isochron analyses of Summit Springs lavas give ages that generally 492 agree with the plateau ages and have atmospheric 36Ar/40Ar ratios (Figure 11b). Our 493 determination of the age of the lava from flow ss09 was less straightforward. Plagioclase 494 separates of two different size fractions from the same sample were dated (Figure 11c,d). 495 The smaller size fraction (63-180 μm) was analyzed first because smaller grains generally 496 have higher potassium and lower calcium concentrations and therefore lower age 497 uncertainties. A single degassing analysis gave two plateau ages with the criteria 498 described in the “40Ar/39Ar Geochronology Procedures” section. A younger plateau 499 consisting of the last six degassing steps gave an age of 17.14 ±± 0.36 Ma (17.03) while 500 an older plateau consisting of the first eight degassing steps gives an age of 17.39 ±± 0.38 501 Ma (17.28). The younger age plateau has more radiogenic gas released, smaller 502 uncertainties, and higher probability so we choose it as the age of this degassing analysis. 503 The age was older than expected, given its normal polarity and Steens-like appearance, so 504 the larger size fraction (180-300 μm) was analyzed (Figure 11d). This analysis again gave 505 a good plateau age [16.71 ±± 0.38 Ma (16.60)]. The larger uncertainty in the Ca/K ratio is 506 due mostly to the larger uncertainties in the 37Ar (half life 35.0 days) abundances because 507 this analysis was performed nine months after the smaller size fraction. This age is 0.43 508 Ma younger than the previous age but their 2σ errors overlap by 0.31 Ma. While we 509 suspect that the plateau age of the larger size fraction is more likely correct, the weighted 510 mean of the two ages [16.92 ±± 0.26 Ma (16.83)] is the most objective 40Ar/39Ar age for 511 flow ss09 although using a weighted mean may underestimate the uncertainty. 512 513 Given the issues described above we also analyzed some groundmass separates from this 514 flow. The generally lower Ca/K of groundmass separates allows for greater precision on 515 each heating step, but often alteration and/or recoil effects can prevent good plateaus 516 from being produced. Two groundmass step-heating analyses yielded disturbed spectra 517 likely due to recoil effects. In both cases (one spectrum shown in Figure 11e) the step 518 ages start low and increase to a maximum at about 1/3 of the 39Ar released and then 519 slowly decrease in age. When only groundmass samples are available and the age spectra 520 are disturbed, the total gas integrated age may define a valid eruption age, provided that 521 alteration is insignificant and recoil effects are limited to argon isotope redistribution 522 within, rather than net loss from, the sample. Our integrated ages for two groundmass 523 analyses are 16.63 ±± 0.16(2σ) (16.52) Ma and 16.68 ±± 0.16 Ma (16.57). These ages are 524 consistent with the weighted mean of the two plagioclase separate ages but, given our 525 inability to verify the abovementioned criteria for validity, we do not include the ages in 526 the weighted mean age of the lava. 527 528 Two other eruptive units from the Summit Springs section were also dated. The first is 529 the Devine Canyon Tuff (V. Camp, pers. comm., 2005), which covers the flat area at the 530 bottom of the section (ss17, Figure 4). Ages of ten single-crystal sanidine grains were 531 determined by step-heating (Figure 11h) and have a weighted mean age of 9.781 ±± 532 0.022 Ma (9.718) that is much younger than the Steens lavas. These very precise ages fall 533 into two groups (Figure 5i,j,k) with ages of 9.756 ±± 0.020 Ma (9.693) and 9.810 ±± 534 0.022 Ma (9.747), suggesting an eruption age for the Devine Canyon Tuff of 9.756 ±± 535 0.020 Ma (9.693) and xenocrystic contamination of the tuff with a population of crystals 536 only 54 ka older. The second is from a basaltic lava of reverse polarity about 1 km east of 537 the main section (ss18, Figure 4). Age determinations from a plagioclase separate were 538 inconclusive (not shown), and a groundmass age spectrum is disturbed with an integrated 539 age of 17.3 ±± 0.6 Ma (17.2) (Figure 11f). Its isochron age is better defined at 16.16 ±± 540 0.16 Ma (16.06) (Figure 11g). Summarizing the most pertinent points of the Summit 541 Spring ages, the two lavas dated in the upper section erupted near the 16.6 Ma Steens 542 reversal while the more isolated reverse polarity lava erupted within 1 My of the Steens 543 reversal. 544 545 Pueblo Mountains 546 An 40Ar/39Ar age of 16.72 ±± 0.21 Ma (16.61) was determined from a plagioclase 547 separate of the reverse polarity flow pm10 (Figure 12a). As found at Summit Springs, this 548 age is indistinguishable from that of the 16.6 Ma Steens reversal. The dated sample lies 549 stratigraphically below the continuous section. The age of the section is also constrained 550 by a 16.511 ± 0.042 Ma (16.404) age from the weighted mean of ten step-heated sanidine 551 grains from a reverse polarity rhyolite located at the top of the section (Figure 12b). 