1 Contribution of AMS studies in understanding the migmatitic terrains 2 of Pointe Géologie, Terre Adélie (East-Antarctica) 3 Jérôme Bascou1, Bernard Henry2, René-Pierre Ménot1, Minoru Funaki3, Guilhem Barruol4 4 5 6 7 8 9 10 11 1 Université de Lyon, Université Jean Monnet and UMR-CNRS 6524, Laboratoire Magmas et Volcans, 23 rue du Dr Paul Michelon, 42023 Saint Etienne, France 2 Paléomagnétisme, Institut de Physique du Globe de Paris, Sorbonne Paris Cité, Univ ersité Paris Diderot and UMR-CNRS 7154, France 3 National Institute of Polar Research, 10-3 Midori-cho Tachikawa Tokyo 190-8518, Japan 4 Université de la Réunion, CNRS and Institut de Physique du Globe de Paris, Géosciences Réunion, 97715 Saint Denis cedex 9, La Réunion, France 12 13 14 15 16 17 18 19 20 Abstract 21 22 Keywords: Migmatite, anatexite, AMS, Pointe Géologie, Antarctique 23 1 24 1. Introduction 25 26 Anatexites result from progressive melting of rocks under high-grade metamorphism 27 conditions. These rocks are often the only key to determine the structural conditions in the 28 deep crust. However, the structural analysis of migmatites is often very difficult because of 29 their complex and multiphase evolution. Moreover, the products from the melting of an initial 30 highly deformed rock have a fabric that mostly cannot be determined by the classical 31 structural approaches. In partially melted gneisses, this fabric can differ from the initial one, 32 and in dominantly melted rocks the single visible fabric is often related to the melanosome 33 orientation and therefore offers an incomplete signature of tectonic events suffered by the 34 rocks. One of the characteristics of the migmatite structures is their local variability and their 35 analysis then passes by a statistical approach. To this aim, the field observations are limited to 36 part of the elements of the fabric and generally not well-adapted. 37 The anisotropy of magnetic susceptibility (AMS) technique (Graham, 1954); see 38 (Tarling and Hrouda, 1993; Borradaile and Henry, 1997; Borradaile and Jackson, 2004) and 39 references therein) has been widely used for structural applications. It offers several 40 advantages relatively to field observations: It gives not only foliation and lineation but also 41 intensity and shape of the fabric and can be applied to a set of samples representative of a 42 significant area allowing simple statistical analysis. Ferré et al. (2003) and Kruckenberg et al. 43 (2010) applied this magnetic tool for migmatites studies. They showed that despite 44 rheological variations during deformation (solid-state deformation followed by viscous flow), 45 AMS axes were consistent with observed regional field structure and thus highlighting the 46 interest of the AMS data for the strain characterizations in high-temperature metamorphic 47 rocks. In paramagnetic migmatites, the biotite fabric can evidenced these two types of 48 deformation (Hasalovà et al., 2008). Others authors have shown that anatexites could have 49 specific AMS signature, associated with changes towards weak solid-state rheology and that 50 AMS characterizations could therefore help to better model the different stages of migmatitic 51 terranes (Charles et al., 2009; Schulmann et al., 2009; Kratinová et al., 2012). 52 The Pointe Géologie archipelago (Terre Adélie, East Antarctica) represents a deep and 53 hot crust that experimented anatectic event during Paleoproterozoic times, 1.69 Ga ago 54 (Ménot et al., 2007 and references therein). This archipelago is partially covered by the ice 55 cap and the limited outcrops are key zones to constrain the Terre Adélie Craton tectonics. 56 Pelletier et al. (2002) and Gapais et al. (2008) proposed a detailed structural and kinematic 57 analyses of the area based on foliation and lineation measurements of migmatites. But we 2 58 believe these structural data may be supplemented by taking into account the magnetic fabric 59 of the leucosomes and anatexites, which correspond to more than 50% of the outcrops and 60 which are devoid of clear markers of deformation. This would greatly improve the knowledge 61 of the structural pattern of this region. 62 The first aims of this paper is thus to specify the deformation framework associated to 63 the Paleoproterozoic event in the Terre Adélie Craton from an enlarge sampling in the Pointe 64 Géologie rocks. For this, a detailed AMS study was performed in the migmatites, the larger 65 granitic dykes and the anatexites observed on the field. Finally, we discuss on the 66 relationships between the various observed migmatitic structures of centimetric to decametric 67 scale, which correspond to various degree of segregation and transportation of magma, the 68 AMS signature and the rheological evolution of the molten crust. 69 70 2. Geological setting 71 72 The Terre Adélie Craton (TAC) is located on the easternmost part of the East 73 Antarctic Shield. It crops out as islands and capes scattered along the coast between 135° and 74 145°E but most of the outcrops are located in three main archipelagos, from West to East: 75 around Pointe Géologie (66°50’S, 140°E), East of Port Martin (66°80’S, 142°25’E) and East 76 of Cape Denison (67°S, 142°25’E) up to the Mertz glacier. This crystalline basement consists 77 of Late Archean and Paleoproterozoic formations devoid of any significant reworking since 78 1.5 Ga and then it is considered as part of the Mawson block or Mawson continent (Fanning 79 et al., 1995; 2002). At the scale of the TAC, the Late Archean and Paleoproterozoic terrains 80 are distributed westwards and eastwards from Port Martin, respectively (Monnier et al., 1996; 81 Ménot et al., 2007), Figure 1. 