Agilent GC/MSD ChemStation and Instrument Operation

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User
Information Plan Template
Document Information:
Filename
FILENAME \* MERGEFORMAT USERINFO.DOC
Current Owner Deborah
Perkins Product Identifier H4043A Project Identifier Customer Training
Course Update to G1701DA E.01.00 Current Lifecycle Phase Release
Revision Log:
Revision Date Reason For Update A.00 22 Mar 02 Initial
revision. B.00 24 June 02 Added additional details C.00 1 Dec
04 Updated material to software revision G1701DA D.01.02 D.02 1 Sep
05 Updated material to software revision G1701DA D.02.00 D.03 29 Jun
06 Updated material to software revision G1701DA D.03.00 E.01 1 June
07 Updated material to software revision G1701EA E.01.00 and added 7890GC
and 5975MS information
Changes from G1701DA D.03 to G1701EA E.01
Changes to H4043A:
General
* Screenshots and descriptions updated has needed
* Changed file (ppt & doc) naming convention for clarity
MS Basics and Hardware Configuration
* Updated hardware/software configuration panel for G1701EA E.01 changes
MS Tuning
* Added gain normalized tune
Data Acquisition Theory
* Added EM Saver
* Added Synchronous SIM/Scan
* Added High performance SIM/Scan
* Added Trace Ion Detection
* Added Hydrogen carrier gas
Setting Up Data Acquisition
* Added screenshots of panels for 7890 GC setup
* Added eMethods
Lab: Scan Data Acquisition
* Calculating Solvent Expansion exercise added
Maintenance
* Added QuickSwap
* Added QuickSwap Backflush
* Added Analyzer Baking
* Added Lab Monitor and Diagnostic (LMD) Software
Qualitative Data Analysis
* Added information about setup of toolbar icons
Quantitative Data Analysis
* Changed to reflect new Edit Compounds panel
Quantitative Data Analysis Labs
* Changed to reflect new Edit Compounds panel
Appendix
* Removed.
Students didn’t use it.
Product Delivery Requirements 1. Course Description:
This course is designed for those who want to enhance their skills in the
use of an Agilent GC/MSD and ChemStation. If you are using EnviroQuant
software, refer to H4050A or H4053A. 2. Course Outline with correlation
to file names:
NOTE: all files are available from the CAG EPI Warehouse at
http://whadmin.cos.agilent.com/
MS Basics and Hardware Configuration………………………….01_basics.ppt &
01_basics.doc
LAB EXERCISE: MSD Instrument Configuration…………………………….01_basicsLab.doc
MS Tuning………………………………………………….……..02_tuning.ppt & 02_tuning.doc
LAB EXERCISE: Tuning the MSD……………… …………..………………..02_tuningLab.doc
Data Acquisition Theory……….03a_dataacquisitiontheory.ppt &
03a_dataacquisitiontheory.doc
Data Acquisition Setup ……… …03b_dataacquisitionsetup.ppt &
03b_dataacquisitionsetup.doc
LAB EXERCISE: Linear Velocity……………….……………………………………Lab03a.doc
LAB EXERCISE: Scan Data Acquisition………………….………………………….Lab03b.doc
LAB EXERCISE: SIM Experiment……………………….……….…………….…….Lab03c.doc
LAB EXERCISE: SIM…………………………………….………………….……….Lab03d.doc
Maintenance………………………………………….04_maintenance.ppt & 04_maintenance.doc
Qualitative Data Analysis………………………………..05_qualitative.ppt &
05_qualitative.doc
LAB EXERCISE: Qualitative Data Analysis……………………… ………05_qualitativelab.doc
Quantitative Data Analysis………………………..…..06_quantitative.ppt &
06_quantitative.doc
LAB EXERCISE: Quantitation of SIM Data………………………………06_quantativelab1.doc
LAB EXERCISE: Quantitation of Scan Data………………………………06_quantativelab2.doc
Custom Reports and Databases…………………………….……07_reports.ppt & 07_reports.doc
LAB EXERCISE: Custom Reports……………………………………………...07_reportslab.doc
Commands and Macros……………………………….…08_commands.ppt & 08_commands.doc
LAB EXERCISE: RPN…………………………………………….……...08_commandslab1.doc
Introduction to Macro Writing……………………………………….Chap07b.ppt & Mod07b.doc
LAB EXERCISE: Macros………………………………………………....08_commandslab2.doc
Sequencing, Secured Control, and RTL...………………09_sequencing.ppt &
09_sequencing.doc
LAB EXERCISE: Sequencing, Secured Control, and
RTL………………...09_sequencinglab.doc
Complete Manual Volume 1………………………………………………………h4043a vol1.doc
Complete Manual Volume 2………………………………………………………h4043a vol2.doc
Additional data files……………………..…………………………………………….datafiles.exe
Sequencing CSV file…………………………………………………………………Sequence.csv 3. For
marketing purposes of this product see the Product Release Bulletin (if
available):
Product Release Bulletin available? No 4. Instructor or Delivery Agent
skills required to deliver the product:
A fundamental knowledge of the WinXP operating system.
A detailed knowledge of the current Agilent GC/MS operating software.
Detailed knowledge of the specific MS tune parameters and their influence
on the acquired data.
Detailed knowledge of the specific MS scan acquisition parameters and
their influence on the acquired data.
Detailed knowledge of the specific MS selected ion monitoring (SIM)
acquisition parameters and their influence on the acquired data.
Detailed knowledge of the PBM library search and Parametric Retrieval
utilities.
Detailed knowledge of the quantitation software and the influence of the
various quantitation parameters.
A fundamental knowledge of RPN commands and macro programming as related
to the current Agilent operating software. 5. Equipment (Instrumentation
and Software) Required for product delivery
Agilent 6890/5973N GC-MSD and/or Agilent 7890/5975 inert GC-MSD
PC with WinXP operating system
G1701EA E.01.00 software
NIST and NBS spectral libraries 6. Consumables required
GC septa
10ul syringe or ALS syringe
30meter HP5MS cap column 7. Samples required
Agilent GC-MSD Performance Evaluation Sample (part # 05970-60045) 8.