552 553 554 Comparing Ages to the Geomagnetic Polarity Timescale 555 The boundaries for geomagnetic polarity chrons for much of the Neogene have been 556 determined from the astronomical tuning of deep-sea ocean cores that have magnetic 557 signatures. These studies have been compiled into a composite geomagnetic polarity time 558 scale (GPTS) in Gradstein et al. (2004). For Neogene times before the C5Ar.3r chron 559 (12.878 Ma) the chron boundaries of Gradstein et al. (2004) were determined using a 560 seafloor-spreading-rate history model of the Australia-Antarctic plate pair with 561 astronomically tuned tie points at the top of C5Ar.3r from Abdul-Aziz et al. (2003), the 562 top and bottom of C5Br from Shackleton et al. (2001), and a recalculated 23.03 Ma 563 Oligocene-Miocene boundary from Shackleton et al. (2000) using the La2003 orbital 564 model. A potentially better GPTS for the Early and Mid-Miocene is was determined by 565 Billups et al. (2004) from orbitally-tuned Ocean Drilling Program (ODP) Site 1090 cores 566 that have a magnetic signature. Their study should give more accurate astronomical time 567 boundaries to Early Neogene chrons, but the chrons relevant for this study are at the very 568 top of the cores and have low sedimentation rates. Both of these factors tend to make the 569 chron boundaries less reliable and we choose to compare to the Gradstein et al. (2004) 570 GPTS (Figure 13), which generally agrees with Billups et al. (2004) to one precession 571 cycle (~20 ka). 572 The younger normal polarity lava at Summit Springs (ss02) likely erupted in the C5Cn.3n 573 chron after the Steens reversal. Its errors (at two sigma confidence) encompass all of the 574 C5Cn.3n normal chron, reaches 1/3 into the younger C5Cn.2n normal chron, and does 575 not reach the older C5Dn normal chron (Figure 13). The two sigma errors of the weighted 576 mean 40Ar/39Ar age for the normal polarity lava ss09 encompass most of the reversed 577 C5Cr chron and one third of the of the normal C5Cn.3n chron. Barring any unknown 578 normal cryptochron during the reverse C5Cr chron and considering the younger 579 groundmass integrated ages, the lava is most likely to have erupted in the C5Cn.3n chron 580 after the Steens reversal. This interpretation is also supported by the similarities between 581 the Summit Springs magnetic field path and Steens Mountain post-reversal magnetic 582 field path. At Pueblo Mountains the reverse polarity flow pm10 likely erupted during the 583 C5Cr chron before the Steens reversal, although the two sigma errors of the 40Ar/39Ar age 584 reach into the short C5Cn.2r after the Steens reversal. The younger and more precise age 585 of the reverse polarity capping rhyolite (pma) at Pueblo Mountains unequivocally places 586 its eruption during the C5Cn.2r chron, indicating that no eruptions took place at this 587 section during the 170 ka-long C5Cn.3n (Gradstein et al., 2004) normal polarity chron. 588 589 Conclusions 590 Paleomagnetic analyses and 40Ar/39Ar ages from Pueblo Mountains, Summit Springs, 591 North Mickey, and Guano Rim suggest that the bulk of these sections were erupted in 592 short bursts (~1-3 ka) within ~300 ka of the Steens reversal. Comparison to the 593 geomagnetic polarity time scale (Figure 7) and two 40Ar/39Ar ages (Table 3) show that the 594 Pueblo Mountains reverse section erupted near and likely before the Steens reversal. 595 Comparing the simple directional path of the remanent magnetization with secular 596 variation of the recent field indicates that the continuously sampled section erupted in 597 about 2.5 ka. At Summit Springs two 40Ar/39Ar ages, dominantly normal polarity (all but 598 one stratigraphically isolated flow), and the simple directional path suggest that the 599 section erupted in the chron after the Steens reversal within about 0.5 to 1.5 ka. At North 600 Mickey geologic mapping and dates by others place the section near the Steens reversal, 601 and secular variation analysis indicates that the lower part erupted in 1-3 ka. At Guano 602 Rim the low (14.1°) dispersion of VGPs and the directional path suggest a ~3 ka eruption 603 duration. The rapid eruption of these sizeable sections near the time of the Steens reversal 604 suggests that the Steens Basalts were all emplaced within a few hundred thousand years 605 on the Oregon Plateau at around 16.6 Ma. 606 607 Although the flows at each individual locality do not average out secular variation, by 608 combining all of the sections enough time is sampled to obtain a meaningful average 609 paleomagnetic pole. From our four sections there are a total 26 normal and 24 reverse 610 directions (Table 2) that yield a positive reversal test. Combining our VGP directions 611 with the non-transitional VGPs at Steens Mountain yields a new pole for the Oregon 612 Plateau that indicates clockwise rotation of 7.4° 5.9° with respect to the CRBG and 613 14.4° 5.4° with respect to cratonic North America. This implies some extension to the 614 east of the study area since 16.6 Ma that dies out rapidly to the north. 615 616 617 Acknowledgements 618 We would like to extend special thanks to Kim Knight for assistance with 40Ar/39Ar 619 sample preparation and analysis methods and Chris Pluhar for assistance with 620 paleomagnetic procedures and methods. Laurie Brown, Andy Calvert, Jim Gill, 621 Johnathan Hagstrum, Peter Hooper, and Brad Singer provided helpful reviews which 622 improved the clarity of this paper. We thank Eli Morris and Walter Schillinger for UCSC 623 paleomagnetic instrumentation and software support, Tim Becker for BGC lab support, 624 and Fred Jourdan for assistance with determining plagioclase alteration. For highly 625 competent field work assistance we would like to thank Mike Dueck, Bijan Hatami, Peter 626 Lippert, and Andy Daniels. 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