82 This paper deals only with the Paleoproterozoic formations of the Pointe Géologie area, 83 i.e. close to the permanent French Polar Station Dumont d’Urville (DDU). As described by 84 (Bellair, 1961b, a), the main rock types are migmatitic to anatectic gneisses that are cross cut 85 by dykes of apparently isotropic coarse-grained pink granites. The detailed mapping, carried 86 on during the GEOLETA project, improves this previous description and points out some new 87 and significant features (Monnier et al., 1996; Peucat et al., 1999; Gapais et al., 2008). 88 Migmatitic gneisses and anatexites derived from a sedimentary sequence dominated by 89 aluminous pelites together with subordinate greywackes, quartzites and calc-silicates. 90 Metagreywakes appear as intercalations ranging from tens of centimetres to hundreds of 91 meters in thickness. Quartzites and calc-silicates form dismembered layers and enclaves of 3 92 mesosomes within the migmatites and they mark out a poorly preserved sedimentary layering 93 (Figure IIa). Amphibolitized dolerites and gabbros occur as dykes and sills and they are 94 coeval with the anatectic event as shown by magma mingling features between the mafic 95 intrusions and the granitic magmas. Isotopic data indicate Paleoproterozoic sources for both 96 sediments and magmas (Peucat et al., 1999 and references therein). According to Monnier et 97 al. (1996), mesosomes, neosomes and anatexites represent respectively 10%, 60% and 30% of 98 the rock types in the Pointe Géologie archipelago. 99 These migmatitic and anatectic formations underwent a polyphased tectonic and 100 metamorphic evolution with three phases of deformation leading to a composite sub vertical 101 regional S0-S1-S2 foliation (Monnier et al., 1996; Pelletier et al., 2002). Neosomes display two 102 successive parageneses related to both the S1 and S2 metamorphic foliations and bearing 103 comparable Sil+/-Kfs+/-Pl+/-Bt+/- Cd+/-Grt+/-Ilm+/-Qtz mineral assemblages. Moreover, 104 mineral chemistry of the S1 and S2 parageneses is similar and argues for a single continuous 105 LP-HT metamorphic event, the peak conditions of which reaching 750-700°C at 0.6-0.4 GPa. 106 Large amounts of anatectic melts have been produced all along the tectonic and metamorphic 107 evolution as suggested by the various habitus of the leucosomes. The oldest leucosomes 108 appear as mylonitic lenses isoclinally folded by the S1-S2 transposition, but most of them are 109 undeformed and concordant within the S2 foliation and the latest melts cross cut the S2 planes. 110 A retrograde imprint with Bt+/-Ms+/-And assemblages marks the later evolution to about 111 550-450°C and 0.5-0.4 GPa (Monnier et al., 1996; Pelletier et al., 2002; Gapais et al., 2008). 112 Bellair and Delbos (1962) assumed a 1.5 Ga age (Rb/Sr on micas) for the partial melting 113 event. More recently, new radiometric data (Peucat et al., 1999, U-Pb on zircons and 114 monazites, Sm-Nd and Rb-Sr on whole rocks and minerals) gave precise time constraints on 115 the geological evolution of the meta-volcano-sedimentary formations of Pointe Géologie. 116 Time of deposition is bracketed between the inherited zircon ages (1.72 -1.76 Ga) and the 117 peak metamorphism and partial melting age at 1.69 Ga. The later cooling path was 118 constrained by Nd garnet ages (650-600°C at 1.63-1.60 Ga) and Rb-Sr muscovite and biotite 119 ages (450-350°C at 1.5 Ga). 120 121 3. High temperature rocks types and regional structures 122 123 While the lithology is very homogeneous in the scale of the archipelago, field 124 relationships between different rock types are much more complex for the scale of outcrops. 125 Four main rocks types have been sampled for AMS measurements: migmatites including 4 126 leucosomes and melanosomes, coarse-grained pink granites, anatexites and strongly mylonitic 127 gneisses. 128 Migmatitic gneisses: They have been described previously as the K feldspar gneisses and 129 they are the dominant facies of the area, especially on the Pétrels Island (Dumont d’Urville 130 station, Figure I). We will discuss more specifically the space and time relationships between 131 leucosomes and melanosomes in the migmatitic gneisses. As partial melting developed all 132 along a polyphased tectonic and metamorphic event, leucosomes display various habitus 133 relative to the composite foliation, which is marked on the field by melanosomes and septas 134 of mesosomes. The melanosomes defined continuous layers in migmatites (Figure IIa): 135 (i) The earliest leucosomes occur as mylonitized and elongated lenses, sometimes 136 affected by intrafolial folds within the foliation. They bear evidence of successive 137 segregation and deformation processes (Figure IIa). 