Electronic Files required
All additional data files are downloadable from the data warehouse. When
you unzip files, set it for the root folder (C:\ or D:\) with the "user
folder names" option. This will place all method and data files in the
location used in the manual.
“Sequence.csv” file (downloadable from the data warehouse) will need to
be placed in the "MSDchem\1\sequence" folder 9. Tools required
MSD Tool Kit (part # 05971-60561) 10. Activities required prior to
product delivery
Delete files created by previous class 11. Activities required during
product delivery
N/A 12. Activities required after product delivery
Delete files created by previous class
User Task Analysis
The user wants to know about and how to use the new hardware and software
feature(s) added with this version of the GC-MSD software.
Audience Analysis
GC-MSD education levels range from high school grad to Ph.D with the
typical user being a college grad. Experience levels range from no
experience to several years with the typical user experience about 3 – 5
years.
Most students require detailed step-by-step lab instructions.
Software differences between 7890A versus 6890/6850 Series with the MSD
ChemStation
Situation:
With the introduction of the 7890A GC and the updated G1701EA MSD
Productivity ChemStation software there are differences between G1701DA
to G1701EA on howthe MSD ChemStation operates and there are differences
between the 7890A versusthe 6890/6850 modes of operation.
Solution/Action:
Areas which are different:
1 - Stopping a sequence via the GC or ChemStation is different
between the 7890A and 6890/6850
2 - Can not override GC not-ready with the 7890
3 - Oven Post Run time is not counting for 7890
4 - Can not input GC set-points from the 7890A keyboard with the
ChemStation software is running.
5 - Updating the 7890A firmware is causing the method corruption
problems(invalid parameters).
6 - 7890 does not support RTL methods created in constant flow mode
7 - 6890 can acquire 2 GC signals while the 7890A can acquire 4 GC
signals
8 - Update 7890A config via a right mouse key and update is possible,
not on a 6890
9 - Differences between the GCs, hardware
10 - Differences between the GCs, software control
1 - Stopping a sequence via the GC or ChemStation is different between
the 7890A and 6890/6850 Examined the behavior of a 6890 on
D.03.00 SP1 with respect to “runs” and sequences of “runs”.
For a 6890 GC
A) If a system is in a “run” (i.e., post injection) and the user hits
the ChemStation STOP sign or the GC’s STOP button, the “run” stops, the
data is processed, and the sequence continues without any further
interaction from the customer.
B) If a system is in “prerun” (i.e., pre injection) and the user hits
the ChemStation STOP sign or the GC’s STOP button, the system aborts the
run, no data processing can occur and the sequence is paused.
C) If a system encounters a critical “prerun” error (missing vial),
the run is aborted and the sequence is paused.
D) The ChemStation provides a PAUSE button to permit the user to pause
a sequence.
A quick summary will be
STOP prior to injection means ABORT the run and the sequence
STOP post injection means Stop-the-run and Continue-the-sequence
Fatal hardware errors (front inlet shutdown, no emission current)
the prevent the hardware from performing a run means ABORT.
For a 7890A GC
A) If a system is in a “run” (i.e., post injection) and the user hits
the ChemStation STOP sign or the GC’sSTOP button, the system aborts the
run,
no data processing can occur and the sequence is paused.
B) If a system is in “prerun” (i.e., pre injection) and the user hits
the ChemStation STOP sign or the GC’sSTOP button, the system aborts the
run, no data processing can occur and the sequence is paused.
C) If a system encounters a critical “prerun” error (missing vial),
the run is aborted and the sequence ispaused.
D) The ChemStation provides a PAUSE button to permit the user to pause
a sequence.
Or in other words,
STOP prior to injection means ABORT the run and the sequence
STOP post injection means ABORT the run and the sequence
Fatal hardware errors (front inlet shutdown, no emission current)
to prevent the hardware from performinga run means ABORT.
2 - Can not override GC not-ready with the 7890
The ability to Override Waiting for Ready on the 7890A GC is not
possible, but it is available for the 6890GC.
The ALS subsystem in the 7890 does not support overriding readiness to
do the injection at this time. Itwill wait indefinitely in the "ready to
inject" position (syringes in the vials) until the instrument goes
ready,and then proceed.
3 - Oven Post Run time is not counting for 7890
Create and run a 7890 method that has an oven post-run time set. The
Post Run Time display remains at 0.00 throughout the time, though the
status shows 'postrun'.
4 - Can not input GC set-points from the 7890A keyboard with the
Chemstation SW running.
While the ChemStation is running (acquiring data), the user can not
input GC set-points for the 7890A GC; this is possible for the 6890.
5 - Updating the 7890A firmware is causing the method corruption problems
(invalid parameters).
The problem is related to the flashing of the firmware to the 7890A
GC. The RAM is missing information on what should be backed up in ram
and flash when the firmware is being updated.
6 - 7890A does not support RTL methods created in constant flow mode
The 7890 method can specify FLOW or PRESSURE as the flow control mode.
If FLOW is used,
the Retention Time Locking feature is inoperative.
The RECOMMENDED mode of operation is and always has been CONSTANT
PRESSURE mode due to it’s more precise control (i.e. any pressure
programming upsets the dynamics of the retention time locking
calibration. Constant flow IS a pressure program)
The physics and application of RTL dictate that constant PRESSURE
should be used. In constant FLOW mode, RTL calibrations are less linear
and the ability to relock over a wide range of pressures is lessened.
7 - 6890 can acquire 2 GC signals while the 7890A can acquire 4 GC
signals
The 6890 can acquire 2 GC signals in GCMS and in GC only modes.
There is a limitation of 3 signals maximum which can be viewed in data
analysis (maximum of 2 GC signals).
The 7890A can acquire 4 GC signals while in the GCMS mode, but only 2
GC signals while in the GC mode. There is a limitation of 3 signals
maximum of which a maximum of 2 GC signals.
