International Journal of Research In Science & Engineering Volume: 1 Issue: 1 e-ISSN: 2394-8299 p-ISSN: 2394-8280 Pressure Drop in Slurry Flow Shubham Grover1, Rajat Jassi2 1 Student, Department of Chemical Engineering, Indian Institute of Technology Delhi, New Delhi, India, ch7120179@chemical.iitd.ac.in 2 Student, Department of Chemical Engineering, Indian Institute of Technology Delhi, New Delhi, India, ch 1120108@chemical.iitd.ac.in ABSTRACT Over the years, slurry flow has been widely investigated because of its wide scale application in transport of materials in industries. Durand, Newitt, Wasp have explained their theories and models in this domain but they are applicable in narrow ranges of conditions. There is still a need to find an optimal method for slurry transportation that can be applied on a variety of slurries. The objective of this research is to experimentally investigate the pressure drops for solid-liquid slurry flow in constant circular cross-section straight and helical pipes of a finite pitch placed horizontally for homogeneous slurry flow regime. The slurry used in the process is calcium carbonate powder (d=56μm) mixed with water and the concentration is varied (0-7%). The results obtained helped in understanding the difference in nature of flow in straight and helical pipes and in comparing the dependence of pressure gradient per unit length on velocity and concentration for the straight and helical pipes. The concept of using the helical flow is to understand the effect of centrifugal forces on the pressure drop and hence the friction factor. The pressure drop in slurry flow is influenced by particle-particle, particle-fluid, fluid-wall and particle-wall interactions. Size of the particles and the tendency to settle has a strong impact on capital and operating cost. Keywords: Pressure drop, Slurry, Helical pipe, Magnetic Pump, Concentration, Pitch, Flow rate, Velocity. ----------------------------------------------------------------------------------------------------------------------------1. INTRODUCTION The pressure drop is considered the most important parameter in slurry flow. Large amount of pumping costs are involved in transporting solid-liquid slurries in chemical industries. Efforts are made constantly to find the most suitable combination of pipe shape and particle size to minimise the energy losses incurred in flow. The pressure drop in a flow depends upon the flow velocity and the interactions between the particle, fluid and the pipe wall. The relationship between pressure gradient and mixture velocity is substantially different from that of a pure liquid flow. Mud slurry is essentially a mixture of a carrying fluid and solid particles held in suspension. In spiral pipe twisted with a constant pitch in relation to the axis a swirling flow occurs when fluids flow in the pipe. For practical application the spiral pipe presents a very useful method for preventing the holdup phenomenon in a transport pipeline for the hydraulic transport of mud slurry. Flow velocity generates turbulence which keeps particles suspended. Mean velocity in a pipeline is a basic parameter characterizing pipeline flow. It is defined as the bulk velocity, v, of a matter (solids, liquids or mixtures) obtained from the volumetric flow rate, Q, of a matter passing a pipeline divided by cross section of the area, A, (Q/A). There are two types of slurries: Settling slurries and non-settling slurries. For non-settling slurries the particle diameter is less than 40 um. Viscosity of a slurry is modified by particles. The flow becomes increasingly nonnewtonian as concentration increases. Settling slurries are identified as with particle diameter greater than 40 um. They are further classified as small (suspensions) 40 μm ~ 200μm, medium (transition) 200 μm~2mm, large (heterogeneous) 2 mm ~ 5 mm, very large (hetero) 5 mm >200 mm. The working particles falls in the small settling suspensions with d=56um. IJRISE| www.ijrise.org|editor@ijrise.org International Journal of Research In Science & Engineering Volume: 1 Issue: 1 e-ISSN: 2394-8299 p-ISSN: 2394-8280 For a pure liquid, the pressure drop in a pipe depends on the flow velocity. In straight pipes, the patterns can be conveniently be classified into the following four regimes: Homogeneous flow: When the flow velocity is sufficiently high, there is a uniform distribution of solids about the straight axis of the pipe. In this regime, turbulent and other lifting forces are capable of overcoming the net body forces as well as the viscous resistance