138 (ii) The most common leucosomes are undeformed and concordant within the 139 migmatites foliation and they may be later folded together with the foliation. They 140 represent syn to late-foliation melts (Figure IIb). 141 (iii) The latest leucosomes form dykelets cross-cutting, and post-dating, the S1-2 142 foliation. They may be connected to the concordant leucosomes, tapping off and 143 transferring melts upwards (Figure IIa, c). 144 Coarse-grained pink granites: they appear as dykes of decimetric to decametric 145 thickness which cross cut the regional foliation (Figure IId). They are devoid of any visible 146 markers of orientation. Such dykes, collecting the dykelets, drain the more evolved melts 147 during the late- to post-tectonic stages of the partial melting and metamorphic event. 148 Anatexites: They outcrop widely on the W area of Pointe Géologie (e.g., Gouverneur, 149 Balance, Taureau and la Vierge islands, Figure VIII). They derived from a higher degree of 150 partial melting than migmatitic gneisses and show a mineral assemblage comparable to that of 151 leucosomes but more enriched in Qtz and depleted in Crd. Anatexites display more isotropic 152 textures but a flow fabric or a palimpsest structure of the parent gneisses is often marked by 153 some oriented rafts of migmatitic gneisses or schlierens of biotite and oxides (Figure IIe). 154 Mylonitic gneisses: they outcrop in a restricted and narrow zone on the western flank of 155 the Pétrels Island (Rocher Jakobsen) and some islands of Pointe Géologie, i.e. along a major 156 shear zone (sites II and V, Figure IX). They consist of Bt + Grt gneisses with only tiny Grt- 157 bearing leucosomes and are characterized by a vertical mylonitic foliation. They derive from 158 the K-feldspar migmatitic gneisses and then may be considered as late- to post-migmatisation 159 tectonites (Figure IIf). 5 160 As carefully described by Pelletier et al. (2002) and Gapais et al. (2008), the Pointe 161 Géologie archipelago show two types of structural domains: NS to N340° striking vertical 162 shear zones and domes both of them developing during the metamorphic and anatectic event. 163 Between the vertical zones, foliation attitudes point out dome-shaped structures marked by 164 flat lying to gently dipping fabrics. Dome displays a mineral lineation outlined by a preferred 165 orientation of sillimanite crystals while such a lineation is almost invisible in the vertical 166 zones. The transition from flat lying to vertical foliation zones may be sharp, with 167 development of vertical foliation planes cutting across the horizontal foliation of domes, or 168 gradual when folds, with horizontal axes, induce vertical planes. Such a transition from dome 169 to vertical shear zone never exceeds five hundred meters in thickness. In both cases, vertical 170 structures seem to be later than flat lying ones. According Gapais et al. (2008), the kinematic 171 markers (lineations, boudinage, ...) suggest that shear zones reflect a dextral transpressive 172 movement while flat areas are the result of shortening combined with stretching parallel to the 173 shear zones. Such patterns might be explained in the frame of a regional convergence of a hot 174 and weak juvenile crust leading to horizontal crustal flow and strain partitioning with 175 localized deformation along transpressional shear zones. 176 177 4. Sampling and analyses procedures 178 179 Because of outcrops restrictions (areas non accessible because of ice cover or of birds 180 protection) and high variability of the visible deformation, sampling was often made in sites 181 relatively close one to another in the main island (Pétrels Island). Other sites were scattered in 182 different smaller islands (Figure VIII). Most sampled sites correspond to a surface up to 50m2. 183 As a test, one site (site i, Figure IX) corresponds to a sampling made on a reduced surface 184 (about 0.5 m2) in gneisses showing visible foliation and lineation. 185 X large samples have been taken for petrographic and rock-magnetism studies. For 186 magnetic fabric study, cores were sampled with a gasoline-powered portable drill. All the 187 cores were oriented only with a sun compass (Figure IIf) because of the immediate proximity 188 of the southern magnetic pole. That introduced a strong limitation for sampling because of 189 climatic conditions. The sampling was made during three different summer fieldworks, in 190 1992, 2009 and 2011. As a whole, 819 rock cores were obtained in 33 sites, including 20 on 191 the Pétrels Island (Figure IX). When possible, different facies (from gneiss to anatexites) were 192 sampled on the same site. The cores were cut in the laboratory in specimen of standard 193 paleomagnetic size. 6 194 Magnetic susceptibility and its anisotropy have been measured using Kappabridges 195 KLY3 and MKF1 (AGICO, Brno). Thermomagnetic experiments were performed on 196 representative samples by heating in argon or in air using the CSL equipment and the CS2-3 197 oven (AGICO, Brno) associated with the Kappabridges. Hysteresis loops were obtained for 198 small cores (cylindrical samples of about 3 cm3) using a laboratory-made translation 199 inductometer within an electromagnet capable of reaching 1.6 T. 200 201 5. Magnetic Mineralogy 202 203 5.1. Thin sections study 204 As the magnetic characteristics of the rocks are tightly controlled by their 205 mineralogical content, the various assemblages recorded in the different rock types need to be 206 specified. This is particularly important in the case of migmatitic gneisses where partial 207 melting induces a redistribution of refractory minerals from the mesosomes to both the 208 melanosomes and leucosomes. 