8 - Update 7890A config via a right mouse key and update is possible, not
on a 6890
With the new drivers for the 7890A it is now possible to download or
upload GC parameters while in the edit parameters screen.
Use the right
mouse button in a clear section of the edit parameters screen and you
will be able to download or upload parameters.
Agilent Technologies
For Internal Use Only
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<xsd:enumeration value="ANTIGUA AND BARBUDA"/>
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<xsd:enumeration value="BOSNIA-HERCEGOVINA"/>
<xsd:enumeration value="BOTSWANA"/>
<xsd:enumeration value="BOUVET ISLAND"/>
<xsd:enumeration value="BRAZIL"/>
<xsd:enumeration value="BRITISH INDIAN OCEAN TERRITORY"/>
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value="BURUNDI"/>
value="CAMBODIA"/>
value="CAMEROON"/>
value="CANADA"/>
value="CAPE VERDE ISLANDS"/>
value="CAYMAN ISLANDS"/>
value="CENTRAL AFRICAN REPUBLIC"/>
value="CHAD"/>
value="CHILE"/>
value="CHINA"/>
value="CHRISTMAS ISLAND"/>
value="COCOS (KEELING) ISLANDS"/>
value="COLOMBIA"/>
value="COMOROS"/>
value="CONGO"/>
value="COOK ISLANDS"/>
value="COSTA RICA"/>
value="COTE D`IVOIRE"/>
value="CROATIA"/>
value="CYPRUS"/>
value="CZECH REPUBLIC"/>
value="DENMARK"/>
value="DJIBOUTI"/>
value="DOMINICA"/>
value="DOMINICAN REPUBLIC"/>
value="EAST TIMOR"/>
value="ECUADOR"/>
value="EGYPT"/>
value="EL SALVADOR"/>
value="EQUATORIAL GUINEA"/>
value="ERITREA"/>
value="ESTONIA"/>
value="ETHIOPIA"/>
value="FALKLAND/MALVINAS"/>
value="FAROE ISLANDS"/>
value="FED. STATES OF MICRONESIA"/>
value="FIJI"/>
value="FINLAND"/>
value="FRANCE"/>
value="FRENCH GUIANA"/>
value="FRENCH POLYNESIA"/>
value="FRENCH SOUTHERN TERRITORIES"/>
value="GABON"/>
value="GAMBIA"/>
value="GEORGIA"/>
value="GERMANY"/>
value="GHANA"/>
value="GIBRALTAR"/>
value="GREECE"/>
value="GREENLAND"/>
value="GRENADA"/>
value="GUADELOUPE"/>
value="GUAM"/>
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value="GUINEA"/>
value="GUINEA-BISSAU"/>
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value="HAITI"/>
value="HEARD AND MCDONALD ISLANDS"/>
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value="HONG KONG"/>
value="HUNGARY"/>
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value="INDIA"/>
value="INDONESIA"/>
value="IRAQ"/>
value="IRELAND"/>
value="ISRAEL"/>
value="ITALY"/>
value="JAMAICA"/>
value="JAPAN"/>
value="JORDAN"/>
value="KAZAKHSTAN"/>
value="KENYA"/>
value="KIRIBATI"/>
value="KUWAIT"/>
value="KYRGYZSTAN"/>
value="LAOS"/>
value="LATVIA"/>
value="LEBANON"/>
value="LESOTHO"/>
value="LIBERIA"/>
value="LIECHTENSTEIN"/>
value="LITHUANIA"/>
value="LUXEMBOURG"/>
value="MACAO"/>
value="MACEDONIA"/>
value="MADAGASCAR"/>
value="MALAWI"/>
value="MALAYSIA"/>
value="MALDIVES"/>
value="MALI"/>
value="MALTA"/>
value="MARSHALL ISLANDS"/>
value="MARTINIQUE"/>
value="MAURITANIA"/>
value="MAURITIUS"/>
value="MAYOTTE"/>
value="MEXICO"/>
value="MOLDOVA"/>
value="MONACO"/>
value="MONGOLIA"/>
value="MONTENEGRO AND SERBIA"/>
value="MONTSERRAT"/>
value="MOROCCO"/>
value="MOZAMBIQUE"/>
value="MYANMAR"/>
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value="NAMIBIA"/>
value="NAURU"/>
value="NEPAL"/>
value="NETHERLANDS"/>
value="NETHERLANDS ANTILLES"/>
value="NEW CALEDONIA"/>
value="NEW ZEALAND"/>
value="NICARAGUA"/>
value="NIGER"/>
value="NIGERIA"/>
value="NIUE"/>
value="NORFOLK ISLAND"/>
value="NORTHERN MARIANA ISLANDS"/>
value="NORWAY"/>
value="OMAN"/>
value="PAKISTAN"/>
value="PALAU"/>
value="PANAMA"/>
value="PAPUA NEW GUINEA"/>
value="PARAGUAY"/>
value="PERU"/>
value="PHILIPPINES"/>
value="PITCAIRN ISLANDS"/>
value="POLAND"/>
value="PORTUGAL"/>
value="PUERTO RICO"/>
value="QATAR"/>
value="REUNION"/>
value="ROMANIA"/>
value="RUSSIA"/>
value="RWANDA"/>
value="SAN MARINO"/>
value="SAO TOME AND PRINCIPE"/>
value="SAUDI ARABIA"/>
value="SENEGAL"/>
value="SERBIA"/>
value="SEYCHELLES"/>
value="SIERRA LEONE"/>
value="SINGAPORE"/>
value="SLOVAK REPUBLIC"/>
value="SLOVENIA"/>
value="SOLOMON ISLANDS"/>
value="SOMALIA"/>
value="SOUTH AFRICA"/>
value="SOUTH KOREA"/>
value="SPAIN"/>
value="SRI LANKA"/>
value="ST. HELENA"/>
value="ST. KITTS AND NEVIS"/>
value="ST. LUCIA"/>
value="ST. PIERRE AND MIQUELON"/>
value="ST. VINCENT AND THE GRENADINES"/>
value="SURINAME"/>
value="SVALBARD AND JAN MAYEN ISLANDS"/>
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<xsd:enumeration value="CAG Miscellaneous Program Activities"/>
<xsd:enumeration value="Data Systems"/>
<xsd:enumeration value="Gas Phase Plus"/>
<xsd:enumeration value="GC Columns"/>
<xsd:enumeration value="ICP-MS"/>
<xsd:enumeration value="IIM Professional Services Organization"/>
<xsd:enumeration value="Informatics"/>
<xsd:enumeration value="J&W Products"/>
<xsd:enumeration value="Lab-on-a-Chip Products"/>
<xsd:enumeration value="LC Columns"/>
<xsd:enumeration value="Liquid Phase Analysis"/>
<xsd:enumeration value="Mass Spectrometry/Sequencers"/>
