2006 Rad Safe Forms 1 Form 1 Date: Name: Title: Office: Phone Office: Home: STATEMENT OF TRAINING Dept.: (Bldg. / Room) RADIATION TRAINING SUMMARY: Course Work: Course Name and Number Dates of Instruction Course Content and Instructor Work Related Experience: Place of Experience Dates Experience and Isotopes Used (Use additional pages if necessary) (Signature) _________________________________ Form 1: 8/6/93; revised 1/1/94, 3/13/95,12/12/00, and 7/15/06 Form 2 STATEMENT OF AGREEMENT The below named individual signifies that she/he has read the Minnesota State University Moorhead policy, has read and has a copy of the Minnesota State University Moorhead radiation safety handbook, and is willing to abide by the Minnesota State University Moorhead regulations concerned with the safe handling, use, and disposal of radioisotopes on campus, following the rules of the Minnesota State University Moorhead ALARA program. The below named person agrees to attend the radiation safety training and refresher courses as required by the Minnesota State University Moorhead Radiation Safety Program as a prerequisite for authorization for use of radioisotopes as research and instructional aids. The below named person, in further compliance with these regulations, agrees to wear a film badge or other prescribed personnel monitoring devices, during all periods of usage of beta emitters with energies of greater than 1 MeV and all gamma emitters of 1 millicurie. The undersigned also agrees to comply strictly with all rules and regulations issued governing the use of radioisotopes and hereby waives any right to recourse against the university, the RSO and the RSC for any damages whatsoever resulting from any failure to fully conform with such rules and regulations. The below named individual also agrees to report any known instances of noncompliance to his/her principal investigator, and/or to the RSO and the RSC. The below named individual also realizes that if he/she is found to be in non-compliance with the regulations outlined in the Minnesota State University Moorhead program, and that investigation demonstrates continued non-compliance, that that person's authorization to use radioisotopes may be revoked by the RSO until further training and/or willingness to comply with the regulations of the ALARA program are demonstrated. The below named individual has taken and passed with a 75% the Radiation Safety Test Date of test___________ RSO Initial ________ The below has watched or participated in the MSUM short course (on-line or in person) AND has been through a personal orientation with the RSO or their Principle investigator. This personal orientation must have included the following: o o o o o o Signed: Tour / Review of site Answer any remaining questions Key & SL 222 (storage and main room) access Completed Forms 1 and 2 Wipe Test / Survey Review Web site and Handbook Review Date: Form 2: 8/6/93; revised 1/1/94, 3/13/95 12/12/00, and 7/15/06 Form 3. REQUEST FOR PERMISSION TO POSSESS AND USE RADIOISOTOPES OR IONIZING RADIATION PRODUCING DEVICES 1. Names1 of all persons who will be in contact with isotope: _______________________________________________________Dept.___________________________ _______________________________________________________Dept.___________________________ 2. _________________________ 3. ____________________________4. _________________________ (Isotope) (Chemical Form) (Quantity) 1. ______________________________________ 6. ___________________________ (Catalog Number and Supplier) (Date Desired) 7. Location of Use2 _____________________________________________________ (Building) (Room No.) 8. Proposed use3 _______________________________________________________________________ _____________________________________________________________________________________ _ 9. Safety Precautions and Personnel Monitoring Required4 ______________________________________________________________________________________ _____________________________________________________________________________________ _ 10. Waste Disposal Procedures5 _____________________________________________________________________________________ _____________________________________________________________________________________ _____________________________________________________________________________________ 11. 12. Signed: This isotope (will) (will not) be used in or on human beings. This isotope (will) (will not) be used in or on animal subjects. ____________________________________________________________ (Licensed Principal Investigator) ____________________________________________________________ (Title) (Date) ---------------------------------------------------------------------Approved (prior to) (after) Committee action 1 2 3 (RSC): _________________________________ (RSO): __________________________________________ Approved (prior to) (after) Committee action Committee Action: ______________________________ Date:________________ All persons whose names appear here must provide a written statement of training in radioisotopes techniques and sign the state of agreement form. For areas of usage not already approved by the Committee, a complete description of facilities and equipment to be used in these studies must be attached. All areas outside of SL 222 radioisotope laboratory must be approved prior to utilization by the Radiation Safety Committee. A complete description of the experimental procedures should be on file with this application. This description should include an outline of the experimental procedures, justification for the use of radioisotopes for this application, safety precautions and personnel monitoring which will be conducted by personnel using this radioisotope, a description of survey procedures which will be conducted in the laboratory while these isotopes are being used, and waste disposal procedures. Form 3: 8/6/93; revised 1/1/94, 3/13/95 12/12/00, and 7/15/06 4 In all descriptions, it should be demonstrated that ALARA principles will be used in the handling and utilization of this radioisotope. 