209 Magnetite and ilmenite are the most abundant oxide minerals. They form discrete grains or 210 clusters with direct contact between magnetite and ilmenite. The larger grains (millimetric in 211 size) are generally found in the melanosomes and therefore in the foliation and they appear as 212 elongated parallel to the lineation defined by the sillimanite when the latter is present (Figure 213 III). For ilmenite deformation also induces a structural axes related lattice preferred 214 orientation (LPO), which is characterized by the c-axes strongly concentrated close to the 215 normal to the foliation, and by the poles of (2-1-10) and (10-10) prism planes 216 concentrated close to the lineation (Figure IIIbis). Oxides are also present in the leucosomes 217 but the fabric (grains alignment) appears more scattered than in the melanosomes. At the 218 melanosome-leucosome border, elongated shape grains, may-be rotated, have been observed 219 perpendicular to the foliation. In the leucosomes oxide grains tend to be more discrete and 220 more rounded (Figure III). 221 Cordierite is also present in migmatitic gneisses and granitic dykes of Pointe Géologie. 222 This mineral that occurs mainly as grains of globular shape (up to a few millimetres in size) is 223 carefully watched because cordierite presents specific magnetic properties. This mineral 224 carries an inverse magnetic fabric (i.e. characterized by a switch between the principal 225 maximum K1 and minimum K3 axes of the AMS ellipsoid with respect to the grain shape 226 (Potter and Stephenson, 1988; Rochette et al., 1992)) that could lead to misinterpretation of 227 the measured magnetic fabrics. However the mean magnetic susceptibility (Km) for 7 228 magnetite, which is ubiquitous in studied thin sections, is significantly higher than for 229 cordierite (Km ratio > 1000). Therefore magnetite should be the main carrier of measured 230 AMS. For relatively large grains of magnetite, the K1 and K3 axes indicate the magnetic 231 lineation and magnetic foliation pole, respectively. 232 233 5.2. Rock-magnetism 234 The mean magnetic susceptibility Km (average 5.2 10-2) of the studied samples is 235 different according to the studied fraction of the migmatites (Figure IV). The gneisses with 236 subordinate melted parts and dominant melanosome fraction have very high susceptibility 237 (average?). Km values for dominant granitic fraction are lower (average?). Migmatite samples 238 including both leucosome and melanosome fractions present intermediate Km values. This 239 variability in leucosome versus melanosome content of gneissic specimens largely explains 240 the relatively large distribution of susceptibilities (Figure IV). The anatexites samples show 241 the highest variation in Km values (from X to Y). 242 All thermomagnetic KT curves (susceptibility K as a function of temperature T) show 243 during heating a sharp susceptibility decrease around 580°C (Figure V), clearly indicating the 244 presence of magnetite. In addition low temperature experiments confirm the presence of this 245 mineral by a large susceptibility increase around -160°C (Figure V). This variation 246 corresponds to the Verwey transition that is characteristic of pure magnetite. Few 247 thermomagnetic curves are perfectly reversible. Susceptibility values from the cooling curve 248 are mostly a little bit higher than the initial values, in air as in argon atmosphere (but 249 sometimes much higher as for the sample AP35). Partial cooling loops during heating 250 evidenced a weak mineral alteration due to heating around 300 to 400°C that probably reflects 251 inversion of a weak amount of maghemite in hematite. New magnetite is also often formed at 252 the highest temperatures. 253 Hysteresis loops show generally a full saturation of the magnetization for moderate 254 field (Figure VI). This saturation was partial only for the sample AP35, evidencing the 255 presence of another component of high coercivity. This component is probably hematite. In 256 most cases, ferrimagnetic minerals have a largely dominant effect for the susceptibility, but 257 two of the studied granite samples highlight also a strong contribution of the paramagnetic or 258 even diamagnetic minerals. Day plot (Day et al., 1977) for samples with mainly magnetite 259 clearly evidences a large size of the magnetite particles (Figure VII). 8 260 Main magnetic mineral is therefore magnetite with a large size. Obtained AMS data 261 are then directly usable for a structural analysis (no inverse magnetic fabric due to small 262 Single Domain particles (Potter and Stephenson, 1988). 263 264 6 - Magnetic fabric 265 266 The AMS ellipsoid yields the three principal susceptibility axes defined as 267 K1 K2 K3. K1 is the magnetic lineation and K3 is perpendicular to the magnetic foliation. 