<xsd:enumeration value="Proprietary Instrument Supplies"/>
<xsd:enumeration value="Support Services"/>
<xsd:enumeration value="Versatest"/>
<xsd:enumeration value="Zorbax Columns"/>
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<xsd:element name="ProductGroup" ma:index="24" nillable="true"
ma:displayName="Product Group" ma:description="Select only the Product
Group that is the primary focus of this publication." ma:hidden="true"
ma:internalName="ProductGroup">
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<xsd:extension base="dms:MultiChoice">
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<xsd:element name="Value" maxOccurs="unbounded" minOccurs="0"
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<xsd:simpleType>
<xsd:restriction base="dms:Choice">
<xsd:enumeration value="Atomic Spectroscopy"/>
<xsd:enumeration value="Automation Solutions"/>
<xsd:enumeration value="Bioreagents, Standards & Kits"/>
<xsd:enumeration value="Columns & Supplies"/>
<xsd:enumeration value="Dissolution"/>
<xsd:enumeration value="Electrophoresis"/>
<xsd:enumeration value="Gas Chromatography"/>
<xsd:enumeration value="GC & GC/MS Columns"/>
<xsd:enumeration value="General Chromatography"/>
<xsd:enumeration value="Informatics & Software"/>
<xsd:enumeration value="Instrument Parts & Supplies"/>
<xsd:enumeration value="LC & LC/MS Columns"/>
<xsd:enumeration value="Leak Detection"/>
<xsd:enumeration value="Liquid Chromatography"/>
<xsd:enumeration value="Magnetic Resonance"/>
<xsd:enumeration value="Mass Spectrometry"/>
<xsd:enumeration value="Microarrays"/>
<xsd:enumeration value="Molecular Spectroscopy"/>
<xsd:enumeration value="Particle Analysis"/>
<xsd:enumeration value="Sample Preparation"/>
<xsd:enumeration value="Services"/>
<xsd:enumeration value="Support"/>
<xsd:enumeration value="Vacuum Technologies"/>
<xsd:enumeration value="X-Ray Crystallography"/>
</xsd:restriction>
</xsd:simpleType>
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</xsd:sequence>
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<xsd:element name="ProductType" ma:index="25" nillable="true"
ma:displayName="Product Type" ma:description="Select only the Product
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ma:internalName="ProductType">
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<xsd:enumeration value="6850 Consumables"/>
<xsd:enumeration value="6890N Consumables"/>
<xsd:enumeration value="Accessories"/>
<xsd:enumeration value="AccuBond II SPE Cartridges"/>
<xsd:enumeration value="Accubond SPE Cartridges"/>
<xsd:enumeration value="Active Gauges"/>
<xsd:enumeration value="Analytical Injection Systems"/>
<xsd:enumeration value="Analytical LC Detectors"/>
<xsd:enumeration value="Analytical LC Fraction Collectors"/>
<xsd:enumeration value="Analytical LC Systems"/>
<xsd:enumeration value="Analytical Pumps & Vacuum Degassers"/>
<xsd:enumeration value="Analytical Thermal Column Compartment"/>
<xsd:enumeration value="Analytical Valve Solution"/>
<xsd:enumeration value="Analytical Workstation"/>
<xsd:enumeration value="Analyzer"/>
<xsd:enumeration value="Apparatus"/>
<xsd:enumeration value="Application Kits"/>
<xsd:enumeration value="APPNS"/>
<xsd:enumeration value="Asahipak Columns"/>
<xsd:enumeration value="Atomic Absorption Accessories"/>
<xsd:enumeration value="Atomic Absorption Spectroscopy"/>
<xsd:enumeration value="Atomic Absorption Systems"/>
<xsd:enumeration value="Barcode"/>
<xsd:enumeration value="Bioanalyzer"/>
<xsd:enumeration value="Bioanalyzer Cell Solution"/>
<xsd:enumeration value="Bioanalyzer Compliance"/>
<xsd:enumeration value="Bioanalyzer DNA Solution"/>
<xsd:enumeration
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<xsd:enumeration
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<xsd:enumeration
value="Bioanalyzer Protein Solution"/>
value="Bioanalyzer RNA Solution"/>
value="Bioanalyzer System"/>
value="Bioanalyzer Workstation"/>
value="Bond Elut SPE"/>
value="Bulk SPE Sorbents"/>
value="Capillary"/>
value="Capillary Electrophoresis & CE/MS"/>
value="Capillary LC"/>
value="Cartridge Reservoirs and Filtration Cartridges"/>
value="CCD Detectors"/>
value="cDNA Kit"/>
value="CE Compliance"/>
value="CE Standards & Reagents"/>
value="CGH Kit"/>
value="Chemical Standards"/>
value="Chip-on-Chip"/>
value="Chiral Columns"/>
value="Chromatographic Data System"/>
value="Columns"/>
value="Compliance"/>
value="Components & Hardware"/>
value="Computer/Peripherals"/>
value="Consulting"/>
value="Content Management"/>
value="CpG Microarray"/>
value="CTC Sample Injectors"/>
value="Custom"/>
value="Data Analysis Software"/>
value="Diatomaceous Earth Sorbents"/>
value="Diffusion Pumps"/>
value="Disk SPE"/>
value="Dissolution"/>
value="Dissolution Systems"/>
value="DNA"/>
value="DNA Methylation"/>
value="Drugs of Abuse Testing"/>
value="Dry Scroll Pumps"/>
value="Dual Mode Gene Expression"/>
value="Electronic Lab Notebook"/>
value="Electrophoresis"/>
value="Enterprise Edition SW"/>