of the particles. Heterogeneous flow: When the slurry velocity decreases, intensity of turbulence and lift forces also decreases due to which, there is a concentration gradient across the pipe cross section with a larger concentration of solids at the bottom. When the velocity further decreases to the critical velocity, some solids start to move along the pipe bottom as a “bed load.” At this point, the pressure drop is usually minimum. Saltation flow: At further reduced velocity, the bed load starts to generate a stationary bed. Further very few solids are transported as the suspended load, and more amount of solid is transported as the bed load. The bed motion is due to the movement of the uppermost particles tumbling over one another. Stationary bed flow: The stationary bed further increases the apparent pipe friction factor, resulting in increased pressure drop. Finally, at further reduced velocity, all solids stop moving. In this regime the slurry velocity is further reduced which leads to the lowermost particles of the bed being nearly stationary. Thus, the relationship between shear stress and shear rate may be described by measuring the pressure drop gradient and the volumetric flow rate. 2. EXPERIMENTAL SET-UP The set up consists of a feed tank having a slurry of (water + CaCO3). The particle size of the powder used in slurry is 56 microns which falls in the category of settling slurries. So, to stop slurry sedimentation the slurry is homogeneously agitated using an agitator. The slurry concentration is varied from 0to7% by weight. The slurry was introduced to the straight pipe and helical pipe using 0.12 hp chemical pump at room temperature. The slurry flow rate was controlled using ball valve in the main stream and a pin valve in bypass stream. The flow rate was measured by volumetric time analysis. The helical pipes were made of flexible tubing with an inside diameter of 0.75 in. or 1.91cm wounded on a cylindrical core of D=22.3cm. To minimize end effects on the pressure drop measurements, the pressure taps were located away from the pipe ends by more than 50 times pipe radii. The pressure drop for the test section was measured using a digital manometer. Since the particle used has a diameter=56um, it falls in the category of a settling slurry and needs an agitator, the velocity was kept above the critical velocity (approximately 20cm) of the slurry. Number of loops Core Diameter Tube Diameter Pitch =3 Pipe diameter = 1.91 cm = 22.3 cm Length of pipe between pressure tapings = 2.4 m = 1.91 cm = 30 cm Fig-1: Experimental setups helical and straight pipe system respectively IJRISE| www.ijrise.org|editor@ijrise.org International Journal of Research In Science & Engineering Volume: 1 Issue: 1 e-ISSN: 2394-8299 p-ISSN: 2394-8280 2.1 PROCEDURE After the flow was developed readings were taken. It was taken into consideration that the slurry level in the holding tank should be high enough to ensure that air was not entrained in the mixture entering the pipe. The joints were made leak proof for minimising any loss of flow. The pump was chosen very carefully as the slurry consists of a chemical slurry which may corrode the iron casting of a normal pump. So we choose a non-corrosive centrifugal chemical pump with polymer casting to develop the flow. Pressure tapings may disturb flow at the point where measurement is being taken. So the tapings should be made carefully. Agitator is switched on regularly so that sedimentation may not take place and it was not switched on continuously because it can disturb the flow. Bubble formation at low flow rate may develop irregularity, so flow was kept above the minimum value. 3. EXPERIMENTAL RESULTS Straight Pipe: 1. From the obtained graphs between pressure gradient per unit length versus velocity, it can be concluded that the frictional losses at high velocity were higher and consecutively higher pressure drop per unit length is seen at high flow rate. 2. Increasing the concentration increases the pressure head loss may be due to increased viscosity. Delta P/L vs Velocity (Straight Pipe) 9 8 delta P/L (mm Hg/m) 7 6 Concentration = 1% 5 Concentration = 3% 4 Concentration = 5% 3 Concentration = 7% Concentration = 0% 2 1 0 20 30 40 50 60 70 Velocity (cm/s) Fig-2: Dependence of pressure drop per unit length on velocity and concentration in straight pipe. IJRISE| www.ijrise.org|editor@ijrise.org International Journal of Research In Science & Engineering Volume: 1 Issue: 1 e-ISSN: 2394-8299 p-ISSN: 2394-8280 Helical Pipe: 1. 