268 The Jelinek (1981) parameters P' and T were used to describe the intensity and the shape of 269 the magnetic fabric, respectively. Data for a group of samples were analysed using normalized 270 tensor variability (Hext, 1963; Jelinek, 1978) statistics. 271 6.1 – Structures from AMS 272 Data for gneiss and for granite are presented separately (often "gneisses" included 273 minor melted parts and "granitic" samples small amounts of melanosome minerals and this 274 separation has been made then considering the dominant presence of one of these facies). 275 Moreover, from the regional structural field pattern, two distinct zones have been 276 distinguished for the AMS analyse: the sub-vertical zones and the dome shaped-zones (Figure 277 VIII and IX). 278 6.1.1. In migmatitic gneisses of sub-vertical shear zones (sites T, R, D, O, XIII, A of 279 Pétrels Island, Figure IX, melanosome layers show generally both well clustered magnetic 280 foliation pole (K3) and magnetic lineation (K1). The magnetic foliation is dominantly 281 subvertical N-S in accord with the observed field foliation and the magnetic lineation presents 282 a weak plunge and N-S trending in agreement with the orientation of mineral lineation 283 outlined in few places by a preferred alignment of sillimanite crystals. That is in particular the 284 case in the site test i (Figure IX) where foliation and lineation are clearly visible. The granitic 285 rich layers (site XIII) display more diffuse fabric, in particular the K1 axes that tend to form a 286 girdle perpendicular to K3. Well-individualized leucosomes (e.g. Figure IIC) show a different 287 magnetic fabric signature than melanosome layers characterized by strongly inclined to sub- 288 vertical magnetic lineation (site XIII 289 than the K1 axes. They are in the horizontal plane with two dominant directions: N-S and E- 290 W. 291 292 . The K3 axes are more scattered In large coarse-grained pink granite dykes (sites A, E, D IXthe K3 axes are relatively well clustered defining a subvertical magnetic of strike close to that of 9 a divergent strike (sites A). The 293 neighbouring gneisses (sites E, D 294 magnetic lineation pattern is characterized by the verticalization of K1-axes in comparison to 295 magnetic lineation measured in the melanosome layers of neighbouring gneisses. They form 296 girdle perpendicular to K3 (site E or strongly inclined to sub-vertical local maximum 297 (sitesD A 298 , Taureau, la Vierge, Balance Islands (sites 299 VIIXV, XIV XVIII, XIXFigure VIII) and South of Pétrels Island (site 300 XX 301 Gouverneur anatexite (sites VII, XV 302 lies in the horizontal plane, relatively scatted or forms clusters at 90 degrees from each other 303 with the N-S and E-W directions that prevails for south Gouverneur Islands (site XV). 304 Sampling sites XIV, XVIII (Figure VIII) show heterogeneities in the partial melting degree 305 that is expressed in the field by more or less regularly presence of migmatitic gneiss rafts in 306 the anatexites. For site XVIII 307 gneisses show distinct magnetic axes orientations characterized by K1 preferentially sub- 308 vertical and K3 horizontal N-S (i.e., magnetic foliation vertical E-W) in anatexites while K1 309 is horizontal to strongly plunging N-S and K3 is horizontal E-W (i.e., magnetic foliation 310 vertical N-S) in neighbouring gneisses. The N-S orientation of magnetic foliation in gneisses 311 fit quite well with the regional vertical shear zone structures. In opposite, the E-W vertical 312 magnetic foliation that appears in the larger dykes and anatexites is less well-constrained by 313 large-scale 314 XIV T 315 and the migmatitic gneisses was difficult to perform. That explains the relatively wide 316 confidence zones at 95% for K1 and K3. However the magnetic fabric is mainly oriented 317 vertical E-W for the foliation and strongly-inclined (westward) for the lineation. 318 K1max tends to have strong inclination or to be sub-vertical. For field structures anatexites and migmatitic (Figure VIII). For site tinction on the field between the anatexites In mylonitic gneisses of Jakobsen (sites II, V, ) the magnetic foliation 319 (K1-K2) is dominantly subvertical N-S in accord with the observed field structures (Figure 320 IIf). On the contrary, the AMS measurement reveals uncommon highly dipping or sub- 321 vertical lineation. 322 323 6.1.2. In the migmatitic gneisses of the dome shaped-zones (sites J, VI, G, K, H, S, 324 XVI, XVII, Figure VIII; sites C, IV, Q, III, VIII, I, B, i, XII, F, ) magnetic 325 fabric display a stronger variability of K1 and K3-axes orientations from one site to another 10 326 one in comparison to structured vertical shear zones. A relatively strong dip (about 45°) for 327 the magnetic foliation is frequently observed, in particular for the sites located in the flanks of 328 domes (sites H, K, Figure VIII; sites IV, Q, III, Figure IX) for the eastern flanks of the 329 Pétrels-Curies Islands dome). The magnetic foliations are generally in agreement with the 330 field measured strike and dip of melanosome layers. The magnetic lineations show gently dip 331 and dominant NNW strike. The innermost zones of domes (sites XVI, XVII, Figure VIII; sites 332 VIII, I, B, Figure IX) show also a strong variability of AMS structure patterns correlated to 333 the complexity of migmatitic structures observed at the domes apex. In these areas are 334 observed the less well-defined magnetic directions (with the widest confidence zones at 95%: 335 site XVI, Figure VIII; site I, Figure IX). Sampling in a granitic dykelet of centimetric width 336 crosscutting flat-lying gneissic foliation was performed in site XVII (Figure VIII). The 337 related AMS pattern is characterized by vertical N-S magnetic foliation and sub-vertical 338 magnetic lineation and then differs from that of gneiss. 