value="Evidex II Drugs of Abuse Cartridges"/>
value="EVIDEX SPE Cartridges"/>
value="Flash Chromatography"/>
value="Flash Chromatography Systems"/>
value="Fluorescence Accessories"/>
value="Fluorescence Spectroscopy"/>
value="Fluorescence Systems"/>
value="FTIR Accessories"/>
value="FT-IR Accessories"/>
value="FT-IR Systems"/>
value="FTMS"/>
value="Gas Analyzer Standards and Accessories"/>
<xsd:enumeration
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value="Gas Chromatography & GC/MS"/>
value="Gas Management"/>
value="Gauge Controllers"/>
value="GC and GC/MS Standards"/>
value="GC Compliance"/>
value="GC Systems"/>
value="GC Techniques"/>
value="GC/MS Compliance"/>
value="GC/MS Systems"/>
value="Gel Permeation/Size-Exclusion"/>
value="Gel Permeation/Size-Exclusion Systems"/>
value="General Supplies"/>
value="General Support"/>
value="Goniometer"/>
value="HPLC Columns for Biotechnology"/>
value="HPLC Columns for DNA Separations"/>
value="HPLC Normal Phase"/>
value="HPLC Reversed-Phase"/>
value="Hypersil columns for HPLC"/>
value="ICP-MS"/>
value="ICP-MS Accessories"/>
value="ICP-MS Standards"/>
value="ICP-MS Systems"/>
value="ICP-OES"/>
value="ICP-OES Accessories"/>
value="ICP-OES Systems"/>
value="Inlets"/>
value="Instrument"/>
value="Instrument Control & Data Handling"/>
value="Instruments"/>
value="Ion Exchange Columns"/>
value="Ion Pumps"/>
value="Ion Sources"/>
value="J&W GC Columns"/>
value="Lab Informatics Framework"/>
value="Lab Informatics Software"/>
value="Laboratory Information Management"/>
value="Laboratory Resource Management"/>
value="LC and LC/MS Standards & Reagents"/>
value="LC Compliance"/>
value="LC Instrument Control"/>
value="LC/MS Compliance"/>
value="LC/MS Systems"/>
value="LC/MSD_Compliance"/>
value="LiChrosorb Columns"/>
value="Lichrospher Columns"/>
value="Life Sciences Informatics"/>
value="Lifecycle Planning"/>
value="Liquid Chromatography & LC/MS"/>
value="Liquid Handling"/>
value="Magnetic Resonance Data System"/>
value="Manifolds and Accessories"/>
value="Manual Leak Detector"/>
value="Mass Spectrometry"/>
<xsd:enumeration value="MassTag"/>
<xsd:enumeration value="Microarray"/>
<xsd:enumeration value="Microarray Kit"/>
<xsd:enumeration value="Microarray Reagents"/>
<xsd:enumeration value="MicroGC"/>
<xsd:enumeration value="Microimaging"/>
<xsd:enumeration value="Microplate Management"/>
<xsd:enumeration value="microRNA"/>
<xsd:enumeration value="MKI Unity"/>
<xsd:enumeration value="MRI Computers & Peripherals"/>
<xsd:enumeration value="MRI Consoles"/>
<xsd:enumeration value="MRI Gradient Coils"/>
<xsd:enumeration value="MRI Monitoring & Gating"/>
<xsd:enumeration value="MRI RF Coils"/>
<xsd:enumeration value="MRI Sample Positioning"/>
<xsd:enumeration value="MRI Specialty Magnets"/>
<xsd:enumeration value="MRI Systems"/>
<xsd:enumeration value="mRP"/>
<xsd:enumeration value="MS_Compliance"/>
<xsd:enumeration value="Multiple Affinity Removal (MARs)"/>
<xsd:enumeration value="NMR Accessories"/>
<xsd:enumeration value="NMR Automation Suite"/>
<xsd:enumeration value="NMR Computers & Peripherals"/>
<xsd:enumeration value="NMR Consoles"/>
<xsd:enumeration value="NMR Magnets"/>
<xsd:enumeration value="NMR Probes"/>
<xsd:enumeration value="NMR Spectrometers"/>
<xsd:enumeration value="Nucleosil Columns"/>
<xsd:enumeration value="Offgel"/>
<xsd:enumeration value="Oligo aCGH"/>
<xsd:enumeration value="Peptide Cleanup Pipette Tips"/>
<xsd:enumeration value="Peptide Cleanup Spin Tubes"/>
<xsd:enumeration value="Physical Testers"/>
<xsd:enumeration value="Pipette Tips"/>
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<xsd:enumeration value="Prep-Process Benchtop LC Injectors"/>
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value="Process LC Systems"/>
value="Processing Hardware"/>
value="Protein"/>
value="Protein Sequencing"/>
value="Protein System"/>
value="Proteomic Consumables"/>
value="Proteomics Accessories"/>
value="Purospher Columns"/>
value="Robotic Automation"/>
value="Rotary Vane Pumps"/>
value="RPS Series Roots Pumping Systems"/>
<xsd:enumeration value="RRHT"/>
<xsd:enumeration value="Sample Device"/>
<xsd:enumeration value="Sample Filtration"/>
<xsd:enumeration value="Sample Introduction"/>
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<xsd:enumeration value="Sampling Systems"/>
<xsd:enumeration value="SampliQ QuEChERS"/>
<xsd:enumeration value="SampliQ SPE"/>
<xsd:enumeration value="Search"/>
<xsd:enumeration value="Selective Detector"/>
<xsd:enumeration value="Small Molecule System"/>
<xsd:enumeration value="Software"/>
<xsd:enumeration value="Software Compliance"/>
<xsd:enumeration value="SPE (Solid Phase Extraction)"/>
<xsd:enumeration value="SPE Cartridge Reservoirs and Stopcocks"/>
<xsd:enumeration value="SPE Method Development Kits"/>
<xsd:enumeration value="Specialized"/>
<xsd:enumeration value="Spectrometry Data System"/>
<xsd:enumeration value="Spectroscopy Data System"/>
