Syntesekemiske metoder 2012
Hold 4:

1-Butyne. Scale: 50%. Opskr. K 391 1-Butyne.

3-Bromo-4-(4-ethoxycarbonylbenzoyl)thiophene. Scale: 20 %. Opskr. K 299, Opskr. K Gen
MnCl2.

4-Methylpyrrolo[1,2-a]quinolone. Scale: To be agreed. Opskr. K 475.

(Z)-2-Methyl-3-trimethylsilyl)-2-Butenoic acid. Scale: To be agreed. Opskr. K 480.

Selenocarbamate. Scale: 1 gram of the phenol. Opskr: Selenocarbamate.

DHA/VHF. Scale: to be agreed. Arkivoc, 2011, 51-67.

Copper(I) iodide-dimethyl sulfide complex. Scale: To be agreed. Opskr. K 483 CuI-MeSMe.

Bis(cyclopentadienyl)zirconium chloride hydride (Schwartz Reagent). Scale: To be agreed.
Opskr. K 484 Schwartz. S21

4-Phenyl-5(E)-decen-2-one. Scale: To be agreed. Opskr. K 482.

(S)-3-Isopropylcyclohexanone, stereoselective 1,4-addition, stereoselecti. Scale: 100%.
Angew 1997 2733.
Fun useful exercises:

N-Pivaloyl-2-toluidine (Titration of Butyllithium). Scale: 100%. Opskr. K 101.

Titration of organomagnesium, organozinc, and organolanthanide comp. Opskr K 481
Titration of Mg Zn and La.

Sodium borohydride Titration. MgI. Opskr. K 473.

Titration of organomagnesium, organozinc, and organolanthanide comp. MgI.

Tetrakistriphenylphosphine palladium. Scale: 0.45 g PdCl2. Opskr. K 116.

Titration of Grignard reagents. Opskr. K 286.

Titration OF DIBAL. OL 2005 2205.