339 Broad dyke of coarse grained pink granites sampling in site F an XII (Figure IX) are 340 characterized as for the granitic sites located in vertical shear zone by verticalization of 341 magnetic lineation in comparison to the magnetic lineation measured in the melanosomes 342 layers of gneisses The magnetic foliation in the dykes is either the same direction as that 343 measured in the gneiss (site F) or discordant (site XII). 344 345 6.2 – AMS parameters (P’ and T) 346 The Figure X presents the characteristics of the susceptibility ellipsoid. The degree of 347 anisotropy P’ is very high in the gneisses (mean 1.479; minimum 1.041; maximum 1.903). It 348 is lower in granites (mean 1.222; minimum 1.040; maximum 1.413). The shape of the 349 susceptibility ellipsoid is dominantly oblate, in gneisses (for T value: mean 0.30; 350 minimum -0.08; maximum 0.66) as in granites (mean 0.25; minimum -0.10; maximum 0.62). 351 In granites, a clear relationship (Figure IV, R2=0.70) between P’ (intensity of the fabric) and 352 Km (related to the concentration in ferrimagnetic minerals) highlights the dominant effect of 353 the magnetite in the AMS (Henry et al., 2004). Another relationship (R2=0.54) between T and 354 P’ in granites suggests that the most prolate fabrics correspond to the weakest anisotropy 355 Figure X. In addition, for granite, the anatexites show the highest variability in P’ and T 356 values, including the extreme values Figure X. 357 11 358 7 – Discussion 359 7.1 Mean susceptibility (Km) and anisotropy (P’) signature 360 The amount of magnetite is clearly different in gneisses and in granites (leucosomes 361 and dyke), as shown by the susceptibility values (Figure IV). This variation of magnetic 362 susceptibility between melanocratic and leucocratic layers is mainly due to the variations in 363 magnetite content. Magnetic studies suggest also mineralogical changes affecting magnetite 364 with formation of ferromagnetic oxides of lower susceptibility like maghemite or hematite. 365 Concerning this mineralogical change, gneiss sample AP35 is the only one with hematite; it 366 also presents the strongest formation of a lot of new magnetite at high temperature 367 (susceptibility becomes 14 times higher on the cooling curve). It is therefore probably due to a 368 strong local mineralogical alteration (interaction with deep fluids, weathering?) and remains 369 an exception. In all the other gneissic samples, no or few maghemite alteration during 370 thermomagnetic experiments has been observed, while such alteration is more important in 371 the granitic ones. This mechanism therefore likely had a significant effect for the 372 susceptibility decrease in granites related to melting. 373 The intensity of magnetic anisotropy, illustrated by the P’ values, is lower in granites 374 than in gneisses (Figure X). In granites, it presents a relationship with the Km values, 375 suggesting that this difference could be explained by the lower amount of magnetite in 376 granites, AMS then resulting mainly from strong magnetite anisotropy and weak anisotropy 377 of a low susceptibility component. Owing to its Km values, this last component is the 378 paramagnetic minerals and not the maghemite. The observed inverse correlation between T 379 and P’ in granites (Figure X) shows that the AMS of this second component is less oblate than 380 the magnetite AMS. 381 Inversely to granitic magmas constituting leucosomes and dykes, a wide range in Km 382 values, according to the samples within a same site, is observed in anatexites. It is due to the 383 presence of more refractory slice of gneisses with high concentration in oxides grains. 384 385 7.2 AMS in gneisses and granites 386 In addition to the Km and P’ values, the main differences in magnetic fabric between 387 melanosome layers of gneisses and granitic magmas concern the orientation of the K1 axis 388 (Figures VIII and IX). K1 axis is dominantly close to the horizontal in melanosomes and close 389 to vertical in granites. In some granitic sites (e. g., sites E, XII, Figure IX), its orientation is 390 relatively scattered within a vertical plane, probably because of the presence of melanosome 391 fragments within the granite. Other difference in orientation of susceptibility axes concerns 12 392 K3. Whereas in melanosome the K3 orientation fits to the field structures, it appears in granite 393 a more complex magnetic orientation pattern with two dominant orientations. The first one 394 matches to the gneissic structures (for example, the magnetic foliation is vertical N-S in the 395 shear zone area) and