<xsd:enumeration value="Spin Concentrators"/>
<xsd:enumeration value="Spin Filters"/>
<xsd:enumeration value="Spin Tubes"/>
<xsd:enumeration value="Superspher Columns"/>
<xsd:enumeration value="SureSelect"/>
<xsd:enumeration value="Synthesizer"/>
<xsd:enumeration value="Syringe Filters"/>
<xsd:enumeration value="Syringes"/>
<xsd:enumeration value="Systems"/>
<xsd:enumeration value="Thermostat Column Compartments"/>
<xsd:enumeration value="TMR 8900"/>
<xsd:enumeration value="TMRAqua70"/>
<xsd:enumeration value="Transducers"/>
<xsd:enumeration value="Turbo Pumping Systems"/>
<xsd:enumeration value="Turbo Pumps"/>
<xsd:enumeration value="UV-VIS Accessories"/>
<xsd:enumeration value="UV-VIS Compliance"/>
<xsd:enumeration value="UV-Vis Standards & Reagents"/>
<xsd:enumeration value="UV-VIS Systems"/>
<xsd:enumeration value="UV-VIS-NIR"/>
<xsd:enumeration value="Vacuum Manifolds, Parts and Accessories"/>
<xsd:enumeration value="Vacuum Supplies"/>
<xsd:enumeration value="Vacuum Technologies"/>
<xsd:enumeration value="Vials"/>
<xsd:enumeration value="VS Series Automatic Leak Detectors"/>
<xsd:enumeration value="Workstations"/>
<xsd:enumeration value="X-ray Source"/>
<xsd:enumeration value="ZORBAX"/>
</xsd:restriction>
</xsd:simpleType>
</xsd:element>
</xsd:sequence>
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</xsd:complexType>
</xsd:element>
<xsd:element name="Product" ma:index="26" nillable="true"
ma:displayName="Product" ma:hidden="true" ma:internalName="Product">
<xsd:complexType>
<xsd:complexContent>
<xsd:extension base="dms:MultiChoice">
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<xsd:element name="Value" maxOccurs="unbounded" minOccurs="0"
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<xsd:simpleType>
<xsd:restriction base="dms:Choice">
<xsd:enumeration value="G2912A"/>
<xsd:enumeration value="G2613A"/>
<xsd:enumeration value="G2614A"/>
<xsd:enumeration value="G2630A"/>
<xsd:enumeration value="G2630B"/>
<xsd:enumeration value="G2855B"/>
<xsd:enumeration value="G2888A"/>
<xsd:enumeration value="G2913A"/>
<xsd:enumeration value="G2916A"/>
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<xsd:element name="IndustryGroup" ma:index="27" nillable="true"
ma:displayName="Industry Group" ma:description="Select only the Industry
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<xsd:complexType>
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<xsd:extension base="dms:MultiChoice">
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<xsd:element name="Value" maxOccurs="unbounded" minOccurs="0"
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<xsd:simpleType>
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<xsd:enumeration value="BioPharma"/>
<xsd:enumeration value="Clinical Research"/>
<xsd:enumeration value="Energy & Fuels"/>
<xsd:enumeration value="Environmental"/>
<xsd:enumeration value="Food Testing & Agriculture"/>
<xsd:enumeration value="Forensics & Drug Testing"/>
<xsd:enumeration value="Genomics"/>
<xsd:enumeration value="Geochemistry, Mining & Metals"/>
<xsd:enumeration value="Homeland Security"/>
<xsd:enumeration value="Integrated Biology"/>
<xsd:enumeration value="Materials Testing & Research"/>
<xsd:enumeration value="Metabolomics"/>
<xsd:enumeration value="Pharmaceuticals"/>
<xsd:enumeration value="Proteomics & Protein Sciences"/>
<xsd:enumeration value="Semiconductor Analysis"/>
<xsd:enumeration value="Specialty Chemicals"/>
<xsd:enumeration value="Vacuum Solutions"/>
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<xsd:element name="IndustryType" ma:index="28" nillable="true"
ma:displayName="Industry Type" ma:hidden="true"
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<xsd:complexType>
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<xsd:element name="Value" maxOccurs="unbounded" minOccurs="0"
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<xsd:simpleType>
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<xsd:enumeration value="AgChem"/>
<xsd:enumeration value="Agriculture"/>
<xsd:enumeration value="Consumer Products"/>
<xsd:enumeration value="Disease Discovery"/>
<xsd:enumeration value="Drug Development"/>
<xsd:enumeration value="Drug Discovery"/>
<xsd:enumeration value="Drug Manufacturing/QA/QC"/>
<xsd:enumeration value="Drug Testing"/>
<xsd:enumeration value="Environmental"/>
<xsd:enumeration value="Foods & Flavors"/>
<xsd:enumeration value="Forensics"/>
<xsd:enumeration value="Fuel Cells"/>
<xsd:enumeration value="Genomics"/>
<xsd:enumeration value="Homeland Security"/>
<xsd:enumeration value="Hydrocarbon Processing"/>
<xsd:enumeration value="Nucleic Acid Analysis"/>
<xsd:enumeration value="Production-QA/QC"/>
<xsd:enumeration value="Proteomics"/>
<xsd:enumeration value="Semiconductor"/>
<xsd:enumeration value="Specialty Chemical"/>
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<xsd:element name="Industry" ma:index="29" nillable="true"