5 See comment #4 See comment #3. Form 3: 8/6/93; revised 1/1/94, 3/13/95 and 12/12/00 5 Form 4 REQUEST FOR ORDERING AND STORAGE OF RADIOISOTOPES OR IONIZING RADIATION PRODUCING DEVICES Date: _____________________ For: ______________________________________ Dept.____________________ Project Title: ______________________________________________________ Grant Number, Title and Agency:______________________________________ To be used in Room(s): __________ To be stored in Room ______________ Isotope: ________________________ Chemical Form: ____________________ Quantity: _______________________ (Becquerels or mBecquerels) Concentration: _____________ (Bq/ml) Volume: ______________________ml. Specific Activity _________________________ (Bq/g; Bq/umole) Assayed at _________________________________________________________________________ _________________________________________________________________________ _________________________________________________________________________ Assay Method _________________________________________________________________________ _________________________________________________________________________ _________________________________________________________________________ _________________________________________________________________________ Total Solids: ___________ mg/ml; Normality: __________; pH: ________ Supplier: _______________________________: P.O. No. _________________ Additional Information:____________________________________________________ _______________________________________________________________________________________ _______________________________________________________________________________________ ____________________________________________________________________________________ Intensity of Radiation at surface of Shield ________________mrem/hr. Completed by: _______________________________________________________ * * * * * * * * * * * * * * * * * * * * * * * * Surveys of material at time of receipt: Background counts: __________; Outside of package: ____________; Outside of container: ___________; Other: _____________________. Accept Reject Shipment: _____________________________________________ (Signature) The original copy of this form shall be held on file in the working laboratory to enable the laboratory director to know the quantity and type of radiomaterials present in his/her laboratory at any given time. After receipt of material and usage has begun, the detailed inventory of material should be kept on Form 6. Radioisotope Inventory and Utilization Log. A duplicate copy of this form shall be maintained in the utilization file and this file stored along with other radioisotope data at the central storage area supervised by the RSO and the RSC. Form 4: 8/6/93; revised 1/1/94, 3/13/95 12/12/00, and 7/15/06 Form 5: REQUEST FOR PERSONAL MONITORING DEVICE(S) Date: For: ; Dept. Principal Investigator: Project Title: Type of Personal Monitor: Amount, Type and Chemical Form of Radioisotope or Ionizing Radiation Producing Device to be Used by Individual Requesting Personal Monitor: Date that monitor is needed: Expected dates during which monitor will be needed: Grant Number, Title and Agency: Principal Investigator (Signature) Radiation Safety Officer: (Signature) Form 5: 8/6/93; revised 1/1/94; 3/13/95, 8/4/95 and 12/12/00 Form 6. RADIOISOTOPE INVENTORY AND UTILIZATION LOG Radioisotope: Chemical Form: Received: ; Date Ordered Catalog Number ; Serial Number: Amount of material received: Specific radioactivity: (Bq or mBq); (Bq/mmole or Bq/umole) Principal Investigator Who Ordered Material: Receipt Surveys conducted by: Outside of box: Date Inner Packing: User Outside of Vial: Other: ________ Purpose Amount Used 8/6/93; revised 1/1/94; 3/13/95, 8/4/95 and 12/12/00 8 Amount Remaining Form 7. DECLARED PREGNANT WOMAN STATEMENT The below named individual signified that she has read the radiation safety information for the embryo/fetus, has discussed that information with her principal investigator and the RSO, and accepts her risks and responsibilities for making the decision to continue working with radioactive materials during the pregnancy. The individual becomes a declared pregnant woman with the date and signature given below, and also gives the estimated time of conception and the estimated time of parturition. This information will be kept in complete confidence and is only used to calculate the potential radiation exposure to the embryo/fetus during the 9 month period and to maintain that exposure below the 0.5 rem limit for the gestational period. Date Pregnancy was Declared to RSO: Date of Instruction on Risks to Embryo/Fetus: Instructional Information Provided Prior to Making this Decision: _____________________________________________________________________ _____________________________________________________________________ _____________________________________________________________________ _____________________________________________________________________ _____________________________________________________________________ Estimated Date of Conception: Estimated Date of Parturition: Do you plan to continue working with radioisotopes in a research/instructional capacity? ____________________________________ Signature: Principal Investigator: (Signature) Radiation Safety Officer: (Signature) Form 9. Wipe Test Analysis Date____________ Name________________ Wipes will be taken once each week in the designated areas ( see attached map) of Science Lab 222, except during weeks in which no radioisotopes are used nor waste handling/disposal is conducted. DPM will be determined using the Beckman LS 3801 liquid scintillation counter. Counts will be done using the appropriate channel(s) for the