the second is at 90 degree of the first one. In some sites the two 396 clustering are present (e.g., site XV Figure VIII and site XIII, Figure IX). The first 397 orientation is associated to the strike-slip deformation, which is at the origin of the large-scale 398 sub-vertical corridors. The cause of the second orientation is less straightforward. In Pétrels 399 Island, the migmatitic layering is locally cut by vertical large granitic dykes of NE—SW to E- 400 W direction (Monnier, 1995). The E-W tending magmatic direction could be then related with 401 the implementation of dykes, which are consistent with a component of NNW-SSE to N-S 402 dextral strike-slip (Gapais et al., 2008). In the western area (Gouverneur island area, Figure 403 VIII) where pieces of melanocrate restites are still packed in anatexites, E-W magnetite could 404 correspond to inheritance of old tectonic foliations. 405 The gneiss sites II and V, on the south-western border of the Pétrels Island (Figure IX) 406 also present mainly subvertical K1 axes. However, contrarily to the granitic leucosome, dyke 407 and anatexite that have not recorded pervasive solid-state deformation, the gneisses of sites II 408 and V are intensely deformed. Thus, AMS fabric is interpreted as resulting of high-strained, 409 late- to post-migmatisation mylonites. The strong K3 clustering indicating a N-S vertical 410 magnetic foliation and the highly tilted to sub-vertical magnetic lineation could be related to 411 deformation in transpressionnal regime that is localised in the N-S vertical shear zones. 412 Thin section analyses show a change of orientation of magnetite grains from 413 melanosome to leucosome. In melanosome, the oxide grains are in the foliation elongated 414 parallel to the lineation marked by the sillimanite alignment. They are interpreted as resulting 415 from solid-state deformation that occurred during the Paleoproterozoic metamorphic event 416 (1.7 Ga ago). In addition, LPO of ilmenite, which strongly correlated with the tectonic fabric, 417 suggest dislocation glide on (0001) as main deformation mechanism. The basal slip for 418 hematite – ilmenite mineral could reflect high-temperature solid-state deformation (e.g., 419 Bascou et al., 2002; Siemes et al., 2003). Migmatitisation processes are also associated with 420 segregation and transportation of melt that result in leucosome, ping granitic dyke and 421 anatexite in the area of higher degree of partial melting. As discussed in Vigneresse et al. 422 (1996), the increase of melt fraction produce changes in rheological behaviour. Plastic 423 deformation evidenced by elongation of oxide minerals, which are abundant in the 424 melanosome and magma flow with transport of relatively isolated solid particles in 425 leucosomes, dykes and anatexites. 13 426 Such types of deformation succession involving magnetite grains deformed under 427 solid-state conditions and, during melting, behaving like passive rigid particles has been 428 observed in various migmatitic terrains (e.g., Barbey et al., 1990; Ferré et al., 2003). In Pointe 429 Géologie migmatites, this generates distinctive AMS signatures. The clearest difference 430 concerns the K1 orientation, which tends to a vertical plunge during segregation and 431 circulation of felsic melt. This is related to gravity-induced upwelling of magmas. K3 432 orientation in granitic layer appears more sensitive to the degree of partial melting and the 433 structuration of neighbouring rock. When the melting started, melt segregation remained 434 strongly constrained by unfused material. Felsic melt formed dykelets and connected lenses 435 concordant with the foliation of gneisses. For higher degree of melting, the melt was injected 436 as concordant or cross-cutting large veins (Figure IIc,d) explaining the various orientations of 437 the magnetic foliation. The dyke emplacement corresponds to areas of lower stress, generally 438 close to the 3 direction (e.g., Cooper, 1990; Hand and Dirks, 1992). 439 440 441 7.3 Methodological and regional-scale implications 442 All these observations evidence that, for migmatites, the AMS study is clearly not a 443 routine method, the single possible approach having to be based on the obtaining of numerous 444 data from rocks showing various degree of melting. For low degree of partial melting the 445 leucocratic layers remain strongly constrained by the structure defined by the unfusible 446 minerals. The AMS principal axes are representative of the local and regional finite strain 447 axes. This observation is conform to those of Ferré et al. (2003) for migmatites of the 448 Superior Province in Minnesota. For more pronounced partial melting degree, well- 449 individualized leucocratic layers can developed specific AMS patterns associated to flow 450 regime. In Pointe Géologie migmatites the difference with the local and regional finite strain 451 axes is marked by the direction of K1-axes. Probability to measure composite AMS is 452 increased and the difficulty of AMS analyses is then to isolate pre-melting and synmelting 453 magnetic fabrics. The anatexites show the strongest variations in AMS principal directions 454 and parameters due to the inhomogeneity of these formations, which can preserve more 455 refractory pieces. 