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<xsd:complexType>
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<xsd:element name="Value" maxOccurs="unbounded" minOccurs="0"
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<xsd:simpleType>
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<xsd:enumeration value="Air"/>
<xsd:enumeration value="Analysis of Process Chemicals"/>
<xsd:enumeration value="Antibacterial Drug Residues"/>
<xsd:enumeration value="Bioanalysis"/>
<xsd:enumeration value="Biological Warfare Agents (BWA)"/>
<xsd:enumeration value="Chemical Warfare Agents (CWA)"/>
<xsd:enumeration value="Components Analysis"/>
<xsd:enumeration value="Contamination Control"/>
<xsd:enumeration value="Environmental Monitoring"/>
<xsd:enumeration value="Flavors"/>
<xsd:enumeration value="Food"/>
<xsd:enumeration value="Fragrances"/>
<xsd:enumeration value="Natural Compounds & Additives"/>
<xsd:enumeration value="Pesticides & Residues"/>
<xsd:enumeration value="Silicon Wafer Analysis for Organic
Contaminants"/>
<xsd:enumeration value="Soil & Sediment"/>
<xsd:enumeration value="Toxic Industrial Chemicals (TIC)"/>
<xsd:enumeration value="Ultra-pure Water Analysis"/>
<xsd:enumeration value="Water, Soil & Sediment"/>
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<xsd:schema targetNamespace="3a52aef6-3c65-41ed-96e3-cac50d1c25cd"
elementFormDefault="qualified"
xmlns:xsd="http://www.w3.org/2001/XMLSchema"
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pes">
<xsd:import
namespace="http://schemas.microsoft.com/office/2006/documentManagement/ty
pes"/>
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</xsd:element>
</xsd:schema>
<xsd:schema targetNamespace="ee42ffa4-88aa-408d-9f63-e2d1068a6810"
elementFormDefault="qualified"
xmlns:xsd="http://www.w3.org/2001/XMLSchema"
xmlns:dms="http://schemas.microsoft.com/office/2006/documentManagement/ty
pes">
<xsd:import
namespace="http://schemas.microsoft.com/office/2006/documentManagement/ty
pes"/>
<xsd:element name="MainCat" ma:index="21" nillable="true"
ma:displayName="MainCat" ma:format="Dropdown" ma:internalName="MainCat">
<xsd:simpleType>
<xsd:restriction base="dms:Choice">
<xsd:enumeration value="Products & Services"/>
<xsd:enumeration value="Education & Events"/>
<xsd:enumeration value="Solutions"/>
<xsd:enumeration value="News Releases"/>
<xsd:enumeration value="Technical Support"/>
</xsd:restriction>
</xsd:simpleType>
</xsd:element>
<xsd:element name="MidCat" ma:index="36" nillable="true"
ma:displayName="MidCat" ma:description="Defines the section that this
page will appear in the "Narrow Your Result" section of the
general site search results." ma:format="Dropdown"
ma:internalName="MidCat">
<xsd:simpleType>
<xsd:restriction base="dms:Choice">
<xsd:enumeration value="Chemical Analysis"/>
<xsd:enumeration value="Classroom Training Courses"/>
<xsd:enumeration value="Columns & Supplies"/>
<xsd:enumeration value="Downloads and Utilities"/>
<xsd:enumeration value="e-Seminars"/>
<xsd:enumeration value="Events"/>
<xsd:enumeration value="FAQs"/>
<xsd:enumeration value="Installation and Maintenance Videos"/>
<xsd:enumeration value="Illustrated Parts Breakdowns"/>
<xsd:enumeration value="Informatics and Software"/>
<xsd:enumeration value="Instruments & Systems"/>
<xsd:enumeration value="Life Sciences"/>
<xsd:enumeration value="Reagents, Standards & Kits"/>
<xsd:enumeration value="Software Familiarization Videos"/>
<xsd:enumeration value="Parts Information"/>
<xsd:enumeration value="Pharmaceuticals"/>
<xsd:enumeration value="Services"/>
<xsd:enumeration value="Support Services"/>
<xsd:enumeration value="..."/>
</xsd:restriction>
</xsd:simpleType>
</xsd:element>
</xsd:schema>
<xsd:schema targetNamespace="d60c28fc-3d14-46f3-b174-9a10a2a6c6f4"
elementFormDefault="qualified"
xmlns:xsd="http://www.w3.org/2001/XMLSchema"
xmlns:dms="http://schemas.microsoft.com/office/2006/documentManagement/ty
pes">
<xsd:import
namespace="http://schemas.microsoft.com/office/2006/documentManagement/ty
pes"/>
<xsd:element name="Analytical_x0020_Technique" ma:index="37"
nillable="true" ma:displayName="Analytical_x0020_Technique"
ma:format="Dropdown" ma:internalName="Analytical_x0020_Technique"
ma:readOnly="false">
<xsd:simpleType>
<xsd:restriction base="dms:Choice">
<xsd:enumeration value="Atomic Absorption (AA)"/>
<xsd:enumeration value="Capillary Electrophoresis (CE)"/>
<xsd:enumeration value="CE/MS"/>
<xsd:enumeration value="Dissolution"/>
<xsd:enumeration value="Fluorescence Spectroscopy"/>
<xsd:enumeration value="FTIR"/>
<xsd:enumeration value="GC"/>
<xsd:enumeration value="GC Analyzer"/>
<xsd:enumeration value="GC QQQ"/>
<xsd:enumeration value="GC Q-TOF"/>
<xsd:enumeration value="GC x GC"/>
<xsd:enumeration value="GC/MSD"/>
<xsd:enumeration value="GC-RapidMS"/>
<xsd:enumeration value="GPC/SEC"/>
<xsd:enumeration value="ICP-MS"/>
<xsd:enumeration value="ICP-OES"/>
<xsd:enumeration value="LC"/>
<xsd:enumeration value="LC QQQ"/>
<xsd:enumeration value="LC Q-TOF"/>