2. From the obtained graphs between pressure gradient per unit length versus velocity, it can be concluded that the pressure head loss decreases with increasing flow rate or the velocity in pipe. The reason for this require further study of the nature of the fluid. Increasing the concentration decreases the pressure head loss. This indicates towards the nature of fluid becoming non-newtonian. Delta P/L vs Velocity (Helical Pipe) 30 delta P/L (mmHg/m) 25 20 Concentration = 1% Concentration = 3% 15 Concentration = 5% Concentration = 7% 10 Concentration = 0% 5 0 25 30 35 40 45 50 55 60 Velocity (cm/s) Fig-3: Dependence of pressure drop per unit length on velocity and concentration in helical pipe. 3. 1 CONCLUSION While the helical pipe offers the advantage of no hold up but it also involves greater loss of pressure head per unit length due to agitated and properly mixed flow that happens in a helical pipe while the particles can settle in a straight pipe. Opposite dependency of pressure drop per unit length on velocity and concentration discussed above may be attributed to the effect of a centrifugal force in a helical pipe which is absent in a straight pipe. Centrifugal force depends upon the density of the solution and the square of the velocity. The effect of the centrifugal force causes the particles in the flow to be pushed to the outer side of pipe which increases the shear forces between the pipe wall and the slurry and ultimately increases the friction factor which causes pressure drop per unit length in the pipe. So, it can be concluded that energy losses in case of helical pipe is although greater than a straight pipe but as we increase the flow rate, the losses decrease and at increased concentration and flow rate helical pipe may cause lesser pressure drop per unit length than a straight pipe as can be inferred if the graph is extrapolated. But the cost of operating at high flow rate is also higher so we have to find an efficient and economic balance between the flow rate and pressure head loss. IJRISE| www.ijrise.org|editor@ijrise.org International Journal of Research In Science & Engineering Volume: 1 Issue: 1 e-ISSN: 2394-8299 p-ISSN: 2394-8280 Delta P/L vs Velocity 30 Concentration = 1% Concentration = 3% 25 delta P/L (mmHg/m) Concentration = 5% 20 Concentration = 7% Concentration = 0% 15 Concentration = 1% 10 Concentration = 3% Concentration = 5% 5 Concentration = 7% 0 Concentration = 0% 25 30 35Velocity40 (cm/s) 45 50 55 60 Fig-3: Dependence of pressure drop per unit length on velocity and concentration compared. 3.2 FUTURE SCOPE The results obtained can be used to develop a new model and propose a theory on slurry flow friction factor. The topic can be further explored for different type of particles, with a particle size distribution of interest for different shapes and materials of pipes to study the effect of particle-particle, particle-fluid, fluid-wall and particle-wall interactions on slurry flow. The schemes and models developed can help in minimising the energy losses occurred during slurry transport. ACKNOWLEDGEMENT We sincerely thank Dr. Sudip Pattnayak, IIT Delhi, for providing us an opportunity to work on this research project and providing us guidance and financial assistance for acquiring all the equipment needed. REFERENCES [1] [2] [3] [4] [5] [6] [7] Yanuar, Ridwan, Budiarso and Raldi A Koestoer, “Hydraulics conveyances of mud slurry by a spiral pipe,” Journal of Mechanical Science and Technology, Vol 23 (2009) pp. 1835-1839 T. Mali, V. Khudabadi, Rana A S, A. Vijay and Adarsh M R, “Slurry flow pressure drop in pipes with modified wasp method,” Presented at SME annual meeting, February 24-26, 2014 S. Liu, A. Afacan, Hisham A. Nasr-el-Din and J. H. Masliyah, “An experimental study of pressure drop in helical pipes,” Mathematical and Physical Sciences, Vol. 444, No. 1921 (Feb. 8, 1994), pp.307-316 R.C. Chen, “Analysis of homogeneous slurry pipe flow”, Journal of Marine Science and Technology, Vol 2, No. 1, pp. 37-45 (1994) Anil R. Oroskar, R.M.Turian, “The Critical velocity in pipeline flow of slurries,” AIChE Journal, Vol. 26 No. 4, pp. 550-557 (1980) P. Doron, D. Granica and D. Barnea, “Slurry flow in straight pipes: experimental and modelling,” International Journal of Multiphase Flow, Vol. 13, No. 4, pp. 535-547, (1987) K. El-Nahhas , N. Gad El-Hak, M. Rayan and I. El-Sawaf, “Effect of particle size distribution on the hydraulic transport of settling slurries,” Thirteenth International Water Technology Conference, IWTC13 2009, Hurghada, Egypt IJRISE| www.ijrise.org|editor@ijrise.org