456 The structural pattern of Pointe Géologie is constituted by two superimposed 457 foliations, one flat-lying and one sub-vertical, both associated with partial melting (Pelletier et 458 al., 2002; Ménot et al., 2007). Mineral lineations are not easy to observe within the foliation, 459 in particular for sub-vertical shear zones. These structural field evidences, coupled with the 14 460 metamorphic pattern and ductile deformation numerical simulations, allowed to propose a 461 model in which hot and weak lithosphere converge during Paleoproterozoic toward a cooler 462 craton (Archean in age). In this model, deformation combines transpression and horizontal 463 flow and/or lateral escape parallel to the Archean basement (Gapais et al., 2008). 464 AMS structural pattern determination provides complementary structural information 465 such as lineations. They are mainly sub-horizontal in sub-vertical foliated gneisses. It 466 underlines the importance of the strike-slip component during the deformation. In mylonitic 467 gneisses that are considered as late- to post-migmatisation tectonites appear lineations with 468 stronger plunge. This is attributed to the effect of transpressionnal regime, which combinates 469 strike-slip and across-strike shortening (ref? voir Tikoff). In migmatite with flat-lying 470 foliation, lineation has moderate plunge, which is conform to field observations. 471 Increase of partial melting degree produce decrease of the grains cohesion and the melt 472 escapes of the frame constituted of solid-state deformed minerals. Thus the former tectonic 473 structures will tend to be erased. Segregated melt will behave as viscous flow and movement 474 are gravity driven forces. Well-defined leucosomes, dykes and anatexites will develop new 475 magnetic fabric corresponding to the transport of the magma upwards. Measurements of AMS 476 then allow to better map the mass transfers associated to the peak temperature and intensive 477 melting and then specify the general framework of a warm and buoyant lithosphere 478 converging toward a cooler craton as proposed for Pointe Géologie. 479 480 8 – Conclusion 481 Pointe Géologie archipelago in Terre Adélie represents a deep and hot crust affected 482 by intensive anatectic event during Paleoproterozoic times, 1.69 Ga ago. This generated 483 different HT rocks types such as: migmatites including leucosomes and melanosomes, coarse- 484 grained pink granites dyke and anatexites. The partial melting affects indifferently the 485 regional structures characterized by the juxtaposition of flat-lying and sub-vertical 486 deformation zones. 487 Magnetic mineralogy study shows that oxide minerals are mainly large grains of 488 magnetite. Ilmenite is also observed constituting cluster with magnetite, which is particularly 489 abundant in melanosome layers. The grains are intensely solid-state deformed and aligned 490 parallel to the lineation marked by sillimanite. Oxides appear more scattered in the 491 leucosomes than in the melanosomes. Their rounded shape suggests rotation of the former 492 elongated grain during melt segregation. 15 493 Melanocratic layers on the one hand and felsic leucosomes, dykes and anatexites on 494 the other hand develop contrasted AMS signatures. The mean magnetic susceptibility (Km) 495 and the anisotropy degree (P’) are high in the gneisses and lower in granitic samples. 496 Orientation of principal susceptibility axes also differs. In gneisses, magnetic foliations are 497 coherent with the local and regional structural pattern. Nevertheless AMS technique provides 498 complementary information on the orientation of lineations, which are difficult to observe in 499 the field. They are subhorizontal in shear zone, except in vertical mylonitic zone where high 500 plunge evidences the transpressionnal regime of the deformation. In well-defined leucosomes, 501 granitic dykes and anatexites, the magnetic ellipsoid is characterized by verticalization of the 502 magnetic lineation. This change of orientation is associated to a rheological contrast between 503 the solid-state deformation suffered by the oxide grains and their reorientation in a viscous 504 flow during the aggregation of felsic melt. 505 Magnetic structure pattern do not disagree with model of hot and weak lithosphere 506 converging toward a cooler Archean craton proposed by Gapais et al. (2008) from 507 metamorphic and field structures analysis, and from numerical modelling (Duclaux et al., 508 2007). The auteurs focussed particularly on structural features compatible with a horizontal, 509 orogen-parallel, subconstrictional flow that could result from oblique convergence and/or 510 from particular boundary conditions facilitating lateral escape. The magnetic structures map 511 allows to highlight the role of the gravity-induced upwelling of a crust undergoing partial 512 melting. 513 From methodological point of view, this work emphases on the importance of the 514 petrological characterization of sites being selectioned for AMS measurements in order to 515 avoid pre-melting and synmelting composite magnetic fabrics. 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