<xsd:enumeration value="LC TOF"/>
<xsd:enumeration value="LC/MS"/>
<xsd:enumeration value="Micro GC"/>
<xsd:enumeration value="MP-AES"/>
<xsd:enumeration value="MS"/>
<xsd:enumeration value="NMR"/>
<xsd:enumeration value="PCR / qPCR"/>
<xsd:enumeration value="Rapid-MS"/>
<xsd:enumeration value="Thin Layer Chromatography"/>
<xsd:enumeration value="UHPLC"/>
<xsd:enumeration value="UV-Vis-NIR Spectroscopy"/>
<xsd:enumeration value="X-ray Crystallography"/>
</xsd:restriction>
</xsd:simpleType>
</xsd:element>
<xsd:element name="Matrix" ma:index="38" nillable="true"
ma:displayName="Matrix" ma:format="Dropdown" ma:internalName="Matrix"
ma:readOnly="false">
<xsd:simpleType>
<xsd:restriction base="dms:Choice">
<xsd:enumeration value="Biodiesel/Biogas"/>
<xsd:enumeration value="Biofuel(s)"/>
<xsd:enumeration value="Biological Mass"/>
<xsd:enumeration value="Biologics"/>
<xsd:enumeration value="Blood"/>
<xsd:enumeration value="Bone"/>
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
<xsd:enumeration
value="Breast Milk"/>
value="Cell culture"/>
value="Cereals"/>
value="Coffee"/>
value="Composites"/>
value="Cosmetics"/>
value="Dairy"/>
value="Designer Drugs"/>
value="Drinking Water"/>
value="Drugs of Abuse"/>
value="Edible Oils"/>
value="Ethanol"/>
value="Feces"/>
value="Flavors"/>
value="Food - Other"/>
value="Fragrances"/>
value="Fruits"/>
value="Gas Fuel"/>
value="Glass"/>
value="Grains"/>
value="Human Tissue"/>
value="Juice"/>
value="Legumes"/>
value="Liquid Fuel"/>
value="Meat"/>
value="Metals"/>
value="Minerals"/>
value="Natural Gas"/>
value="Nutraceutical(s)"/>
value="Nuts"/>
value="Oil"/>
value="Optical Coatings"/>
value="Optical Component"/>
value="Packaging Materials"/>
value="Paint"/>
value="Pharmaceuticals"/>
value="Plants"/>
value="Plastics"/>
value="Polymers"/>
value="Refinery Gas"/>
value="Rock"/>
value="Rubbers"/>
value="Saliva"/>
value="Seafood"/>
value="Shale"/>
value="Soft Drinks"/>
value="Soils, Sludges & Sediments"/>
value="Supplement"/>
value="Surface Water"/>
value="Tea"/>
value="Thin Films"/>
value="Urine"/>
value="Vegetables"/>
value="Vitamin"/>
<xsd:enumeration value="Waste Water"/>
<xsd:enumeration value="Water"/>
<xsd:enumeration value="Wood"/>
<xsd:enumeration value="Yeast"/>
</xsd:restriction>
</xsd:simpleType>
</xsd:element>
</xsd:schema>
<xsd:schema
targetNamespace="http://schemas.openxmlformats.org/package/2006/metadata/
core-properties" elementFormDefault="qualified"
attributeFormDefault="unqualified" blockDefault="#all"
xmlns="http://schemas.openxmlformats.org/package/2006/metadata/coreproperties" xmlns:xsd="http://www.w3.org/2001/XMLSchema"
xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance"
xmlns:dc="http://purl.org/dc/elements/1.1/"
xmlns:dcterms="http://purl.org/dc/terms/"
xmlns:odoc="http://schemas.microsoft.com/office/internal/2005/internalDoc
umentation">
<xsd:import namespace="http://purl.org/dc/elements/1.1/"
schemaLocation="http://dublincore.org/schemas/xmls/qdc/2003/04/02/dc.xsd"
/>
<xsd:import namespace="http://purl.org/dc/terms/"
schemaLocation="http://dublincore.org/schemas/xmls/qdc/2003/04/02/dcterms
.xsd"/>
<xsd:element name="coreProperties" type="CT_coreProperties"/>
<xsd:complexType name="CT_coreProperties">
<xsd:all>
<xsd:element ref="dc:creator" maxOccurs="1" ma:index="9"
ma:displayName="Author"/>
<xsd:element ref="dcterms:created" minOccurs="0" maxOccurs="1"/>
<xsd:element ref="dc:identifier" minOccurs="0" maxOccurs="1"/>
<xsd:element name="contentType" minOccurs="0" maxOccurs="1"
type="xsd:string" ma:index="35" ma:displayName="Content Type"/>
<xsd:element ref="dc:title" maxOccurs="1" ma:index="1"
ma:displayName="Title"/>
<xsd:element ref="dc:subject" minOccurs="0" maxOccurs="1"/>
<xsd:element ref="dc:description" minOccurs="0" maxOccurs="1"/>
<xsd:element name="keywords" maxOccurs="1" ma:index="7"
ma:displayName="Keywords">
<xsd:simpleType>
<xsd:restriction base="xsd:string">
<xsd:minLength value="1"/>
</xsd:restriction>
</xsd:simpleType>
</xsd:element>
<xsd:element ref="dc:language" minOccurs="0" maxOccurs="1"/>
<xsd:element name="category" minOccurs="0" maxOccurs="1"
type="xsd:string"/>
<xsd:element name="version" minOccurs="0" maxOccurs="1"
type="xsd:string"/>
<xsd:element name="revision" minOccurs="0" maxOccurs="1"
type="xsd:string">
<xsd:annotation>
<xsd:documentation>
This value indicates the number of saves or
revisions. The application is responsible for updating this value after
each revision.
</xsd:documentation>
</xsd:annotation>
</xsd:element>
<xsd:element name="lastModifiedBy" minOccurs="0" maxOccurs="1"
type="xsd:string"/>
<xsd:element ref="dcterms:modified" minOccurs="0" maxOccurs="1"/>
<xsd:element name="lastPrinted" minOccurs="0" maxOccurs="1"
type="xsd:dateTime"/>
<xsd:element name="contentStatus" minOccurs="0" maxOccurs="1"
type="xsd:string"/>
</xsd:all>
</xsd:complexType>
</xsd:schema>
</ct:contentTypeSchema>
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