isotope(s) which was (were) used during that week; counts will be conducted a minimum of 5 minutes/count. Wipes will be taken with water moistened filter paper or cotton swabs, wiping a 100 cm2 area, and placed in a vial with an appropriate volume of water-soluble liquid scintillation cocktail (5.0 ml for the small vials). Wipe results of greater than 3X background counts will indicate the need for re-washing and reassessment of the area. Any additional areas (based on use) will also be wiped. Additional wipes will be marked on the map with a number indicating the area and the resulting counts included below. If additional wipes are needed, Simply re-number this form for your needs and not the activity and reason on an attached page. All counts are to be stored in the log. Area 1 DPM Avg Background Counts:__________ Area DPM Area 21 41 2 22 42 3 23 43 4 24 44 5 25 45 6 26 46 7 27 47 8 28 48 9 29 49 10 30 50 11 31 51 12 32 52 13 33 53 14 34 54 15 35 55 16 36 56 17 37 57 18 38 58 19 39 59 20 40 60 DPM Describe action taken if any of the areas tested were above the acceptable radiation limits. Include a second wipe test analysis of the areas following this action. 8/6/93; revised 20/07/06 10 Form 10 Radioactive Waste Disposal Date: _____________ Authorized User: ______________________________________________________. (Signature) Radioisotope: ______________ Chemical Form: _________________________. Aqueous Waste Disposal1: Volume: _____________ Amount: ______________ (Becquerel or µCi). Concentration of radionuclide: ________________ (µCi/gm or Bq/gm). Location of Disposal: __________________________________________. Solid Waste Disposal2: Amount: _________________________________(Becquerel or µCi) Shipped to Disposal Site: _____ or Stored on Site ___________ Location of Disposal Site:_______________________________________. Scintillation Cocktail Waste3: Volume: ____________; Amount: __________________(Becquerel or µCi). Concentration of Radionuclide: ___________________(µCi/gm or Bq/gm) Location of Disposal: ____________________________________________. Additional Description of Disposal Activities: ************************************ 1. One sink should be designated for aqueous waste disposal in each restricted facility. Each time a container is disposed, one of these forms must be filled out and kept on file with the principal investigator. It is suggested that a duplicate copy be placed on file in central storage. Records of aqueous waste disposals must be kept for three years. 2. All solid waste must be given to the RSO for disposal. No solid waste will be disposed by anyone other than the RSO. 3. 0.05 microcurie (1.85 kBq), or less, or tritium or carbon-14 per gram of medium used for liquid scintillation cocktail may be disposed of as aqueous, nonradioactive, waste, providing the cocktail is a grade which is sewerable. If not a sewerable cocktail, the cocktail must be disposed of as organic waste. Again, records of these disposals must be made on this form, one copy kept on file by the principal investigator while a second copy is placed in central storage. Non-aqueous waste must be reported to the university chemical hygiene officer for proper disposal. 8/6/93; revised 20/07/06 11 PROCEDURES FOR THE SAFE HANDLING AND USE OF RADIOACTIVE BYPRODUCT MATERIALS AND IONIZING RADIATION PRODUCING DEVICES TO MAINTAIN EXPOSURE LEVELS "ALARA." Radiation Safety Officer: Joseph J Provost Office -- 477-5085; Home-- 271-0537 Radiation Safety Chair: Judith Strong Office -- 477-2075 Radiation Safety Committee Members: Mark Wallert Chris Chastain 1. While performing experiments with radioisotopes, the experimenter is not to engage in eating, drinking, smoking or applying cosmetics. 2. Protective clothing (lab coats) should be worn while performing experiments using radioisotopes. All protective clothing worn while performing experiments with radioisotopes in the laboratory is to be left in the radioisotope laboratory. 3. All persons working with radioisotopes are to wear disposable gloves at all times while working with these materials. These gloves must be disposed of in the designated container at the end of each experiment. 4. After completion of experimentation, a survey of the working area and person (if applicable) is to be made by wipe testing. If detectable amounts of radioisotopes are found, the area is to be washed thoroughly until surveys demonstrate that levels have been decreased to less than 3X background counts. A record should be kept of each of these washes and surveys, wash solutions are to be treated as aqueous, sewerable waste and should be monitored and the disposal documented on Form 11: Radioactive Waste Disposal. 5. If surveys of experiment areas reveal counts of 5X background counts or greater, the Radiation Safety Officer should be contacted to assist with the decontamination. 6. All radioactive wastes are to be disposed of according to approved waste disposal procedures. All sewerable waste is to be documented on Form 11: Radioactive Waste Disposal in the designated disposal sink, only. 7. Thorough hand-washing must be done at the end of each experiment using radioisotopes, as should be done upon completion of any chemistry or biology experiment. 8. Apparatus and glassware used in radioactive experimentation and used in the radioisotope laboratory are not to be transported into non-restricted areas. 9. All incidents, including spills and incidents are to be immediately reported to the principal investigator and to the RSO. The procedures for incidents and spills involving radioactive materials must be followed when working with these materials. 10. If you have any questions, wish to report incidents or wish to report incidents of noncompliance with the Minnesota State University Moorhead radiation safety program, contact the Radiation Safety Officer or other members of the Radiation Safety Committee. 8/6/93; revised 20/07/06 12